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Miscellaneous - 312 BOXFORD STREET 4/30/2018 (2)
BOXFO 312 4.B-00 O=oTREET 210/104.B-005=�-0000.0 \\ i i i i i Ik Lyt & Street b x-LA -St Map/Parcel CONSTRUCTION APPROVAL Has plan review fee been paid: YES NO Permit# Plan Approval: Date: ----— Approved by: ---� Designer: Plan Date:�—� -- Conditions: Water Supply: Town. _ Well - -- Well Permit. _Driller: Well Tests: Chemical Date,Approved Bacteria I Date-Approved Bacteria 11 _Date-Approved Plumbing.Sign-Off- �` Wiring Sign-Off: Comments: Form"U" Approval: Approval to'Issue: YES NO Date Issued By: -\ Conditions: Final Approval: All Permits Paid? YES NO Well Construction Approval? YES NO Septic System Construction Approval? YES NO Certification? YES 0 Other YES NO Any Variance Needed? YES NO FINAL BOARD OF HE LT APPROV L. DATE: APPROVED BY: .- SEPTIC SYSTEM INSTALLATION Is the installer licensed? YES N ——--- Type of Construction: NEW pA�IR --- -- _._._ NevrConstruction: __—Certified Plot Plan Review YES -_ Floor Plan Review YES NO -- -- -_ Conditions of Approval from Form U YES NO �ti _ ,. Issuance.ofDWC-permit YES- NO —DWC-Permit Paid? NO . -DWC'Permit# Installer: BegiirTiispection _ �NO Fxcavatioiilnspe'on ._..__ _ `--=Needed:- • . _ _� - By - : Construction Inspection: -AsHuilt-P-lan-Satisfactory:`— .. YEg: Approval of Backfill: Date: . By: _ Final.Grading Approval: Date: By: Final Construction Approval- Date: By: Certificate of Compliance:- Approval: Date: r ~ A Y• "L a I I Commonwealth of Massachusetts North Andover, Massachusetts System Pumping Record -a [RE:CEjv7EDSystem Owner& Address: Z0'2Paul Kroon RTt a"scOVER312 Boxford Street EPT-VENT North Andover, MA 01845 I Location of system: Rear yard Date of Pumping: August 29, 2012 Type of system: Septic Tank Gallons Pumped: 1000 gallons i System pumped bv: Service Pumping& Drain Co., Inc. S Hallberg Park North Reading,Ma License#: BHP-2011-0413,0412,0411,0410,0409,0408 Contents transferred to: Greater Lawrence Sanitary District bate: Aug. 29,2012 Pumping Technician: PK This is PROPRIETARY and CONFIDENTIAL information that may be used only by the Board of Health for regulatory purposes i I � � r4W � I � � h � { � n `u�,�,•�ticJ k I J �✓ �� V� a f ar ' ti 1� ' ,�° , y � � , �� • �.:k � � -- �� 1- J -� i �� � i -- -J ar`r 1��I�7J ✓ T t .................. k } r L4 - i I UILC)I ES UH MA Y o �R'f5 bi.t� ►.► a A >� G " 1J. E—EX is'r, L V7' WrIO A04ZS —*I I jrPnfiM0W rj ' .c}p' Z,2( 12, 08 �jLow We 05,6,-7 F,-r i 611 L---r) Per-E X 1111T7 �� ., _ k . ,►aPiz,- E m e tJt9Tk- -rAll- .I?L�►.� t Gt�'(EFIGA'f"Iohy 19 OOT A UAI&IcskOTY OVs't�C S�gSUa.�oG6 o L. ANcP CLEvclnod OF -rilE e,. -APTINt, 4,yie )-r co�,Po�+ti►�rh. z h i x. > '. ti i r V33.7, T' AS BUILT PLAN OF SUBSURFACE DISPOSAL SYSTEM LOCATED IN AS PREPARED FOR D�•i i O C��2Uso I,.? . DATE : JU 0 E rl, I q JA" SCALE. -rawso�?;TVN 2 .JUN MERRIMACK ENGINEERING SERVICES, INC. PROFESSIONAL ENGINEERS • LAND SURVEYORS • PLANNERS 66 PARK STREET • ANDOVER. MASSACHUSETTS 01810 G TEL (617) 475-3553, 373-5721 . TO: NORTH ANDOVER, MASS 57 19 7-Y-- BOARD OF HEALTH FROM: DESIGN ENGINEER Re: Soil Absorption Sewage System Inspection This is to certify that I have inspected the construction of the said disposal system at �t3/ yr- (219-l l–SO Al X�CO/e D -57- - North Andover, Mass. SITE LOCATION The grades and construction are as specified in my plans and specifications dated C'/3 c 19 7S— OF MgSS9c3G ' I eg• P o kWf/-Weg``V itarian I ! / v Nn. 464 10 > l 'FSSlO N AC SP Commonwealth of Massachusetts MSystem City/Town of System Pumping Record 61� Form 4 F NORTH DEPART ENT DEP has provided this form for use by local Boards of Heat Record must be submitted to the local Board of-Health or other approving authority. . A. Facility Information Important: When filling out 1. System L � ft' (� �� forms on the �,A�-- 0"Q` computer,use only the tab key Address S to move your cursor-do not use the return City/Town state Zip Code key. 2. System Owner: 142L Name ill Address(if different from location) Cdyrrown State . Zip Code' Telephone Number B. Pumping Record 1. Date of Pumping Date 2. Quantity Pumped: Gallons 3. Type of system: ❑ Cesspool(s) lc Tank- ❑ Tight.Tank ❑ Other(describe)` 4. Effluent Tee Filter present? ❑ Yes El—No ~� If yes, was it cleaned? ❑ Yes ❑ No 5. Condition of System: 6. System Pumped By Name �---- Vehicle License Number Uk. Company — 7. Location where contents.were disposed:. Signat re H ter Oate http://www.mass.gov/dep/Water/cipprovalt,/t5forms.htm#inspect t5form4.doc•06103 System Pumping Record•Page 1 of 1 i TOWN OF SYSTEM PUM NG RECORD RECEIVED MAY 3 12005 DATE: 5-�1-0 TOWN OF NORTH ANDOVER HEALTH DEPARTMENT SYSTEM OWNER& ADDRESS SYSTEM LOCATION � L 1^ (example:left front of house) 1 ` \ -ya 64 DATE OF PUMPING: 31 O QUANTITY PUMPED : GALLONS CESSPOOL: NO YES SEPTIC TANK: NO YES NATURE OF SERVICE: ROUTINE EMERGENCY OBSERVATIONS: GOOD CONDITION FULL TO COVER HEAVY GREASE BAFFLES IN PLACE ROOTS LEACHFIELD RUNBACK EXCESSIVE SOLIDS FLOODED SOLIDS CARRYOVER OTHER(EXPLAIN) SYSTEM PUMPED BY: Bateson Enterprises, Inc. COMMENTS: CONTENTS TRANSFERRED TO: G.L.S.D Lowell Waste I TOWN OF SYSTEM PUMPING RECORD 1� 2 , DATE: > { 62003 SYSTEM OWNER & ADDRESS SYSTEM LOCATION _ (example:left front of house) I � O.0 o rC� i DATE OF PUMPING: QUANTITY PUMPED : GALLONS CESSPOOL: NO YES SEPTIC TANK: NO YES NATURE OF SERVICE: ROUTINE EMERGENCY OBSERVATIONS: GOOD CONDITION FULL TO COVER HEAVY GREASE BAFFLES IN PLACE ROOTS LEACHFIELD RUNBACK EXCESSIVE SOLIDS FLOODED SOLIDS CARRYOVER OTHER(EXPLAIN) SYSTEM PUMPED BY: Bateson Enterprises, Inc. COMMENTS: i CONTENTS TRANSFERRED TO. y TOWN OF NORTH ANDOVER SYSTEM PUMPING RECORD DATE: SYSTEM OWNER &ADDRESS SYSTEM LOCATION (example: left front of house) 3 DATE OF PUMPING:?��—an?-IQUANTITY PUMPED GALLONS CESSPOOL: NO YES SEPTIC TANK: NO YES NATURE OF SERVICE: ROUTINE ' EMERGENCY s� OBSERVATIONS: GOOD CONDITION FULL TO COVER HEAVY GREASE BAFFLES IN PLACE ROOTS LEACHFIELD RUNBACK EXCESSIVE SOLIDS FLOODED SOLIDS CARRYOVER OTHER (EXPLAIN) SYSTEM PUMPED BY: �Y COMMENTS: I ✓ui"I OF ivoRC i Ai„DO'. / I T14JUL J 0-1 0 CONTENTS TRANSFERRED TO: Commonwealth of Massachusetts 411,L).omassachusetts System Pumping Record System Owner System Location Date of Pumping: �j Jam =✓ Quantity Pumped: /gallons Cesspool: -No-[t----- Yes [] Septic Tank: No [] Yes System Pumped by: Va&"w � License# i Contents transferred to: Greater Lawrence Sanitary District Date: Inspector: 7C Commonwealth of Massachusetts ' -Massachusetts Svstem Pumping Record System Owner System Location 73f Date of Pumping: - Quawity Pumped: gall ons Cesspool: No Yes U Septic Tank: No L1 Yes System Pumped by: Stre'de-I License# -_- Contents transferrred to : Greater"wrence sanitary District a, .Date: Inspector: t' Mi 1! AR , I SU l FACE RE[`� IATI TC'HNOL I , INC. *a ENVIRONMENTAL CONSULTING & REMEDIATION SE1�4�4CES 355 Central Street Rowley, Massachusetts 01969 (978) 948-3861 m x> / WOOD/ September 4, 2001 __. Massachusetts DepartmenLofEnvironmental Protection North East Regional Office 205A Lowell Street Wilmington, MA 01887 RE: Trask Residence, 312 Boxford Street,North Andover 01845 Release Notification Form, and Immediate Response Action Plan Submittal Dear Sir/Madam: On behalf of Deborah and Robert Trask, owners of the subject residence, Subsurface Remediation Technologies, Inc. (SRT) is submitting the following Release Notification Form (RNF) and Immediate Response Action (IRA) Plan in conformance with Department of Environmental Protection (DEP) and the Massachusetts Contingency Plan (MCP) requirements. No other federal, state, or local permits are required to conduct this IRA Plan. Enclosed separately are the original RNF and IRA Plan transmittal forms with copies also included in Attachment 1. The Trask family returned home after being away on July 3, 2001 to find that lightning had struck a tree approximately fifteen or twenty feet from the rear corner of their house. They also found that their #2 fuel oil tank had emptied through a ruptured furnace feed line and had seeped onto and below the concrete floor through cracks. The North Andover Fire Department responded and cleaned up, and bagged, oil soaked rugs, clothing, etc. affected by the oil. SRT later contained them in one properly labeled 55- gallon drum, which is still at the site. Notification to Mr. Victor Fonkeim, of your office (DEP), was made by the North Andover Fire Department on July 3, 2001 at 4:35 PM. Mr. Steve Ross of your office conducted a site visit in mid-July. Further action at the site was delayed while the owners' insurance company (Safety Insurance Company) evaluated the cause of the release to determine if coverage applied. It was determined that the line break was somehow caused by the lightning strike, and full coverage has been determined. The above ground 330 gallon storage tank is estimated to have lost approximately 150 gallons of fuel oil based on available records. A monitoring well was installed on August 13, and 14, 2001, at the front end of the garage in the driveway at the opposite end of the house (see Figure 1), undf-- co^t::-act with the insurance company, by Exeter Environmental, Inc. The boring log, included herein as Attachment 2, shows groundwater at 24 feet below ground surface (bgs). Based on blow count data, the glacial till appears to become much more consolidated at approximately 6 feet bgs. From 6 feet to 15.3 feet, the very dense till had many boulders, and bedrock was encountered at 15.3 feet. Coring was accomplished to 30 feet bgs. Due to adverse drilling conditions, only one of the three monitoring wells proposed by Exeter Environmental, Inc. was completed. A verbal IRA Plan approval was received by SRT from Mr. Victor Fonkeim of your office (DEP) on August 15, 2001. The approved IRA Plan consisted of the excavation of affected soils up to 150 cubic yards, and the dewatering and on-site storage of groundwater up to 50,000 gallons, if deemed necessary. Should groundwater treatment and discharge be required, an EPA NPDES Permit would be required. SRT was formally retained on August 22, 2001. The monitoring well and drinking water well were sampled by SRT that same day, August 22, 2001, and sent to AMRO Laboratories for EPA Method 524, VOC, drinking water analyses. Results, included herein as Attachment 3, were Not Detected(ND). Hand excavation of the room in question began on August 22, 2001, and has continued. Today, approximately 45 cubic yards of contaminated soils are stockpiled in a paved parking area, over and under poly cover. Progress is slow because the glacial till is so dense it has to be jack hammered, and it also contains numerous, relatively large, rocks. SRT will continue to excavate to the bottom of affected soils until appropriate EPH/VPH analyses results are attained. SRT will also attain samples beneath foundation walls for appropriate critical exposure pathway evaluation. Should the oil contamination continue into the bedrock, appropriate measures will be deployed to evaluate and recover oil at the source area. These actions, if necessary, will be delineated in an IRA Modification submittal to DEP, and may significantly increase project schedules. Hnu screening of soils, accomplished with every foot of depth, show decreasing concentrations to where SRT expects to reach the bottom of contamination prior to reaching bedrock, barring unforeseen outcrops. If this presumption is correct,the IRA should be completed prior to the first required IRA Status Report (120 days). SRT conducted 26 electric drill powered borings throughout the basement and garage areas inside the house on August 23, 2001, and found the contamination to be under the floor outward from the furnace room into the adjacent room and also the adjacent garage. These borings were used to measure trapped vapors beneath the floor with an Hnu Photoionization detector. Locations and affected areas are delineated on the site plan, Figure 1. Levels in uncontaminated areas were at or very close to 0 ppmv, and ranged from 15 ppmv to 80 ppmv in contaminated areas. These areas will also be excavated. Two of these borings were attempted at the corners of the building outside the furnace SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 i 2 room. (P-1, and P-2). P-1 went to approximately 6.5 feet where refusal was encountered, and a soil gas vapor probe monitoring point was installed at'that depth, which is at the approximate elevation of the foundation footing. No vapors were detected in P-1. P-2 encountered refusal at ,`,,o f::et and v_ -as not further evaluated. Further drilling and monitoring well installation is scheduled for September 5, and 6, 2001, outside the affected corner of the house. SRT will attempt to install two to three additional monitoring wells to evaluate the Spill that could potentially affect the drinking water well approximately 50 feet from the residence. Since contamination does not appear to have impacted this well at this time, other, more distant, potential receptors have not been evaluated. `. ' "._ — s � - Please contact the undersigned if you have any questions regarding the attached Immediate Response Action Plan. Sincerely, °� Timothy Toomey LSP President Enclosures cc: Town of North Andover BOH Town of North Andover Chief Municipal Officer Mr. &Mrs. Robert Trask SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 Driveway I '' I p, j?2 15-80 ppm vapors beneath floor Furnace Rooml I 4-- I ! Stockpiled Soil 1 IRA Ikelease MW-1 • 4- Soil Kelhova>! Area GarageAF v rRASK RESIDENCE I ° BASEMENT LEVEL AREA I I I I I � I Drinking water well I 0 I I I I _ I I I BOXFORD STREET LEGEND Bar Scale(in feet): SITE MAP/IRA Removal Area N Sample Powered hand auger gas probe borings 0 10 20 312 Boxford Street-Trask Property Location SRT NORTH ANDOVER, MA§SACHUSET 1'S ® Gcoprobe Location Scale: NA-sketch SUBSURFACE REMEDIATION - - Monitoring Well (proposed) Date: 4/27/01 TECHNOLOGIES, INC. Monitoring Well 0 furnace 355 CENTRAL STREET cy. g -�- Drn By: 1tOWLEY, MA. 01969 , . FIGURE 1 Release Point C= AST Location X hole in feed line Ck By- (508) 948-3861 a t �. ATTACHMENT,1 It Massachusetts Department of Environmental Protection BWSC-103 • Bureau of YVasie SIiB Cleanup Release Tras►ong Nun-'u RELEASE NOTIFICATION 8. r�OTiFIC,�MN RETRACTION L 1 -�Lp 8 i 4 I I - FORM Pursuant to 310 CtVa 40.0335 and 310 Cti4R 40.0371 (subpart C) 11 assgned by DEP A- RELEASE OR THREAT OF RELEASE LOCATION: Streit: c Location Aid: Cty!o+nn: 01845 ZIP B. 7HIS FORM IS BEING USED TO: (check;�) Submit a Release Notification(ca�nple:e all ser is^.s of this to,m). Subrnta Re'jaction of a Previously Reported Notifies ion of a Release or h'ea:zf Release(=m?le!e Se'z5ons A.B.E,F aro G of V,s form). You MUST attach the suPPOMng 0--c n'a';an requi d_.y 310 CMR 40.C335. C,r INFORMATION DESCRIBING THE RELEASE OR THREAT OF RELEASE(TOR): Dave and time you ob':ained►mcwledge of the Release or TOR. Dare: 'rune: specify:� AM _ PM The date you obtained knowledge is atways required. The tine you obtained knowledge is not rer�uirtK.'it reporting only 120 Day CondiAarrs i irne: $'�eGify: PM KNOWN,record cafe and tine release or TOR occurred. Date: _ f�},11 Check here if you pre,,iousty provided an Oral Notification to DEP(2 Hour and 72 Hour Repot- ng Conditions only). Provide date and line of Oral NotiftcaliDn. Date: 7/31012 Time: 4' 3 5 Specify: L ii AM PM Check all Noti'5=21ion Thresholds that appy to the Release or Threat of Release: (for-*,e information see 310 CMR 40.0310-AO.0315) 2 HOUR REPORTING CONDITIONS 72 HOUR REPORTING CONDITIONS 12J DAY REPORTING CONDITIONS --- S:hsu'ace Non-Aqum.;s Phase _� Release of Hazardous Materal(s)10 Soil ar Sucden Release Poi — Licurd(NAPL)Equal to or Greater t`.an Croueonin�Re ,ab,e Threat of SuDcen Reiease 112 Inch 'ax Y.'ater UnderyrDund S.:-&;e Tank(US7) E= win;of oil to soil win;Repo.'.able I Oct Sheen on Su ._ --� Release `.J C '=:bn(s)and Affecting Mom than 2 Cu-;c Yams i Poses Imminent Hard ; of UST Re+me 1 Could Pose Imminent Hz�rd [] Reiesese of Oil to Groundha;er Ex�i ;R4a''� (—i Rer+ease to Groundwater near Cxxrrt*sbon(s) Release De:ec ed in Private Well \Fater Suppy r^ — J Subs:rr ax Non Aqueo Phase Liquid(NAPI) Release to Storm Drain ❑ Re;ease to GmineweW near Equal LD or Gres er 12"an 1t6 Inch and Less than 12 - SchDol or Resi�ence Inch Sanity Seater Release (Imminent Hazard Only) L:51 below the Oils or Haar'ous Materials that exceed weir Re•?a`•abte Corr,.e^rv'a�n or Repo-2-'le ouana'y by the greatest amtwnt. If necessary,a Bch a lot of additional Oil and Hazardous Nater--al su!=arxxs sum to rePo't'*g- Name and Quantities of Oils(0)and Hacardo:.s Materials(HM.)Re"sed: R .sbk atio•n O or HM Released O HM CAS 0 Annex r or Unft ExcOe .It (a,eck one) (d k0wn) Conoc'zsbon (RCS-1,RCS-2;RCGW-1,RCGW-2) #Z heating oil ® ❑ 150 gallons 10 gal,.. ❑ ❑ 0 D. ADDITIONAL INVOLVED PARTIES: Check berm H attaching ramex and add, of awr+eKs of pr apesrties affected hr the Release ex Throat d Reiesse,othex than an o++ner wf+o is submitting this Release Notifcrt on(required). ❑`Check here d aft hinp Licassed Site Professional(LSP)name and sddrsss(optiorn!).Timothy A. T OOtn e y ` Central f ' ' M A c/o Subsurface on� �d� e „ oma � Ira ,Street, R( Revrsea 311195 Supersedes Form BWSC-003 Pape 1 sd 2 Do Not Alter This Fora Massachusetts Department of Environmental Protection BWSC-103 I Bureau of V✓aste Site Cleanup Release Tracking Number I RELEASE NOTIFICATION & NOTIFICATION RETRACTION lJ- j" It assigned b DEP "5 FORit1 Pursuant to 310 CMR 40.0335 and 310 CFJ�R 40.0371 (Subpart C) 9 Y E. PERSON REQUIRED TO NOTIFY: Trask Residence Name of organ3tion: Name of Corttct: 11 C7 szMe 312 Boxford Street Ci:ylTor+n: Aor th Andover State: MA ZIP code: 01845 Telephone: (9$) 5 57:-114 7 Esc: FAX(cp!ional) F. RELATIONSHIP OF PERSON REQUIRED To NOTIFY TO RELEASE OR THREAT OF RELEASE: (check one RP or PRP Specify: Omer O Operator O Generator O T ransponer Q,L'�er RP or PRP:~ Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G:L.c.21 S.2) 1J Agency w Public Uti1'y on a Rinht of 14'ay(as defined by 11.G.L.c.21 E.s. r_I Any Persarn oihenvise R--;uired to Naay 'Specify Relationship: G. CERTIFICATION OF PERSON REQUIRED TO NOTIFY: Deborah Trask a-:est under the pains and pena!:ies of perjury()that I have personalty examined and am f• pan Y g (..) y 'y familiar with the information contained in this submr,.al•includng any and all documents a=rn 7 .n this L ersmiYal fain, a that,based an m inquiry of those indi✓�duals immediately responsible for o7aining the infarma�on,the ratenal informe-lon=rmined in this su5rni=l is,tD the best of my knowledge and be fief,true,accurate and camp,e:t•and(iii)that 1 am tulty a lhoriZed to make L1 s a"es on on behalf of the entity Ictally re5ponsed to, this submrtal. lithe person or entity on whose behalf this submri al is maoe am%:s aware that bare are significant penalties,including,but not limed to, Possible nes and imprisonment,for wilttulry submrring false.inaccurau,or incomp;ee info---ation. Title: Q e (signaure Pr A. t(�}�S1✓ ���I® f Date: (print name of pecan or ersfty retarded in Section E) Eater address of the person providing certifiullion,if different from address rec*rded in Sr_'ion a: Street: CiylTown: " State: ZIP Code: Telephone: Ext.: FAX(optional) YOU MUST COMPLETE ALL RELEVANT SECTIONS•OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. t .. Rewsed 311195 Supercedes Form BWSC-003 Page 2 of 2 00 Not Mar This Form Massachusetts Department of Environmental Protection BWSC-105 Bureau of Waste Site Cleanup s Release Tracking Number IMMEDIATE RESPONSE ACTION (IRA) TRANSMITTAL FORM Pursuant to 310 CMR 40.0424-40.0427(SubpartD) E -1 20874:] A. RELEASE OR THREAT OF RELEASE LOCATION: Release Name:(op;ionsal) Trask Residence Street: 312 Boxford S-L r e e% Location Aid: Cayfrovm: North Andover ZIP code: 01845 Check here if a Tier Classification Submittal has been provided to DEP for this Release Tracking Number. ❑ Check here if this location is Adequately Regulated,pursuant to 310 CMR +0.0110-0114. Specify Program: ❑ CERCLA ❑ HSWA Corrective Action ❑ Solid Waste Management ❑ RCRA State Program(21C Facilities) Related Release Tracking Numbers That This IRA Addresses: B.THIS FORM IS BEING USED TO: (check all that apply) ;X Submit an IRA Plan(complete Sections A,B,C,D,E,H,I,J and I). Check here if this IRA Plan is an update of modification of a previously approved wri ten IRA Plan. Date Submitted: 17 Submit an Imminent Hazard Evaluation(complete Sections A,B,C,F,H,I,J and I). ❑ Submit an IRA Status Report(complete Sections A,B,C,E,H.I,J and I). Submit a Request to Terminate an Active Remedial System and/or Terminate a Continuing Response Action(s)Taken to Address an Imminent Hazard(complete Sections A,B,C,D,E,H,I,J and K). ❑ Submit an IRA Completion Statement(complete Sections A,B,C,D,E,G,H,I,J and K). You must attach all supporting documentation required for each use of form indicated,including copies of any Legal Notices and Notices to Public Officials required by 310 CMR 40.1400. C. RELEASE OR THREAT OF RELEASE CONDITIONS THAT WARRANT IRA: Identify Media and Receptors Affected: (check all that apply) �j'{ Air ❑ Groundwater ❑ Surface Water ❑ Sediments D Soil ❑ Wetland ❑ Storm Drain ❑ Paved Surface U Private Well ❑ Public Water Supply ❑ Zone 2 g Residence ❑ School ❑ Unknown ❑ Other Specify: Spill o c c u r e d within 100 feet private well Identify Conditions That Require IRA,Pursuant to 310 CMR 40.0412 (check all,that apply) [�- 2 Hour Reporting Condition(s) ❑ 72 Hour Reporting Conditions) ❑ Substantial Release Migration ❑ Other Condition(s) Describe: Identify Oils and Hazardous Materials Released: (check all that apply) L Oils ❑ Chlorinated Solvents ❑ Heavy Metals ❑ Others Specify: D. DESCRIPTION OF RESPONSE ACTIONS: (check all that appy) ❑ Assessment and/or Monitoring Only ❑ Deployment of Absorbent or Containment Materials u Excavation of Contaminated Soils ❑ Temporary Covers or Caps Re-use,Recycling or Treatment ❑ Bioremediation Q On Site a Off Site Est.Vol.: 15 0 cubic yards ❑ Soil Vapor Extraction Describe: pcs disposal at recycling facilit}I❑ Structure Venting System ❑ Store O On Site O Off Site Est.Vol.: cubic yards ❑ Product or NAPL Recovery ❑ Landfill O Cover O Disposal Est,Vol.: cubic yards ❑ Groundwater Treatment Systems Removal of Drums,Tanks or Containers ❑ Air Sparging Describe: ❑ Temporary Water Supplies SECTION D IS CONTINUED ON THE NEXT PAGE. Revised 224/95 Supersedes Forms BWSC-005, 006, 010(in part)and 011 Page 1 of 3 rin Nnf GNor Thic Fnrm Massachusetts Department of Environmental Protection BWSC-105 L, Bureau of 14/Gs'e Sife Cleanup Release Tracking Numt,�r ?� IMMEDIATE RESPONSE ACTION (IRA) TRANSMITTAL t FORM Pursuant to 310 CMR 40.0424- 0.041- (Subpart D).. 13 -12 874 D. DESCRIPTION Or RESPONSE ACTIONS(continued): Removal of Other Co;a;n?nate!t.".:- '? Temporary Evacuation or Relocation of Residents Specify Type and Volume: 1 drum o i 1 debris Fencing and Sign Posting OX Other Response Actions Describe: pat;o n t-i a 1 nt-pr rprn\7pry 5.0,000 gallon est . 17 Check here if this IRA involves the use of Innovative Technologies(DEP is interested in using this information to aid in creating an Innovative Technologies Clearinghouse). ' Describe Technologies: E. TRANSPORT OF REM EDIATION WASTE: (if Remediation Waste has been sent to an off-site facility,answer the following questions) Name of Facility. none to'T�3•te Town and State: Quantity of Remediation Waste Transported to Date: := F. IMMINENT HAZARD EVALUATION SUMMARY: (check one of the following) (] Based upon an evaluation,an Imminent Hazard exists in connection with this Release or Threat of Release. Based upon an evaluation,an Imminent Hazard does not exist in connection with this Release or Threat of Release. Based upon an evaluation,it is unknown whether an Imminent Hazard exists in connection with this Release or Threat of Release,and further assessment activities will be undertaken. Based upon an evaluation,it is unknown whether an Imminent Hazard exists in connection with this Release or Threat of Release. However, response actions will address those conditions that could pose an Imminent Hazard. G. IRA COMPLETION STATEMENT: ❑ Check here if future response actions addressing this Release or Threat of Release will be conducted as part of the Response Actions planned +, for a Site that has already been Tier Classified under a different Release Tracking Number,or a Site that is identified on the Transition List as described in 310 CMR 40.0630(.e.,a Transition Site,which includes Sites with approved Waivers). These additional response actions must occur according to the deadlines applicable to the earlier Release Tracking Number(i.e.,Site ID Number). 8-88888 State Release Tracking Number(i.e.,Site ID Number)of Tier Classified Site or Transition Site: If any Remediation Waste will be stored,treated,managed,recycled or reused at the site following submission of the IRA Completion Statement,you must submit either a Release Abatement Measure(RAM)Plan or a Phase IV Remedy Implementation Plan,along with the appropriate transmittal form,as an attachment to the IRA Completion Statement. H. LSP OPINION: I attest under the pains and penalties of perjury that I have personally examined Ad am familiar with this transmittal form,including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 330 CMR 4.02(1),(i)the applicable provisions of 309 CMR 4.02(2)and(3),and(ii)the provisions of 309 CMR 4.03(5),to the best of my knowledge, information and belief, > if Section B of this form indicates that an Immediate Response Action Plan is being submitted,the response action(s)that is(are)the subject of this submittal n has(have)been developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are) appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)complies(y)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B of this form indicates that an Imminent Hazard Evaluation is being submitted,this Imminent Hazard Evaluation was developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.003,and the assessment activity(ies)undertaken to support this Imminent Hazard Evaluation complies(y)with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0.700; > if Section B of this form indicates that an Immediate Response Status Report is being submitted,the response action(s)that is(are)the subject of this submittal O is(are)being implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(i)is(are) appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(i)complies(y)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B of this form indicates that an Immediate Response Action Completion Statement ora Request to Terminate an Active Remedial System and/or Terminate a Continuing Response Action(s)Taken to Address an Imminent Hazard is being submitted,the response action(s) that is(are)the subject of this submittal(i)has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.c.21E and 310 CMR 40.0000,(i)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provision&of M.G.L.c.21 E and 310 CMR 40.0000 and(ii)complies(y)with the identified provisions of all orders,permits,and approvals identified in this submittal. SECTION H IS CONTINUED ON THE NEXT PAGE. A Revised 224195 Supersedes Forms BWSC-005,006, 010(in part)and 011 Page 2 of 3 M Nnl l Nor Thie Fnrm Massachusetts Department of Environmental Protection BWSC-105 !j,-e;!2rr of 1A4- Site C' ?,7UP Release Tracking Number IMMEDIATE RESPONSE ACTION IRA} TRANSMITTAL � FORM Pursuant to 310 CIAR 40.0424-4 .042 (Subpart D) D3 20874 H. LSP Opinion(continued): I am aware that sioni`::ant penis";es may re-suit,inclvdinp,but not tim3ed to,h--,sibie fsnes and imprisonment,if I submit information which I know to be false, inaccur-ate or materaily incomplete. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order tiAg%s�andlor approval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement ident.ifying the applicable provisionsp. F h LSP Name: y A.Timoth AToomey LSP#: 2891 stamp: 978 948 3861 Ext.: �I� ��'1 Telephone: -+ FAX:(optional) �oNO.2WI y eSignature: Date: 1. PERSON UNDERTAKING IRA: Name of Organization: t r a c k residence NameofContact Deborah Trask Title: Street: 312 Boxford Street City/Town.. North Andover State: MA ZIP Code: Telephone: 978 557 1147 Ext.: FAX(optional) u Check here if there has been a change in the person undertaking the IRA. J. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING IRA: (check one) RP or PRP Specify: (�) Owner O Operator O Generator O Transporter Other RP or PRP: Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E,s.2) Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.5(j)) Any Other Person Undertaking IRA Specify Relationship: K. CERTIFICATION OF PERSON UNDERTAKING IRA: I, Deborah Trask ,attest under the pains and penalties of perjury(l)that I have Fersonal!y examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(ii)that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. Irthe person or entity on whose behalf this submittal is made ams aware that there are significant penalties,including,but not limited to, rvtcc7h1a f and imnricnnmPnt fnr willfiilly ct ihmittinn fwlsP inam vatP ry inrmmniPtP infnrmatinn Title: ) l�VA-e� By: For (signaITf&o r A XTP-fiS�— Date: (print name of person or entity recorded in Section 1) Enter address of the person providing certification,if different from address recorded in Section I: Street City/Town: State: ZIP Code: Telephone: Ext,: FAX:(optionaQ YOU MUST COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Revised 2/24195 IN. Supersedes Forms BWSC-005,006, 010(in part)and Ot 1 Page 3 of 3 f)n Nnt Aar This Fnrm ATTACHMENT 2 EXETER ENVIRO!!'MITNTAL ASSOCIATES, WC. ?e^ o^;ng! P.O.Box 451,Exeter, NH 03833 (603) 778-3988 Boring Number f` '�'1 Pr 'ect Trask property,312 Boxford Street,North Andover, MA Sheet No. 1 of 2 Client Safety Insurance Company Protect No. 1294.13 Boring Contractor NH Baring Casino Elevation NA Dian s.?e Pay 2 C,Lund=(e.• San NA Well ConstructionDate 8-13 to 8-14, 201 Screen Length 10' 30.2-20.21 Top of Bentonite 14.0 Driller Bob Dohertv Top of Sand 17.0 Standpipe: flush mount Inspector or Tim Warr CL Sample Sample Descripbzt-s Well VOC 0 No. Blow Comed Cl Comet and Const Remarks (ppm) NA 0-0,3 Asphalt. - Bkg 1 S-1 Brown, Gravelly fine to coarse S and, ^ w^ little Silt. Dry. 2 2" PVC riser pipe w 3 4 A" A" 5 S-2 16 Very Dense, brown,Gravelly fine to Bkg 52 coarse Sand, little Sift. Dry. Till. native back fill 6 100/3" 7 A cored through boulder from "A 6.5-9.0 feet 8 9 S-3 48 Very Dense, brown, Silty fine to coarse Bkg 56 Sand, little fine to coarse Gravel. Dry. Till. 10 76 11 78 12 13 A A" 14 15 S-4 103/30 No recovery. 16 C-1 9 min bentonite seal Cored from 15.5-21.0. Highly fractured 4 min Diorite. Took 7 runs to get to 21 feet. 17 High angle fractures present. 3 min ROD=0%. 18 Minor iron staining on fracture faces. mi 19 3 n 20 5 min 21 _ C 25 min 2 P 1.0-25.5. Competent Diorite. Weathered fracture at 23.1 feet. 22 6 min OD R 93%. well >:.y.;. 2 PVC screen 6 min u x z:_ ® measured water EXETER ENVIRONMENTAL A SSOCIA TES, INC. Test Boring Log P.O. ;"DXx 451, 03833 (603) 776-3988 Boning Nurnbar Prcy,ect Trask property,312 Boxford Street,North Andover,IAA Sheet No. 2 of 2 Client Safety Insurance Company Praect No. 1294.13 Haring Contractor NH Boring J Casing Elevation NA Locafon s,7-3 Faure 9 G-ound Eeva'atron NA Well Constiction Date 8-13 to 8-14, 201 I.., Screen Length 10' (30.2-20.2) Top of Bentonite 14.0 Duller Bob Dohertv Top of Sand 17.0 Standpipe: flush mount Inspecor Tim Warr jk Sample Sample Des-m. ptions Well Remarks VOC NoBlmv Count and Clas0cation Const. (ppm) . 25 C-3 6 min Diorite from 25.55 to 27.5. ROD=90% silica sand 26 Quartz vein: 27.5 to 30.2. ROD=50%. — 6 min Vertical fractures in quartz with minor 27 minerlization. 2" PVC well screen 5 min —28 9 min —29 8 min —30 —31 —32 —33 34 —35 —36 —37 —38 —39 —40 —41 —42 —43 —44 45 —46 L 47 Environmental Labora#ories Corporation 111 Herrick Street, Merrimack, NH 03054 TEL: (603)424-2022•FAX: (603)429-8496 August 30,2001 Tian Toomey Subsurface Remediation Technologies 355 Central St. Rowley,MA 01969 _:TEL (978)948-3861 .- FAX: (978)948-')861, RE: Trask Residence Order No.: 0108217 Dear Tim Toomey: AMRO Environmental Laboratories Corp. received 2 samples on 8/23/01 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds national Environmental Laboratory Accreditation Conference(NELAC), state,and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s)upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time, AN- IRO will properly dispose of the remaining sample(s). If you require further analysis,or need the samples held for a longer period, please contact us immediately. This report consists of a total of pages. This letter is an integral part of your data report. If you have any questions regarding this project in the future,please refer to the Order Number above. Sincerely, �V Nancy Stewart Vice President/Lab Director AMRO Environmental Laboratories Corp. Date: 30-Aug-01 CLIENT: Subsurface Remediation Technologies Project: Tr;sly P�--Jde!-ze Wor�1 Order Sample Summary Lab Order: 0108217 Date Received: 8/23/01 Lab Sample ID Client Sample ID Collection Date 0108217-01 A Drinking Water Well 8/22/01 0108217-02A Exeter MW 8/22/01 a y` 1 2 yr r AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 AIM R0 i0: Project Name: [ e5i�:i�CA_ Date Rec.: Snip via: (circle one) Fed Ex.. UFS �t,ouner. Date Due: - 50-0 t Hand Del.. Other Courier. Other o� +, .� , Ys 1 Ne NA I Comments 1!ams to be Checked. _?on .�_:p. 1. Army Samples received in individual plastic bacs? 1 2. Custody Seals present? 1 3. Custody Seats Intact? I i V 1 4. Air Sill included in folder if received? I 1 5. Is COC included with samples? ✓ 1 ( I 5. Is COC signed and dated by client? C 1 7. Laboratory receipt temperature. TEMP = 1 Samples rec.with ice— packs_neitrer 8. Were samples received the same day they were sampled? ( ( 1 Is client temperature 4'C ±2'C? ✓ I 1 1 If no obtain authorization from the client for the analyses. 1 Client authorization from: Date: Obtained by: 1 9. Is the COC filled out correctly and completely? I 1 1 10. Does the info on the COC match the samples? V I 11.Were samples rec.within holding time? ✓ 1 1 12.Were all samples property labeled? 1 1 1 13.Were all samples properly preserved? 1 1 1 14.Were proper sample containers used? ✓ 1 1 1 15.Were all samples received intact? (none broken or Ie-=kinc) i 1 15.Were VOA vials rec.with no air bubbles? ✓ 1 I 1 17. Were the sample volumes sufficient for requested analysis? ✓ 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH(circle one): M=Methanol, E=EnCore (air-tight c,ntainer) Sampling Method VGA(circle one): M=Methanol, So=Sodium Bisulfate. E=EnCore, S=Bulk If M or SB: I I Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial?. If NO then client must be faxed. Were vials provided by AMRO? 1 If NO then weights MUST be obtained from client Was dry weight aliquot provided? I i I If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: I ✓ 1 1 1 What samples sent: 0A l ( 1 Where sent:CVS eOk5ewe- Date: $111;111 /0 k Analysis: TAT: cQ $ 21. Information entered into. Internal Tracking Log? ✓ Dry Weight Log? Client Log? I ✓ Composite Log? Filtration Log? Received By: fA Date: g�'a,370{ Logged in By: J`?Lw�. Date: �a'+l of Labeled By: LV--, Date: 'a o��lo l Checked By: Date: -v - NA= Not Applicable gc'gcmemos/formsisamplerec Rev.18 06100 AMRO Environmental 111 Herrick Street Laboratories Corporation Merrimack, NH 0304 � Please Circle Ir:Sample= Soil Soil Samole=Waste List := I� Preserv. Volume Final ._ _ nc-r `i n I m Preservative ad� VC�Um� f..-c.V. I u"ll;lcl nG�..r:culC. n�.C�u by JOIE.C Dadjusted Sample !D Analysis I Samo!e l vUsted cH Y or N AMRO of FreseN. Added pH 01-oaA L- 15%gbm<I FIC I I I it i I I I I i i I i I i i I I i i I I i i i I i l i l i i I t i I i I I I I i I I i pH Checked A Date: pH adjusted By: Date: gcfgcmemos/forms/samplerec Rev.18 06100 AMRO Environmental Laboratories Corporation CIIAIN-OF-CUSTODY RECORD Office: (603)424-2022 ' I I I Merrick Street 40381 Fax: (603)429-8496 Merrimack,N1103054 Project No.: Project Name: r -e Pruject Manager: Sam ters Swi, ure): AMRO Pro'ect No.: 3.' Project State: (/(/t S J14 -ss?Sample ID Date/Time Matrix Total -Analysis Rc quircd' — • C Remarks Sampled A=Air of Cont. a ? S=Soil &Size ;o r•, 10 GW=Ground W. ' r WW=Waste W. � DW=Drinking W. O=Oil �J� se Other—Specify �l 3 lac.L Preservauve: -EI ,McOH,N-HNO ,S-H2S 4,Na-Na H,O-Ot to ontatner ype: P-Y astnc, - as. -V to, -1 a on,(T-0—t 11er NOTES: rescrva�fives,S�ccial reporting limits,Known Contamination,etc; Please print clearly,legibly and completely.Samples can not be logged in and the turnaround time clock will not start until any FAX No.: ambiguities are resolved. Send Results To: ScalIntact? GW-I G1V-2 GIV-3 'Yes No N/A MCILcvcl�'Nccdcd: fi-• •..Relin uish By Date/Time d -cived By natc/Time P.O.No: /�(kJ PRIORITY TURNAROUND TIME AUTHORIZATION Before submitting samples for expedited TAT,you mutt have requested Results Needed in advance and received a coded TAT AUTHORIZA ION NUM is i R • By: �"'�.QUTIIOKIZATION No. 13Y: Whi/. ab Copy Yellow:Accompani s RcpQrt._.% Pink:Client Copy ' 317 Elm Street Tel(603)673-5440 r-cT '-- r "� •- '� Fax(603)673-0366 August 28, 2001 Ms.Nicole Borduz AMRO Environmental Laboratories Corp 111 Herrick Street Merrimack, NH 03054 Job Name: AX � Laboratory#: 01080150 Job#: 0108217 Purchase Order#: N/A Location: NIA Control#: 38118 Dear Ms. Borduz Enclosed please find the laboratory results for the above reference samples that were received by the ChemServe sample custodian, under chain of custody control number 38118 on 08/27/01. Samples were collected on 08/22/01. Any abnormalities to the samples on receipt would be noted on the enclosed chain of custody document. This report is not valid without a completed ChemServe chain of custody with the corresponding control number, attached. All samples analyzed by ChemServe are subject to quality standards. These standards are either as stringent or more stringent that those established under 40 CFR Part 136, state certification and corresponding methodologies. ChemServe h written programs, P 9 as ,tten QA/QC Procedures Manual that outlines these standards, and is available, upon reque t, for your reference. Unless otherwise stated on the Chain of Custody or within the report, all holding times, preservation techniques, container types, and analytical methods are analogous with those outlined by them U.S. EPA. certify that I have reviewed the above referenced analytical data and state forms, and I have found this report within compliance with the procedures outlined in the ChemServe QA/QC Procedures Manual. Ellen Abrams-QA/QC Manager Jay Chrystal-,Prei e La ratory Director This report contains 8 pages. \N ACCp .90 ` ♦ .. tic T 'C C� C? Jsua4 ..4 a _ s Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-01 JOB NAME: 0108217 JOB#: N/A LOCATION: NIA SAMPLE IDENTITY:0 1 A Drinking Water Well CONTROL#:38118 DATE SAMPLED:08/22/01 DATE RECD:08/24/01 DATE ANALYZED:08/27/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL. COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE ADL ,�L ; .-- _ 0.5•>,.: _. _ BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHAN E BDL 0.5 DIBROMOME T HANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 5 0.5 2,2-DICHLOROE'ROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL .0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED:1 OF 2 PAGES Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-01 JOB NAME: 0108217 LOCATION: NIA SAMPLE IDENTITY:01A Drinking Water Well CONTROL#:38118 DATE SAMPLED:08/22/01 DATE RECD:08/24/01 DATE ANALYZED:08/27/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1..1.1-TRICHLOROETHANE: ..., ,9DL 1,1,2-TRICHLOROETHANE SDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES. BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZEN E BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD t� 00. �, 3 Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB":01080190-02 JOB NAME: 0108217 JOB'": NLA LOCATION: N/A SAMPLE IDENTITY:02A Exeter MW CONTROL It:38118 DATE SAMPLED:08/22/01 DATE REC'D:08!24/01 DATE ANALYZED:08/27/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE -PDL 0.5..= �a,_:.__ BROMOBENZENE BDL 0.5 BROMOCHLOROM ETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 D ISROMOCHLOROM ETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHAN E BDL 0.5 1,1=DICHLOROETHENE BDL 0.5 CIS-1,2-OICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL -0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED:1 OF 2 PAGES C? I '. Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 A METHOD HOD 524.2 CUSTOMER:AMRO LAB#:01080190-02 JOB NAME: 0108217 LOCATION: N/A SAMPLE IDENTITY:02A Exeter MW CONTROL#:38118 DATE SAMPLED:08!22/01 DATE RECD:08/24101 DATE ANALYZED:08!27/01 • MATRIX:LIQUID " DETECTION LIMIT BASED ON PO'L COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) ,j (UG/L)X 1 1,1;1-TRICHLOROETHANE ;. _ .FDL .-V- :»�,-` , 0.5.:..- 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-11SOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD j CHEMSERVE VOA SPIKE RECOVERY FORM EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-01 JOB NAME: 0108217 LOCATION: NIA SAMPLE IDENTITY:MATRIX SIPKES 01080169-01 &01080190-01 CONTROL#:38118 DATE ANALYZED:08/27/01 COMPOUND CONC ADDED AMT REC DUP AMT REC %REC DUP%REC %RPD (UG/L) (UG/L) (UG/L) 1,1-DICHLOROETHENE 4 3.3 4.7 83% 118% 9% BENZENE 4 4.8 4.4 120% 110% 2% TRICHLOROETHENE 4 4.3 4:0 i_ = >r 08%"a: =100%: -_= 2% = CHLOROBENZENE 4 3.6 3.4 90% 85% 1% 1,2-DICHLOROBENZENE 4 4.3 4.0 108% 100% 2% 1,3,5-TRIMETHYLSENZENE 4 3.9 3.7 98% 93% 1% 1,2,4-TRICHLOROBENZENE 4 4.8 4.4 120% 110% 2% VOA MATRIX SPIKE REC 6 �5 4 _ _ i M CONC ADDED UG/L 3 13 LW RECOVERY OLD RECOVERY RECOVERY 1 Y _ 0 - 1 2 3 4 5 6 7 SPIKE RECOVERY LIMITS 70-130% I (; [it; ► lull s C.!ain of Custody No. 38118 • ,1 v .317 Elm Street Milford, NH 03055 Nlidtiple COC's Yes No (603) 673-5440/Fax (603) 673-0366 —�— CHAIN OF CUSTODY B 1 1 C 1 ' 1 C1JSTOMER: %'7�C. r _ JOB NAME: TURNAROUND TIME:(CIRCLE ONE:) ADDRESS: JOB NUMBER: STANDARD TUSH 7 <<( fi; RUSH T.A.T. (CHECK w/LAB) CITY/STATE/ZIP LOCATION: - TI iLEPI LONE: TELEPHONE: AMBER GLASS(AG) / GLASS(G) I PLASTIC(P) p 4 Ri TORT TO: CONTACT: P0 NUMBER: QUOTE NUMBER: Go �wQ SAMPLE 1 MATRIX Q44 li^j Z SAMPLE IDENTIFICATION&LOCATION COLLECTED TYPE a sol-11)(s) a O CONIBINFD(C) ® ANALYSIS Q V HAZARD(It) OQj DAIE TIME LiAIL 1011: VAIL• TIME DATI 11ME DALE UbIL DALls UrAL DAT TIML CUSTODY SAMPLER: LN1111ARY SAMPLE CHECK LIST: FIELD READING(S): DATE TIME RECEIVED WITIIIN IIOLD TIME- FiSIOR NO (print name) RECEIVED IN GOOD CONDITIOrtaES/OR NO SIGNATURE: TEMP BLAN C e0-c-o DALL• 7im-, SHIPPED ONCHA�NDELIVERED. RF ,INQUISI IED: SAMPLES WERE PROPERLY PRESERVED YF.� IID_NIA 11A1'L• ]]ME SAMPLES WERE FILTERED IN FIELD B N/A RE-1 F;IVED: IF NO EXPLAIN: , DA1E TIMI: RELINQUISHED: 4�0 RIS I IVSD POR i_All112A 11ME GI AMRO Envirorunental Laboratories Corporation CHAIN-OIC-CUSTODY RECORD Office:(603)424-2022 111 lierricic Strect 41 57 6 Tax:(603)429-8496 Merrimack,NII 03054 Project No.: Project Name:, 0 n 2� -0 Qa A Project Manager: Samplers(Signature): AMRO Project No.: Project State: Sample ID Date/Time R� Matrix Total t/ Analysis Required Remarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. „WW=Waste W. Cti :r DW=Drinking W. - ii 0=Oil ? Other-Specify L'I l J j 7 i f i I'reserv_:tive:,C1-ICI, e . 1,N-1-IN03,S-112SO4,Na-NaOH,I, -Other Contat%rr ype: P-P anti G- ass,7-Vial,T-Te pin—O-Ot ter Please print clearly,legil; V and completely.SantpRs can not he NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnarwind time clock will not start until any FA\No.: Q ambiguities are resolved. Send Recalls To: ¢ Seallntact? G11'-I GW-2 GW-3 1 Z e 'C !-S, . Yes No N/A MCP Level Needed: �- Relinquished By Date/Time gceived By Date/Time P.O.No: I PRIORITY TURNAROUND TIME AUTHORIZATION FXT 1-b / � / t Before submitting samples fbi expedited TAT,you must have requested Results Needed in advance and received a coded.TAT AUTHORIZATION NUMBER r lly: AUTHORIZATION No. BY: SHEET Ol. Wfzite: 1'�b Copy Yellow: Accompanies Report Pink:Client Copy 111z I SIR NEW HAMPSHIRE ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM Laboratory:Chemserve.Inc.,317 Elm Street,Milford,NH 03055 16031 673.5440 Page 1 of 4 i Certificate Number: 100600•E • 0310 Of 11131,18: June 25,2001 . Expiration Date:December 2,2001 ACCREDITS THE ABOVED MENTIONED LABORATORY FOR THE FOLLOWING ANALYSES: (tate of Debit J hlllpgl)ire z ,� EPA 200.0 ORtNKNO WATER MICRO ORINKINO WATER INORGANIC CONTAMINANTS l6nt 1 f�k,. tj 0ibironmentai laboratorp RIVrogrant 1 ' •,rt EJ :• E.Cog ICoh4nt SM 9227 a a VV Mtdu•N: K. •,, 1:, 1t.w.1,.ph6C Flu.Cant: SM 9215 a ,, Sulfa: EPA 200.0 ,:;,,r„1:.:• {' � Toul CoKlam: SM 9211 a ��- �•,'y`' 4 Toth Fat,Re.W-tTOSI: SM 264OC i Toal Coelom: SM 9271 a LS iot.l Co.Iam: SM 9123 a Turbldlryt EPA Ia0.1 Awards Primary Acctditalion to 1 DRINKING WATER METALS �,r 4 DRINKING WATER TRIHALOMETNANES N T_ aS Ak my i: EPA 200.7 Amtmonr: EPA 200.9aromodkhlwcmeth.m: EPA$24.2 I� {' Mrsrre: EPA 200.7 aromolorm EP CA'R4.2 (�etn1crbe,_'�IIc. a..bm: EPA 200.7 Chlorodlbromom.tmm: EPA 524.2 r Or a.ha/^ N : EPA 200.7 Chbroform: EPA 574.2 d C.dm:.n: EPA 200.7 rotor Trlh.tom.th.m.: : EPA 524.2 ' ' liitorb, C.khw : EPA 100.7 EPA 200.7 (� DRINKING WATER VOLATILE ORGANICS topp.r: EPA 700.7 , v'4l l_ eon; EPA 200.7 't• \ L4.d: EPA 200.9 1,11,1,2-Twtetdowethem: EPA 324.2 ' For the analyses listed on the attached"page(s) in accordance with 1 M.ng.m.s: EPA 200,7r 1,1.1•TrkMoroath.nu EPA 524.2 7 Mercury: EPA 245.1 1,1,2.2-T.Otchloroeth4mt EPA$24.2 the provisions of the NELAC Standards and Env-C 300. ,: EPA 200•7 ,,1.2-Trkhkreah.m: EPA 524.2 EPA 200.9 1,1.Okhtoresthan.: EPA 924.2 EPA 200.7 1,t•Okhloro.thvie.e: EPA$24.2 t ,5 ff A Sodhn,: EPA 200.7 1,1.Okhlomprep.m: EPA 514.2 T1.111um: EPA 200.9 1,2.2•TrIcNambenlsoa: ' EPA 324.2 `• 1,2.2•TrkMaroprep.m -•�EPA 534.2 w� /`• 22r.c: EFA 200.7 ' `..'�1 / 1,2,4.1rkMoreb4num: s EPA$14.2 L; DRINKING WATER INORGANIC CONTAMINANTS 1,2.4•TrImNAYib.nnml EPA$24.2 }Y EPA 524,2 Ara.TvaiiT; EPA 3tO.l 1,2.01cMoro.th.n4: EPA 514.2 di f' Mj1i 1T; SM 2710 0 1,2.01chtoroproP.m: EPA 524.2 ^ k,."%' tt 1,2-Okhloreb.nr.m; EPA 524.2 EPA 700.0 i a.onJds: 4• 11 Certificate Number 100800 �r" ` C,�,,d.: EPA 700.0 1.2.OkMaopr.O.n4: EPA 524.2 EPA 624, C.rd..ctmrti3wcdk Cond,l:ErA 120.1 Date of Issue:January 2A.2001 Cabwh..ntsp«dk Com.I:SM»w a 1.4 DkNoroMnt.m: EPA 314.2 2.2•01cidoropropeme EPA 924.1 Rs.du.l F..s SM 4SOO-CT C J2•CAlorotolwm: EPA 324.2 C►.rJd.,Tot.l: EPA 775.7 ✓'y'{.f`5 Expiration Date:December 2,2001 -J .1�LG..O �.•/ C9..Jd..Toth: SM 45OO-CN C 4-CNorotolwnst 1w EPA 924.2 n V Ptoyam Mamgct � C9••d•.iotd: SM 4SOO CNE 449opr0p911o1u.n4; EPA 524.2 f,• : F*world.; EPA 700.0 a.nt.m: EPA 524.2 .. ��y''.s! � j Mu.w•N: EPA 100.0 Womob.m°m: EPA 324.2 , 1;tiSiY_ C-,-dg dbr"a.m.L aV-d,m__dW mN^i►.,k4.Af.o 6 v r'^/- Cs.r .. � -eq-U),d.I.t...r,.,'.....aa..,r M Dain,1601)371.1991 w 1601)171.7995 o< \ . e a 1Hs e.nlGe.0 wupemdes an prniowM k.wd cen11k6N.. ��'�'�"•-• hogrem M 4f ATTACHMENT 3 i Town of North Andover �/ ! Health Department Date: I �.Oe � Location: (Indicate Address, if Residential ame of Business)) �)1 Check#: `�f�✓D' Type of Permit or License: (Circle) ➢ Animal $ ➢ Dumpster $ ➢ Food Service-Type: $ ' ➢ Funeral Directors $ ➢ Massage Establishment $ ➢ Massage Practice $ ➢ Offal(Septic)Hauler $ ➢ Recreational Camp $ ➢ SEPTIC PERMITS: ❑ Septic-Soil Testing $ ❑ Septic-Design Approval $ ❑ Septic Disposal Works Construction(DWC)$ ❑ Septic Disposal Works Installers(DWI) $ ➢ Sun tanning $ ➢ Swimming Pool $ ➢ Tobacco $ ➢ Trash/Solid Waste Hauler $ ➢ Well Construction $ .� �11� ➢ OTHER:(Indicate) 7= .117 Health Agent Initials SI- 0 White-Applicant Yellow-Health- Pink-Treasurer COMMONWEALTH OF MASSACHUSETTS �O EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS blZl DEPARTMENT OF ENVIRONMENTAL--P Lg1N f M# 5" APR 18 2006 TOWN OF NORTH ANDOVE' HEALTH DEPARTMENT TITLE 5 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM FORM PART A CERTIFICATION Property Address: 312 Boxford Street_ —North Andover Owner's Name:_Robert Trask_ Owner's Address:_312 Boxford Street _North Andover,MA 01845_ Date of Inspection:_3/31/2006_ Name of Inspector: Neil J Bateson_ Company Name: Bateson Enterprises Inc._ Mailing Address:_111 Argilla Road_ _Andover,Ma.01810_ Telephone Number:_(978)4754786_ CERTIFICATION STATEMENT I certify that I have personally inspected the sewage disposal system at this address and that the information reported below is true,accurate and complete as of the time of the inspection.The inspection was performed based on my training and experience in the proper function and maintenance of on site sewage disposal systems. I am a DEP approved system inspector pursuant to Section 15.340 of Title 5(310 CMR 15.000). The system: X Passes Conditionally Passes Needs Further Evaluation by the Local Approving Authority "Rffls Inspector's Signature: Date: 3/31/2006 The system inspector shall submit a copy of this inspection report to the Approving Authority(Board of Health or DEP)within 30 days of completing this inspection.If the system is a shared system or has a design flow of 10,000 gpd or greater,the inspector and the system owner shall submit the report to the appropriate regional office of the DEP.The original should be sent to the system owner and copies sent to the buyer,if applicable,and the approving authority. Notes and Comments: ****This report only describes conditions at the time of inspection and under the conditions of use at that time.This inspection does not address how the system will perform in the future under the same or different conditions of use. Page 2 of 11 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART A CERTIFICATION (continued) Property Address: 312 Boxford Street _North Andover— Owner:—Trask— Date Trask_Date of Inspection: 3/31/2006_ Inspection Summary: Check A,B,C,D or E/ALWAYS complete all of Section D A. System Passes: X I have not found any information which indicates that any of the failure criteria described in 310 CMR 15.303 or in 310 CMR 15.304 exist.Any failure criteria not evaluated are indicated below. Comments: B. System Conditionally Passes: One or more system components as described in the"Conditional Pass" section need to be replaced or repaired.The system,upon completion of the replacement or repair,as approved by the Board of Health,will pass.Answer yes,no or not determined(Y,N,ND)in the for the following statements. If"not determined"please explain . The septic tank is metal and over 20 years old*or the septic tank (whether metal or not)is structurally unsound,exhibits substantial infiltration or exfiltration or tank failure is imminent. System will pass inspection if the existing tank is replaced with a complying septic tank as approved by the Board of Health. *A metal septic tank will pass inspection if it is structurally sound,not leaking and if a Certificate of Compliance indicating that the tank is less than 20 years old is available. ND explain: Observation of sewage backup or break out or high static water level in the distribution box due to broken or obstructed pipe(s)or due to a broken,settled or uneven distribution box. System will pass inspection if(with approval of Board of Health): broken pipe(s)are replaced obstruction is removed distribution box is leveled or replaced ND explain: The system required pumping more than 4 times a year due to broken or obstructed pipe(s).The system will pass inspection if(with approval of the Board of Health): broken pipe(s)are replaced obstruction is removed ND explain: Page 3 of 11 OFFICIAL INSPECTION FORM - NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART A CERTIFICATION(continued) Property Address: 312 Boxford Street _North Andover Owner:_Trask_ Date of Inspection: 3/31/2006_ C. Further Evaluation is Required by the Board of Health: Conditions exist which require further evaluation by the Board of Health in order to determine if the system is failing to protect public health,safety or the environment. 1. System will pass unless Board of Health determines in accordance with 310 CMR 15.303(1)(b)that the system is not functioning in a manner which will protect public health,safety and the environment: _ Cesspool or privy is within 50 feet of a surface water _ Cesspool or privy is within 50 feet of a bordering vegetated wetland or a salt marsh 2. System will fail unless the Board of Health(and Public Water Supplier,if any)determines that the system is functioning in a manner that protects the public health,safety and environment: _ The system has a septic tank and soil absorption system(SAS)and the SAS is within 100 feet of a surface water supply or tributary to a surface water supply. The system has a septic tank and SAS and the SAS is within a Zone 1 of a public water supply. _ The system has a septic tank and SAS and the SAS is within 50 feet of a private water supply well. The system has a septic tank and SAS and the SAS is less than 100 feet but 50 feet or more from a private water supply well". Method used to determine distance_ "This system passes if the well water analysis,performed at a DEP certified laboratory,for coliform bacteria and volatile organic compounds indicates that the well is free from pollution from that facility and the presence of ammonia nitrogen and nitrate nitrogen is equal to or less than 5 ppm,provided that no other failure criteria are triggered.A copy of the analysis must be attached to this form. 3. Other: Page 4 of 11 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART A CERTIFICATION (continued) Property Address:_312 Boxford Street_ _North Andover— Owner:_Trask_ Date of Inspection: 3/31/2006 D. System Failure Criteria applicable to all systems: You must indicate"yes"or`ho"to each of the following for all inspections: No Backup of sewage into facility or system component due to overloaded or clogged SAS or cesspool No Discharge or ponding of effluent to the surface of the ground or surface waters due to an overloaded or clogged SAS or cesspool No Static liquid level in the distribution box above outlet invert due to an overloaded or clogged SAS or cesspool _No Liquid depth in cesspool is less than 6"below invert or available volume is'/2 day flow. No Required pumping more than 4 times in the last year NOT due to clogged or obstructed pipe(s). Number of times pumped No Any portion of the SAS,cesspool or privy is below high ground water elevation. _No_ Any portion of cesspool or privy is within 100 feet of a surface water supply or tributary to a surface water supply. _No_ Any portion of a cesspool or privy is within a Zone 1 of a public well. No Any portion of a cesspool or privy is within 50 feet of a private water supply well. No Any portion of a cesspool or privy is less than 100 feet but greater than 50 feet from a private water supply well with no acceptable water quality analysis. [This system passes if the well water analysis, performed at a DEP certified laboratory,for coliform bacteria and volatile organic compounds indicates that the well is free from pollution from that facility and the presence of ammonia nitrogen and nitrate nitrogen is equal to or less than 5 ppm,provided that no other failure criteria are triggered.A copy of the analysis must be attached to this form.] No (Yes/No)The system fails.I have determined that one or more of the above failure criteria exist as described in 310 CMR 15.303,therefore the system fails.The system owner should contact the Board of Health to determine what will be necessary to correct the failure E. Large Systems: To be considered a large system the system must serve a facility with a design flow of 10,000 gpd to 15,000 gpd. You must indicate either"yes"or"no"to each of the following: (The following criteria apply to large systems in addition to the criteria above) yes no the system is within 400 feet of a surface drinking water supply the system is within 200 feet of a tributary to a surface drinking water supply the system is located in a nitrogen sensitive area(Interim Wellhead Protection Area—IWPA)or a mapped Zone Il of a public water supply well If you have answered"yes"to any question in Section E the system is considered a significant threat,or answered "yes"in Section D above the large system has failed.The owner or operator of any large system considered a significant threat under Section E or failed under Section D shall upgrade the system in accordance with 310 CMR 15.304.The system owner should contact the appropriate regional office of the Department. Page 5 of 11 I OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART B CHECKLIST Property Address:_312 Boxford Street_ _North Andover_ Owner:_Trask_ Date of Inspection: 3/31/2006_ Check if the following have been done.You must indicate"yes"or"no"as to each of the following: Yes No _Yes_ _ Pumping information was provided by the owner,occupant,or Board of Health No Were any of the system components pumped out in the previous two weeks? Yes_ _ Has the system received normal flows in the previous two week period? No Have large volumes of water been introduced to the system recently or as part of this inspection? Yes_ _ Were as built plans of the system obtained and examined? Yes Was the facility or dwelling inspected for signs of sewage back up? Yes _ Was the site inspected for signs of break out? Yes _ Were all system components,excluding the SAS,located on site? _Yes _ Were the septic tank manholes uncovered,opened,and the interior of the tank inspected for the condition of the baffles or tees,material of construction,dimensions,depth of liquid,depth of sludge and depth of scum? _Yes_ _ Was the facility owner(and occupants if different from owner)provided with information on the proper maintenance of subsurface sewage disposal systems? The size and location of the Soil Absorption System(SAS)on the site has been determined based on: Yes no _Yes_ — Existing information. _Yes_ _ Determined in the field(if any of the failure criteria related to Part C is at issue approximation of distance is unacceptable)[3 10 CMR 15.302(3)(b)] Page 6 of 11 I OFFICIAL INSPECTION FORM-NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION Property Address:_312 Boxford Street_ _North Andover– Owner:_Trask_ Date of Inspection: 3/31/2006_ FLOW CONDITIONS RESIDENTIAL Number of bedrooms(design):_3_ Number of bedrooms(actual):_3_ DESIGN flow based on 310 CMR 15.203_330_ Number of current residents:_4 Does residence have a garbage grinder(yes or no):�1 T6 �!`�S dr"J Kl/�� Is laundry on a separate sewage system(yes or no): No_ ` Laundry system inspected(yes or no): Seasonal use:(yes or no):_No_ Water meter reading:_On well water_ Sump pump(yes or no):_No_ Last date of occupancy:— Current-COMMERCIAL/INDUSTRIAL Type of establishment: Design flow(based on 310 CMR 15.203):_gpd Basis of design flow(seats/persons/sgft,etc.):_ Grease trap present(yes or no):_ Industrial waste holding tank present(yes or no): Non-sanitary waste discharged to the Title 5 system(yes or no):— Water meter readings,if available: Last date of occupancy/use: OTHER(describe): GENERAL INFORMATION Pumping Records Source of information: Pumped last year,owner_ Was system pumped as part of the inspection(yes or no): Yes_ If yes,volume pumped:_1000_gallons--How was quantity pumped determined?_Measured tank_ Reason for pumping: _Inspect tank&tees_ TYPE OF SYSTEM X Septic tank,distribution box,soil absorption system Single cesspool_Overflow cesspool Privy _Shared system(yes or no)(if yes,attach previous inspection records,if any) _Innovative/Alternative technology.Attach a copy of the current operation and maintenance contract(to be obtained from system owner) _Tight tank _Attach a copy of the DEP approval _Other(describe):_ Approximate age of all components,date installed(if known)and source of information:_31 years old,tank&two pits.D-box&pit #3 replaced 6/17/1998,as built plan_ Were sewage odors detected when arriving at the site(yes or no): No i i Page 7 of I 1 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION(continued) Property Address:_312 Boxford Street _North Andover_ Owner:_Trask_ Date of Inspection: 3/31/2006_ BUILDING SEWER_X_ (locate on site plan) Depth below grade:_20" Materials of construction: _X_cast iron _X_40 PVC_other Distance from private water supply well or suction line: Comments(on condition of joints,venting,evidence of leakage,etc.) 4"Cast iron thru wall.3"PVC in house, no leaks visible SEPTIC TANKS: X Depth below grade:_8"_ Material of construction: X concrete metal_fiberglass—polyethylene _other(explain) If tank is metal list age:____ Is age confirmed by a Certificate of Compliance(yes or no):`(attach a copy of certificate) Dimensions: 7'x 5'x 4'_ Sludge depth: 3"_ Distance from top of sludge to bottom of outlet tee or baffle: 24"_ Scum thickness:_3" Distance from top of scum to top of outlet tee or baffle: 8" Distance from bottom of scum to bottom of outlet tee or baffle:—18"— How 8"How were dimensions determined:_Tape Measure_ Comments(on pumping recommendations,inlet and outlet tee or baffle condition,structural integrity,liquid levels as related to outlet invert,evidence of leakage,etc Pumped septic tank.Inlet baffle ok.Outlet baffle ok.Outlet tee ok.Depth at outlet invert.No evidence of leakage._ GREASE TRAP:,(locate on site plan) Depth below grade:_ Material of construction: concrete metal fiberglass polyethylene Tother (explain): Dimensions: Scum thickness: Distance from top of scum to top of outlet tee or baffle: Distance from bottom of scum to bottom of outlet tee or baffle: Date of last pumping: Comments(on pumping recommendations,inlet and outlet tee or baffle condition,structural integrity,liquid levels as related to outlet invert,evidence of leakage,etc.): i Page 8 of 11 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION(continued) Property Address: 312 Boxford Street North Andover – Owner:_Trask_ Date of Inspection: U31/2006_ TIGHT or HOLDING TANK: (tank must be pumped at time of inspection)(locate on site plan) Depth below grade: Material of construction: concrete metal fiberglass__polyethylene other(explain): Dimensions: Capacity: gallons Design Flow: gallons/day Alarm present(yes or no): Alarm level: Alarm in working order(yes or no): Date of last pumping: Comments(condition of alarm and float switches,etc.): DISTRIBUTION BOX:_X_ Depth below grade _8"_ Depth of liquid level above outlet invert:–0"– Comments "Comments(note if box is level and distribution to outlets equal,any evidence of solids carryover,any evidence of leakage into or out of box,etc.):_D-box level&distribution equal. No evidence of leakage.Evidence of light carryover.Pumped d-box to clean._ PUMP CHAMBER: _(locate on site plan) working es or no): Pump in wo g order(y — Alarm in working order(yes or no):— Comments(note condition of pump chamber,condition of pumps and appurtenances,etc.): Page 9 of 11 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION (continued) Property Address: 312 Boxford Street _North Andover_ Owner:_Trask_ Date of Inspection: 3/31/2006_ SOIL ABSORPTION SYSTEM(SAS):—X (locate on site plan,excavation not required) If SAS not located explain why: Type X leaching pits,number: _3 leaching chambers,number:_ leaching galleries,number: leaching trenches,number,length:— leaching field,number,dimensions:_ overflow cesspool,number: innovative/alternative system Type/name of technology: Comments(note condition of soil,signs of hydraulic failure,level of ponding,damp soil,condition of vegetation, etc.):_Soil oL Vegetation oL No sign of ponding to surface.Camera inside of pits thru outlets in d-box.No liquid up in pipe inverts._ CESSPOOLS: Number and configuration: Depth–top of liquid to inlet invert:— Depth of sludge layer:_ Depth of scum layer:_ Dimensions of cesspool: _ Materials of construction:_ Indication of groundwater inflow(yes or no):— Comments(note condition of soil,signs of hydraulic failure,level of ponding,condition of vegetation,etc.):_ PRIVY: (locate on site plan) Materials of construction: Dimensions: Depth of solids: Comments(note condition of soil,signs of hydraulic failure,level of ponding,condition of vegetation,etc.): Page 10 of 11 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION(continued) Property Address:_312 Boxford Street _North Andover— Owner:_Trask_ Date of Inspection: 3/31/2006_ SKETCH OF SEWAGE DISPOSAL SYSTEM Provide a sketch of the sewage disposal system including ties to at least two permanent reference landmarks or benchmarks.Locate all wells within 100 feet.Locate where public water supply enters the building. Driveway To well House A B Deck Septic Tank 1 2 AtoI=14'7" A to 2=20' Box Pit 3 A to D-Box=69'7" B to 1=5110" Bto2=6'4" B to D-Box=54'5" Pit 1 Pit 2 .t i Page 11 of 11 OFFICIAL INSPECTION FORM—NOT FOR VOLUNTARY ASSESSMENTS SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION(continued) Property Address: 312 Boxford Street _ _North Andover — Owner:_Trask_ Date of Inspection: 3/31/2006_ SITE EXAM Slope Surface water Check cellar Shallow wells Estimated depth to groundwater _6'_ Please indicate(check)all methods used to determine the high ground water elevation: X Obtained from system design plans on record-If checked,date of design plan reviewed:_6/5/1975_ (abutting p perty Observed site abuttin property/observation/observation hole within 150 feet of SAS) t 1 Checked with local Board of Health-explain: _ Checked with local excavators,installers-(attach documentation) Accessed USGS database-explain:_ You must describe how you established the high ground water elevation: As per test pit data on design plan on water 6'deep. P _ Tel: (978) 475-4786 • Fax: (978) 475-5451 BATESON ENTERPRISES, INC. Excavating-Water.& Sewer Lines-Septic Systems &Pumping Service 111 Argilla Road Andover, Mass. 01810 Title 5 Inspection Report Property Address: 312 Boxford Street, North Andover Owner: Trask Date of Inspection: 3/31/2006 My report contained herein does not constitute a guarantee of future usage and the functionality of the existing septic system. Such report issued herewith is merely based upon my observations, and I hereby disclaim any further operation of your current septic system. Neil J. Bateson Bateson Enterprises, Inc. ytp SUBSURFACE REMEDIATION TECHNOLOGIES, INC. i ENVIRONMENTAL CONSULTING & REMEDIATION SERVICES 355 Central Street • Rowley, Massachusetts 01969 o � 978 948-3861 N OF NORTH ANDD BOARD OF HEALTH February 2q,,.2002 � 2 5 X002 � c Massachusetts Department of Enviromnental Protection North East Regional Office 205A Lowell Street Wilmington, MA 01887 RE: Trask Residence, 312 Boxford Street, North Andover, MA 01845 Immediate Response Action Status Submittal, RTN 3-20874 Dear Sir/Madam: On behalf of Deborah and Robert Trask, owners of the subject residence, Subsurface Remediation Technologies, Inc. (SRT) is submitting the following Immediate Response Action (IRA) Plan Status in conformance with Department of Environmental Protection (DEP) and the Massachusetts Contingency Plan (MCP) requirements. Enclosed separately are the original IRA Plan Status transmittal forms, with copies attached as Attachment 1. Also enclosed separately is the original Bill of Lading, with copies in Attachment 3. Background The release of approximately 150 gallons of heating oil occurred at this site on July 3, 2001. The Trask family returned home after being away after this date to find that lightning had struck a tree approximately fifteen or twenty feet from the rear corner of their house. They found that their #2 fuel oil tank had emptied through a ruptured furnace feed line and had seeped onto and below the concrete floor through cracks. Information regarding notification, verbal IRA approval, soil boring, monitoring well installations, soil and groundwater testing and excavation of contaminated soil in the furnace room Trask IRA Status,N Andover RTN 3-20874 Feb. 20,2002 and garage areas of the residence, were all described and submitted with the written IRA Pian, submitted to the DEP on October 18, 2001. The above ground 330 gallon storage tank is estimated to have lost approximately 150 gallons of fuel oil based on available records. The site is in a hilly, glacial till area of single family homes, with on-site septic systems and private wells'. The surrounding receptors most at risk due to this release are `ihdTrask's- wn drinking water well, and indoor air at the residence itself. Immediate Response Action As described in the IRA Plan, hand excavation of the room in question began on August 22, 2001, under a verbal IRA, and had continued up to the resubmittal of the IRA Plan on Oct. 18, 2001. Progress was very slow because the underlying glacial till was so dense it had to be jack hammered. It also contained numerous, relatively large, rocks. At the time of the IRA Plan submittal, the bottom of the contamination had been found at 10 feet in the furnace room and at 5 feet in the affected part of the garage. Jar headspace readings taken on Oct. 16, 2001 in the 5 to 10 foot depth range of the furnace room had shown three grids of sidewall area (JKM) still had high headspace readings. Sidewall location FGHIL (5 to 1.0 feet depth) was also screened (2 ppmv) and sampled on Oct. 16, 2001 for EPH and was found to meet the required SI/GW-1, Method 1, soil standard. Sample analyses confinned that the JKM sidewall exceeded EPH parameters but not VPH parameters. The JKM sidewall had previously passed Method 1 standards for VPH (Oct.2, 2001, FGHIJK). Picking up where the work described in the IRA Plan left off, SRT continued the excavation of the still contaminated sidewalls in the 5 to 10 foot depth. SRT separated the furnace room into grids, as shown on the enclosed Figure 1, and used the lettering sequences to track the sidewall samples. Removal efforts were directed at the 5 to 10 foot depth range in order to backfill to a 5 foot depth and then work on the sidewalls and beneath the foundation in the 0 to 5 foot range. Soil removal on Oct. 18 and Oct. 22, 2001 of soils on the JKM sidewalls used jar headspace readings again. Approximately two and one half feet of soil was removed from these sidewalls, reducing soil jar headspace readings from the 28 to 50 ppmv range to the 2 to 12 ppmv range. SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 t Trask IIIA Status,N Andover RTN 3-20874 Feb. 20,2002 Two composite soil samples were collected on the JKM sidewalls, one from 0' to 5' and another from 5'-10'. These two samples were designated as J1K1M1. SRT submitted them to AMRO Environmental Laboratories of Merrimack, NH for EPH analysis. Analytical results showed that these sidewalls were now well below MCP Method 1 Standards (Table 1 and Attachment 2). On Oct. 29, 2001, clean sand backfill was placed and compa_ cted, n one foot lifts from the bottom of the excavation to the five foot level. Sidewall JKM was-also cleaned'from 0 to 5 feet by Oct. 22, 2001. Once all affected soils beneath the 5 foot depth were removed and the excavation backfilled, efforts were directed at 0 to 5 feet affected soils. Screening and further hand excavation and removal of the 0'-5' sidewalls continued on October 30, 2001 until SRT reached a point where further excavation jeopardized the stability of the foundation. Two composite samples (sidewall locations LAI IA A and FGH LF ALF A) were both collected and sent to the laboratory for both EPH and VPH analysis. Figure 2 and Figure 3 show the lettering sequences used to track the subject sidewall samples, all taken as composites. Both samples obtained on Oct. 30, 2001, had exceedances to MCP Method 1S1/GW-1 soil standards. A structural evaluation to determine underpinning requirements was conducted on November 7, 2001. Underpinning was put in place on November 13, 2001 with excavation of the still contaminated sidewalls in the 0'-5' range continuing from the 13th through November 15, 2001. On November 15, after achieving jar headspace readings in the 0'-5' range of 8 to 14 ppmv, two more composites (AFGH and IA) were collected and sent to the lab for EPH/VPH analyses. Results were well below MCP Method 1 Standards. Table 1 enclosed summarizes all soil testing results, and Attachment 2 contains copies of laboratory analytical reports. These reports go back to the October 2, 2001 sampling event because the final reports were not available at the time of the IRA Plan submittal. On November 28 and 29, 2001, and after receiving laboratory analyses displaying soil concentrations well below applicable Method 1 Standards, the 0' to 5' excavation was backfilled, and compacted in one foot lifts to grade. At this time, the concrete floors have been replaced and the basement has been restored to usable condition. SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 Trask IRA Status,N Andover RTN 3-20874 Feb.20,2002 Attachment 3 contains copies of the Bills of Lading for the contaminated soil removal to Brox Industries of Dracut Massachusetts for recycling. A total of 120.04 tons were removed on September 20 and 21, and November 9 and 16, 2001. The original Bill of Lading is also included in this submittal. Also enclosed is the copy of the manifest, dated Sept. 14, 2001, for one drum of oily solids/debris generated during the initial response action. Ori'December`31;-2001; the'remaining monitoring well (MW-4) proposed as part of the IRA Plan was installed. The boring log is included in Attachment 4. Work remaining in the proposed IRAP is to monitor the relatively deep groundwater depths in the four on site monitoring wells., and the drinking water well, for groundwater flow direction, with another round of groundwater analyses to be taken in the spring, at a higher groundwater season. To date, all water samples were found to be below detection limits, using EPA Method 524 Volatile Organic Compound analysis. Please contact the undersigned if you have any questions regarding the attached Immediate Response Action Plan. Sincerely, Subsurface Remediation Technologies, Inc. Timothy A Toome President Enclosures cc: Town of North Andover BOH Town of North Andover Chief Municipal Officer Mr. & Mrs. Robert Trask Exeter Environmental SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 i i ! PAGE 1 OF 1 I I SOIL SAMPLES Boring/ Sol[ Reg. EXTRACrAHLE to VOLATILE PETROL lar headspace Sampling Sample SOIL/GW C9-C18 C19-C36 Cll-C22 Xylenes sample Notes "cat on Date Depth catagory** ahphatics ali hatics aromatics ale Hnu/OVA FGH 9/13/01 0'-10' S1-GW1 330 120 120 0.71 10 HK 9/13/01 0'-10' Sl-GW1 1800 330 500 19.9 40 Acenaphthene=1.6* i IJK 9/13/01 0'-10' S1-GW1 1700 330 430 14.5 45 FI 9/13/01 0'-10' S1-GW1 3600 540 760 13.6 40 Acenaphthene=1.4* Bottom 9/13/01 10' S1-GW1 62 ND ND ND 5 Acenaphthene=7.1* ABottom 9/13/01 5' S1-GW1 110 ND ND ND 4 ASidewalls 9/13/01 0'-4' S1-GW1 4300 720 920 12 40 Acenaphthene-7.8 * i FGHIJK 10/2/01 0'-5' S1-GW1 2800 690 1100 10.2 45 Acenaphthene=1.9* FGHIJK 10/2/01 5'-10' S1-GWI 640 230 380 0.37 30 FGHIL 10/16/01 5'-10' S1-GW1 ND ND ND NS 2 JKM 10/16/01 5'-10' S1-GW1 3700 430 780 NS 50 Acenaphthene=3.8* i I J1K1M1 10/22/01 5'-10' S1-GW1 230 84 ND NS 10 I J1K1M1 10/22/01 0'-5' S1-GW1 180 70 64 NS 8 LAI IA*A 10/30/01 0'-5' S 1-GW 1 3800 1600 1800 1 2.12 6 to 70 Acenaphthene=2.1* (*l,in FGH LF* ALF A 10/30/01 0'-5' S 1-GW 1 2400 880 1200 l 4.4 0-70 Acenaphthene=2* *1 m AFGH 11/15/O1 0'-5' SI-GW 1 140 ND 52 I ND 14 I IA 11/15/01 0'-5' S1-GWl ND ND ND 1 ND 6 :. wa .11SfQ <:2 :d # W 9 :..... . ::::> ,.:........:... ....:....s. :.:::::........::.::...:.::...::::::.:::::::::::::::::.:::::.:.....................::.::::::::::::::::::::::::::::::::::::.:::::::. .. ::::::::::::::::: llb:>::.... 11G1Area<>:»>:»t�09:a:>:>Z 59U:>:z:>8®9::::::::................................:..::::::::::::::::::::::::.::::::::::::::::::..::............ .....................::::......:::::.:::::::::: t ::::::::::..., ..::::::::::::::::::.. ..: :.::::::::::::: DEII!: 2:T#m#ts:>:«<»:»:>:<TG1 #hrea:s:;:>:>::2 0&«:.>:50®Q:<z< 2991:.... >?..:»...............................:...::::.:::.:::::::::..:::::..:...................:..............:..:::::::::::: 1 W. ......:::<:::I ::::..�:......:::::::: , D@:::::. ,.U@ .::.:. :::::::::.::::::::::::.:.::.::.::.............:...::::::::::::::::::::::::::::::: :::::::::::::::.:...................:.::::: ... t ;:: tt BSD 4e;:.>;;::;.;:.;:.;:.;:.;:.;::.::.;:.;:.;:.;:.;;:.;:.;;:.;;>:.;:.;:.;:.;:.:<::;::......:::::>::>::>::»::»>::>:»::>::>::>::>::>::;:<:::: 1) l€''r3 Gtm#ts.:.:::::::::::::1.3Cr ?:.#.e1xe :._:::::::3,e .:::::. p;:.;:.;:.;: @ .:.::::._:::::::::.::...................:::.:::::::::.:::::.:::::::::::::::::::::..:.................. :::::::::::::::::::::::. ....:::::: ::::.:. .r..:.:.:..::. . . ... . .....:...................:.::::. ............ �::::::: iiiiii :iS::;:;lF@:;>:;:i :;;;:;:>;>:;:>;;;:a:o::>:s: o::::>:r.:::::::: ::c>rr.:::;;;::;o;:::::::: �..:.:.::.:::..:.::.:::::::: ::::::::::::::::::::::::::.:::::::.:::........ ........:::::::::i:::<:::>::::>::::>::::>::::;:..fid >.,.....::;;::«:>::>:: «:::: >::<:>::>:>.:::>::>::>::»::»:::>::»::>:>:::>:::<:>:: t. .... Asea. . .:::: aD .:::..: Wp:::.::.5 .:::::: p... NOTES: ND-Compound not detected above the minimum S-1 through S-3 Soil S concentration limit or method detection limit of MCP. Applicable cc the particular analytical procedure(See Analytical CMR 40.0975(6)(a TABLE 1 Report). GW-1 Standards-Drh >-Indicates the detection limit GW-2 Standards-Reg NS-Not Sampled for Particular Chemical and where groundwe Bold/Italic print indicate values over MCP limits. surface. GW-3 Standards-Reg areas are subject to t Bottom Garage(A)&Bottom furnace room met MCP Standards on 9/13/01 MW-3 Sidewall Sample FGHIL Met Standards on 10/16/01 4- IRA Soil F G Removal Furnace Room M 4— MW-2 I K J1K1M1 Sidewall met MCP Standards on Garage 10/22/01 TRASK RESIDENCE 4— MW-4 5 - 10 foot ran depth e g 2 10/2 /01 LEGEND N 10/22/01 IRA SOIL REMOVAL MAP 312 Boxford Street NORTH ANDOVER, MASSACHUSETTS SUBSURFACE REMEDIATION Chimney TECHNOLOGIES,INC. 355 CENTRAL STREET Drn By: PDM y ROWLEY, MA. 01969 I Ck By: TAT (508) 948-3861 Date: 20 Jan 02 Bar Scale o 20 40 FIGURE 1 Scale: 1-in=40-ft (in feet): r � MW-3 Sidewall Sample FGH LF* ALFA (*-Vin) 4- IRA Soil F G H Removal 35ppm Oppm Oppm t ar. 7 PPm ._35ppm F 28 L Furnace Room M PP A 6ppm MW-2 M 0-50ppm Sample LAI IA* A (*-Vin) I J K J1 Kl J1K1D'il Sidewalk met MCP Standards on 10/22/01 Garage TRASK RESIDENCE 4— MW-4 0 - 5 foot ran depth e g 10/30/01 LEGEND N 10/30/01 IRA SOIL REMOVAL MAP 312 Boxford Street NORTH ANDOVER, MASSACHUSETTS SUBSURFACE REMEDIATION Chimney TECHNOLOGIES,INC. 355 CENTRAL STREET ���� Dm By: PDM — Y ROWLEY, MA. 01969 Ck By: TAT (508) 948-3861 <;>' Date: 20 Jan 02 Bar Scale 2 _ 4 FIGURE 2 Scale: 1-in=40-ft (in feet): i I MW-3 Confirmation Sidewall 4— Sample AFGH IRA Soil Removal F F G H Furnace Room A L M 4— MW-2 I J R J1K1M1 Sidewalls Confirmation Sidewall I Sample AI met MCP Standards on 10/22/01 Garage MW-4 TRASK RESIDENCE `�' 0 5 foot ran depth e g 11/15/01 LEGEND N 11/15/01 IIIA SOIL REMOVAL MAP Underpin 312 Boxford Street Temporary Support For NORTH ANDOVER, MASSACHUSETTS Foundation SUBSURFACE REMEDIATION Chimney TECHNOLOGIES,INC. 355 CENTRAL STREET : ' Drn By: PDM ROWLEY, MA. 01969 Ck By: TAT (508) 948-3861 ""' Date: 20 Jan 02 Bar Scale 0 20 40 - FIGURE 3 Scale: 1-in=40-ft (in feet): - J ATTACHMENT 1 hlassaCh'usstts Department of Environmental Protection _ BWSC-105 n Bureau of Waste Site Cleanup • :, k I RESPONSE ACTION IRATRANSIIIITTAL Release Tracking Number "MEDIATE - - � � Sub-a1 D - _ lh, 3D- ;:.20874:_, _-_. - Pursuant to 310 Cfr,R 40.0424 4070 27( r ) FOR ; .:_ A RELEASE OR THREAT OF RELEASE OCATION: Rtlerse Name:(oXi:A Trask Residence--_- Street:;312 Boxford Sttaec -to:a'JanAid: cryrlo+rl:— Forth Andover_ 21?code:- 01845 Check bete Ka Tier Ctzssificz to••t Subml".al hzs been p:ovide:d Ito DEP fa s Rei�.Lse Tr�ckin;!:urlber. ❑ Check here d.L'is)xa:Boa iSJ,degt e!y Regu'�ed,prs_�nt io 310 CI-1.R-0.0110-0114 t $p�.ify Prog.o`\' ❑ C=jCLlk"D F SWA Conec9•e Ac ian_ ❑ SO%1';isle IJ.a:.zgeme it RC=A S ate P:ogzrt(21C Facit ies) ne:ated Rettzse Trckii�WumS��s Tfzl Th:s iF.A f.dd?ersses: �r �' -_- ' B.THIS FORM IS BEING USED TO: (che:k all t-at z;>;N-) Sub:1n zn IRA P:zn(complete Se:ljons A,B.C.D._,H.I,J and . (� Check hert E this IRA Plan is an updz'e of rn i us'y pp eil; 'en IRA Paan. Dare Su!).-Xed: ad,'.�:z:an o1 z p:e�4a z :ov 17 Sub.-nn an 1.7 ninent Hazard Evaluation(co:aple:e Sections A,B.C,F.H.I,J and K). Sub:r,t an IRA status Rep :i» ort Ses A.B.C.E,H,1.J ane ri. ., 1:3 Svb.,,E.t.Re;ue-.1 10 7ermin2It an Active Remedial systexn andr• ;or Ter :reale a Contiming Reponse Action(:)Tat:en to Addre:s an l nninen�Yzzard(�nple:e Sec ions A,3,C.D.E.H,1,J and►n. Sut)—1 an IRA Completion Slzlernent(eomplelt Srlirs A,B.C,D,E.G,H,1,J and K)- You must arach all supporing docu-nenlation requited for each use of for-,n indiczled,including copies of any Legal 1dolices and 12otiees to Public OY'jclals require-6 by 310 C1 1R LO.;<DD. ` C. RELEASE OR TY.REAT OF RELEJ.SE CON'D1T10;;S Tr.AT 1'%":R;.,t-NT IRA: _ XU G:aJ1.+•cter J Serz za Yi z:er ❑ Se.::-,en'.s � Sail ln'e:;znd Slorn D.zin ❑ ?z�e�Su.'.a:e I Ii ?rn�:e\'dell I Pubt:\4'ater Sup:y I� -ane 2 X X Residence Ssho:i �'�,,,� dyers Y S.Dill OCCured Within 100 feet DTivate well ldenti'y Candi ions;*z Req .e 1Rf�Pvs ant 10.10 Cb:R 40.C412 (check at?z1 zpp!y) �� c Hour Re�.'.ir g Condi ions) 72 hour i+ep ting Condi i0n�s) ❑ Su:-s anliat ie:czse t:iy a:of ❑ C:`�eJ Cond'i:��=) Des::be: 1derV'y Ops znd Y.a�:d0 n lJz:e:'zts F.eiersed: (ch�k zn at zpr;•) COs ❑ Ch1a rz:ed S:>vvens Heavy IJ1e:a's O:he-s e pe:`Y• D. DESCRIPTION OF RESPONSE ACTIONS: (chezk at:1`•zl zpp`) Assessment andror IJ.onto.•ing only ❑ Deplayme t of A:so 'd or Con:ain-rent 1J.alera!s :XDEx=�aSot of Co:tar�i naled So?s ❑ Tempa ay Crn e's or Cars © Re-4, or Treatment ❑ 8ixene�ia:ian- on Ste Off Safe- Esi Vd� 120. 04 tons . ❑ sonvzpor Exr-oaian 0 ( cvb�:)ands cs disposal at-recycling facilit� , +x; P Sltudure eating s)s e n Des= . Slo-e 0 On Sts 0 Off Ste Est Vol-- 0 cubic yards ❑ Produd or NAPL Recove.Y. ❑ Landfin 0 Cavel 0 Disposal Est VoL: ❑ GroundNaler Treatment Systems s. Cubic)arils Remv at of Dnuns.Tanks or Conlarners ❑ Air Spar2,+g Destl�3e: ❑ Temporary\Valet Svpprles SECTION D IS CONTINUED ON THE NEXT PAGE Revisr�2r2Supersedes Forms EWSC-005,005,010 O taro and 011 Pale t of 3 a• M l.L,l t X a T}rc Ervin K I Massachusetts Department of Environmental Protection B`4SC-105 -01ireau of 141=C-1.3 Rele2se Tracking Nu:7lber — Itt4t►SEDIATE RESPONSE ACTION (IRA) TRANSMITTAL ' FORM puts U261to 310 CI:R 40.0:24• 0.0,44-7(Subpal D) . ❑3 ' 20874 D. DESCRIPTION OF RESPONSE ACTIONS(Continued): �-1 Re no•al of Cher C -'�ru-�_'1:✓• .0 e.-:p,zy E%zrua:.i or Reio:.a:ion ol.Residents Spee-y Type znd Votunt: I riy o o i l d p r; c - Q Fez:.ing and Sign Pcs:ing 1 X Other Respor*a Actio:-.s D=rU: x a a r o o r 1 c C, --heft L L.i IRA inv:N'es the L•se of 1xiv.zf:e Te--M:4 --ies;.=P ss i^:E:es:ed i 1:sing:`.s i lio:rr:alio l to aid in c:ezun3 an lanol�:n•e Technolo,ies CIE�•L�.ho:.se). ' .. Descn->e Te--M »;eS:,: , k_ E. TRANSPORT OF RE);tDIAT)6iJ 1'1ASTE: .(r Rer�Ed 2:;: zs:e hes Seen seal fo a-_:f=s e'acili-J answer the folio..:ng evEs ions) YA ones. env. Se"r .. Brost Industries:=- -•• - To:%,and Vale: Lowel MA Dracut . MA Ouar.:iy of Ferre:;:ion t'V2s:e Transpo"ed to trait:s• 1 drum 120. 04 tons F. 114MIt'ENT FtZARD EVALUATIO'J SUIJ,1;'—:kY: (chw k one ol1`e lol:n.r) E2sed Upon an an i.-'i.'.unvu I=ve Exs:s in cv)ne: ;--nv.�h 1.`.:S Release or i h1E3:C:Fe'-:25,e- an lazed d>°s ne Ex:s:in c.nnE.ti.n v.�h lhs nrlEZse o T.`.:Eat o!r`ei:zst. 2sed L•gx1 2n t'•Z! 2:ion is is L:.vnzy.,%':'�Chtr an l--.inEnl 1-:2_c:d Ex:S:S i1 C:n'.e ion�.��:�S Rre lease or i h'E2:Of nE:E2St,End fJ.'ti_r -gent 2C:'t;es v:.l;Y Und!n0r.En. assess. E25Pd L'p�n a't��1;;2:io1, i5 U.'1nCv.^v.'1e:her a. 1--inenl i'2_:2 EX:S:S in.^'�nnP::i0:7 v.�n iS Re: s• Eze or i h:Ea:cl net-2se. }i0'::e% iesponse 2C.'i7n-s v:11 adVesS that c in"iC.^.S L�.'c:=j!U ;>?Se an.:-�inE«�•�-2:d. G. 1;:LA C Ol.!PLE i)ON STAT EI.;ENT: C! k bete 2llrc tespo^sez ddressi-, r=t:Ezse o 'rEz:of i.elazse v:T be ecne�_Ed 2s p_ al1hE nespvn� izns p'.nned fa a Sia L'.2i t.25 2L'Eady bsn Tit:Ct2ssi5ed UYer 2 o.':erer .E✓;se �ra:K:ny i:U-.`Jet,0:a S.'.t'`.21 iS i=e-.7f�e�On:'�t lranS.::C'1 Li51 2s ,• dE'SJi`.'�L�U1�1��1.:�L���L t..a i 12ns'iCn�:-,t,N1iC!'1 i'1:1�:E5 S'QS�•.'•1:a��7:7.•Er 1'i'a':E's). !.`.Et-e Z7:.:iO-.ol re'SpO^.SE"oC1i0::S fn;:51 OGCUr ar.-"O:d;n�1D:hE dEadline5 apprt:able t:Lhe fa.':er�EiE25{i.Y-kind l:L-ber�1.e.,Sia I�I�a'tir). State Fele2Se-,,2:k:-i;Nv-5e1(te.,5(e ID N -'..E:)of Tier 5'.e a l ranstion Ste: If any Remed;2:;on% asle will be slored,lreale-d,manage,recyclE-d or ieus.e-d at the sae follev ing svbTission of the iRA Cornplelion S,z*erxnt,you muss cubrnh either I Release l;:2:e-.ent 1.'.E2su:e(F,Itd)Plan or a Phase rJ Re,--edy l-nplen'.n:;lion Plan,along wah the a?�rcaria:e tranw,:^ 21 for rL as zn 2 ach Hent to lY:e 1nA Com;)le ne: :ion Sta:Err. H. LSP OPINION: 1 a est under Lhe p2i s and per a .es of i,e t)if 21 1`a.t pe sonal•y e -iined zi:an fzrnar rah Lh 5 1�n5-n'a!fosrn,inctvd;ny any 2nd all doeumer s a=npany:.r,this svb:r.•r..zl. 1;Ty pit:essio-.zl cpin;on and iudg men wase-d upon 2ppi ;:ion of(D,I)e stanta:d of case in 3x-CI;R 4.C2(1),(�71he 2;pL:z51e p:orsions of 30:CI:R 4.C2(2)and[d),and(r Lhe p.or:sions of 3'n cvR 4.C:a s).to Lhe yes;of ny kno::edge, and belief, > r SrCon B a't`e fo.-m indcefes the"an Imne:riate Fczpons a Action Plan is f+eing wbni•td.Lhe response zd'+on(s)that is(ate)Lhe su5jed of .h-.s sub n al n has(hive)5-en developed in z ; can a v.�1 the app5�ble p:a�;sians of 11,.G.L e.2/E and 310 GI.:R a�.DJ�O. in) is(ate) zpptopria:e and rc2sonable to ac amplsh Lhe pv,eyes o!sv h respc-�e acl;zn-,' zs sei fo:.h in Lhe zppL;z51e p:o.Esia:u o!IJ,.G.L e.27 E znd 370 CIAR 4D.C=and w =-M?T e W wth the ide-rerled p:cvisians a ar o:de_-s,pe.-,ts,and zpptovals i3en:4fied 1:1 L`i.-S sv!xntal; > r Sedon B Of ri.:i form i7&0Z!eS thaf an Imminent He22rd Evaluation is be!-);s.,5rar.°ed,this ln-ninent p..2_-zrd %%-as developed in aacardan=whh the zppfr„able provisions of IJ G.L e.21 E And 310 CUR 4:).t7 .and the zsse--sunert ac%h y(es)underaken to Suppo*l this Imminent HLzztd E>aluzl;on=mpfies;y)veth Ux eppf cable p:ovisro s of IkG.L e.21 E and 310 Ci4R 4:)-CCC0. > r Sedon B of n4 s faon in cares n of an Immeeafe Respons a S,,2ws Repa4 is beiop s✓btnt:ed,the iespor m aclion(s)the!is(are)the subject of this subrrelal n is(are)bung implemented in axa:danx with Lhe applicable prmisions of 14G.L e.21 E and 310 CMR 40.0000.n is(are) appropr ate and iersor.able to aiwa^ipfsh the pu.^poses of such response aclion(s)as set fa-ih in the appLczble p:ovnions of Id1.G.L c.21E and 310 C1l.R 40.03M and w cornpLes(y)WL%Lax iden;if�ed pto.%siom of at a de..s,pe-rh1s,and xppiovals iStnntified in this sub:ntial; > r Sedon B of this/a-m indcafes Leat an Immediate Response Aejon Completion Statement or a Request to Te=inafe an AcOve Remedial System and/or Tenninate a Continuing Response Aciion(s)Taken to Address an Imminenf Hazard is being wbinL-fed,the response aclion(s) that is(are)the svbjed of tlis submMW 01 hes(have)betin developed a.-4 imple-nenled in acs;dame%-.h the applicable provrsio:is of id.G.L C.21E and 310 CMR 4D.O=. an, is(are)appropriate and reasonable to ae=.^ipLsh the p'.arposes of such response ac�3on(s)es set forth in the applicable prov,siazi of NI.G.L G 21 E and 310 CMR 40-CC00 and Ciii compbesW%th the identified provisions of all orders,permlls,and appro-Is identified in W's subirii:SaC SECTION H IS cohnNUED ON THE NEXT PAGE ,Re&ed 2124.95• IN Supersedes Forms EWSC-005.WS. 010(in pat')and 011 Pate 2 of 3 ' 7 Massachusetts Department of Environmental Protection BWSC-105 Bureau of Waste Site Cleanup Release Tracking Number IMMEDIATE RESPONSE ACTION (IRA) TRANSMITTAL FORM Pursuant to 310 CMR 40.0424-40.0427 (Subpart D) Li -(20874 i H. LSP Opinion (continued): I am aware that significant penalties may result,including,but not limited to,possible fines and imprisonment,if I submit information which I know to be false,inaccurate or materially incomplete. t Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),permit(s a / pproval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable provisions thereof. LSPNameTimothy A. Toomey. LSP z: 2891 Stamp: s Telephone.9 7 8 948 38.6.1 Ext.: TINS-= o FAX:(6041-nal No. j 2: . / 1 Signature: Gi Date: ef� OS ,rte ice^ I. PERSON UNDERTAKING IRA: Name of Organization: Trask Residence Nameofcontact: Deborah Trask Title: Street: 312 Boxford Street C;tyrrown:Nor th Andover State: MA ZIP Code: 01845 Telephone: (9 7 8) 557 114 7 Ext.: FAX:(optional) E] Check here if there has been a change in the person undertaking the IRA. J. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING IRA: (check one) © RP or PRP Specify: 0 Owner O Operator O Generator O Transporter Other RP or PRP: Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E,s.2) Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) Any Other Person Undertaking IRA Specify Relationship: K. CERTIFICATION OF PERSON UNDERTAKING IRA: Deborah Trask attest under the pains and penalties of perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true accurate and complete, iii 9 p and( )that I am fully authorized to make this attestation on behalf of the entity legally res . ttY g y ponsible for this submittal. lAhe person or entity on whose behalf this submittal is made amts aware that there are significant penalties,including,but not limited to, possible fines and limprisonment, for willfully submitting false,inaccurate,or incomplete information. 0-7 ,n By. � (J"y 1.��(� / Title: (sig re) For. /:6(� � - IJ9-r`J�` Date: Z —Z O (/ (print name of person or entity recorded in Section I) Enter address of the person providing certification,if different from address recorded in Section I: Street: City/Town: State: ZIP Code: Telephone: Ext.: FAX:(optional) I YOU MUST COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Revised 2/24195 Supersedes Forms BWSC-005, 006, 010(in pari)and 011 Page 3 of 3 Do Not Aller This Form s � _ r �r ATTACHMENT 2 ,r Environmental Laboratories Corporation 111 Herrick Street, Merrimack, NH 03054 TEL:(603)424-2022• FAX: (603)429-8496 October 18, 2001 Tim Toomey Subsurface Remediation Technologies 35,5 Central St. Rowley;MA C(1969- TEL: '1969 TEL: (978)948-3861 FAX: (978)948-3861 RE: TRASK RESIDENCE Order No.: 0110043 Dear Tim Toomey: AMRO Environmental Laboratories Corp. received 5 samples on 10/3/01 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference (NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s) upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time, AMRO will properly dispose of the remaining sample(s). If you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of 5 pages. This letter is an integral part of your data report. If you have any questions regarding this project in the future, please refer to the Order Number above. Sincerely, Nancy Stewart Vice President/Lab Director AMRO Environmental Laboratories Corp. Date: 18-Oct-01 CLIENT: Subsurface Remediation Technologies Project: TRASK RESIDENCE Work Order Sample Summary Lab Order: 0110043 Date Received: 10/3/01 Lab Sample ID �.�.Client Sample ID Collection Date 011-0041%0 IA - �t' M W-2 f 10/2/01 0110043-02A MW-3 ` 10/2/01 0110043-03A Drinking Water Well 10/2/01 0110043-04A EXC.FGHIJ(5-10) 10/2/01 0110043-04B EXC.FGHIJ(5-10) 10/2/01 01 10043-05A EXC.FGHIJ(0-5) 10/2/01 0110043-05B EXC.FGHIJ(0-5) 10/2/01 A AMRO Environmental Laboratories Corp. Date: 18-Ocr-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: EXC.FGHIJ(0-5) Lab Order: 0110043 Project: TRASK RESIDENCE Collection Date: 10/2/01 Lab ID: 0110043-05B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE;'r' D2216 Analyst: JC Percent Moisture 3.9 0 Wt% 1 10/4/01 Qualifiers: ND-Not Detected at the Reporting`Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded tl -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. AMRO Environmental Laboratories Corp. Date: 18-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: EXC.FGHIJ(5-10) Lab Order: 0110043 Tag Number: Project: TRASK RESIDENCE Collection Date: 10/2/01 Lab ID: 0110043-04A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUVHYbROCARBOI�S, MAVPH, Analyst: SK C5-C8 Aliphatic Hydrocarbons 3.5 3.0 mg/Kg-dry 1 10/9/01 10:27:00 PM C9-C12 Aliphatic Hydrocarbons 7.9 0.75 mg/Kg-dry 1 10/9/01 10:27:00 PM C9-C10 Aromatic Hydrocarbons 47 0.75 mg/Kg-dry 1 10/9/01 10:27:00 PM Methyl tert-butyl ether ND 0.060 mg/Kg-dry 1 10/9/01 10:27:00 PM Benzene ND 0.060 mg/Kg-dry 1 10/9/01 10:27:00 PM Toluene ND 0.060 mg/Kg-dry 1 10/9/01 10:27:00 PM Ethylbenzene ND 0.060 mg/Kg-dry 1 10/9/01 10:27:00 PM m,p-Xylene 0.23 0.060 mg/Kg-dry 1 10/9/01 10:27:00 PM o-Xylene; 0.14 0.060 mg/Kg-dry 1 10/9/01 10:27:00 PM Naphthalene 0.93 0.15 mg/Kg-dry 1 10/9/01 10:27:00 PM Surr:Dibromofluoromethane 104 70-130 %REC 1 10/9/01 10:27:00 PM Surr: 1,2-Dichloroethane-d4 102 70-130 %REC 1 10/9/01 10:27:00 PM Surr:Toluene-d8 100 70-130 %REC 1 10/9/01 10:27:00 PM Surr:4-Bromofluorobenzene 107 70-130 %REC 1 10/9/01 10:27:00 PM Surr:2,5-Dibromotoluene 79.3 70-130 %REC 1 10/9/01 10:27:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: -V-/- Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: yL Yes _ No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. SIGNATURE: C-C�d— DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range ]-Analyvi�detected below quantitation limits R-RPD outside accepted recovery limits t1-See Case Narrative B-Analyic detected in the associated Nicthod Blank I I-'`Icthod prescribcd holding time excecded 5 � y AMRO Environmental Laboratories Corp. Date: 18-ocr-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: EXC.FGHIJ(0-5) I Lab Order: 0110043 Tag Number: Project: TRASK RESIDENCE Collection Date: 10/2/01 Lab ID: 01 10043-05A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLELJ HYDROCARBONS. .:,. MAVPH_ Analyst: SK C5-C8 Aliphatic Hydrocarbons 45 33 mg/Kg-dry 10 10/10/01 3:02:00 AM C9-C12 Aliphatic Hydrocarbons 60 8.3 mg/Kg-dry 10 10/10/01 3:02:00 AM C9-C10 Aromatic Hydrocarbons 480 8.3 mg/Kg-dry 10 10/10/01 3:02:00 AM Methyl tert-butyl ether ND 0.66 mg/Kg-dry 10 10/10/01 3:02:00 AM Benzene ND 0.66 mg/Kg-dry 10 10/10/01 3:02:00 AM Toluene 0.86 0.66 mg/Kg-dry 10 10/10/01 3:02:00 AM Ethylbenzene 1.8 0.66 mg/Kg-dry 10 10/10/01 3:02:00 AM m,p-Xylene 6.6 0.66 mg/Kg-dry 10 10/10/01 3:02:00 AM o-Xylene; 3.6 0.66 mg/Kg-dry 10 10/10/01 3:02:00 AM Naphthalene 9.9 1.7 mg/Kg-dry 10 10/10/01 3:02:00 AM Surr:Dibromofluoromethane 106 70-130 %REC 10 10/10/01 3:02:00 AM Surr: 1,2-Dichloroethane-d4 113 70-130 %REC 10 10/10/01 3:02:00 AM Surr:Toluene-d8 98.9 70-130 %REC 10 10/10/01 3:02:00 AM Surr:4-Bromofluorobenzene 101 70-130 %REC 10 10/10/01 3:02:00 AM Surr:2,5-Dibromotoluene 86.3 70-130 %REC 10 10/10/01 3:02:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Yes _ No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No -../— Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: \ DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte,detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte dctccfcO jn the associatcd Mcthod Blank 11-Method prescribcd holding time excccded 6 w � AMRO Environmental Laboratories Corp. Date: 18-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: EXC.FGHIJ(5-10) Lab Order: 0110043 Tag Number: Project: TRASK RESIDENCE Collection Date: 10/2/01 Lab ID: 0110043-04B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE-PETRdLEUM HYDROCAF�BONS MAEPH. Analyst: RKK C9-C18 Aliphatic Hydrocarbons 640 53 mg/Kg-dry 1 10/10/01 2:50:00 AM C19-C36 Aliphatic Hydrocarbons 230 53 mg/Kg-dry 1 10/10/01 2:50:00 AM C11-C22 Aromatic Hydrocarbons 380 53 mg/Kg-dry 1 10/10/01 2:50:00 AM Naphthalene 1.8 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM 2-Methylnaphthalene 6.9 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Acenaphthylene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Acenaphthene 0.36 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Fluorene -. 0.85 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Phenanthrene 1.2 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Anthracene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Fluoranthene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Pyrene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Benz(a)anthracene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Chrysene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Benzo(b)fluoranthene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Benz o(k)fluoranthene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Benzo(a)pyrene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Dibenz(a,h)anthracene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Indeno(1,2,3-cd)pyrene ND 0.27 mg/Kg-dry, 1 10/10/01 2:50:00 AM Benzo(g,h,i)perylene ND 0.27 mg/Kg-dry' 1 10/10/01 2:50:00 AM Surr. 1-Chlorooctadecane 89.0 40-140 %REC 1 10/10/01 2:50:00 AM Surr.2-Bromonaphthalene 111 40-140 %REC 1 10/10/01 2:50:00 AM Surr:2-Fluorobiphenyl 110 40-140 %REC 1 10/10/01 2:50:00 AM Surr:o-Terphenyl 81.5 40-140 %REC 1 10/10/01 2:50:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Yes _ No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed /attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief, accurate and complete. SIGNATURE: DATE: ! ( � PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range -Analyte�Oetected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte dclectedin the associated Method Blank H-Method prescribed holding time exceeded 7 AMRO Environmental Laboratories Corp. Date: I8-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: EXC.FGHIJ(0-5) Lab Order: 0110043 Tag Number: Project: TRASK RESIDENCE Collection Date: 10/2/01 Lab ID: 0110043-05B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS. MAEPH Analyst: RKK C9-C18 Aliphatic Hydrocarbons 2,800 510 mg/Kg-dry 10 10/9/01 10:40:00 AM C19-C36 Aliphatic Hydrocarbons 690 51 mg/Kg-dry 1 10/8/01 9:36:00 PM C11-C22 Aromatic Hydrocarbons 1,100 51 mg/Kg-dry 1 10/8/01 9:36:00 PM Naphthalene 5.1 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM 2-Methylnaphthalene 23 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Acenaphthylene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Acenaphthene 1.2 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Fluorene3.8 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Phenanthfene 5.4 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Anthrac,ene 0.82 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Fluoranthene NO 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Pyrene 0.86 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Benz(a)anthracene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Chrysene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Benzo(b)fluoranthene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Benzo(k)fluoranthene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Benzo(a)pyrene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Dibenz(a,h)anthracene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Indeno(1,2,3-cd)pyrene ND 0.25 .mg/Kg-dry: 1 10/8/01 9:36:00 PM Benzo(g,h,i)perylene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Surr: 1-Chlorooctadecane 65.2 40-140 %REC 1 10/8/01 9:36:00 PM Surr:2-Bromonaphthalene 103 40-140 %REC 1 10/8/01 9:36:00 PM Surr:2-Fluorobiphenyl 93.6 40-140 %REC 1 10/8/01 9:36:00 PM Surr:o-Terphenyl 79.8 40-140 %REC 1 10/8/01 9:36:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbonsdrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Z Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed /attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: 1D�D PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range 7-Arraly;yc'detecte8 below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded Q � r AMBO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Laboratories Corporation -eet Merrimack, NH 03044 Client L' (603) 424_2022 AMRO ID: d 110 q Project Name: S F Date Rec.: Ship via:(circle one) Fed Ex., UPS , MRO Courier Date Due: ,. Hand Del., Other Courier, Other. I Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? Y 3. Custody Seals Intact? 4. Air Bill included id foldgr if received? r- 5. 1s'COr-1hcludedwith`s'amples? t 6. Is COC signed and dated by client? 7. Laboratory receipt temperature. TEMP = 3 s Samples rec.with ice_ packs_neither 8. Were samples received the same day they were sampled? r/ Is client temperature 4°C t 2'C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? s� 10. Does the info on the COC match the samples? J 11.Were samples rec.within holding time? v 12.Were all samples properly labeled? 13.Were all samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact?(none broken or leaking) 16.Were VOA vials rec,with no air bubbles? 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH(circle one . M=tvlethanol =EnCore (air-tight container) Sampling Method VOA(circle one): M=Methanol,SB=Sodium Bisulfate, E=EnCore, B=Bulk If M or SS: Does preservative cover the soil? f If NO then client must be faxed. Does preservation level come close to the fill line on the vial? If NO then client must be faxed, � Were vials provided by AMBO? � If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP, 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into: Internal Tracking Log? Dry Weight Log? Client Log? _ Composite Log? Filtration Log? Received By: Date: 10-3-01 Logged in By: eC Date: p_��I 0 Labeled By: C Date: 16—cF—p/ Checked By: in Date: AMR0 cnvircnmental r14,C 14 SStreet Laboratories Corporation Merrimack, MH 03G-=4 (603) 424-2022 Please Circle if: Sampl = Soil Sample- este List Preserv. Vclume Final Volume Preserr. Initial Acceptable? rdded by Seludon 10 T Preservative adjusted Sample 10 Analysis Sample Listed pH Y or N ANIRO of?resew. Added pH I I � • i I I I I i i I i i II I I I I I i I I I I I I I I i I i I I ( I I I i pH Checked'6y: Cate: pH adjusted Sy: Cate: AMRO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORD 40382 Office:(603)424-2022 1 I I Herrick Street �` Fax:(603)429-8496 Merrimack,NH 03054 Project,No.: _ Project Name: Tptir Q Project 1%,tanagcr: Snatu erg AM O Project No.: I ILA Project State: Sample ID Date/Time Matrix Total# Analysis Required Remarks •. Sampled A=Air of Cont. - S=Soil &Size �� �� , �4•�4 GW=Ground W. WW=Waste W. ;. DW=Drinking W. q �\ O=Oil b a LO I Other—Specify -X<_ F( N.T ► —lam ;.��/�.�t' f ��a,�i%n ✓ r (,•T , i Preservative:C1-HCl,McOH,N-HNU3,S-1-112SO4,Na-NaOH,O-Other ontainer Type: P-Plastic,G-G ass,V- is,T-Teflon,O-Other Please print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,ctc; logged in and the turnaround time clock will not start until any FAX No.: ambiguities are resolved. Send Results To: — /A/t Seal Intact? GW-I GW-2 GW-3 Yes No: N/A MCP Level Needed: N Relipquished By Date/Time Received BY-,' Date/Time _ //.;Vl PRIORITY TURNAROUND TIME AUTHORIZATION Before submitting samples for expedited TAT,you must have requested r Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER By- AUTHORIZATION No. BY: /ti/.G� v' /O/3// SHEET OF e: Lab Copy ell w:Accompanies R .poi3---`-/ Pink:Client Copy/ �t. • Ii. •.,:\ i�. .,\� Iii. .�\��\ i �I I••I•. .'\\�\\\1i.�j/II•Ii. �\�\\\\�• •'%IIS•%' :\�\\\\'. ;�Ii�./,I \ \:N;.• :IIII/1 i• \ \\,:���.�•�•!://•�' i��\\lii 1�. i��i.//IIi\�1'� ::' :!I.i�;'i��• �•\1��iii . II/:: i �\ \ •i����. �:III ,i•\1, ��. ..!ii i� / � 1 \ � IIII •\ ',• • : I I iii ...' 11 11.1 "':,r!••• � Ij ; ;•�• �� III . 1 ..... /,Ili �\I\'• ...:!• /Ir,• \\ .... .I, ,`\' II,I•. ♦,,. /'I'. `I,I \ :�• •/��•r�1!% •\•'•.��\\:�..i1I1���•••!!' ��•�.�;�,��..ir�%��•, ,� .•\\11\�•.:'%1///•r' i\\\.\i„%11%II �\\\\�\•�.%%I%�/�r�'i•. �\���.���� �II%••�./!r-: •:\\\\1\ I/1I / ' .�\I\•i ♦i�III�.•! •\•.\1�•'%%,Ilii I'r•'' ,•.,\\\.\\�•./I,/I,�I�/rr'' ,,\'\ \�1•./IIII / ��� The Commonwealth of Massachusetts Department of Environmental Protection Division of Environmental Analysis Senator William X. Wall Experiment Station certifies r/ M-NH012 AMRO ENVIRONMENTAL LAB 111 HERRICK ST MERRIMACK, NH 03054-0000 Laboratory Director: Nancy Stewart for the analysis of NON POTABLE WATER(CHEMISTRY) POTABLE WATER(CHEMISTRY) pursuant to 310 CMR 42.00 This certificate supersedes all previous Massachusetis certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CMR 42.00. This certificate is valid only when accompanied by the latest dated Certified Parameter List as issued by the Massachusetts D.E.P. Contact the Division of Environmental Analysis to verify the current certification status of the laboratory. Certification is no guarantee of the validity of the data. This certification is subject to unannounced laboratory inspections. Issued: 01 JUL 2001 (2,, cz.�. Expires: 30 JUN 2002 Director, Division of Environmental Analysis �"•:•����:�' ?�.':aiirSi:7�•ti�::i```� j,�1�.i''i :i�i•\\;'r:: '•/I/riii:;..\\•\\`:'r' •'viii 11/11,•..\.\\\;�•:�:• .,I,/I/r;.;.'\N,\.;'. './/••��• ,•�� .�1�.. .,::iii;%::�\.\'��,. .I:,�•" • ;. . �: •``:Ci��\:� '•I/ilLiii!1..:1�Cd::�i�j�. '!$I��Sii�:"�Ci:i�:,)- ,!'iliiiii;'.a�\�iii\:•!, �:/iiilii%';'�::ii���. 1!:�ii:Ii/;'.''^;\�:ii�i!' �!!i�iii�i•:' •��;;\�\..' .r,iiiiS •:�ii���. •!/iii!." '•ip i�!.• '••!i/,/' \•���.• /I/1 •��.. i3 CONBIOVWF_4LTH OF NW S AC HUS FITS DEPARTNWl T OF ENVTRONINIL ITAL PROTEMON Certified Parameter List as of: 01 JUL 2001 n NH012 AMRO ENVIRONMENTAL LAB NIERMACK NH NON POTABLE WATER(CHE IISMY) Effecthe 01 JUL 2001 Expiration 30 JUN 2002 Date Date Analvtes and Methods ALUMINUM EPA 200.7 NITRATE-N EPA 353.2 ANTIMONY EPA 200.7 KJELDAHL-N EPA 351.1 ANTIMONY r EPA 204.2 KJELDAHL-N EPA 351.2 ARSENIC EPA 200.7.,,- - ORTHOPHOSPHATE EPA 365.2 -^' .a. ....._,. ,; :; ARSENIC EPA 206.2 ORTHOPHOSPHATE EPA 300.0 ARSENIC ASTM D2972-93(C) TOTAL PHOSPHORUS EPA 365.2 BERYLLIUM EPA 200.7 CHEMICAL OXYGEN DEMAND EPA 410.4 CADMIUM EPA 200.7 CHEMICAL OXYGEN DEMAND HACH METHOD 8000 CHROMIUM EPA 200.7 BIOCHEMICAL OXYGEN DEMAND EPA 405.1 COBALT EPA 200.7 TOTAL CYANIDE EPA 335.2 COPPER EPA 200.7 NON-FILTERABLE RESIDUE EPA 160.2 IRON EPA 200.7 TOTAL RESIDUAL CHLORINE SM 4500-CL-G LEAD J EPA 200.7 OIL AND GREASE EPA 413.1 LEAD EPA 239.2 TOTAL PHENOLICS EPA 420.1 MANGANESE EPA 200.7 VOLATILE HALOCARBONS EPA 624 MERCURY EPA 245.1 VOLATILEAROMATICS EPA 624 MOLYBDENUM EPA 200.7 CHLORDANE EPA 608 NICKEL EPA 200.7 ALDRIN EPA 608 SELENIUM EPA 200.7 DIELDRIN EPA 608 SELENIUM EPA 270.2 DDD EPA 608 SILVER EPA 200.7 DDT EPA 608 STRONTIUM EPA 200.7 HEPTACHLOR EPA 608 THALLIUM EPA 200.7 HEPTACHLOR EPDXIDE EPA 608 THALLIUM EPA 279.2 POLYCHLORINATED BIPHENYLS(WATER) EPA 608 ZINC EPA 200.7 POLYCHLORINATED BIPHENYLS(OIL) EPA 600/4-81-045 PH EPA 150.1 SPECIFIC CONDUCTIVITY EPA 120.1 TOTAL DISSOLVED SOLIDS EPA 160.1 TOTAL HARDNESS(CAC03) EPA 200.7 CALCIUM EPA 200.7 MAGNESIUM EPA 200.7 SODIUM EPA 200.7 POTASSIUM EPA 200.7 TOTAL ALKALINITY EPA 310.1 CHLORIDE EPA 325.3 CHLORIDE EPA 300.0 FLUORIDE EPA 340.2 FLUORIDE EPA 300.0 SULFATE EPA 375.4 SULFATE EPA 300.0 AMMONIA-N EPA 350.2 NITRATE-N EPA 300.0 June 27,2001 * ProNisional Certification Patie 1 of 2 A. 317 Elm Street �r ye Milford NH 03055 Tel (603)673-5440 • Fax(603)673-0366 October 12, 2001 Ms. Nicole Borduz AMRO Environmental Laboratories Corp 111 Herrick. treet Merrimack, NH 03054' Job Name: Trask Residence Laboratory#: 01100072 Job#: 0110043 Purchase Order#: N/A Location: N/A Control#: 38651 Dear Ms. Borduz Enclosed please find the laboratory results for the above reference samples that were received Py the ChemServe sample custodian, under chain of custody control number 38651 on 10/09/01. Samples were collected by CC on 10/02/01. Any abnormalities to the samples on receipt would be noted on the enclosed chain of custody document. This report is not valid without a completed ChemServe chain of custody with the corresponding control number, attached. All samples analyzed by ChemServe are subject to quality standards. These standards are either as stringent or more stringent that those established under 40 CFR Part 136, state certification programs, and corresponding methodologies. ChemServe has written QA/QC Procedures Manual that outlines these standards, and is available, upon request, for your reference. Unless otherwise stated on the Chain of Custody or within the report, all holding times, preservation techniques, container types, and analytical methods are analogous with those outlined by them U.S. EPA. I certify that I have reviewed the above referenced analytical data and state form.;, and I have found this report within compliance with the procedures outlined in the ChemServe QA/QC Procedures Manual. Ellen Abrams-QA/QC Manager JayC"*�\A4 Ch tal - i a-oratory Director rY rY This rep rt con ins 10 pages. O \N ACCO.9 �Y a ane a_ I . Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratories Corporation LAB#: 01100072-01 JOB NAME:Trask Residence JOB#:0110043 LOCATION: N/A SAMPLE IDENTITY: MW-2 CONTROL#: 38651 DATE SAMPLED: 10/02/01 DATE REC'D: 10/05/01 DATE ANALYZED: 10/11/01 MATRIX: LIQUID DETECTION LIMIT BASED ON PQL 7.1 COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROM ETHANE BDL 0.5 BROMODICHLOROM ETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE - BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratories Corporation LAB#:01100072-01 JOB NAME:Trask Residence LOCATION: NIA SAMPLE IDENTITY: MW-2 CONTROL#: 38651 DATE SAMPLED: 10/02/01 DATE REC'D: 10/05/01 DATE ANALYZED: 10/11/01 rMATRIX: LIQUID _ _.. .� ••- _ DETECTION LIMIT BASED ON PQL COMPOUND }. F CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON D15ULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratories Corporation LAB#:01100072-02 JOB NAME:Trask Residence JOB#:0110043 LOCATION: N/A SAMPLE IDENTITY: MW-3 CONTROL#: 38651 DATE SAMPLED: 10/02/01 DATE RECD: 10/05/01 DATE ANALYZED: 10/11/01 MATRIX:LIQUID -� - DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION_ DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROM ETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPEN E BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES A 4 4 Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratories Corporation LAB#:01100072-02 JOB NAME:Trask Residence LOCATION:N/A SAMPLE IDENTITY: MW-3 CONTROL#: 38651 DATE SAMPLED: 10/02/01 DATE RECD: 10/05/01 DATE ANALYZED: 10/11/01 MATRIX:LIQUID - - DETECTION LIMIT BASED ON POL COMPOUND T. F jCONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD � �� 5 Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratories Corporation LAB#:01100072-03 JOB NAME:Trask Residence JOB#:0110043 LOCATION: N/A SAMPLE IDENTITY: Drinking Water Well CONTROL#: 38651 DATE SAMPLED: 10/02/01 DATE RECD: 10/05/01 DATE ANALYZED: 10/11/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION ION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROM ETHANE BDL 0.5 BROMODICHLOROM ETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOME THANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPEN E BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED:1 OF 2 PAGES i 1 I � Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratories Corporation LAB#:01100072-03 JOB NAME:Trask Residence LOCATION:N/A SAMPLE IDENTITY: Drinking Water Well CONTROL#: 38651 DATE SAMPLED: 10/02/01 r DATE REC'D: 10/05/01 DATE,ANALYZED: 10/11/01 MATRIX: LIQUID DETECTION LIMIT BASED ON PQL COMPOUND N t' CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTAD IENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 0.5 DI-ISOPROPYL ETHER BDL 20 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD i CHEMSERVE VOA SPIKE RECOVERY FORM EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratories Corporation LAB#:01100072 JOB NAME:Trask Residence LOCATION:N/A SAMPLE IDENTITY:MATRIX SPIKE 01100086-02 CONTROL#: 38651 DATE ANALYZED:10/11/01 COMPOUND 6ONC ADDED AMT REC DUP AMT REC %REC_ DUP%REC %RPD R..,...._. (UP/L) f (UG/L) (UG/L) 1,1-DICHLOROETHENE 14 �, 4.3 108% BENZENE 4 4.1 103% TRICHLOROETHENE 4 3.7 93% CHLOROBENZENE 4 4.0 100% 1,2-DICHLOROBENZENE 4 3.8 95% 1,3,5-TRIMETHYLBENZENE 4 3.8 95% 1,2,4-TRICHLOROBENZENE 4 3.5 88% duplicate not available due to matrix interference VOA MATRIX SPIKE REC 6 5 4 ■CONC ADDED 3 O LW RECOVERY 2i OLD RECOVERY 1 0 ' 1 2 3 4 5 6 7 SPIKE RECOVERY LIMITS 70-130% AMBO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORD Office: 38498 Office:(603)424-2022 111 Herrick Street Fax:(603)429-8496 Merrimack,NII 03054 Project No.: Project Name: (� S _[�./VC Project Manager: Sam p rs Signature): AMRO Project No.: Project State: Sample ID Date/Titne Matrix Total# Analysis Required 1E Remarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. WW=Waste W. �t) DW=Drinking W. 0=Oil Other—Specify � - =Gt/— o � 9• G H/ �- o � AWA Wcrw o v 4•2G IVo Preservative:C-HC,McO11,N-HNO3,S-HI 504,Na-Na011,O-Ot ter ontainer Type: P-P astic,G-G ass, -Via,T-Te on,O- tier Please print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will pot start until any FAX No.: ambiguities are resolved: Send Results To: Seal Intact? GW-1. GW-2 GW-3 - ti O z2 Yes No N/A MCP Level Needed: Relinquished By Date/Time ,Received By Date/Time P.O.No: v PRIORITY TURNAROUND TIME AUTHORIZATION Before submitting samples for expedited TAT,you must hAYc VFquested Gy _ Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER By: CC-- AUTHORIZATION No. BY: f / 07 SKEET OF White: Lab Copy Yellow:Accompanies Report Pink:Client Copy Chain of Custody No. 38651 C-51K �� �erVe 317 Elm Street Milford, NH 03055 Multiple COC's Yes No (603) 673-5440/ Fax (603) 673-0366 t CHAIN OF CUSTODY A 10 0141114,71 CUSTOMER: / r� l JOB NAME: TURNAROUND TIME:(CIRCLE ONE:) ADDRESS: JOB NUMBER: STANDARD RUSH CITY/STATE/ZIP LOCATION: RUSH T.A.T. (CHECK w/LAB) ..� 4: AMBER GLASS(AG) / GLASS(G) / PLASTIC(P) TELEPHONE: TELEPHONE: w4 � REPORT TO: CONTACT: O�P ,P�,J QUOTE NUMBER: 0 4 P O NUMBER: Q SAMPLE 1 MATRIX 444 Z SAMPLE IDENTIFICA'I'ION& LOCATION(D COLLECTED m •TYPE � S()1.11)(S) � ° 1.1Qt11"('•) ANALYSIS 0 F O COMHINED(C) ; HOp Q © ® U IIAZARD(11) 0$ RATE 11h1E RATE, 11MM1 RATE 11II11: RAIL• TIME . DA11: 11Il1L• RATE IML ' RATE 1lML• DALETI L I I 1lME MILITARY SAMPLE CHECK LIST: FIELD READING(S): Q CUSTODY SAMPLER: RATE 11th RECEIVED WITIIIN IIOLDTIME YES OR NO (print name) RECEIVED IN GOOD CONDITION YES OR NO SIGNATURE: TEMP BLANK C DAIS TIME SIIIPPED OR HAND DELIVERED RELINQUISHED: �' \` SAMPLES WERE PROPERLY PRESERVED YES NO N/A 7 i; .. DAIL. 111AL. SAMPLES WERE FILTERED IN FIELD LAB N/A RECEIVED: ; IF NO EXPLAIN: f DAIS 11ML. RELINQUISHED: /' o I1MC �. RECEIVED FOR LAB: /� E/'P'L_. D-;. J/.'y GROUT'#D WOv ,t� � D =_ Environmental Laboratories Corporation 111 Herrick Street, Merrimack, NH 03054 TEL: (603)424-2022 FAX:(603)429-8496 October 22,2001 Tim Toomey Subsurface Remediation Technologies 355 Central St.'-f', - Rowley,MA 01469 TEL: (978)948-3861 ` FAX: (978)948-3861 RE: TRASK Order No.: 0110160 Dear Tim Toomey: AMBO Environmental Laboratories Corp. received 2 samples on 10/16/01 for the analyses presented in the.following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Conference SLAC state and EPA requirements. A copy of the Laboratory Accreditation Con (N ), q appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s)upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time, A_MRO will properly dispose of the remaining sample(s). If P you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of pages. This letter is an integral part of your data report. If you have any questions regarding this project in the future,please refer to the Order Number above. Sincerely, Nancy Stewart Vice President/Lab Director AMRO Environmental Laboratories Corp. Date: 22-Oct-01 CLIENT: Subsurface Remediation Technologies Project: TRASK Work Order Sample Summary Lab Order: 0110160 Date Received: 10/16/01 Lab Sample ID Client Sample ID Collection Date Q1.1016.0-01A_ {y,F,(aH I L(5-10') 10/16/01 0 110 1 60-02A. J K M($'-10') 10/16/01 2 AMRO Environmental Laboratories Corp. Date: 22-Oct-01 CLIENT: Subsurface Remediation Technologies Project: TRASK CASE NARRATIVE Lab Order: 0110160 MADEP-EPH 1-. The surrogate 1=Ohlor©octadecane recovered above the QC limits (40-140%) in sample J'K M(5'-10')(0110160-02A) due to sample specific matrix interference. 2. The laboratory control sample recovered above the QC limits for most target analytes due to suspected concentration of the spiking solution. ,r AMRO Environmental Laboratories Corp. Date: 22-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: F G H I L(5'-10') Lab Order: 0110160 Project: TRASK Collection Date: 10/16/01 Lab ID: 0110160-OIA Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTAJRE..'�' D2216. . Analyst: JC ,- Percent Moisture 5.5 0 wt%, 1 10/17/01 • i Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL.-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. v 4 AMRO Environmental Laboratories Corp. Date: 22-ocr-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: J K M(5'-10') Lab Order: 0110160 Project: TRASK Collection Date: 10/16/01 Lab ID: 0110160-02A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE;r. .�: D2216 Analyst: JC Percent Moisture t 5.1 0 wt% 1 10/17/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL-Reporting Limit:defined as the lowest concentration the laboratory can accurately quantitate. AMRO Environmental Laboratories Corp. Date: 22-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: F G H I L(5'-10') Lab Order: 0110160 Tag Number: Project: TRASK Collection Date: 10/16/01 Lab ID: 0110160-OIA Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK C9-C18 Aliphatic Hydrocarbons ND 52 mg/Kg-dry 1 10/19/01 7:29:00 AM C19-C36 Aliphatic Hydrocarbons ND 52 mg/Kg-dry 1 10/19/01 7:29:00 AM C11-C22 Aromatic Hydrocarbons ND 52 mg/Kg-dry 1 10/19/01 7:29:00 AM Naphthalene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM 2-Methylnaphthalene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Acenaphthene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Fluorene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Phenanthrene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Anthracene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Pyrene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Chrysene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Dibenz(a,h)anth racene ND 0.26 mg/Kg-dry 1 10/19/01 7:29:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry. 1 10/19/01 7:29:00 AM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry. 1 10/19/01 7:29:00 AM Surr: 1-Chlorooctadecane 95.8 40-140 %REC 1 10/19/01 7:29:00 AM Surr:2-Bromonaphthalene 88.2 40-140 %REC 1 10/19/01 7:29:00 AM Surr:2-Fluorobiphenyl 101 40-140 %REC 1 10/19/01 7:29:00 AM Surr:o-Terphenyl 62.2 40-140 %REC 1 10/19/01 7:29:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required OA/QC procedures achieved: _ Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is,to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: PRINTED NAME: Nancy StewaA POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte.detected below quantitation limits R-RPD outside accepted recovery limits k-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded AMRO Environmental Laboratories Corp. Date: 22-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: J K M(5'-10') Lab Order: 0110160 Tag Number: Project: TRASK Collection Date: 10/16/01 Lab ID: 0110160-02A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXT RACTABLE_PETROLEUM HYDROCARBONS MAEPH Analyst: RKK C9-C18 Aliphatic Hydrocarbons 3,700 530 mg/Kg-dry 10 10/19/01 12:47:00 PM C19-C36 Aliphatic Hydrocarbons 430 53 mg/Kg-dry 1 10/19/01 8:04:00 AM C11-C22 Aromatic Hydrocarbons 780 53 mg/Kg-dry 1 10/19/01 8:04:00 AM Naphthalene 7.1 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM 2-Methylnaphthalene 26 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Acenaphthene 3.8 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Fluorene4.9 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Phenanthrene 6.3 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Anthracerie 0.57 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Pyrene 0.69 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Chrysene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Dibenz(a,h)anthracene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Benzo(g,hJ)perylene ND 0.26 mg/Kg-dry 1 10/19/01 8:04:00 AM Surr: 1-Chlorooctadecane 302 40-140 S %REC 1 10/19/01 8:04:00 AM Surr:2-Bromonaphthalene 80.5 40-140 %REC 1 10/19/01 8:04:00 AM Surr:2-Fluorobiphenyl 70.6 40-140 %REC 1 10/19/01 8:04:00 AM Surr:o-Terphenyl 76.6 40-140 %REC 1 10/19/01 8:04:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION / Were all QA/QC procedures required by the VPH or EPH method followed: _XZ Yes No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed t attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: /Q PRINTED NAME: Nancy Stewad POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analvfe detected below quantitation limits R-RPD outside accepted recovery limits 4-See Case Narrative B-Analyfe detected in the associated Method Blank H-)\Method prescribed holding time exceeded 7 AMRO Environmental Laboratories Corp. 22-ocr-01 Lab Order: 0110160 I .'I Client: Subsurface Remediation Technologies DATESREPORT Project: TRASK Y Sample ID Client Sample ID Collection Date Matrix Tcst Name TCLP Date Prep Date Analysis Date 0110160-01A F G 1-11 L(5'-10') 10/16/01 Soil GPI 1,Soil,Full List 10/17/01 10/19/01 Percent Moisture ` h;.,,. 10/17/01 t 0110160-02A J K M(5'-10') EPI I,Soil,Full List 10/17/01 10/19/01 1:1'11,Soil,Full List ` 10/17/01 10/19/01 Percent Moisture - 10/I7/01 00 AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 603 42 _ 4-2022 Client: AMRO ID: / V I/0 l 0 Project Name: %/�/ Date Rec.: /Q- 146-01 Ship via:(circle one) Fed Ex., UPS iv1R0 Courier Date Due: i 0_ -,93-t7/ Hand Del., Other Courier, Other. Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? 3. Custody Seals Intact? 4. Air Bill included in k5lder4f received? ✓ 5: Is"CO0included y+ith sampleq? 6: Is COC signed and dated by-client? 7. Laboratory receipt temperature. TEMP = T Samples rec.with ice ce packs_neither 8. Were samples received the same day they were sampled? , Is client temperature 4°C±2°C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? 10. Does the info on the COC match the samples? 11.Were samples rec.within holding time? 12.Were all samples properly labeled? t/ 13.Were all samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact? (none broken or leaking) t/ 16.Were VOA vials rec.with no air bubbles? v 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA Soils only: f/ Sampling Method VPH (circle one): M=Methanol, E=EnCore(air-tight container) Sampling Method VOA(circle one): M=Methanol, S6=Sodium Bisulfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? If NO then client must be faxed. Were vialsprovided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into: Internal Tracking Log? Dry Weight Log? Client Log? Composite Log? Filtration Log? Received By:,g�-' Date: 10-16-01 Logged in By: L C— Date: /0—/7—o Labeled By: Date: /0-/'7-p/ Checked By: Date: 0_/ — AMRO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORDZ p 4 �C O Office:(603)424-2022 :111 Herrick Street J U Fax: (603)429-8496 Merrimack,NH 03054 j t Projcet,No.: Project Name: Project Manager: S� plers(SJ gna' r ): AMRO Project No.: 1 l 1 (00 Project State: Sample ID Date/Time Matrix Total# Analysis Rc uirgd Remarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. WW=Waste W. DW=Drinking W. 0=Oil Other-Specify A/I/ '2' -O EG HL of 5 -�a' 1.va P�1 J` .a� Err 'reservahve'C-H McOH N-HNO3•S-H2SO4,Na-NaOH,O-Ot ier :ontainerType: P-Plastic,G-G ass, -Vta,T-Te on,O-Ot er ,lease print clearly,legibly and completely.Samples can not be (Cwa NOTES:Preservatives,Special reporting limits,Known Contamination,etc; )gged in and the turnaround time clock will not start until any FAX No.: mbiguities are resolved. end Results To: z ScalIntact? GW-1 GW-2 GW-3 Yes No N/A MCP Level Needed: Relinquished By Date/Time 'Re eived Bye Date/Time P.O.lYa PRIORITY TURNAROUND TIME AUTIIORIZATION Before submitting samples for expedited TAT,you must have requested Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER By: AUTHORIZATION No. BY: • l ��t r( / ) %' /,•t �_!' C` /l ,J SHEET OF V .La"b Copy ell . ccomoanies Report Pink: Client opy ;�;:;. '.•\;::i:;. r iii/�/•i :`.•�:ii:�• ::r���•• • ;\:�,••. r ii •r %�. : \\ :`;.��/.:.I ••. : \••\,;��:I��• . : � :\�'. .%i;.'� ,.;i� �'. :,iij;�•:�•;' ``: . ��i:::.., •% \i:i:..:ii".. \��i:..:r%i j•r,•.�:'• i�:;..�'ii'r,, '•".•,.a• ,•;\\::i:i"ii::;r;r;,' .�.�\•:i:�;•i::•:•i;.!�:•• ���i•::::"iii i•:rr•. •�•i`.::.",i::•:•r.'::•• ';�•��•::i' it::•:•r•,�''• :.l:::.... The Commonwealth of Massachusetts i F ' _ r c. '1M Sv•�. Department of Environmental Protection Division of Environmental Analysis Senator William X. Wall Experiment Station certifies M-NH012 AMRO ENVIRONMENTAL LAB 111 HERRICK ST MERRIMACK, NH 03054-0000 Laboratory Director: Nancy Stewart .•• for the analysis of NON POTABLE WATER(CHEMISTRY) POTABLE WATER(CHEMISTRY) pursuant to 310 CMR-12.00' This certificate supersedes all previous Massachusetts certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CMR 42.00. This certificate is valid only when accompanied by the latest dated Certified Parameter List as issued by the Massachusetts D.E.P. Contact the Division of Environmental Analysis to verb the current certification status of the laboratory. Certification is no guarantee of the validity of the data. This certification is subject to i unannounced laboratory inspections. Issued: 01 JUL 2001 Expires: 30 JUN 2002 Director, Division of Environmental Analysis I •,.• •.�i•.• •.,�. ggr•a' ��.•• .,r r,i. ��. ii:i,. �,.•��•�. • i:iai�. ..��:�ii!\. � int. qqr � J CONINIONAVFALTH OF MAS SACHUSETTS DEPARTMENT OF EVVIRONAffiNTAL PROTECTION Certified Parameter List as of: 01 JUL 2001 M NH012 AMRO ENVIRONMENTAL LAB MII2RIMACK NH NON POTABLEWATER(CHEMTRY) Fffecthe 01 JUL 2001 l piration 30 JUN 2002 Date Date Analvtes and Methods ALUMINUM EPA 200.7 NITRATE-N EPA 353.2 ANTIMONY EPA 200.7 KJELDAHL-N EPA 351.1 ANTIMONY kr. EPA 204.2 KJELDAHL-N EPA 351.2 .;: , ARSENIC ' `' EPA?00.7.:, ORTHOPHOSPHATE EPA 365.2 ARSENIC EPA 206.2 ORTHOPHOSPHATE EPA 300.0 ARSENIC ASTM D2972-93(C) TOTAL PHOSPHORUS EPA 365.2 BERYLLIUM EPA 200.7 CHEMICAL OXYGEN DEMAND EPA 410.4 CADMIUM EPA 200.7 CHEMICAL OXYGEN DEMAND HACH METHOD 8000 CHROMIUM EPA 200.7 BIOCHEMICAL OXYGEN DEMAND EPA 405.1 COBALT EPA 200.7 TOTAL CYANIDE EPA 335.2 COPPER EPA 200.7 NON-FILTERABLE RESIDUE EPA 160.2 IRON EPA 200.7 TOTAL RESIDUAL CHLORINE SM 4500-CL-G LEAD EPA 200.7 OIL AND GREASE EPA 413.1 LEAD EPA 239.2 TOTAL PHENOLICS EPA 420.1 MANGANESE EPA 200.7 VOLATILE HALOCARBONS EPA 624 MERCURY EPA 245.1 VOLATILE AROMATICS EPA 624 MOLYBDENUM EPA 200.7 CHLORDANE EPA 608 NICKEL EPA 200.7 ALDRIN EPA 608 SELENIUM EPA 200.7 DIELDRIN EPA 608 SELENIUM EPA 270.2 DDD EPA 608 SILVER EPA 200.7 DDT EPA 608 STRONTIUM EPA 200.7 HEPTACHLOR EPA 608 THALLIUM EPA 200.7 HEPTACHLOR EPDXIDE EPA 608 THALLIUM EPA 279.2 POLYCHLORINATED BIPHENYLS(WATER) EPA 608 ZINC EPA 200.7 POLYCHLORINATED BIPHENYLS(OIL) EPA 600/4-81-045 PH EPA 150.1 SPECIFIC CONDUCTIVITY EPA 1.20.1 TOTAL DISSOLVED SOLIDS EPA 160.1 TOTAL HARDNESS(CAC03) EPA 200.7 CALCIUM EPA 200.7 MAGNESIUM EPA 200.7 SODIUM EPA 200.7 POTASSIUM EPA 200.7 TOTAL ALKALINITY EPA 310.1 CHLORIDE EPA 325.3 CHLORIDE EPA 300.0 FLUORIDE EPA 340.2 FLUORIDE EPA 300.0 SULFATE EPA 375.4 SULFATE EPA 300.0 AMMONIA-N EPA 350.2 , NITRATE-N EPA 300.0 -June 27,2001' - * Pro-,isional Certification Page I of 2 12, i COAL1IONINN EALTH OF MAS S ACHUS FITS DEPARTDIFVT OF ESN ROINNI1H\T.AL PROTECTION Certified Parameter Listas of. 01 JLL2001 M-NH012 AMRO ENVIRONMENTAL LAB MERRIMACK NH POTABLE WATER(CHEVUSTRY) Effec6Ne 01 JUL 2001 &Tiration 30 JtN 2002 Date Date Analvtes and Methods ANTIMONY EPA 200.9 ARSENIC EPA 200.7 ARSENIC � Y EPA 200.9 BARIUM t . BERYLLIUM EPA 200.7 CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COPPER EPA 200.7 LEAD EPA 200.9 MERCURY EPA 245.1 NICKEL EPA 200.7 SELENIUM EPA 200.9 THALLIUM EPA 200.9 NITRATE-N EPA 353.2 NITRITE-N EPA 353.2 FLUORIDE EPA 300.0 FLUORIDE SM 4500-F-E SULFATE EPA 300.0 CYANIDE SM 4500-CN-C,E TURBIDITY EPA 180.1 RESIDUAL FREE CHLORINE SM 4500-CL-G CALCIUM EPA 200.7 TOTAL DISSOLVED SOLIDS SM 2540C PH EPA 150.1 1,2-DIBROMOETHANE EPA 504.1 1,2-DIBROMO-3-CHLOROPROPANE EPA 504.1 June 27,2001 - *Provisional Certification Page 2 of 2 � J Environmental Laboratories Corporation `- 111 Herrick Street,Merrimack, NH 03054 TEL:(603)424-2022 FAX: (603)429-8496 October 29,2001 Tim Toomey Subsurface Remediation Technologies kr . 355 Central St."r; .Rowle.y,MA 01969 ., TEL: (978)948-3861 FAX: (978)948-3861 RE: TRASK-N. ANDOVER Order No.: 0110214 Dear Tim Toomey: AMBO Environmental Laboratories Corp. received 1 sample on 10/22/01 for the analyses presented in the:-following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference(NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s)upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty (30) days from this report date. After this time, AMRO will properly dispose of the remaining sample(s). If you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of I a pages. This letter is an integral part of your data report. If you have any questions regarding this project in the future, please refer to the Order Number above. Sincerely, Nancy Stewart Vice President/Lab Director ' I AMRO Environmental Laboratories Corp. Date: 29-Oct-01 CLIENT: Subsurface Remediation Technologies Project: TRASK-N.ANDOVER Work Order Sample Summary Lab Order: 0110214 Date Received: 10/22/01 Lab Sample ID ,.Client Sample ID Collection Date 10/22/01 01 W214'-01-A - J I FK 1,M 1,(0-5)..- La. J I AMRO Environmental Laboratories Corp. Date: 29-Oct-01 CLIENT: Subsurface Remediation Technologies Project: TRASK-M ANDOVER CASE NARRATIVE Lab Order: 0110214 MADEP-EPH L The`batch LCS Arid MS had some high recoveries due to suspected evaporation of the spike mix. � " 3 AMRO Environmental Laboratories Corp. Date: 29-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: J1,K1,Ml,(0-5') Lab Order: 0110214 Project: TRASK-N.ANDOVER Collection Date: 10/22/01 Lab ID: 0110214-01A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE.t, - D2216 , Analyst: JC Percent Moisture t 5.6 0 wt% 1 10/23/01 Al. Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded q -See Case Narrative RL- Limit;defined as the lo)vcst concentration the laboratory can accurately quantitate. 4 AMRO Environmental Laboratories Corp. Date: 29-Oct-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: JI,KI,M1,(0-5') Lab Order: 0110214 Tag Number: Project: TRASK-N.ANDOVER Collection Date: 10/22/01 Lab ID: 0110214-01A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETRdLEUM HYDROCARBONS. MAEPH, Analyst: RKK C9-C18 Aliphatic Hydrocarbons 180 52 mg/Kg-dry 1 10/23/01 7:42:00 PM C19-C36 Aliphatic Hydrocarbons 70 52 mg/Kg-dry 1 10/23/01 7:42:00 PM C11-C22 Aromatic Hydrocarbons 64 52 mg/Kg-dry 1 10/23/01 7:42:00 PM Naphthalene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM 2-Methylnaphthalene 1.1 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Acenaphthylene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Acenaphthene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Fluorene _ 0.27 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Phenanthrene 0.28 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Anthracene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Fluoranthene NO 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Pyrene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Chrysene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Senzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Dibenz(a,h)anthracene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry 1 10/23/01 7:42:00 PM Surr: 1-Chlorooctadecane 88.6 40-140 %REC 1 10/23/01 7:42:00 PM Surr:2-Bromonaphthalene 109 40-140 %REC 1 10/23/01 7:42:00 PM Surr.2-Fluorobiphenyl 112 40-140 %REC 1 10/23/01 7:42:00 PM Surr:o-Terphenyl 78.0 40-140 %REC 1 10/23/01 7:42:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the.concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and-concentration of C9-C10 Aromatic Hydrocarbons. – c CERTIFICATION / Were all QA/QC procedures required by the VPH or EPH method followed: ✓ Yes _/NN:-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes _✓No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No :LxYes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief, accurate and complete. SIGNATURE: ��' l�� DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range i J-Analj e'detected below quantitation limits R-RPD outside accepted recovery limits #1•See Case Narrative B-Anaicte detected in the associated Method Blank lj-Method prescribed holding time exceeded AMRO Environmental Laboratories Corporation 111 Herrick Street Merrimack,NH 03054 Volatile Petroleum Hydrocarbons (VPH) Massachusetts Department of Environmental Protection (MADEP) Method 1.0 -January 1998 AMRO Modifications This modification is based on the use of a purge and trap gas chromatography mass spectrometer(GC/MS)system to analyze samples for VPH. The hydrocarbon ranges are quantified using predominant mass fragmentation ions which are characteristic for the range•.beipg measured. This approach eliminates potential false positives for the target analytes while providing accurate hydrocarbon.range data. The chromatographic column is an HP-624 capillary column which has been validated by GUMS analysis of a gasoline standard to correctly identify the marker compounds and elution order of specific gasoline components. Batch quality control includes, at a minimum, method blank, laboratory control sample, and duplicate analysis. A matrix spike and/or matrix spike duplicate is analyzed if sufficient sample is submitted to the laboratory. The Reporting Limit(RL)of this method for each of the collective aliphatic and aromatic ranges is approximately 0.6-2.8 mg/kg in soil and 25-110 µg/L in water. The RL of this method for the target analytes ranges from approximately 0.05-0.13 mg/kg in soil and 2.0- 5.0µg/L for water samples. Extractable Petroleum Hydrocarbons (EPH) Massachusetts Department of Environmental Protection (MADEP) Method 1.0 -January 1998 AMRO Modifications This modification is based on a solvent extraction and gas chromatography mass spectrometer (GC/MS) analysis. The hydrocarbon ranges are quantified using predominant mass fragmentation ions which are characteristic for the range being measured. This approach eliminates the silica gel solid-phase fractionation step. False positives for targeted PAH analytes are eliminated by using GC/MS as the primary analysis technique. The chromatographic column is a AW Scientific DB-5ms capillary column. Internal standard calibration is performed using 5a-Androstane at a concentration of 40 ng/µL. o-Terphenyl and 1-Chlorooctadecane are added as surrogate compounds at 20 ng/µL in the sample extract. These two surrogates monitor the effects of the sample matrix and extraction efficiency. Two additional surrogates, 2-Fluorobiphenyl and 2- Bromonaphthalene, are added to the finished extract prior to analysis to monitor instrument performance. Batch quality control includes, at a minimum, a procedure blank, laboratory control sample and duplicate sample analysis. A matrix spike is analyzed if sufficient sample is submitted to the laboratory. The Reporting Limit (RL) of this method for each of the collective aliphatic and aromatic ranges is approximately 2-15 mg/kg in soil and 10-50 µg/L in water. The RL of this method for the Target PAH analytes ranges from approximately 0.25 to 0.5mg/kg in soil; 1.0µg/L for water when operating the GUMS in full scan mode, and 0.1 to 1.0µg/L when operating the GUMS in SIM mode. For sites requiring the lowest levels cited in the Massachusetts Contingency Plan for water, GUMS in the Selected Ion Monitoring (SIM) mode is used. qc/gcmemos/forms/ephvph Rev. 1 11/00 AMRO Environmental Laboratories Corp. 29-0a-01 Lab Order: 0110214 Client: Subsurface Remediation Technologies DATES REPORT Project: TRASK-N. ANDOVER :Y ` Sample ID Client Sample ID Collection Date Matrix Tcst Name TCLP Date Prep Date Analysis Date 0110214-01A 11,KI,M1,(0-5') 10/22/01 Soil EPI I,Soil,Pull List h10/23/01 10/23/01 10/23/01 Percent Moisture �" t _ AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 Client: / T AMRO ID: Q / Project Name: —r �i _ f n(oO A Date Rec.: . Shi via: (circle on Fed Ex., UPS ,AMRO Courier, Date Due: _ _d and D ., Other Courier, Other: Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? 3. Custody Seals Intact? 4. Air Bill included in folder if received? 5. Is COC included with samples? V 6. Is COC signed and d2ted by client? 7. Laboratory.receipt ten*rature. _. ,TEMP= obi�.►lk Samples rec.with ice "ice pack s_neither—i -Ain 8. Were samples received the same day they were sampled? Is client temperature 4°C±2°C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? t/ ;/ 6 10. Does the info on the COC match the samples? 11.Were samples rec.within holding time? 12.Were all samples properly labeled? 1/ 13.Were al(samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact? (none broken or leaking) l/ 16.Were VOA vials rec.with no air bubbles? 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH (circle one): M=Methanol, E=EnCore(air-tight container) Sampling Method VOA(circle one): M=Methanol, SB=Sodium Bisulfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? - If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into: Internal Tracking ck g Log. C/ Dry Weight Log? t/ Client Log? l/ Composite Log? l/ Filtration Log? Received By:. Date: ;p •a1_v Logged in By: cc_ Date: 3—O� Labeled By: Date: Checked By: Date: — --p 1 NA= Not Applicable gc/gcmemos/forms/samplerec Rev.18.06100 AMRO Environmental Laboratories Corp. 24-0ci-01 Lab Order: 0110213 Client: Subsurface Remediation Technologies DATES REPORT V. Project: TRASK-N. ANDOVER ' Sample IU Client Sample ID Collection Date Matrix Test Name TCLP Da1te Prep Date Analysis Dale 0110213-0 1A JI,KI,MI,(5'-10') 10/22/01 Soil 131111,Soil,Pull List 10/23/01 10/23/01 10/23/01 Percent Moisture �.r f i AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 Client: SE-7- AMRO ID: 0 ` Project Name: TySk-/VDate Rec.: 10— Shi .(circle one) Fed Ex., UPS ,AMRO Courier, Date Due: /0--'�c —U 1 Hand Del. Other Courier, Other: Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? 3. Custody Seals Intact? 4. Air Bill included in folder if received? 5. Is COC included with.samples? 6.,Is C_OC,.sigaed.and dafd by,client?. 7. LaboratoryPeceipt temperature. TEMP =. yJ� Samples rec.with ice_ice packs_neither �/ L 8. Were samples received the same day they were sampled? Is client temperature 4°C±2°C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? 10. Does the info on the COC match the samples? 11.Were samples rec.within holding time? V 12.Were all samples properly labeled? 13.Were all samples properly preserved? 1/ 14.Were proper sample containers used? 15.Were all samples received intact?(none broken or leaking) 16.Were VOA vials rec.with no air bubbles? l/ 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH (circle one): M=Methanol, E=EnCore(air-tight container) _ Sampling Method VOA(circle one): M=Methanol, SB=Sodium Bisulfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into: Internal Tracking Log? ✓ Dry Weight Log? L/ Client Log? t/ Composite Log? Filtration Log? �✓ Received B�_.C Date: )p_ a a-O/ Logged in By:_ Date: /D `Za-'O/ Labeled By: Date: p—a Checked By: Date: NA= Not Applicable gc/gcmemos/forms/samplerec Rev.18 06/00 AMRO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORD Office: (603)424-2022 1111 Herrick Street r5 4039Rax: (60 429-8496 Merrimack,NH 03054 r. Projcct,No,: Project Name: — Al. Am b ✓E;Q Project Manager: ,e./!` r 53 plers(Sj na r� AM o i%va%3 Project Sample ID Date/Time Matrix Total# Analysis Required Remarks Sampled A=Air of Cont. S=Soil &Size �US t t GW=Ground W. t /Q .+ ' WW=Waste W. / r,.., DW=Drinking W. O=Oil �()-227-,0 Other- j Specify " 6 / / S - 1- ' o;Z t 'reservative:Cl-HCl,McOH,N-HNO3,S-1-12SO4,Na-Na011,O-Other ontamer Type: -Plastic,6-61ass, -Via,T-Te on,O-Other er 'lease print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; )gged in and the turnaround time clock will not start until any FAX No.: (?79) �4 - 38 mbiguities are resolved. CC end Results To: �r Seal Intact? GW-I GW-2 GW-3 s' C7 �t/T�P11 E Yes No N/A MCP Level Needed: Relinquished By Date/Time Received By Date/Time P.O.No: ` PRIORITY TURNAROUND TIME AUTHORIZATION 0s,�,�J ` " + ` Before submitting samples for expedited TAT,you must have requested J ' " Rsuits Needed in advance and received a coded TAT AUTHORIZATION NUMBER " By: AUTHORIZATION No. BY: r�<•.. C, / ? l %) )/ C�'(Jri SHEET OF ite:Lab Copy Yellow:Accompanies Report Pink:Client Copy .��,•;� � N� . �I�� / / '� \ iii rI�� /il i. \ •1\\i..riii i� I I • \ \viii}• •r�//i� /rr• ,,,1\\ •�\••.i /,.II r \11\\••� ��II•I \•\,1� i�./I•r i 11\\ i�• i:: III ,'\i•• i�I1• •\•.�• i/ \;\�••,,,.'....i•..••I.I•r'. �\i••.7.•',• /•,I I,/ \\ • ' I I \1•• .. • I `,`,, • • III ,`,• Ire.• \\ii..i�1/• '`�• ♦ \ , • % ,\:•..ir 11 � •,\\\�\��.i'II11 / i\•\1\.. I•• .,\\�•\\\•r r;i�I�• •\ -,'• The Commonwealth of Massachusetts Department of Environmental Pi,otection Division of Environmental Analysis Senator William X. Wall Experiment Station - .r certifies M-NHOI2 AMRO ENVIRONMENTAL LAB I I1 HERRICK ST MERRIMACK, NH 03054-0000 Laboratory Director: Nancy Stewart for the analysis of NON POTABLE WATER(CHEMISTRY) POTABLE WATER(CHEMISTRY) pursuant to 310 CMR 42.00 This certificate supersedes all previous Massachusetts certificates issued to this laboratoy. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CMR 42.00. This certificate is valid only when accompanied by the latest dated Certified Parameter List as issued by the Massachusetts D.E.P. Contact the Division of Environmental Analysis to c verify the current certification status of the laboratory. Certification is no guarantee of the validity of the data. This certification is subject to unannounced laboratory inspections. r' Issued: 01 JUL 2001 Expires: 30 JUN 2002 Director, Division of Environmental Analysis ���::\..�\ 1 ,r�,�...�r�',::•••:\i`• ,!l:Il�iiil;'•.:"�:i\�li!�• •':Ii/:�ir•• ';�i::\�i�i`• rr�i�iii i•.:.:`��:i��i�!�• �•il i�iS�/���;:�:i\\11.' !•./,/,/..'. ��,.\\:11!� .rl;iii;%•�n��li�\,•,•, I;,,//�. .::�1• .. '.�,,//r;C •.�:����. '.r,i;;!.,. .,��♦ \n '.�,iii�i%! '��iQi��. '.i�i��/,i.. CON IONNVEALTH OF MASSACHUSETTS DEPARDM1 T OF ENVMONMEF TAL PROTE)MON Certified Parameter List as of: 01 JUL 2001 Al-NH012 A lR0 ENVIRONMENTAL LAB MFRRINIACK NH NON POTABLEWATER(CMUSTR1) Effective 01 JUL 2001 EiTiration 30 JUN 2002 Date Date Analvtes andNlet6ds ALUMINUM EPA 200.7 NITRATE-N EPA 353.2 ANTIMONY EPA 200.7 KJELDAHL-N EPA 351.1 �•,. ANTIMONY . „ EPA 204.2 KJELDAHL-N EPA 351.2 ARSENIC `EPA 200.7 ORTHOPHOSPHATE EPA 365.2 ARSENIC EPA 206.2 ORTHOPHOSPHATE EPA 300.0 ARSENIC ASTM D2972-93(C) TOTAL PHOSPHORUS EPA 365.2 BERYLLIUM EPA 200.7 CHEMICAL OXYGEN DEMAND EPA 410.4 CADMIUM EPA 200.7 CHEMICAL OXYGEN DEMAND HACH METHOD 8000 CHROMIUM EPA 200.7 BIOCHEMICAL OXYGEN DEMAND EPA 405.1 COBALT EPA 200.7 TOTAL CYANIDE EPA 335.2 COPPER EPA 200.7 NON-FILTERABLE RESIDUE EPA 160.2 IRON j EPA 200.7 TOTAL RESIDUAL CHLORINE SM 4500-CL-G LEAD FPA 200.7 OIL AND GREASE EPA 413.1 LEAD EPA 239.2 TOTAL PHENOLICS EPA 420.1 MANGANESE EPA 200.7 VOLATILE HALOCARBONS EPA 624 MERCURY EPA 245.1 VOLATILE AROMATICS EPA 624 MOLYBDENUM EPA 200.7 CHLORDANE EPA 608 NICKEL EPA 200.7 ALDRIN EPA 608 SELENIUM EPA 200.7 DIELDRIN EPA 608 SELENIUM EPA 270.2 DDD EPA 608 SILVER EPA 200.7 DDT EPA 608 STRONTIUM EPA 200.7 HEPTACHLOR EPA 608 THALLIUM EPA 200.7 HEPTACHLOR EPDXIDE EPA 608 THALLIUM EPA 279.2 POLYCHLORINATED BIPHENYLS(WATER) EPA 608 ZINC EPA 200.7 POLYCHLORINATED BIPHENYLS(OIL) EPA 600/4-81-045 PH EPA 150.1 SPECIFIC CONDUCTN MY EPA 120.1 TOTAL DISSOLVED SOLIDS EPA 160.1 TOTAL HARDNESS(CAC03) EPA 200.7 CALCIUM EPA 200.7 MAGNESIUM EPA 200.7 SODIUM EPA 200.7 POTASSIUM EPA 200.7 TOTAL ALKALINITY EPA 310.1 CHLORIDE EPA 325.3 CHLORIDE EPA 300.0 FLUORIDE EPA 340.2 FLUORIDE EPA 300.0 SULFATE EPA 375.4 SULFATE EPA 300.0 AMMONIA-N EPA 350.2 NITRATE-N EPA 300.0 June 27;-2001 * Pro\isional Certification Page 1 of 2 CONDIONANIFALTH OF ALAS SACHUS ETTS DFPARDIENT OF E NVIRONNIE\`TAL PROTECTION Certified Parameter List as of- 01 JUL 2001 A1-NH012 AMRO ENVIRONMENTAL LAB NIQ2 MIACK NH POTABLE WATER(CHEVIISTRY) EffectiNe 01 JUL 2001 Expiration 30 JUN 2002 Date Date Anahles and Methods ANTIMONY EPA 200.9 ARSENIC r EPA 200.7 ARSENIC .a " EPA 200.9 BARIUM ... FPA 200.7 BERYLLIUM EPA 200.7 CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COPPER EPA 200.7 LEAD EPA 200.9 MERCURY EPA 245.1 NICKEL EPA 200.7 SELENIUM ' EPA 200.9 THALLIUM EPA 200.9 MTRATE-N EPA 353.2 NITRITE N EPA 353.2 FLUORIDE EPA 300.0 FLUORIDE SM 4500-F-E SULFATE EPA 300.0 CYANIDE SM4500-CN C,E TURBIDITY EPA 180.1 RESIDUAL FREE CHLORINE SM 4500-CL-G CALCIUM EPA 200.7 TOTAL DISSOLVED SOLIDS SM 2540C PH EPA 150.1 1,2-DIBROMOETHANE EPA 504.1 1,2-DIBROMO-3-CHLOROPROPANE EPA 504.1 June 27;2001 * ProNisional Certification Page 2 of 2 t Environmental Laboratories Corporation 111 Herrick Street,Merrimack, NH 03054 TEL:(603)424-2022 FAX: (603)429-8496 November 06,2001 Tim Toomey Subsurface Remediation Technologies 355 Central St Rowley,MA 01969,' TEL: (978)948-3861 FAX: (978)948-3861 RE: TRASK IRA,BOXFORD ST,N ANDOVER Order No.: 0110305 Dear Tim Toomey: AMBO Environmental Laboratories Corp. received 2 samples on 10/31/01 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference (NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s) upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time,A.MRO will properly dispose of the remaining sample(s). If you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of Vo pages. This letter is an integral part of your data report. If you have any questions regarding this project in the future, please refer to the Order Number above. Sincerely, Nancy Stewart Vice President/Lab Director AMRO Environmental Laboratories Corp. Date: 06-Nov-01 CLIENT: Subsurface Remediation Technologies Project: TRASK IRA,BOXFORD ST,N ANDOVER Work Order Sample Summary Lab Order: 0110305 Date Received: 10/31/01 Lab Sample ID 14,..Client Sample ID Collection Date 01103610IA ------ j' (LAI)(1�k�(A) I;INS, ` 10/30/01 r: OI 10305-OIB (LAI)(IAAA) F IN'—'1` 10/30/01 0110305-02A FGH(LFftALF)(A) I'IN" 10/30/01 0110305-02B FGH(LFf(ALF)(A) F IN" 10/30/01 .r AMRO Environmental Laboratories Corp. Date: 06-Nov-01 CLIENT: Subsurface Remediation Technologies Project: TRASK IRA,BOXFORD ST,N ANDOVER CASE NARRATIVE Lab Order: 0110-05 MADEP-VPH 1: Sample.01.10305 b2A'hadFhigl'r&overy of the 2,5.Dibromotoluene surrogate spike due to matrix interference. AMRO Environmental Laboratories Corp. Date: 06-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: (LAI)(IA)(A) PIN Lab Order: 0110305 Tag Number: Project: TRASK IRA,BOXFORD ST,N ANDOVER Collection Date: 10/30/01 Lab ID: 0110305-01A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS._ MAVPH Analyst: SK C5-C8 Aliphatic Hydrocarbons ND 18 mg/Kg-dry 10 11/3/01 1:52:00 AM C9-C12 Aliphatic Hydrocarbons 43 4.6 mg/Kg-dry 10 11/3/01 1:52:00 AM C9-C10 Aromatic Hydrocarbons 240 4.6 mg/Kg-dry 10 11/3/01 1:52:00 AM Methyl tert-butyl ether ND 0.37 mg/Kg-dry 10 11/3/01 1:52:00 AM Benzene ND 0.37 mg/Kg-dry 10 11/3/01 1:52:00 AM Toluene ND 0.37 mg/Kg-dry 10 11/3/01 1:52:00 AM Ethylbenzene 0.38 0.37 mg/Kg-dry 10 11/3/01 1:52:00 AM m,p-Xylene 1.4 0.37 mg/Kg-dry 10 11/3/011:52:00 AM o-Xylene,; 0.72 0.37 mg/Kg-dry 10 11/3/01 1:52:00 AM Naphthalene 5.7 0.92 mg/Kg-dry 10 11/3/01 1:52:00 AM Surr: Dibromofluoromethane 86.9 70-130 %REC 10 11/3/01 1:52:00 AM Surr: 1,2-Dichloroethane-d4 82.5 70-130 %REC 10 11/3/01 1:52:00 AM Surr:Toluene-d8 90.3 70-130 %REC 10 11/3/01 1:52:00 AM Surr:4-Bromofluorobenzene 89.2 70-130 %REC 10 11/3/01 1:52:00 AM Surr:2,5-Dibromotoluene 102 70-130 %REC 10 11/3/01 1:52:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: _XYes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Yes _ No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No -,.,—,/Yes-Details enclosed 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief, accurate and complete. SIGNATURE: SIGNATURE: DATE: // — D -0' PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range ]-Analytc'dctected below quantitation limits R-RPD outside accepted recovery limits /t-See Case Narrative B-AnaLy*detected'in the associated Method Blank H-Method prescribed holding time exceeded AMRO Environmental Laboratories Corp. Date: 06-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FGH(LF)(ALF)(A) 1'IN Lab Order: 0110305 Tag Number: Project: TRASK IRA,BOXFORD ST,N ANDOVER Collection Date: 10/30/01 Lab ID: 0110305-02A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK C5-C8 Aliphatic Hydrocarbons t ND 19 mg/Kg-dry 10 11/3/01 2:27:00 AM C9-C12 Aliphatic Hydrocarbons 62 4.7 mg/Kg-dry 10 11/3/01 2:27:00 AM C9-C10 Aromatic Hydrocarbons 330 4.7 mg/Kg-dry 10 11/3/01 2:27:00 AM Methyl tert-butyl ether ND 0.38 mg/Kg-dry 10 11/3/01 2:27:00 AM Benzene ND 0.38 mg/Kg-dry 10 11/3/01 2:27:00 AM Toluene ND 0.38 mg/Kg-dry 10 11/3/01 2:27:00 AM Ethylbenzene 0.87 0.38 mg/Kg-dry 10 11/3/01 2:27:00 AM m,p-Xylene 2.7 0.38 mg/Kg-dry 10 11/3/01 2:27:00 AM o-Xylene,, 1.7 0.38 mg/Kg-dry 10 11/3/01 2:27:00 AM Naphthalene 7.5 0.95 mg/Kg-dry 10 11/3/01 2:27:00 AM Surr:Dibromofluoromethane 80.6 70-130 %REC 10 11/3/01 2:27:00 AM Surr: 1,2-Dichloroethane-d4 80.9 70-130 %REC 10 11/3/012:27:00 AM Surr:Toluene-d8 81.2 70-130 %REC 10 11/3/01 2:27:00 AM Surr:4-Bromofluorobenzene 82.7 70-130 %REC 10 11/3/01 2:27:00 AM Surr:2,5-Dibromotoluene 141 70-130 S %REC 10 11/3/012:27:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION / Were all QA/QC procedures required by the VPH or EPH method followed: ✓ Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is,to the best of my knowledge and belief,accurate andel complete. SIGNATURE: DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyledetected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Anala'te detected in the associated Method Blank H-Method prescribed holding time exceeded v 5 AMRO Environmental Laboratories Corp. Date: 06-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: (LAI)(IA)(A) F IN Lab Order: 0110305 Tag Number: Project: TRASK IRA,BOXFORD ST,N ANDOVER Collection Date: 10/30/01 Lab ID: 0110305-01B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRAC.TAOLE..PETROLEUM HYDROCARBONS MAEPH Analyst: RKK C9-C18 Aliphatic Hydrocarbons 3,800 500 mg/Kg-dry 10 11/2/01 1:26:00 PM C19-C36 Aliphatic Hydrocarbons 1,600 500 mg/Kg-dry 10 11/2/01 1:26:00 PM C1 1-C22 Aromatic Hydrocarbons 1,800 500 mg/Kg-dry 10 11/2/01 1:26:00 PM Naphthalene 4.4 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM 2-Methylnaphthalene 15 2.5 mg/Kg-dry 10 11/2/01 1:26:00 PM Acenaphthylene 0.54 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Acenaphthene 2.1 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Fluorene 1.7 0.25 mg/Kg-dry 1 11/2/013:36:00 AM Phenanttlrene 4.0 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Anthracene 0.44 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Fluoranthene 0.39 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Pyrene 1.9 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Benz(a)anthracene ND 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Chrysene ND 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Benzo(b)fluoranthene NO 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Benzo(k)fluoranthene ND 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Benzo(a)pyrene ND 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Dibenz(a,h)anthracene ND 0.25 mg/Kg-dry 1 11/2/01 3:36:00 AM Indeno(1,2,3-cd)pyrene ND 0.25 mg/Kg-dry- 1 11/2/01 3:36:00 AM Benzo(g,h,i)perylene NO 0.25 mg/Kg-dry- 1 11/2/01 3:36:00 AM Surr: 1-Chlorooctadecane 96.0 40-140 %REC 1 11/2/01 3:36:00 AM Surr:2-Bromonaphthalene 113 40-140 %REC 1 11/2/01 3:36:00 AM Surr:2-Fluorobiphenyl 117 40-140 %REC 1 11/2/01 3:36:00 AM Surr.o-Terphenyl 71.0 40-140 %REC 1 11/2/01 3:36:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: L/Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _✓Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No ✓ Yes-Details enclosed 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief, accurate and complete. SIGNATURE: DATE: Z/—T-0) PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Anal Codetected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyfc detected in the associated Method Blank ti-Method prescribed holding time exceeded AMRO Environmental Laboratories Corp. Date: 06-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FGH(LF)(ALF)(A) FIN Lab Order: 0110305 Tag Number: Project: TRASK IRA,BOXFORD ST,N ANDOVER Collection Date: 10/30/01 Lab ID: 01 10305-02B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTAI.LE.PETR&EUM HYDROCARBONS MAEPH Analyst: RKK C9-C18 Aliphatic Hydrocarbons Y. 2,400 520 mg/Kg-dry 10 11/2/01 2:01:00 PM C19-C36 Aliphatic Hydrocarbons 880 520 mg/Kg-dry 10 11/2/01 2:01:00 PM C11-C22 Aromatic Hydrocarbons 1,200 520 mg/Kg-dry 10 11/2/01 2:01:00 PM Naphthalene 5.5 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM 2-Methylnaphthalene 21 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Acenaphthylene 0.35 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Acenaphthene 2.0 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Fluorene ' 0.99 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Phenanthrene 3.5 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Anthracene 0.51 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Pyrene 1.0 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Benz(a)anthracene NO 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Chrysene ND 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Benz o(b)fluoranthene ND 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Benzo(k)fluoranthene NO 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 11/2/014:11:00 AM Dibenz(a,h)anthracene NO 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 11/2/01 4:11:00 AM Benzo(g,h,i)perylene NO 0.26 .mg/Kg-dry 1 11/2/01 4:11:00 AM Surr: 1-Chlorooctadecane 73.9 40-140 %REC 1 11/2/01 4:11:00 AM Surr:2-Bromonaphthalene 116 40-140 %REC 1 11/2/01 4:11:00 AM Surr:2-Fluorobiphenyl 113 40-140 %REC 1 11/2/01 4:11:00 AM Surr:o-Terphenyl 80.2 40-140 %REC 1 11/2/01 4:11:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes — No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ZYes _ No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Z Yes-Details enclosed 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: I L__ PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Ana 1xicAetected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analytt detected in the associated Method Blank H-Method prescribed holding time exceeded 7 AMRO Environmental Laboratories Corp. Date: 08-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: (LAI)(IA)(A) FIN Lab Order: 01 10305 Project: TRASK IRA,BOXFORD ST,N ANDOVER Collection Date: 10/30/01 Lab ID: 0110305-OIB Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE r.. D2216 Analyst: JC Percent Moisture 2.4 0 wt%, 1 11/1/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limit B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. i AMRO Environmental Laboratories Corp. Date: 08-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FGH(LF)(ALF)(A) FIN Lab Order: 0110305 Project: TRASK IRA,BOXFORD ST,N ANDOVER Collection Date: 10/30/01 Lab ID: 0110305-02B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE-jt."; D2216 Analyst: JC Percent Moisture 4.7 0 wt% 1 11/1/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recoveryoutside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative P -Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. AMRO Environmental Laboratories Corporation 111 Herrick Street Merrimack,NH 03054 Volatile Petroleum Hydrocarbons (VPH) Massachusetts Department of Environmental Protection (MADEP) Method 1.0 -January 1998 AMRO Modifications This modification is based on the use of a purge and trap gas chromatography mass spectrometer(GC/MS) system to analyze samples for VPH. The hydrocarbon ranges are quantified using predominant mass fragmentation ions which are characteristic for the ;'range being measured. This approach eliminates potential:false positives for the target ahalytes.while providing accurate hydrocarbon range data. The chromatographic column is an HP-624 capillary column which has been validated by GC/MS analysis of a gasoline standard to correctly identify the marker compounds and elution order of specific gasoline components. Batch quality control includes, at a minimum, method blank, laboratory control sample, and duplicate analysis. A matrix spike and/or matrix spike duplicate is analyzed if sufficient sample is submitted to the laboratory. The Reporting Limit(RL) of this method for each of the collective aliphatic and aromatic ranges is approximately 0.6-2.8 mg/kg in soil and 25-110 µg/L in water. The RL of this method for the target analytes ranges from approximately 0.05-0.13 mg/kg in soil and 2.0- 5.0 pg/L for water samples. Extractable Petroleum Hydrocarbons (EPH) Massachusetts Department of Environmental Protection (MADEP) Method 1.0 -January 1998 AMRO Modifications li This modification is based on a solvent extraction and gas chromatography mass spectrometer (GC/MS) analysis. The hydrocarbon. ranges are quantified using predominant mass fragmentation ions which are characteristic for the range being measured. This approach eliminates the silica gel solid-phase fractionation step. False positives for targeted PAH analytes are eliminated by using GC/MS as the primary analysis technique. The chromatographic column is a AW Scientific DB-5ms capillary column. Internal standard calibration is performed using 5a-Androstane at a concentration of 40 ng/µL. o-Terphenyl and 1-Chlorooctadecane are added as surrogate compounds at 20 ng/µL in the sample extract. These two surrogates monitor the effects of the sample matrix and extraction efficiency. Two additional surrogates, 2-Fluorobiphenyl and 2- Bromonaphthalene, are added to the finished extract prior to analysis to monitor instrument performance. Batch quality control includes at a minimum a procedure P q ty � blank, laboratory control sample and duplicate sample analysis. A matrix spike is analyzed if sufficient sample is submitted to the laboratory. The Reporting Limit (RL) of this method for each of the collective aliphatic and aromatic ranges is approximately 2-15 mg/kg in soil and 10-50 µg/L in water. The RL of this method for the Target PAH analytes ranges from approximately 0.25 to 0.5mg/kg in soil; 1.0µg/L for water when operating the GUMS in full scan mode, and 0.1 to 1.0µg/L when operating the GC/MS in SIM mode. For sites requiring the lowest levels cited in the Massachusetts Contingency Plan for water, GC/MS in the Selected Ion Monitoring (SIM) mode is used. qc/qcmemos/forms/ephvph Rev. 1 11/00 ^ � 10 AMRO Environmental Laboratories Corp. 06-Nov-0/ Lab Order: 0110305 Client: Subsurface Remediation Technologies DATES REPORT Project: TRASK IRA, BOXFORD ST,N A Sample ID Client Sample ID Collection Date Matrix Test Name TCLP Datc Prep Date Analysis Date 0110305-01A (LAI)(IA)(A) P IN 10/30/01 Soil Volatile Petroleum I lydrocarbons 10/30/01 11/3/01 0110305-01 d 13I111,Soil,Full List t I I/l/01 11/2/01 GPI I,Soil,Pull List 11/1/01 11/2/01 Percent Moisture II/1/01 0110305-02A FGH(LF)(ALP)(A)P IN Volatile Petroleum I lydrocarbons 10/30/01 11/3/01 0110305-0213 1:1111,Soil,Dull List I I/l/01 11/2/01 61111,Soil,Full List 11/1/01 11/2/01 11/I/01 Percent Moisture ,t AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 Client: ARO ID: - ( Project Name: T,,,&5 k -Tr F}ncf,u 11Y1y M n Date Rec.: 10/31101 Ship via: (circle one) Fed Ex., UPS RO Coun Date Due: /1 Hand Del., Other Courier, Other: Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? c/ 3. Custody Seals Intact? 4. Air Bill included in folder if received? 5. Is COC included with 5eLMplep2 v 6...Is COC-signed-and dated by•client? 7. Laboratory receipt temperature. , z TEMP =3 � Samples rec.with ice V ice packs_neither 8. Were samples received the same day they were sampled? v Is client temperature 4°C±2°C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? 10. Does the info on the COC match the samples? 11.Were samples rec.within holding time? l/ 12.Were all "samples properly labeled? 13.Were all samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact? (none broken or leaking) 16.Were VOA vials rec.with no air bubbles? t/ 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA S I Sampling Meth d VP ircle one . M= ethanol, E=EnCore (air-tight container) Sampling Metho A(circle one): =Methanol, SB=Sodium Bisulfate,'E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? • If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into: Internal Tracking Log? Dry Weight Log? Client Log? Composite Log? (/ •Filtration Log? Received t3y;. Date:JO 31 Logged in By: Date: Labeled 9j.- C� Date: — Checked By: ft lj Date: NA= Not Applicable gc1gcmemos/forms/samplerec Rev.,18 06/0 r� �, 1 G AMRO Environmental Laboratories Corporation ChIAIN-OF-CUSTODY RECORD 38451 Office:(603)424-2022 111 Herrick Street Fax:(603)429-8496 Merrimack,NH 03054 Project No.: Project Name: n C(e< ��2{�A J�U�t t�z�/ ,S Projcct Managcr: f am lcrs iLnatttc).N AMBO Project No.: Project State: Sample ID Date/Time Matrix Total# Analysis Requil•ed Remarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. WW=Waste W. DW=Drinking W. 0=oil Other=Specify I ' / RV Ato Preservative:C-HC,McOH,N-HNO3,S-1-12SO4,Na-NaOH,O-Other [Container Type: P-Plastic,G-Glass, - to,T-Te on,O-Ot er Please print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will not start until any FAX No.: ambiguities are resolved. Send Results To: G Scallntact? GW-1 i GW-2 GW-3 Nth O1 (p' "y Yes No N/A MCP Level Needed: Relitt uished By Date/Time Received By Date/Time P.O.No: PRIORITY TURNAROUND TIME AUTHORIZATION 141 /1 Before submitting samples for expedited TAT,you must have requested „. Resylts Need in advance and received a coded TAT AUTHORIZATION NUMBER / By: AUTHORIZATION No. BY: SHEET OF • L o pr,"�VvlitoovMc=panies Report Pink: Client Copy .'%il,./III. .,.\\,\,1:.�'%I%;•�'. .•:\�\�\\i..' • I•j��' '•�'�:\•' II:' \\;\.. II�. •�;�\�. I�. ..�\�;\ ;% i;Il�i •.I\�i�i:� i�iii�//I• ','\\�iii:�•.iii�: •IIi �•i\ ���\ .ii•//I.; .�i;\\\\,..i'I11/,III ,;.'�\\\\•.i'IIi/,iii ,,•'\\.\\ �•. •iii; /I, \ \.\\\ i���: I . .\� III The Commonwealth of Massachusetts Department of Environmental Protection Division of Environmental Analysis Senator William X. Wall Experiment Station certifies J, M-NHO12 AMRO ENVIRONMENTAL LAB 111 HERRICK ST MERRIMACK, NH 03054-0000 Laboratory Director: Nancy Ste-wart for the analysis of NON POTABLE WATER(CHEMISTRY) POTABLE WATER(CHEMISTRY) pursuant to 310 CMR 42.00 C= This certificate supersedes all previous Massachusetts certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CAIR 42.00. This certificate is valid only when accompanied by the latest dated Certified Parameter List as issued by the Massachusetts D.E.P. Contact the Division of Environmental Analysis to verify the current certification status of the laboratory. Certification is no guarantee of the validity of the data. This certification is subject to . % unannounced laboratory inspections. Issued: 01 JUL 2001 }�- ���' a-► �t.•.� Expires: 30 JUN 2002 Director, Division of Environmental Analysis 14 COADIONINVEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRON'A�TTAL PROTECTION 1. Certified Parameter List as of- 01 JUL 2001 Al-NH012 AAIRO INVIROnUN TAL LAB AIERRIA'1ACK NH NON POTABLE WATER(CHEMISTRY Effective 01 JUL 2001 Expiration 30 JUN 2002 Date Date Anah4es and A3et6ds ALUMINUM EPA 200.7 NITRATE N EPA 353.2 ANTIMONY EPA 200.7 . KJELDAHL-N EPA 351.1 ANTIMONY € " EPA 204.2 KJELDAHL-N EPA 351.2 ARSENIC ` �+ EPA 200;7 ORTHOPHOSPHATE EPA 365.2 ARSENIC EPA 206.2 ORTHOPHOSPHATE EPA 300.0 ARSENIC ASTM D2972-93(C) TOTAL PHOSPHORUS EPA 365.2 BERYLLIUM EPA 200.7 CHEMICAL OXYGEN DEMAND EPA 410.4 CADMIUM EPA 200.7 CHEMICAL OXYGEN DEMAND HACH METHOD 8000 CHROMIUM EPA 200.7 BIOCHEMICAL OXYGEN DEMAND EPA 405.1 COBALT EPA 200.7 TOTAL CYANIDE EPA 335.2 COPPER EPA 200,7 NON-FILTERABLE RESIDUE EPA 160.2 IRON EPA 200.7 TOTAL RESIDUAL CHLORINE SM 4500-CL-G LEAD EPA 200.7 OIL AND GREASE EPA 413.1 LEAD EPA 239.2 TOTAL PHENOLICS EPA 420.1 MANGANESE EPA 200.7 VOLATILE HALOCARBONS EPA 624 MERCURY EPA 245.1 VOLATILEAROMATICS EPA 624 MOLYBDENUM EPA 200.7 CHLORDANE EPA 608 NICKEL EPA 200.7 ALDRIN EPA 608 SELENIUM EPA 200.7 DIELDRIN EPA 608 SELENIUM EPA 270.2 DDD EPA 608 SILVER EPA 200.7 DDT EPA 608 STRONTIUM EPA 200.7 HEPTACHLOR EPA 608 THALLIUM EPA 200.7 HEPTACHLOR EPDXIDE EPA 608 THALLIUM EPA 279.2 POLYCHLORINATED BIPHENYLS(WATER) EPA 608 ZINC EPA 200.7 POLYCHLORINATED BIPHENYLS(OIL) EPA 600/4-81-045 PH EPA 150.1 SPECIFIC CONDUCTIVITY EPA 120.1 TOTAL DISSOLVED SOLIDS EPA 160.1 TOTAL HARDNESS(CAC03) EPA 200.7 CALCIUM EPA 200.7 MAGNESIUM EPA 200.7 SODIUM EPA 200.7 POTASSIUM EPA 200.7 TOTAL ALKALINITY EPA 310.1 CHLORIDE EPA 325.3 CHLORIDE EPA 300.0 FLUORIDE EPA 340.2 FLUORIDE EPA 300.0 SULFATE EPA 375.4 SULFATE EPA 300.0 AMMONIA-N EPA 350.2 NITRATE-N EPA 300.0 Jiine 27;2001' * ProNisional Certification Page 1 of 2 15 MIDIONAN FALTH OF A'IAS SACHUSEITS DFPARTn�'T OF E WMONNIENTAL PROTECTION Certified Parameter List as of: 01 JUL 2001 Al-NH012 AMRO ENTMONNIWrAL LAB AIERRIMACK NH POTABLENVATER(CHE USTRY Effecthe 01 JUL2001 Expiration 30 JUN 2002 Date Date Anahles andA7ethods ANTIMONY EPA 200.9 ARSENIC EPA 200.7 ARSENIC '' _'- EPA 200.9 BARIUM ,� •- _. .. , ., FEPA 200,7 - BERYLLIUM EPA 200.Y CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COPPER EPA 200.7 LEAD EPA 200.9 MERCURY EPA 245.1 NICKEL EPA 200.7 SELENIUM EPA 200.9 THALLIUM '` EPA 200.9 NITRATE-N EPA 353.2 NITRITE-N EPA 353.2 FLUORIDE EPA 300.0 FLUORIDE SM 4500-F-E SULFATE EPA 300.0 CYANIDE SM 4500-CN-C,E TURBIDITY EPA 180.1 RESIDUAL FREE CHLORINE SM 4500-CL-G CALCIUM EPA 200.7 TOTAL DISSOLVED SOLIDS SM 2540C PH EPA 150.1 1,2-DIBROMOETHANE EPA 504.1 1,2-DIBROMO-3-CHLOROPROPANE EPA 504.1 June 27,2001~ * ProNisional Certification Page 2 of 2 16 Environmental Laboratories Corporation 111 Herrick Street, Merrimack, NH 03054 TEL: (603)424-2022•FAX: (603)429-8496 November 30,2001 Tim Toomey Subsurface Remediation Technologies 355 Central St:',- Rowley,MA 41969. ` TEL: (978)948-3861 FAX: (978)948-3861 RE: TRASK PROPERTY Order No.: 0111169 Dear Tim Toomey: ANTRO Environmental Laboratories Corp. received 2 samples on 11/16/01 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference (NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s) upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time, AMRO will properly dispose of the remaining sample(s). If , you require further analysis, or need the samples held for a longer period, please contact us immediately. an integral art of our data report. If you This report consists of a total of 1'J pages. This letter is g p y P Y have any questions regarding this project in the future,please refer to the Order Number above. Sincerely, Nancy Stewart Vice President/Lab Director 1 AMRO Environmental Laboratories Corp. Date: 30-Nov-01 CLIENT: Subsurface Remediation Technologies Project: TRASK PROPERTY Work Order Sample Summary Lab Order: 0111169 Date Received: 11/16/01 Lab Sample ID r.�r,Client Sample ID Collection Date 011-1169=01'A t' AFGH(0-5)- 11[15/01 0111169-01B AFGH(0-5) 11/15[01 0111169-02A IA(0-5) 11115[01 0111 169-02B IA(0-5) 11115101 ,r 7 AMRO Environmental Laboratories Corp. Date: 30-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: AFGH(0-5) Lab Order: 0111169 Tag Number: Project: TRASK PROPERTY Collection Date: 11/15/01 Lab ID: 0111169-OIA Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS- MAVPH Analyst: JC C5-C8 Aliphatic Hydrocarbons ND 2.2 mg/Kg-dry 1 11/19/01 10:57:00 PM C9-C12 Aliphatic Hydrocarbons 15 0.55 mg/Kg-dry 1 11/19/01 10:57:00 PM C9-C10 Aromatic Hydrocarbons 12 0.55 mg/Kg-dry 1 11/19/01 10:57:00 PM Methyl tert-butyl ether ND 0.044 mg/Kg-dry 1 11/19/01 10:57:00 PM Benzene ND 0.044 mg/Kg-dry 1 11/19/01 10:57:00 PM Toluene ND 0.044 mg/Kg-dry 1 11/19/01 10:57:00 PM Ethylbenzene ND 0.044 mg/Kg-dry 1 11/19/01 10:57:00 PM m,p-Xylene 0.046 0.044 mg/Kg-dry 1 11/19/01 10:57:00 PM o-Xylene ND 0.044 mg/Kg-dry 1 11/19/01 10:57:00 PM Naphthalene 0.23 0.11 mg/Kg-dry 1 11/19/01 10:57:00 PM Surr:Dibromofluoromethane 106 70-130 %REC 1 11/19/01 10:57:00 PM Surr:1,2-Dichloroethane-d4 103 70-130 %REC 1 11/19/01 10:57:00 PM Surr:Toluene-d8 106 70-130 %REC 1 11/19/01 10:57:00 PM Surr:4-Bromofluorobenzene 103 70-130 %REC 1 11/19/01 10:57:00 PM Surr:2,5-Dibromotoluene 106 70-130 %REC 1 11/19/01 10:57:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbonsexclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: }'es _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes —JJo-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No _✓Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: "7 DATE: //-30 —-6/ PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not.Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Anal)-le detected below quantitation limits R-RPD outside accepted recovery limits 4-See Case Narrative B-Analyfe detected in the associated Method Blank H-Method prescribed holding time exceeded 7 AMRO Environmental Laboratories Corp. Date: 30-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: IA(0-5) Lab Order: 0111169 Tag Number: Project: TRASK PROPERTY Collection Date: 11/15/01 Lab ID: 0111 169-02A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: JC C5-C8 Aliphatic Hydrocarbons t. ND 2.0 mg/Kg-dry 1 11/29/01 1:08:00 PM C9-C12 Aliphatic Hydrocarbons NO 0.50 mg/Kg-dry 1 11/29/01 1:08:00 PM C9-C10 Aromatic Hydrocarbons NO 0.50 mg/Kg-dry 1 11/29/01 1:08:00 PM Methyl tert-butyl ether ND 0.040 mg/Kg-dry 1 11/29/01 1:08:00 PM Benzene ND 0.040 mg/Kg-dry 1 11/29/01 1:08:00 PM Toluene ND 0.040 mg/Kg-dry 1 11/29/01 1:08:00 PM Ethylbenzene NO 0.040 mg/Kg-dry 1 11/29/01 1:08:00 PM m,p-Xylene ND 0.040 mg/Kg-dry 1 11/29/01 1:08:00 PM o-Xylene' ND 0.040 mg/Kg-dry 1 11/29/01 1:08:00 PM Naphthalene ND 0.10 mg/Kg-dry 1 11/29/01 1:08:00 PM Surr: Dibromofluoromethane 88.7 70-130 %REC 1 11/29/01 1:08:00 PM Surr: 1,2-Dichloroethane-d4 105 70-130 %REC 1 11/29/01 1:08:00 PM Surr:Toluene-d8 98.9 70-130 %REC 1 11/29/01 1:08:00 PM Surr:4-Bromofluorobenzene 102 70-130 %REC 1 11/29/01 1:08:00 PM Surr:2,5-Dibromotoluene 99.6 70-130 %REC 1 11/29/01 1:08:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all OA/QC procedures required by the VPH or EPH method followed: -<Yes _ No-If No,See Case Narrative Were all performance/acceptance tance standards for required QA/QC procedures achieved: —/Y _ P p q p _ es No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No JL Yes-Details enclosed 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief, accurate and complete. SIGNATURE: 6�7DATE: /I —3d—O PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery Iimits E-Value above quantitation range J-Analyte,detected below quantitation limits R-RPD outside accepted recovery limits it-See Case Narrative B-Analyfe detected.in the associated Mcthod Blank H-Method prescribed holding time exceeded AMRO Environmental Laboratories Corp. Date: 30-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: AFGH(0-5) Lab Order: 0111169 Tag Number: Project: TRASK PROPERTY Collection Date: 11/15/01 Lab ID: 0111169-OIB Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK f t- C9-C18 Aliphatic Hydrocarbons 140 51 mg/Kg-dry 1 11/27/01 4:32:00 AM C19-C36 Aliphatic Hydrocarbons ND 51 mg/Kg-dry 1 11/27/014:32:00 AM C11-C22 Aromatic Hydrocarbons 52 51 mg/Kg-dry 1 11/27/01 4:32:00 AM Naphthalene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM 2-Methylnaphthalene 0.72 0.25 mg/Kg-dry 1 11/27101 4:32:00 AM Acenaphthylene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Acenaphthene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Fluorene ' NO 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Phenantt rene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Anthracene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Fluorarithene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Pyrene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Benz(a)anthracene ND l 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Chrysene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Benzo(b)fluoranthene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Benzo(k)fluoranthene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Benzo(a)pyrene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Dibenz(a,h)anthracene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Indeno(1,2,3-cd)pyrene ND 0.25 mg/Kg-dry- 1 11/27/01 4:32:00 AM Benzo(g,h,i)perylene ND 0.25 mg/Kg-dry 1 11/27/01 4:32:00 AM Surr: 1-Chlorooctadecane 78.8 40-140 %REC 1 11/27/01 4:32:00 AM Surr:2-Bromonaphthalene 92.9 40-140 %REC 1 11/27/01 4:32:00 AM Surr:2-Fluorobiphenyl 91.2 40-140 %REC 1 11/27/01 4:32:00 AM Surr:o-Terphenyl 77.3 40-140 %REC 1 11/27/01 4:32:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: _Z Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: ZYes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No V Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. JSIGNATURE: 6Z DATE: /I—3 0 —0I/ PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte,detected below quantitation limits R-RPD outside accepted recovery limits N-See Case Narrative B-Analyfe detected in the associated Method Blank Ii-Method prescribed holding time exceeded r i AMRO Environmental Laboratories Corp. Date: 30-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: IA(0-5) Lab Order: 0111169 Tag Number: Project: TRASK PROPERTY Collection Date: 11/15/01 Lab ID: 0111169-02B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK V_.. .. C9-C18 Aliphatic Hydrocarbons ND 51 mg/Kg-dry 1 11/27/01 5:07:00 AM C19-C36 Aliphatic Hydrocarbons ND 51 mg/Kg-dry 1 11/27/01 5:07:00 AM C11-C22 Aromatic Hydrocarbons ND 51 mg/Kg-dry 1 11/27/01 5:07:00 AM Naphthalene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM 2-Methylnaphthalene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Acenaphthene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Fluorene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Phenanthrene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Anthracene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Pyrene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Chrysene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Dibenz(a,h)anthracene ND 0.26 mg/Kg-dry 1 11/27/01 5:07:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 ".mg/Kg-dry- 1 11/27/01 5:07:00 AM Benzo(g,h,i)perylene ND 0.26 'mg/Kg-dry: 1 11/27/01 5:07:00 AM Surr: 1-Chlorooctadecane 75.0 40-140 %REC 1 11/27/01 5:07:00 AM Surr:2-Bromonaphthalene 95.5 40-140 %REC 1 11/27/01 5:07:00 AM Surr:2-Fluorobiphenyl 94.1 40-140 %REC 1 11/27/01 5:07:00 AM Surr:o-Terphenyl 73.9 40-140 %REC 1 11/27/01 5:07:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ZYeso-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed /attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is,to the best of my knowledge and belief,accurate and complete. / SIGNATURE: DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analytwdetected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded AMRO Environmental Laboratories Corp. Date: 30-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: AFGH(0-5) Lab Order: 0111169 Project: TRASK PROPERTY Collection Date: 11/15/01 Lab ID: 0111169-OIB Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: SL Percent Moisture ` 2.6 0 wt% 1 11/16/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded tl -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. AMRO Environmental Laboratories Corp. Date: 30-Nov-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: IA(0-5) Lab Order: 0111169 Project: TRASK PROPERTY Collection Date: 11/15/01 Lab ID: 0 1 1 1 169-02B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE':'. D2216 Analyst: SL Percent Moisture 3.8 0 wt% 1 11/16/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. AMRO Environmental Laboratories Corp. 30-Nov-01 Lab Order: 0111169 Client: Subsurface Remediation Technologies DATES REPORT Project: TRASK PROPERTY Sample ID Client Sample ID Collection Date Matrix "fest Name TCLP Datc Prep Date Analysis Date 0111169-01A AFGH(0-5) 11/15/01 Soil Volatile Petroleum Hydrocarbons 11/19/01 11/19/01 0111169-01B EPI 1,Soil,Full List ``` 11/19/01 11/27/01 Percent Moisture 11/16/01 0111169-02A IA(0-5) Volatile Petroleum I lydrocarbons ' 11/27/01 11/29/01 0111169-02B E11I1,Soil,Full List 11/19/01 11/27/01 Percent Moisture 11/16/01 • r - AMRO EnvironmentalSAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 603) 424-2022 Client: 4 AMROID: Cr Project Name: R -x ' N. �dSsu� Date Rec.: , /P p Ship via:(circle one) Fed Ex., OPS,A Courie Date Due: Hand Del., Other Courier, Other. Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? L1-- 2. /2. Custody Seals present? 3. Custody Seals Intact? ✓ 4. Air Bill included in folde[if rpiceived? 5..Is.COC included with'gamples?_. 6. Is COC signed and dated by client? 7. Laboratory receipt temperature. TEMP - Samples rec,with ice_ice packs✓either 8. Were samples received the same day they were sampled? (/ Is client temperature 4°C±2°C? L/ If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? 10. Does tl+e info on the COC match the samples? ec, 11.Were_samples rec.within holding time? LZ I 12.Were all samples properly labeled? J 13.Were all samples properly preserved? 14.'VJere proper sample containers used? 15.Were all samples received intact?(none broken or leaking) 16.Were VOA vials rec.with no air bubbles? 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA i i)nISampling Meth d VPHircle one�vM-- (ethanol, E=EnCore (air-tight container) Sampling Method A(circle one): M=Methanol, SB=Sodium Bisulfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come dose to the fill line on the vial? If NO then client must be faxed. Were vials provided by AMBO? If NO then weights MUST be obtained frogi client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into. Internal Tracking Log? Dry Weight Log? Client Log? Composite Log? Filtration Log? Received 8y-. Date: Logged in By: GLS Date: 11 1&-o/ Labeled By: CL, Date: //—/(P—b/ Checked By: /1 6-1 Date: /1—/9-7 10 • COMN,lONWEA,LTH OF MAS S ACHUS ETTS DEPARTNIFVT OF ENVIR0N'i1ILNTAL PROTECTION Certified Parameter List as of- 01 JUL 2001 M-NH012 AMRO ENVIRON.MEVTAL LAB MERRIM ACK NH NON POTABLE WATER(CHEMISTRY) Effective 01 JUL 2001 Expiration 30 JUN 2002 Date Date Analvtes and Methods ALUMINUM EPA 200.7 NITRATE-N EPA 353.2 ANTIMONY EPA 200.7 KJELDAHL-N EPA 351.1 ANTIMONY EPA 204.2 KJELDAHL-N EPA 351.2 ARSENIC - EPA 200:7,': ORTHOPHOSPHATE EPA 365.2 ARSENIC EPA 206.2 ORTHOPHOSPHATE EPA 300.0 ARSENIC ASTM D2972-93(C) TOTAL PHOSPHORUS EPA 365.2 BERYLLIUM EPA 200.7 CHEMICAL OXYGEN DEMAND EPA 410.4 CADMIUM EPA 200.7 CHEMICAL OXYGEN DEMAND HACH METHOD 8000 CHROMIUM EPA 200.7 BIOCHEMICAL OXYGEN DEMAND EPA 405.1 COBALT EPA 200.7 TOTAL CYANIDE EPA 335.2 COPPER EPA 200.7 NON-FILTERABLE RESIDUE EPA 160.2 IRON EPA 200.7 TOTAL RESIDUAL CHLORINE SM4500-CL-G LEAD EPA 200.7 OIL AND GREASE EPA 413.1 LEAD EPA 239.2 TOTAL PHENOLICS EPA 420.1 MANGANESE EPA 200.7 VOLATILEHALOCARBONS EPA 624 MERCURY EPA 245.1 VOLATILE AROMATICS EPA 624 MOLYBDENUM EPA 200.7 CHLORDANE EPA 608 NICKEL EPA 200.7 ALDRIN EPA 608 SELENIUM EPA 200.7 DIELDRIN EPA 608 SELENIUM EPA 270.2 DDD EPA 608 SILVER EPA 200.7 DDT EPA 608 STRONTIUM EPA 200.7 HEPTACHLOR EPA 608 THALLIUM EPA 200.7 HEPTACHLOR EPDXIDE EPA 608 THALLIUM EPA 279.2 POLYCHLORINATED BIPHENYLS(WATER) EPA 608 ZINC EPA 200.7 POLYCHLORINATED BIPHENYLS(OIL) EPA 60014-81-045 PH EPA 150.1 SPECIFIC CONDUCTIVITY EPA 120.1 TOTAL DISSOLVED SOLIDS EPA 160.1 TOTAL HARDNESS(CAC03) EPA 200.7 CALCIUM EPA 200.7 MAGNESIUM EPA 200.7 SODIUM EPA 200.7 POTASSIUM EPA 200.7 TOTAL ALKALINITY EPA 310.1 CHLORIDE EPA 325.3 CHLORIDE EPA 300.0 FLUORIDE EPA 340.2 FLUORIDE EPA 300.0 SULFATE EPA 375.4 SULFATE EPA 300.0 AMMONIA-N EPA 350.2 NITRATE-N EPA 300.0 June 27,2061'.-. * ProNisional Certification Page 1 of 2 13 CONBIONNVEALTH OF NWS S ACHUS EITS DFPARTNIENT OF FNVIRONN'ILNTAL PROTECTION Certified Parameter List as of: 01 JUL 2001 N1-NH012 AMRO E VIRON MM TAL LAB INEIMMACK NH POTABLEWATFR(CHEMISTRY) Effective 01 JUL 2001 Expiration 30 JUN 2002 Date Date Analvtes and Methods ANTIMONY EPA 200.9 ARSENIC EPA 200.7 ARSENIC n EPA 200.9 BARIUM EPA 260.7 BERYLLIUM EPA 200.7 CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COPPER EPA 200.7 LEAD EPA 200.9 MERCURY EPA 245.1 NICKEL EPA 200.7 SELENIUM J' EPA 200.9 THALLIUM EPA 200.9 NITRATE-N EPA 353.2 NITRITE-N EPA 353.2 FLUORIDE EPA 300.0 FLUORIDE SM 4500-F-E SULFATE EPA 300.0 CYANIDE SM 4500-CN-C,E TURBIDITY EPA 180.1 RESIDUAL FREE CHLORINE SM 4500-CL-G CALCIUM EPA 200.7 TOTAL DISSOLVED SOLIDS SM 2540C PH EPA 150.1 1,2-DIBROMOE HANE EPA 504.1 1,2-DIBROMO-3-CHLOROPROPANE EPA 504.1 i June 27,2001 . *ProNisional Certification Page 2 of 2 14 ATTACHMENT 3 COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION DIVISION,OR.HAZARDOUS MATERIALS • __ One Winter Street Boston, Massachusetts 02108 - - " Please print or type.(Form designed for use on elite(12•pitch pewriter)_ UNIFORM HAZARDOUS 1.Generator's US EPA ID No. Manifest Document No. 2.Page 1 Information in the shaded areas WASTE MANIFEST of is not required by Federal law." a - �.:. a 3.Generator's Name and Mailing Address A State Marnfest Document Number MA, M47---749311 DIEM H `RASK B State Gen (D 312 suxRD sTRpErr7. WORTH AN1X)VER, MA 01845 a.Generators Phone 978) 557-1147 N 5.Transporter 1 Company Name 6.US EPA ID Number C.State Trans.ID O co ENFRO SERVICF-9, I14C. A D 9 8 0 6 7 0 0 0 4 r q 7.Transporter 2 Company Name 8.US EPA ID Number 4 .C\j D.Transpoe(sPhone Uj 't E.State Trans.ID �+ 9.Designated•Faci5ty Name and Site Address. 10.US EPA ID Number O F:Transportees Phone JONES ENVIRONMENTAL S RVI%S (NE) INC _ O X53 �0 '.�J $ G.State Facility's ID NOT REQUIRED. 0 LaREI Twp 14A 016_S12'. A D 0 4 7 0 7 5 7 3 4 H.Facility's Phone' (P78- 453-7172, _ C 11.US DOT Descri tion Includin Proper Shipping Name,Hazard Class and ID Number iz.containers ,3. p ( 9 p pP 9 ) No. TvDe Tota)OuantiN uvoi WASTE NO. U aSTATE fi$GLL TED OIL WTE UM P. Y.AUl Z V) -D c O n G to E b. M cC N E _ � cR r D o A -- - T .. Z 0 cJ d. U r3 `> U J:Additional Descriptions for Materials Listed Above Include physical state and hazard code.) K.Handling Codes for Wastes Listed Above �. E �t _ 1a PPLc, r. Ea. -. :.--.. S :.` c. Ia. . c: - N b d . [d. 15.Special Handling Instructions and Additional Information 0 M!l3RCKNCY C014Vf rt EJiF`RO SERVICM9, INC. -24 HOURS-- (800)-966-1202 ER GUIDEBOOK NO..: - U j U 1E T C I CA IO hereby declare that the contents of this consignment are fully and accurately described above by proper shipping namg,,,and are classified, 0) packed,marked,and labeled,and are in all respects in proper condition for transport by highway according to applicable international and national government regulations. N tf 1 am a large quantity generator,I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that 1 have selected the practicable method of treatment,storage,or disposal currently available to me which minimizes the preserk and future threat to human E health and the environment;OR,if I am a small quantity generator,I have made a good faith effort to minimize my waste generation and elect the best waste management 0 method that is available to me and that I can afford. ,, , Date N PrintedlTyped Name Signature r ; r: y Mo i h 1D�y. l.Y;ar VT 17.Transporter 1 Acknowledgement of Receipt of Materials Date: R t✓ A Printed/Typed Name SignatureMpnth Day Year - P Az .� q _18.Transporter 2 Acknowledgement of Receipt of Materials - Date ' E Printed/TypedName- - Signature _ Montn` Day.; Year If F 10.Discrepancy Indication Space _ t' ,. C - 20 FacrTity Owner.or Operator Certrfication'oi receipt of haiardous materials covered by this manifest except as noted in iteml9 _ Date T'- Printed/ d-Na m - - / /! CUM( ` e v Form Approved MB No.2050.0039.Expires 9.30-99 EPA Form 8700-22(Rev..9-88)Previous editions are obsolete. - COPY>5:TRANSPORTER 1 RETAINS Massachusetts Department of Environmental Protection BWSC-0a2a Bureau of Waste Site Cleanup Release Tracking Number' BILL OF LADING (pursuant to 310 CMR 40.0030) �3 -[20874 A. LOCATION OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED: Release Name(optional): Trask Residence Street: 312 Boxford Street Location Aid: Cityrrown: North Andover ZIP Code: 01845 �r DatelPeriodofGeneration- J'22'/VO1. to:. . Additional Release Tracking Numbers Associated with this Bill of Lading: Note: If this B91 of Lading is the result of a Limited Removal Action(LRA) taken prior to Notification, a Release Tracking Numberis not needed. B. PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: Name of Organization: T r a s k Residence Name of Contact: Deborah A. Trask Title: owner Street 312 Boxford Street Cityfrown: North Andover state: MA ZIP Code: 01845 Telephone: k 9 7 8) 557-1147 Ext.: C. RELAT16NSHIF I O RtLtASt OF PtRSON(;ONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: © RP or PRP Specify: ® owner E] Operator F� Generator F1 Transporter Other RP or PRP: Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E.s.2) Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) ❑ Other Person: If an owner and/or operator is not conducting the response action associated with the Bill of Lading,provide on an attachment the name, contact person,address and telephone number,including any area code and extension,for each,if known. D. TRANSPORTER OR COMMON CARRIER INFORMATION: Transporter/Common Carrier Name: Holland Energy Contact Person: Mr . Peter Holland Title: GM _ Street 63 Jefferson Ave . , PO Box 831 Cityr town: Salem State: MA ZIP Code: 01970-0931 Telephone: (9 7 8) 741-2900 Ext.: _ E. RECEIVING FACILITY/TEMPORARY STORAGE LOCATION: Operator/FadlityName: Brox Industries Inc . Contact Person: Mr . Erik Stevenson Title: Eng. Street 1471 Methuen Street City/Town: Dracut State: MA ZIP Code: Telephone: (9 7 8) 454-9105 Ext.: Type of Facility. Asphalt Batch/Cold Mix Landfill/Disposal F] Incinerator F-1 Temporary Storage (check one) ® Asphalt Batch/Hot Mix F-1 Landfill/Daily Cover F-] Other. El Thermal Processing Landfill/Structural Fill EPA Identification#: MAD 9 8 5 2 6 7 7 9 8 Division of Hazardous Waste/Class A Permit#: NE-96-1 0 0 Division of Solid Waste Management Permit#: Actual/Anticipated Period of Temporary Storage(specify dates If applicable): to: Reason for Temporary Storage: Massachusetts Department of Environmental Protection BWSC-012A' Bureau of Waste Site Cleanup i iRelease Tracking Number' BILL OF LADING (pursuant to 310 CMR40.0030) 3� 20874 E RECEMNG FACIUTYrrEMPORARY STORAGE LOCATION(continued): Temporary Storage Address: Street: City/Town: State: ZIP Code: F. DESCRIPTION OF REMEDIATION WASTE: (check all that�apply) ® Contaminated Media(check all that'apply): c (9 Soil O Groundwater O Surface Water O Other._ ElContaminated Debris(check all that apply): O Vegetation or Organic Debris Demolition/Construction Waste OInorganic Absorbant Materials O Other: EJNon-hazardous Unoontainerized Waste(check all that apply): O Non-aqueous Phase Liquid 0 Other: Non-hazardous Containerized Waste(check all that apply): O Tank Bottoms/Sludges O Containers 0 Drums OEngineered Impoundments O Other: . Type of Contan-Anation(check all that apply): ElGasoline 11 Diesel Fuel a 02 Oil #4 Oil 0 96 Oil Waste Oil .r Kerosene Jet Fuel Other:_ Estimated Volume of Materials: Cubic Yards: 1 60± Tons: 120 . 04 Other: Contaminant Source(check one/specify): El Transportation Accident n Underground Storage Tank 10 Other:f Response Action Associated with Bill of Lading(check one): ® Immediate Response Action E] Release Abatement Measure F1 Utility-Related Abatement Measure n Limited Removal Action Comprehensive Response Action E] Other Remediation Waste Charcterization Support Documentation attached: MV Site History Information a Sampling and Analytical Methods and Procedures Laboratory Data MV Field Screening Data If supporting documentation is not appended,provide an attachment stating thedate and in connection with what document such information was previously submitted to DEP. G. LICENSED SITE PROFESSIONAL(LSP)OPIMON: Name of organization: Subsurface Remediation Technologies , Inc . LSP Name: Timothy A. Toomey Title: GM Telephone: . (978_) 948-1961 Ext.: I attest under the pains and penalties of perjury that 1 have personally exarnired and am familiar with this submittal,including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of (i)the standard of care in 309 CMR 4.02(1), (ii)the applicable provisions of 309 CMR 4,02(2)and(3),and (Ho the provisions of 309 CMR 4.03(5), to the best of my knowledge,information and belief,the assessment actions undertaken to characterize the Remediation Waste which is(are)the subject of this submittal for acceptance at the facility identified in this submittal comply with the applicable provisions of 310 CMR 40.0000,and such facility is permitted to accept Remediation Waste having the characteristics d(scribed In this submittal. I am awar ificant penalties may result, including,but not limited to,possible fi es and imprisonment,if 1 submit inbrmation which I know to be false WN- S'99Cyrially incomplete. LSP Signature: Seal: ��O TIMOTHY %P Sept. 13 2 0 0 1 TOOM� Date: a _ No.2891 � O License Number. 2891 FGISTEp'� ` a - Massachusetts Department of Environmental Protection BWSC-012A Bureau of Waste Site Cleanup Release 7racldng Number' BILL OF LADING (pursuant to 310 cMR40.0030) a3 - 20874 H. CERTIFICATION OF PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: I certify under penalties of law that I have personally examined and am familiar with the information contained in this submittal,Including any and all documents accompanying this certification,and that,based on my inquiry of those individuals immediately responsible for obtaining the Information,the material information cortained herein is,to the best of rry knowledge and belief,true,accurate and comptete. I am aware that there are significant penalties,incl ' ,but not limned to,possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. Signature: h~ �!`� Date: Sept13 2001 Name of Person(print): DeboL ah,F A. Trask i .I I I�,assac, u,etts Depadvnsnt of EnVironmental Protection i3'Ifvz) q k . Bureau of Waste Site Cleanup ORIGINAL BILL OF LADING (pursuant to 310 LIAR 40.0030) Release Trac"Number FW SUMMARYSHEET of 2- 1. I. LOAD INT=O"' A i iON: Signatiure -1 T ,*rter Representative: i Re vire FaciRy/Temporary Storage Representative: Load 1: 11-1011-10• =11s ' 0 Date of 74, ' Time of Shipment ld Date of Receipt Time of Receipt / } �o.',S6 A,.� CPM ; C1_Zp ;vl YJAM PM Truck/Tractor Registration, ' ;-�raiierRegistration(f any): i Load Size(cu.ydslo. 2.0. 51 Load 2: Signatiur f T spoder Repre:rdAtive: i Receiving wFadli.�, Temporary Storage Representative: 17 Date of Shipment: Time of Shipment: Time of Reoeipt: �c� Date�f Receipt: I�Z )0/ / v [] AME— PM i —2O - p1 IZ:Ste' ❑ AM ,PM i TruclJTrador Registration: Trailer Registration(if any): i z /n� i Load Size(cu.y ,ons): Zq,09AA o 2 Load 3: Signatiure of Transporter epresentative: Re iving Facili;y,'Teqnrary _Storage Representative: Date of Shipment: Time of Shipment: 'AM �M Date of Receipt: Time of Receipt:�./� Jb l Z; QU ❑ Truck/Tractor Registration: Trailer Registration(if any): l i 100"10 Load Size(cu.ydso Z-3,(Z,1 r7 Z Load 4• Signatiure of Transporter Repr sentative: i Receiving Facility/Temporary Storage Representative: Time of Shipment: ' Date of Shipment: p i- Time of Receipt: Date of Receipt �AM ❑ PM 7lZlIJI 6s. Ce aAM ❑ PM 9 —Z� — O I rI'US TruddTractor Registration: Trailer Registration(f any): i /?',4 L/f P�Z i Load Size(cu.yds ns): Load 5: Signatiure of Trans,�orte presentative: Receiving Faciliy,7en-porary Storage Representative: J 6o-L Date of Shipment: Time of Shipment: ' Date of Receipt Time of Receipt: AM ❑ PM r lI_ —G I I Z:1 Z NAM NJ PM Truck/Tractor Registration: Trailer Registration(f any): i a i Load Size(cu.yds "l ,62 r Load 6: Slgnatiu f T nsporter Repre r Receiving Facility/Temporary Storage RepresentafNe: Date of ipme : Time of Shipment i Date of Receipt Time of Receipt: �❑ PM b ZO T I AM PM -01 Truck/Tractor Reglstration: Trailer Registration(if any). 1 Load Size(cu.yds 7 .G q J. LOG SHEET VOLUME INFORMATION: Total Volume Recorded This Page(cu.yd� /47 SZ ��- Total Carried Forward(cu.y4194.Sr ' Total Carried Forward and This Page(cu.ydi 107 :5 �.... s aws Ri 'V A c-o ZB_ ft�assachusotts Department of Environmen a f � :_-,_:� Bureau of Waste Site Cleanup BILL OF LADING (pursuant to 310 CMR 40.0030) Release Tracking Number SUMMARYSHEET Z z ❑3 - 20874 I. LOAD INFORMATION: natiure of Tran ese ve: i Receiving Facility/Temporary Storage Representative: Load 1: Dateo Sty� Time e of Shi /�/ J�/6 U Date of Receipt Time of Receipt AM Pt�l i D f' Z.as Q AM "�PM Truck/Tractor Registration: #fraile(;Registration(if any): Load Size(cu.yds _.. 2 Load 2: Signatiure of Transporter Representative: i Recelving'Fadlityrren-porary Storage Representative: i Date of Shipment: Time of Shipment:• Date of Receipt Time of Receipt: AM F7, PM i AM PM Truck/Tractor Registration: Trailer Registration(d any): , i Load Size(cu.yds./tons): Load 3: Signatiure of Transporter Representative: Receiving Facilay/7emporary Storage Representative: Date of Shipment: Time of Shipment: AM PM , Date of Receipt: Time of Receipt: AM PM i Tr'ucklTractor Registration: Trailer Registration(f any): i i i Load Size(cu.yds.Aons): Load 4• Signatiure of Transporter Representative: i • Receiving Fadlity/Tenporary Storage Representative: i Date of Shipment Time of Shipment: p i Date of Receipt Time of Receipt: [] AM F� PM AM F-1 PM i Tnx*jTractor Registration: Trailer Registration(f any): i i. Load Size(cu.yds tions): Load 5: Signatiure of Transporter Representative: i Receiving Facili ylTemporary Storage Representative: Date of Shipment: Time of Shipment: i Date of Receipt Time of Receipt: AM PM AM F-1 PM , i Truck/Tractor Registration: Trailer Registration(f any): i i Load Size(cu.ydsibns): i Load 6: Signatiure of Transporter Representative: i Receiving Facility/Temporary Storage Representative: i Date of Shipment: Time of Shipment Date of Receipt Time of Receipt � i EjAM El Pm El Am. PM i Truck/Tractor Registration: Trailer Registration(ff any): I Load Size(cu.yds.Aons): i J. LOG SHEET VOLUME INFORMATION: Total Volume Recorded This Page(cu.yd ons 44 SZ Total Carried Forward(cu. ons 107-52 Total Carried Forward and This Page(cu.Y Aons Massachusetts Department of Environmental Protection BWSC-012C Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030) 0 R I G I N A L Reiesse Traddng Number t SUNIMARYSHEET 1 OF 1 20874 K. SUMMARY OF SHIPMENTS: Daily Volume Shipped Date of Shipment: Date of Receipt: Number of Loads Shipped: (cu.ydsJtons): :�' Li of / 12 •�8 52- 0i Zni .r f Summary Sheet Total Shipped: / ,-0 , O Bill of Lading Total Shipped (only if different): Massachusetts Department of Environmental Protection BWSC-O 2C Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030 ORIGINAL Release Traddng Number SUMMARYSHEET E - 20 ONLY CO.14 LETS ONE COPY OF THIS PAGE AND ATTACH TO THE FINAL COPY OF THE SUMMARY SHEET. L ACKNOWLEDGMENT OF RECEIPT OF REMEDIATION WASTE AT RECEIVING FACILITY OR TEMPORARY STORAGE: Receivi FacilitylTempora for True: age R�e�I�-�` �V � K V' / /li�✓�N� T��L►'�Ti�C .h9 t Date: Signature: M. ACKNOWLEDGMENT OF SHIPMENT AND RECEIPT OF REMEDIATION WASTE BY PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: I certify under penalties of law that I have personally examined and am familiar with the inforration contained in this submittal,including any and all documents accompanying this certification,and that,based on rrmm y inquiry of those individuals immediately responsible for obtaining the information,the nY material information contained in herein is,to the best of rtry knowledge and belief,true,accurate and complete, I am aware that there are significant penalties,including,but not limited to,possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. Date: Signature: Name of Person(print): I � ( 4 Massachusetts Department of Environmental Protection BWSC=012C Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030 Release Tracldng Number SUMMARY SHEET 3� - 20874 ONLY COMPLETE ONE COPY OF THIS PAGE AND ATTACH TO THE FINAL COPY OF THE SUMMARY SHEET. L ACKNOWLEDGMENT OF RECEIPT OF REMEDIATION WASTE AT RECEIVING FACILITY OR TEMPORARY STORAGE: Receiving Facility/Temporary Storage Representative(print): Title: Signature:" .. :Y` s.._ Date: M. ACKNOWLEDGMENT OF SHIPMENT AND RECEIPT OF REMEDIATION WASTE BY PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: I certify under penalties of law that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this certification,and that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material Information contained in herein is,to the best of rry knowledge and belief,true,accurate and complete, I am aware that there are significant penalties,including,but not limited to,possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. Signature: �� Date: Name of Person(print).. Deborah Trask ,T .r .. .:, ATTACHMENT 4 .i i SUBSURFACE REMEDIATION TECHNOLOGIES,INC. Page: 1 355 Central Street, Rowley, MA.01969 Boring No. MW-2 508) 948-3861 SRT Job No. 235 Project Name: IRA Assessment-Trask Property Well Elevation: 100.41 arb. Client Name: Deborah Trask Well Elevation: George Boring Location: 312 Boxford Street North Andover SRTGeologist Toomey Drilling Contractor: Soil Exploration IStarl Date: 9/5/01 Drilling Method: HOLLOW STEM AUGER/Coreing Casing/Auger Size: I Date End: 9/6/01 Standard Sampler: Unless noted,sampler consists of a 2"split-spoon driven using a D SAMPLE Penetration 140 Ib hammer falling 30 in. N E Type Range Test Casing: Unless noted,casing driven using 300 Ib hammer falling 24 in. O Well P $ From Headspace Strata Field Classification T Diagram T No. I Blows per 6" Pen Rec OVA Change and E H To on split-spoon (in) (in) Reading Depth Drilling Information S (ppm) S-1 0 Tan very dense silty.SAND&GRAVEL some boulders ` TILL 5 S-2 5 SAME 10' 10 8S-3 15 35 120 SAME 16 20' SS-4 25 42 120 SAME 26 30, SS-5 30 38 120 SAME 31 40' End of Exploration ® 39 GRANULAR SOILS COHESIVE SOILS NOTES: Blows/Ft Density Blows/Ft Density Screen at 29 to 39 feet 0 -4 v.loose < 2 v. soft 0.010 slot 2"PVC screen 4 - 10 loose 2-4 soft Bentonite seal at 25' to 27' 10 - 30 m.dense 4-8 m. stiff Roadbox-1.5 concrete approx 1 toot diameter 30 - 50 dense 8- 15 stiff GROUNDWATER READINGSae SRT > 50 v.dense 15 - 30 v. stiff DATE TIME WATER AT CASING AT BORING > 30 hard 6-Sep 33 NUMBER 1 OA/OC CHECKED BY: 16-Oct 37.62 MW-2 1 1 i ,per .\ COMMON'WEALTH OF MASSAC14U.SETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS DEPARTMENT OF ENVIRONMENTAL PROTECTION it 11"p , ONE WINTER STREET. BOSTON. NIA 02108 617-292-5500 er , TRUDY COXE WILLIAM F.WELD A" ���1V Secrctan Governor '`�_--_,.,,,, ARGEO PAUL CELLUCCI � +.t,DAVID B.SIRUHS Lt.Govemor SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM Commissioner PART A CERTIFICATION Property Address: c� «. Z, �� ' "' ' ` ,,`5'�u9SAddress of Owner: Date of Inspection:` ' (If different) (�., ,- Name of Inspector: }v v�-�C•'Y I am a D appro ed system i. pector ursuant to Se ion 15.340 of Title 5 (310 CMR 15.000) Company Name: r �S TL Mailing Address: 2 - JU-Q (` r) ( t) Telephone Number: — CERTIFICATION STATEMENT I certify that I have personally inspected the sewage disposal system at this address and that the information reported below is true, accurate and complete as of the time of inspection. The inspection was performed based on my training and experience in the proper function and maintenance of on-site sewage disposal systems. The system: Passes-- nditionally Passes Nees Further Evaluation By the Local Approving Authority C FI ' Signature: Ins ectors Si nature: '��'�c^-� Date- The ate: P g The System Inspector shall submit a copy of this inspection report to the Approving Authority within thirty (30) days of completing this inspection. If the system is a shared system or has a design flow of 10,000 gpd or greater, the inspector and the system owner shall submit the report to the appropriate regional office of the Department of Environmental Protection. The original should be sent to the system owner and copies sent to the buyer, if applicable, and the approving authority. INSPECTION SUMMARY: Check A, 8, C, Or D: AI SYSTEM PASSES: I have not found any information which indicates that the system violates any of the failure criteria as defined in 310 CMR 15.303. Any failure criteria not evaluated are indicated below. COMMENTS: BI SYSTEM CO ITIONA'LLY PASSES: One or more system components as described in the "Conditional Pass" section need to be replaced or repaired. The system, upon 4rte cQm�pl�tion of the replacement or repair as approved the rd of H Ith ill pass Indicate yes, no, or ndt det�rmined�, N, or ND). Describe basis of detetmtnatlon in all instances. if not determined", expla n why not The septic tank is metal, unless the owner or operator has provided the system inspector with a copy of a Certificate of Compliance (attached) indicating that the tank was installed within twenty(20)years prior to the date of the inspection; or the septic tank, whether or not metal, is cracked, structurally unsound, shows substantial infiltration or exfiltration, or tank failure is imminent. The system will pass inspection if the existing septic tank is replaced with a conforming septic tank as approved by the Board of Health. (r*vixod 04/25/97) Page 1 of 30 DEP on the World Wide Web: http://www.magnetstate.ma.ustdep 0 Printed on Recycled Paper SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART A CERTIFICATION (continued) fj Property Address- Owner: C< < Date of Inspection: r/ ( , t✓ 61 SYSTEM CONDITIONALLY PASSES (continued) Sewage backup or breakout or high static water level observed in the distribution box is due to broken or obstructed pipe(s) or due to a broken, settled or uneven distribution box. The system will pass inspection if(with approval of the Board of Health). Describe observations: broken pipe(s) are replaced obstruction is removed distribution box is levelled or replaced _ The system required pumping more than four times a year due to broken or obstructed pipe(s). The system will pass inspection if(with approval of the Board of Health): broken pipe(s) are replaced obstruction is removed C] FURTHER EVALUATION IS REQUIRED BY THE BOARD OF HEALTH: Conditions exist which require further evaluation by.the Board of Health in order to determine if the system is failing to protect the public health, safety and the environment. 1) SYSTEM WILL PASS UNLESS BOARD OF HEALTH DETERMINES THAT THE SYSTEM IS NOT FUNCTIONING IN A MANNER WHICH WILL PROTECT THE PUBLIC HEALTH AND SAFETY AND THE ENVIRONMENT: _ Cesspool or privy is within 50 feet of a surface water Cesspool or privy is within 50 feet of a bordering vegetated wetland or a salt marsh. 2) SYSTEM WILL FAIL UNLESS THE BOARD OF HEALTH (AND PUBLIC WATER SUPPLIER, IF APPROPRIATE) DETERMINES THAT THE SYSTEM IS FUNCTIONING IN A MANNER THAT PROTECTS THE PUBLIC HEALTH AND SAFETY AND THE ENVIRONMENT: The system has a septic tank and soil absorption system (SAS) and the SAS is within 100 feet to a surface water supply or tributary to a surface water supply. The system has a septic tank and soil a5sorption system and the SAS is within a Zone I of a public water supply well. _ The system has a septic tank and soil absorption system and the SAS is within 50 feet of a private water supply well. _ The system has a septic tank and soil absorption system and the SAS is less than 100 feet but 50 feet or more from a private water supply well, unless a well water analysis for coliform bacteria and volatile organic compounds indicates that the well is free from pollution from that facility and the presence of ammonia nitrogen and nitrate nitrogen is equal to or less than 5 ppm. Method used to determine distance (approximation not valid). 3) OTHER (revised 04/25/97) page 2 of 10 SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART A ( CERTIFICATION (continued) Property Address: ��j (c� G �� �F Ca �• /v" -�•- '�/�X_ Owner: CG�� 1V1 Date of Inspection: D) SYSTEM FAILS: You must indicate either "Yes" or"No" as to each of the following: I have determined that the system violates one or more of the following failure criteria as defined in 310 CMR 15.303. The basis for this determination is identified below. The Board of Health should be contacted to determine what will be necessary to correct the failure. Yes No Backup of sewage into facility or system component due to an overloaded or clogged SAS or cesspool. Discharge or ponding of effluent to the surface of the ground or surface waters due to an overloaded or clogged SAS or cesspool. Static liquid level in the distribution box above outlet invert due to an overloaded or clogged SAS or cesspool. Liquid depth in cesspool is less than 6" below invert or available volume is less than 1/2 day flow. Required pumping more than 4 times in the last year NOT due to clogged or obstructed pipe(s). Number of times pumped_. Any portion of the Soil Absorption System, cesspool or privy is below the high groundwater elevation. Any portion of a cesspool or privy is within 100 feet of a surface water supply or tributary to a surface water "supply. r Any portion of a cesspool or privy is within a Zone I of a public well. Any portion of a cesspool or privy is within 50 feet of a private water supply well. _ Any portion of a cesspool or privy is less than 100 feet but greater than 50 feet from a private water supply well with no acceptable water quality analysis. If the well has been analyzed to be acceptable, attach copy of well water analysis for coliform bacteria, volatile organic compounds, ammonia nitrogen and nitrate nitrogen. E) LARGE SYSTEM FAILS: You must indicate either "Yes" or "No" as to each of the following: The following criteria apply to large systems in addition to the criteria above: The system serves a facility with a design flow of 10,000 gpd or greater (Large System) and the system is a significant threat to public health and safety and the environment because one or more of the following conditions exist: Yes No the system is within 400 feet of a surface drinking water supply the system is within 200 feet of a tributary to a surface drinking water supply the system is located in a nitrogen sensitive area (Interim Wellhead Protection Area-IWPA)or a(napped Zone'll of a public water supply well) The owner or operator of any such system shall bring the system and facility into full compliance with the groundwater treattnbnt program requirements of 314 CMR 5.00 and 6.00. Please consult the local regional office of the Department for further information. (revised 04/2S/97) Page 3 of 10 i i I SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART B CHECKLIST Property Address: '13 Owner: C« C S",\ Date of Inspection: Check if the following have been done: You must indicate either "Yes" or"No"as to each of the following: Yes -- No---�� Pumping information was provided by the owner, occupant, or Board of Health. None of the system components have been pumped for at least two weeks and the system has been receiving normal flow rates during that period. Large volumes of water have not been introduced into the system recently or as part of this inspection. A/// (0_, �� As buili p ns hLI been btained and exami Note if they are not available with N/A. The facility or dwelling was inspected for signs of sewage back-up. The system does not receive non-sanitary or industrial waste flow. w The site was inspected for signs of breakout. L' component stem All s s, excluding the Soil Absorption System, have been located on the site. _ Y The septic tank manholes were uncovered, opened, and the interior of the septic tank was inspected for condition of L baffles or tees, material of construction, dimensions, depth of liquid,depth of sludge, depth of scum. L / The size and location of the Soil Absorption System on the site has been determined based on: The facility owner (and occupants, if different from owner) were provided with information on the proper maintenance of j Sub-Surface Disposal System. Existing information. Ex. Plan at B.O.H. Determined in the field (if any of the failure criteria related to Part C is at issue, approximation of distance is unacceptable) (15.302(3)(b)J (revised 04/2S/97) Pigi ei 10 SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C [ ( \ SYSTEM,INFO TION Property Address: .C— Owner: ( � Date of Inspection: FLOW CONDITIONS RESIDENTIAL: Design flow: /10 t;.p.d./bedroom for S.A.S. i Number of bedrooms:_ Number of current residents: Garbage gander (yes or no): 5 Laundry connected to system (yes or no):-yes Seasonal use (yes or no): 0 Water meter readings, if v ilable (last two (2)year usage (gpd): a'-\ Sump Pump (yes or no): IVO Last date of occupancy: COMMERCIAUINDUSTRIAL: Type of establishment: Design flow:_gallons/day Grease trap present: (yes or no)_ Industrial Waste Holding Tank present: (yes or no)_ Non-sanitary waste discharged to the Title 5 system: (yes or no)_ Water meter readings, if available: Last date of occupann OTHER: (Describe) Last date of occupancy: GENERAL INFORMATION PUMPING RECORDS and source of information: ,1�J� U?n"-s a S]J ��v„O�- System pumped as part of inspection: (yes or no) U `-t j ' If yes, volume pumped: Gallons Reason for pumping TYPE Of_SYSTEM i n ox/ it absorption sy_tem Septic tank/distribution b so rp Single cesspool Overflow cesspool Privy Shared system (yes or no) (if yes, attach previous inspection records, if any) VA Technology etc. Copy of up to date contract? Other APPROXIMATE AGE of all components, date installed (if known) and source of information: Sewage odors detected when arriving at the site: (yes or no) N'v (revised 04/25/97) Page 9 of 10 SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORAATION (continued) Property Address: + - ..Owner: _ Date of Inspection: BUILDING SEWER:,/`" (Locate on site plan) 11 Depth below grade: Material of constru io L� t iron 40 PVq�� other expo in), � II d) ' � ° V hou , t �5 �«� `A'VOy �CJt/I , 1 Distance from private water supply well or suction hr•,� h5k9 — Diameter �r Comments:-(condiyon Of jgints, venting, evidence of leakage, etc.) SEPTIC TANK:' TANK:._ (locate on site plan) Depth below grade:,( Material of construction: �4co�nrete _metal _Fiberglass _Polyethylene —other(explain) If tank is metal, list age Is age confirmed by Certificate of Compliance —(Yes/No) Dimensions-. 11 Ix IX L 1 X~7' _ 9 L `S Sludge depth:_ �� Disfance from top of sludge to bottom of outlet tee or baffle: Scum thickness: a ,, Q Distance from top of scum to top of outlet tee or baffle. Distance from bottom of scum to bottom,o out et�tee qr How dimensions were determined: Gy° Comments: p (recommendation for pumping, condition of i let a d ou I t tees r affles, de th of liqui I vel 'n r ation let inve , structural integrity, evi enceof lea e, etc.) e5 7-A. QF GREASE TRAP:��Q� (locate on site plan) - Depth below grade: Material of construction: !concrete _metal _Fiberglass _Polyethylene —other(explain) Dimensions: Scum thickness: Distance from top of scum to top of outlet tee or baffle: Distance from bottom of scum to bottom of outlet tee or baffle: Date of last pumping: Comments: (recommendation for pumping, condition of inlet and outlet tees or baffles, depth of liquid level in relation to outlet invert, structural integrity, evidence of leakage, etc.) (revised 04/25/97) Page 6 of 10 SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION (continued) Property Address: Owner: Date of Inspection: TIGHT OR HOLDING TANK: Rank must be pumped prior to, or at time, of inspection) (locate on site plan) Depth below grade: Material of construction: concrete ,metal _Fiberglass _Polyethylene ,_other(explain) Dimensions: Capacity:_,gallons Design flow: gallons/daN Alarm level: Alarm in working order_ Yes; _ No Date of previous pumping: Comments: (condition of inlet tee, condition of alarm and float switches, etc.) DISTRIBUTION BOX:L" (locate on site plan) Depth of liquid level above outlet invert: t�t f f r tJQ�C�-ti/ l/�VOT Comments: '' (note iflevef�nd ribution is ual, ev'dence of solids car r, e�d nce of leakage into or f t oy, etc.) PUMP CHAMBER: N�.>. locate on site Ian) ( P I Pumps in working order: (Yes or No) Alarms in working order (Yes or No) Comments: (note condition of pump chamber, condition of pumps and appurtenances, etc.) (revised 04/25/97) hate 7 of 10 • SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION (continued) Property Address: s'i ' Owner: �ec�' k- --),C\ Date of Inspection: SOIL ABSORPTION SYSTEM (SAS):— (locate on site plan, if possible; excavation'not required, but may be approximated by non-intrusive methods) If not determined to be present, explain: Type: leaching pits, number: leaching chambers, number: leaching galleries, number: leaching trenches, number,length: leaching fields, number, dimensions: overflow cesspool, number: Alternative system: Name of Technology: Comments: (note condition of soil, signs of hydr ulic fai ure, level of po idi`g, togdjtion ofetation, etc.) {'© � a CESSPOOLS: (locate on site plan) Number and configuration: Depth-top of liquid to inlet invert: Depth of solids layer: Depth of scum layer: Dimensions of cesspool: Materials of construction: Indication of groundwater: inflow (cesspool must be pumped as pan of inspection) Comments: (note condition of soil, signs of hydraulic failure, level of ponding, condition of vegetation, etc.) PRIVY:U`l _ Jlocate on site plan) Materials of construction: Dimensions: Depth of solids: Comments: (note condition of soil, signs of hydraulic failure, level of ponding, condition of vegetation, etc.) (revised 01/25/97) Page a of 10 i SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION (continued) Property Address: ��1,4 �',��� � � i'. �• .�i(,�SJ _.(� Owner: C .('�1.� �+ . .� Date of Inspection: �� SKETCH OF SEWAGE DISPOSAL SYSTEM: include ties to at least two permanent references landmarks or nchma s locate all wells within 100' (Locate where public water supply omes int house) t = c y 1 r� Z7l'7 15/f 3 _ CC) I 1-7 -Ano" A n A = 5 9 Y � Q , � a (revised 04/2S/97) Pago 9 of 10 SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM PART C SYSTEM INFORMATION (continued) Property Address: Owner: Date of Inspection: Depth to Groundwater 6-Feet Please indicate all the methods used to determine High Groundwater Elevation: f Obtained-from-Design Plans on record Observation"of Site (Abutting property, observation hole, basement sump etc.) (�- 6etermine it from local conditions L'- Check with local Board of health Check FEMA Maps Check pumping records Check local excavators, installers Use USGS Data Describe in your own words how you established the High Groundwater Elevation. Must be completed) (N� (revised 04/25/97) Page 10 of 10 ` 4 TFC.: (50q) 475-1474 FAX_ (508) 47_S-.5,17) 1 T [))A ES0N ENTERPRISES, INS , ! Fxcavatlnr-Water R Sewer 1.1net- Serllc Systems & humping Service I I I Aigilla Road a Andover, Mass. 01810 Title 5 Inspection Report F'd:oprt. l y 11)rl.r. ess : -- --- -- --- - -- - OS+.iller : --- -- -- - - -- - ---- --��-II---- Date Of. --- My report contained herein does not constitute a guarantee of ft.iture usage and the functionality of the existing septic system. Such report issued herewith is merely based upon my observations , and I hereby disclaim any further operation of your current septic system. Neil J: Bateson Batesoh Enterprises Ince Page 1- 1 .of 11 Town of North Andover-, Massichusetts Form No. 4 BOARD OF HEALTH June 24 98 CERTIFICATE OF COMPLIANCE 19- Th is is to certify lbat the Individual Soil Absorption Sewage. Disposal Syste by Bateson m constructed or repaired (X iNSTALLER at 312 Boxford: I S treet, N. Ansover, MA !! _OCATION has been installed in accordance with Board: of Health Regulations as described in the Design Approval Site System Permit No. NIA d a t e d 9___. The issuance of this certificate shall not be construed as a guarantee hat the systern will function satisfactorily- BOARD OF HEAL;;1NE -,,UINEER ss� APPLICATION FOR DISPOSAL WORKS CONSTRUCTION PERMIT DATE: Z-11 —3 / CURRENT INSTALLER'S LICENSE# LOCATION: o- (10x LICENSED INST R: ,g SIGNATURE: / TELEPHONE# '4�J,S—/'j��J CHECK ONE: REPAIR: y NEW CONSTRUCTION: IF NEW CONSTUCTION, PLEASE ATTACH FOUNDATION AS-BUILT. Adminis ative Use Only $75.00 Fee Attached? Yes No Foundation As-Built? Yes No Floor Plans? Yes No Approval Date: Form No.3 Town of North Andover, Massachusetts BOARD OF HEALTH ^ NORTFM CJ 3roet�..o 1tio0 .3 19 ` ��•°,A,;;,.��� DISPOSAL WORKS CONSTRUCTION PERMIT SSACHUSE .. Applicant TELEPHONE fJ✓�x�d- NAME ADDRESS Site Location 3ilk � ` ) �n>C Q � Vie„ �•- � i� 6�,� Permission is hereby granted to Construct ( ) or Repair cQ an Individual Soil Absorption Sewage Disposal System as shown on the Design Approval S.S. No. CHAIRMAN,BOARD OF HEALTH • Fee D.W.C. No. i ('nint�ia�lwenill�u�'Messechu�ells II sqd useUg System PUMP-111AItersurd 5yslc�il (hvue� _" - System Lucoliod U le of i'um ►in _ [Quantity Pumped: gallons Rte lbs Cennhuiil: Nig ( VeA 1961100 Tank., 5yslent Pungped by: ctCedo� , Kt' tEd�d Llc�tisd# w ('t�itienls lianslet�red Its : c�ealet a r�tl�rl�bettll�rtt Ulgtticl •.-. p�clur, Dnfe __ ._---- ----_ in , COMMONWEALTH OF MASSACHUSETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS "C� DEPARTMENT OF ENVIRONMENTAL PROTECTION • ONE WINTER STREET. BOSTON. MA 02108 617-292-5500 WILLIAM F.WELD TRUDY COQ Goycmo: SecretarN ARGEO PAUL CELLUCCI DAVID B.S7RUHS Lt.Govcmor, SUBSURFACE SEWAGE DISPOSAL SYSTEM INSPECTION FORM Commission PART A t CERTIFICATION Property Address: U �"/��("�IFOU Address of Owner: Date of I Inspector: nspeco r:�� �� � (If different) Name of Inspector•. � l �� c I am a D pd prov system inspq purs ant to Section 15.340 of Title 5 (310 CMR.15.000) Company Name: _. Mailing Address: ` Telephone Number: CERTIFICATION STATEMENT I certify that I have personally inspected the sewage disposal system at this address and that the information reported below is true, accurate and complete'as of the time of inspection. The inspection was performed based on my training and experience in the proper function and maintenance of on-site sewage disposal systems. The system: Conditionally Passes _ Needs Further Evaluation By the Local Approving Authority Fails Inspector's Signature: Date: The System Inspector shall submit a copy of this inspection report to the Approving Authority within thirty (30) days of completing this inspection. If the system is a shared system or has a design flow of 10,000 gpd or greater, the inspector and the system owner shall submit the report to the appropriate regional office of the Department of Environmental Protection. The original should be sent to the system owner and copies sent to the buyer, if applicable, and the approving authority. INSPECTION SUMMARY: Check A, B, C, or D: AJ SYSTEM SSES. I have not found any information which indicates that the system violates any of the failure criteria as defined in 310 CMR 15.303. Any failure criteria not evaluated are indicated below. AA COMMENTS: Q ULA e Ul �— �� C�'C� wCl�/1 Y�(��. BJ SYSTEM CONDITIONALLY PASSES: _.G` S One or more system components as described in the "Conditional Pass" section need to be replaced or repaired. The system, upon completion of the replacement or repair, as approved by the Board of Health, will pass. Indicate yes, no, or not determined (Y, N, or ND). Describe basis of determination in all instances. If"not determined", explain why not. _ The septic tank is metal, unless the owner or operator has provided the system inspector with a copy of a Certificate of Compliance (attached) indicating that the tank was installed within twenty (20) years prior to the date of the inspection; or the septic tank, whether or not metal, is cracked, structurally unsound, shows substantial infiltration or exf0tration, or tank failure is imminent. The system will pass inspection if the existing septic tank is replaced with a conforming septic tank as approved by the Board of Health. i (revis&d 04/25/97) Page 1 of 10 DEP on the Wond Wide Web: http:uwww.magnet.state.ma.uwdep A Printed on RecycAed Paper Commonwealth of Massachusetts `A C, Massachusetts 30 19"S J s� S f r 1 System Pumping Record Systent Owner System Location so D- Date of Pumping: ` `� Quantity Pumped: C�C� gallons Cesspool: No Yes Septic Tank: No U Yes wl Syslent Pumped by: vegre'dea License# f Contents trartsferrred to : Greater Lawrence Sanitary District Date: _ Inspector: I WELL DATABASE ADDRESS: d AGE OF WEE? i : WELL DRILLE-R: WELL PERKi"i'm: WELL LOCATION: "' f —WELL.PER1tiiIT-DA-?E:- DEPTH OF WELL: ,r --TYZEOF WELL.:-=a_ DRILLED b. DLiG c. Uw" iJ OWN - TYPE OF WATERM4RING RO CK: �\ _ WAS ANALYSIS DAA'-- EIGH M"ANGANESE: Y N' ELG TIRaN: Y 1V OTHERCONTAMLNANTS. Y N - _- l WELLDATAEAEE ADDRESS: AGE OF Wr.L: WELL DRILLER. xf ? 414tcl-A W=PER. fIT m:- ', WELL L OCATIO g WELL;PERNBTDATE: `DEPTH OF WELL: TYPE OF WELL: a. DI LED b DUG c. U l\�NO f TYPE OF WATER BEARL lG °SOCK WATER ANALYSIS DATE: HIGH MANGANESE: Y N HIGH IRON: Y N OTHER CONTAINS TANTS: Y N COMMONWEALTH OF MASSACHUSETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS IF DEPARTMENT OF ENVIRONMENTAL PROTECTION Metropolitan Boston—Northeast Regional Office _ T. F NORTH A� ,C ARD OF HEA--,,-; JANE SWIFT BOB DURAND Governor J-4 �� 2001 Secretary J�� � -3 ZOOS � LAUREN A LISS t Commissioner URGENT LEGAL MATTER: PROMPT ACTION NECESSARY CERTIFIED MAIL: RETURN RECEIPT REOUESTED Mr. &Mrs.Robert Trask RE: NORTH ANDOVER 312 Boxford Street Residential Property North Andover,MA 01845 312 Boxford Street RTN:#3-20874 NOTICE OFRESPONSIBHUTY, M.G.L. c. 21E&310 CMR 40.0000 Dear Mr.&Mrs.Trask: On July 3,2001 at 4:35 p.m.,the Department of Environmental Protection(the Department or DEP) received oral notification that there is or has been a release or threat of release..of oil and/or hazardous material at the above referenced property which requires one or more response actions. Based on this information, the Department has reason to believe that the subject property or portion(s) thereof is a disposal site as defined in the Massachusetts Oil and Hazardous Material Release Prevention and Response Act, M.G.L. c. 21E, and the Massachusetts Contingency Plan, 310 CMR 40.0000 (the MCP). The assessment and cleanup of disposal sites is governed by M.G.L.c.2 1 E and the MCP. The purpose of this notice is to inform you of your legal responsibilities under state law for assessing and/or remediating the subject release. For purposes of this notice, the terms and phrases used herein shall have the meaning ascribed to them by the MCP unless the text clearly indicates otherwise. STATUTORY LIABILITIES The Department has reason to believe that you (as used in this letter, "you" refers to Mr. & Mrs. Robert Trask) are a Potentially Responsible Party (a PRP) with liability under M.G.L. c. 21E, § 5, for This information is available in alternate format by calling our ADA Coordinator at(617)574-6872. 205A Lowell St. Wilmington,MA 01887 • Phone(978)661-7600 Fax(978)661-7615 • TTD#(978)661-7679 Printed on Recycled Paper i response action costs. Section 5 makes the following parties liable to the Commonwealth of Massachusetts: current owners or operators of a site from or at which there is or has been a release/threat of release of oil or hazardous material; any person who owned or operated a site at the time hazardous material was stored or disposed of; any person who arranged for the transport,disposal, storage or treatment of hazardous material to or at a site; any person who transported hazardous material to a transport, disposal, storage or treatment site from which there is or has been a release/threat of release of such material; and any person who otherwise caused or is legally responsible for a release/threat of release of oil or hazardous material at a site. This liability is "strict", meaning it is not based on fault, but solely on your status as an owner, operator, generator,transporter or disposer. It is also joint and several, meaning that you may be liable for all response action costs incurred at the site,regardless of the existence of any other liable parties. The MCP requires responsible parties to take necessary response actions at properties where there is or has been a release or threat of:release of oil and/or hazardous material. If you do not take the necessary response actions, or fail to perform them in an appropriate and timely manner,the Department is authorized by M.G.L. c. 21E to have the work performed by its contractors. By taking such actions, you can avoid liability for response action costs incurred by the Department and its contractors in performing these actions,and any sanctions which may be imposed for failure to perform response actions under the MCP. You may be liable for up to three (3) times all response action costs incurred by the Department. Response action costs include, without limitation, the cost of direct hours spent by Department employees arranging for response actions or overseeing work performed by persons other than the Department or their contractors, expenses incurred by the Department in support of those direct hours, and payments to the Department's contractors. (For more detail on cost liability,see 310 CMR 40.1200.) The Department may also assess interest on costs incurred at the rate of twelve percent (12%), compounded annually. To secure payment of this debt,the Commonwealth may place liens on all of your property in the Commonwealth. To recover the debt, the Commonwealth may foreclose on these liens or the Attorney General may bring legal action against you. In addition to your liability for up to three (3) times all response action costs incurred by the Department, you may also be liable to the Commonwealth for damages to natural resources caused by the release. Civil and criminal liability may also be imposed under M.G.L. c. 21E, § 11, and civil administrative penalties may be imposed under M.G.L. c.21A, § 16 for each violation of M.G.L.c.21E,the MCP,or any order,permit or approval issued thereunder. NECESSARY RESPONSE ACTIONS The subject site shall not be deemed to have had all the necessary and required response actions taken unless and until all substantial hazards presented by the site have been eliminated and a level of No Significant Risk exists or has been achieved in compliance with M.G.L. c. 21E and the MCP. In addition, the MCP requires persons undertaking response actions at disposal sites to perform Immediate Response Actions (IRAs) in response to "sudden releases", Imminent Hazards and Substantial Release Migration. Such persons must continue to evaluate the need for IRAs and notify the Department immediately if such a need exists. The Department has determined that an IRA is necessary to respond to the sudden release of an estimated one hundred fifty (150) gallons of#2 heating fuel oil to below the basement floor at the above referenced residential property. Page 2 of 4 a The release of#2 heating fuel oil occurred when an aboveground storage tank(AST) system feed line started leaking, resulting in the release of oil to below the basement floor. According to information provided to the Department, the fuel oil feed line failure is suspected to have been caused by a lightning strike. You are authorized to conduct only the specific response actions for which you received oral approval from the Department at the time you provided oral notification to the DEP of the subject release. All additional Immediate Response Actions require DEP approval in accordance with 310 CMR 40.0420. You must employ or engage a Licensed Site Professional (LSP) to manage, supervise or actually perform the necessary response actions at the.,subject site. In addition, the MCP requires persons undertaking response actions at a disposal site to submit to the Department a Response Action Outcome Statement(RAO)prepared by an LSP in accordance with 310 CMR 40.1000 upon determining that a level of No Significant Risk already exists or has been achieved at a disposal site or portion thereof. [You may obtain a list of the names and addresses of these licensed professionals from the Board of Registration of Hazardous Waste Site Cleanup Professionals at(617)556-1091.] There are several other submittals required by the MCP which are related to release notification and/or response actions that may be conducted at the subject site in addition to an RAO, that, unless otherwise specified by the Department,must be provided to DEP within specific regulatory timeframes.The submittals are as follows: (1) If information is obtained after making a oral or written notification to indicate that the release or threat of release didn't occur, failed to meet the reporting criteria at 310 CMR 40.0311 through 40.03 15, or is exempt from notification pursuant to 310 CMR 40.03 17, a Notification Retraction must be submitted within 60 days of initial notification pursuant to 310 CMR 40.0335;otherwise, (2) If one has not been.submitted, a Release Notification Form (RNF) must be submitted to DEP pursuant to section 310 CMR 40.0333 within 60 calendar days of the initial date of oral notification to DEP of a release pursuant to 310 CMR 40.0300 or from the date the Department issues a Notice of Responsibility(NOR),whichever occurs earlier; (3) Unless an RAO is submitted earlier, an Immediate Response Action (IRA) Plan prepared in accordance with 310 CMR 40.0420,or an IRA Completion Statement(3 10 CMR 40.0427)must be submitted to DEP within 60 calendar days of the initial date of oral notification to DEP of a release pursuant to 310 CMR 40.0300 or from the date the Department issues an NOR, whichever occurs earlier;and (4) Unless an RAO is submitted earlier, a completed Tier Classification Submittal pursuant to 310 CMR 40.05 10, and, if appropriate, a completed Tier I Permit Application pursuant to 310 CMR 40.0700,must be submitted to DEP within one year of the initial date of oral notification to DEP of a release pursuant to 310 CMR 40.0300 or from the date the Department issues an NOR,whichever occurs earlier. (5) Pursuant to the Department's "Timely Action Schedule and Fee Provisions", 310 CMR 4.00, a fee of$750 must be included with an RAO statement that is submitted to the Department more than 120 calendar days after the initial date of oral notification to DEP of a release pursuant to 310 CMR 40.0300 or after the date the Department issues an NOR,whichever occurs earlier, and before Tier Classification. A fee is not required for an RAO submitted to the Department within 120 days of Page 3 of 4 the date of oral notification to the Department, or the date the Department issues an NOR, whichever date occurs earlier,or after Tier Classification. It is important to note that you must dispose of any Remediation Waste generated at the subject location in accordance with 310 CMR 40.0030 including, without limitation, contaminated soil and/or debris. Any Bill of Lading accompanying such waste must bear the seal and signature of an LSP or, if the response action is performed under the direct supervision of the Department,the signature of an authorized representative of the Department. The Department encourages parties with liabilities under M.G.L. c. 21E to take prompt action in response to releases and threats of release of oil and/or hazardous material. By taking prompt action, you may significantly lower your assessment and cleanup costs and avoid the imposition of, or reduce the amount of,certain permit and annual compliance fees for response actions payable under 310 CMR 4.00. If you have any questions relative to this notice,you should contact Steven S.Ross at the letterhead address or (978) 661-7600. All future communications regarding this release must reference the Release Tracking Number(RTN#3-20874)contained in the subject block of this letter. Sincerely, - L7 • o ss Steven S.Ross Environmental Analyst Emergency Response Branch v Roger T.Chu Branch Chief Emergency Response Branch CC* North Andover Fire Department North Andover Board of Health DEP Data Entry/File Attachment: Release Notification&Release Retraction Form,BWSC-103 Page 4 of 4 BUTTERWORTH & O'TOOLE, INC. P.O. BOX 8294 SALEM,MA 01971-8294 ADJUSTERS/APPRAISERS FOR INSURANCE COMPANIES ONLY TELEPHONE (978)741-5731 FAX (978)740-9109 July 05, 2001 FORM OF NOTICE OF CASUALTY LOSS TO BUILDING UNDER MASS. GEN. LAWS, CH. 139, SEC. 3B TO: Building Commissioner or Board of Health or Inspector of Buildings Board of Selectmen City/Town Hall City/Town Hall ADDRESSES North Andover, MA 01845 North Andover, MA 01845 RE: Insured: Deborah Frank Address : ' 312 Boxford Street North Andover, MA 01845 Policy No. H000003532 `'` _ 9 2001 Loss of: 07/02/01 File or Claim No. : 16-1357 Claim has been made involving loss, damage or destruction of the above captioned property, which may either exceed $1, 000. 00 or cause Mass. Gen. Laws, Chapter 143, Section 6 to be applicable. If any notice under Mass. Gen. Laws, Ch. 139, Sec. 3B is appropriate, please direct it to the attention of the writer and include a reference to the captioned insured, location, policy number, date of loss and claim or file number. If no reply is received from your office within ten days, we will assume you have no liens of any type against this property and we will recommend to the insuring company that this claim is paid. Robert L. Smith, Jr. Adjuster f, SUBSURFACE REMEDIATION TECHNOLOGIES, INC. ENVIRONMENTAL CONSULTING & REMEDIATION SERVICES 355 Central Street • Rowley, Massachusetts 01969 (978) 948-3861 October 17, 2001 Massachusetts Department of Environmental Protection OCT 1 9 2001 North East Regional Office 205A Lowell Street Wilmington, MA 01887 RE: Trask Residence, 312 Boxford Street, North Andover, MA 01845 Immediate Response Action Plan Submittal RTN#3-20874 Dear Sir/Madam: On behalf of Deborah and Robert Trask, owners of the subject residence, Subsurface Remediation Technologies, Inc. (SRT) is submitting the following Immediate Response Action (IRA) Plan in conformance with Department of Environmental Protection (DEP) and the Massachusetts Contingency Plan (MCP) requirements. No other federal, state, or local permits are required to conduct this IRA Plan. Enclosed separately is the original IRA Plan transmittal forms with copies also included in Attachment 1. This is a re- submittal of an IRAP originally submitted on September 5, 2001. This plan presents more information and detail, much of which was not available at the time, per Mr. Steve Ross' letter dated September 25, 2001. Background The Trask family returned home after being away on July 3, 2001 to find that lightning had struck a tree approximately fifteen or twenty feet from the rear corner of their house. They also found that their #2 fuel oil tank had emptied through a ruptured furnace feed line and had seeped onto and below the concrete floor through cracks. The North Andover Fire Department responded and cleaned up, and bagged, oil soaked rugs, clothing, etc. affected by the oil. SRT later contained them in one properly labeled 55- gallon drum, which is still at the site. Notification to Mr. Victor Fonkeim, of your office (DEP), was made by the North Andover Fire Department on July 3, 2001 at 4:35 PM. The release was called in as a "sudden Release", a two hour reporting condition. Mr. Steve Ross of your office conducted a site visit in mid-July. Further action at the site was delayed while the owners' insurance company (Safety Insurance Company) evaluated the cause of the release to i I;M Trask HUP,N Andover RTN 3-20874 Oct. 17,2001 determine if coverage applied. It was determined that the line break was somehow caused by the lightning strike, and full coverage has been determined. The above ground 330 gallon storage tank is estimated to have lost approximately 150 gallons of fuel oil based on available records. A monitoring well was installed on August 13, and 14, 2001, at the front end of the garage in the driveway at the opposite end of the house (see Figure 1), under contract with the insurance company, by Exeter Environmental, Inc. The boring log, included herein as Attachment 2, shows groundwater at 24 feet below ground surface (bgs). Based on blow count data, the glacial till appears to become much more consolidated at approximately 6 feet bgs. From 6 feet to 15.3 feet, the very dense till had many boulders, and bedrock was encountered at 15.3 feet. Coring was accomplished to 30 feet bgs. Due to adverse drilling conditions, only one of the three monitoring wells proposed by Exeter Environmental, Inc. was completed. The site is in a hilly, glacial till area of single family homes, with on-site septic systems and private wells. The surrounding receptors most at risk due to this release are the Trask's own drinking water well, and indoor air at the residence itself. Immediate Response Action Immediate Response Actions (IRAs) are required at any site with a two-hour reporting condition (3 10 CMR 40.0412(1)). A verbal IRA Plan approval was received by SRT from Mr. Victor Fonkeim of your office (DEP) on August 15, 2001. The approved IRA Plan consisted of the excavation of affected soils up to 150 cubic yards, and the de-watering and on-site storage of groundwater up to 50,000 gallons, if deemed necessary. Should groundwater treatment and discharge be required, an EPA NPDES Permit would be required. SRT was formally retained on August 22, 2001. The monitoring well and drinking water well were sampled by SRT that same day, August 22, 2001, and sent to AMRO Laboratories for EPA Method 524, VOC, drinking water analyses. Results, included herein as Attachment 3, were Not Detected (ND). The drinking water sample was collected from the well itself after removing the cap, and, after evacuating the well of at least 480 gallons of water(24 gallons per minute(gpm)over 20 minutes). Hand excavation of the room in question began on August 22, 2001, and continued through September 6, 2001. Monitoring during the excavations with a portable photoionization detector (Hnu), calibrated to the benzene standard, showed indoor volatile organic compound levels at 0.5 ppmv in the kitchen on the driveway side of the house, and 0.2 to 0.4 ppmv at the other end of the house above the furnace room. Levels in the garage and cellar area were kept at approximately 1 ppmv with fans constantly ventilating the work area. Follow up Hnu monitoring conducted on October 16, 2001, showed 0.1 to 0.2 ppmv inside the house, virtually the same as outside the house, but with the garage door open. SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 Trask IRAP,N Andover • RTN 3-20874 Oct. 17,2001 SRT conducted 24 electric drill powered borings throughout the basement and garage areas inside the house on August 23, 2001, and found the contamination to be under the floor outward from the furnace room into the adjacent room and also the adjacent garage. These borings were used to measure trapped vapors beneath the floor with the Hnu. Locations and affected areas are delineated on the site plan, Figure 1. Levels in uncontaminated areas were at or very close to 0 ppmv, and ranged from 15 ppmv to 80 ppmv in contaminated areas. These areas were excavated. Two of these borings were attempted at the corners of the building outside the furnace room. (P-1, and P-2). P-1 went to approximately 6.5 feet where refusal was encountered, and a soil gas vapor probe monitoring point was installed at that depth, which is at the approximate elevation of the foundation footing. No vapors were detected in P-1. P-2 encountered refusal at two feet and was not further evaluated. Approximately 60 cubic yards of contaminated soils were stockpiled on in a paved parking area, over and under poly cover. Progress was very slow because the underlying glacial till is so dense it has to be jack hammered, and, it also contains numerous, relatively large, rocks. SRT,separated the furnace room into grids, as follows: Outside wall H M K G J F L I Outside garage cellar wall Headspace screening was conducted at every foot of depth during the excavation with composite soil samples taken from each of the grids(during excavation, only six grids were used, excluding L and M; this eight square grid was used for sidewall contamination screening and testing'conducted on Oct. 16, 2001). In the top four feet, Hnu readings ranged from 45 to 70 ppmv. At five feet, the range increased to 60— 120 ppmv. From 6.6 feet to 8 feet the range returned to 13 to 70 ppmv. At 9 feet, 6 to 45 ppmv, and at 10 feet, the range reduced drastically to 5 ppmv and below. Several small shelves were excavated in the garage. The deepest at 5 feet under the interior wall, and two to three feet deep for another shelf five or six feet into the garage. All Hnu readings from soils not removed from this section of the excavation ranged from 2 to 6 ppmv. It appears that the original oil spill traveled fastest in the sand underlying the cement floor, and then leached straight down until completely dissipated at 10 feet or less bgs. SUBSURFACE REMEDIATION TECHNOLOGIES, INC. ' 355 Central Street • Rowley, Massachusetts 01969 i Trask IRAP,N Andover RTN 3-20874 Oct. 17,2001 On September 13, 2001, SRT collected bottom and sidewall samples from the extent of the excavation and submitted them to AMRO Environmental Laboratories of Merrimack, NH for VPH/EPH analysis. Results are summarized on the attached Table 1, with laboratory reports included as Attachment 4. "A bottom" is the bottom of the five-foot shelf under the interior wall between the furnace room and the garage. Exceedances to appropriate standards are bold printed in the table. Because the sidewall samples were composited over the entire 10 foot depth, SRT returned on Oct. 2, 2001, and collected a 0 —5 foot composite, and a 5 - 10 foot composite, which showed most of the exceedances are in the 0— 5 foot range, with only a slight exceedance in the 5 —10 foot range. On Oct. 16, 2001, SRT collected 8 sidewall samples in the 5 — 10 foot depth range, corresponding to the above shown grid pattern, to isolate the offending areas. Sidewall composites from F, G, H, I, and L showed headspace readings of 0.5 to 2 ppmv with the Hnu, and were composited again for laboratory EPH. Sidewall composites for J and K 50 ppmv in the headspace, and M read 25 ppmv. These three were also composited again for EPH analysis. SRT is planning the excavation of the offending sidewalls in the 5 — 10 foot depth range to attain levels below MCP Method 1 standards on October 18, 2001. When it can be shown that the 5 to 10 foot range meets MCP Method 1 Standards, that depth will be backfilled and compacted. A structural evaluation will be necessary to evaluate the feasibility of removing the contaminated soils in the sidewalls, and under the foundation, in the 0 to 5 foot range. In order to provide the residents of the home their parking area, SRT removed the existing stockpile of contaminated soil to Brox Industries of Dracut, Massachusetts for recycling on Sept. 20, 2001. 90.36 tons were transported under a Bill of Lading that has not yet been closed. Two borings and two monitoring well installations were conducted on September 5 through 10, 2001, outside the affected corners of the house as shown on Figure 1. Since drilling water was introduced into the borings for rock coring, the wells were repeatedly bailed over several weeks to effect ambient groundwater conditions. Boring Logs and monitoring well installation details are appended as Attachment 2. On October 2, an elevation survey was conducted, as well as the bailing and sampling of the two new monitoring wells and the drinking water well. The drinking water well was allowed to run for twenty minutes at approximately 24 gpm, and sampled from the well itself, as in the first testing round. The monitoring wells were bailed of at least three times their water volume, and groundwater samples were appropriately collected, preserved, and delivered to the laboratory for analysis by EPA Method 524, for Volatile Organic Compounds. MW-3, was not sampled until Oct. 3, 2001 because it did not recharge, and had still not completely recharged when sampled the next day. Results, appended in Attachment 3, were all below the detection limit of 0.5 µg/L, or parts per billion(ppb). ' A SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 c Trask HUP,N Andover RTN 3-20874 Oct. 17, 2001 Critical Exposure Pathways SRT has determined that vapor phase hydrocarbons in indoor air, and the on-site drinking water well, present the Critical Exposure Pathway concerns relating to this release. Fans have been on in the cellar continuously since the release occurred. Monitoring has been accomplished inside the living quarters and in the cellar area showing very low vapors, even while the worst of the contamination was being manually removed. The extent of the release vertically has been found and it is still approximately 24 feet above the groundwater table in that area. The drinking water well has not shown any effect whatsoever after two rounds of testing. Monitoring wells located relatively close to the spill area do not show any trace of the contamination. The remaining IRA Plan work will be focused on the removal of contaminated soil under the walls and foundation walls of the building to completely remove the threat to indoor air. SRT does not believe at this time that the drinking water well remains a threat of any kind. Further evaluation of groundwater flow will be conducted to determine if the installed monitoring wells are appropriately located. Imminent Hazard/Substantial Release Migration As previously stated, the only threat of exposure to human and /or environmental receptors resulting from this release are the residual contaminant levels remaining around the sidewalls of the existing excavation, in hard to reach areas. Although the drinking water well could have been at risk, the relatively deep groundwater, in extremely impervious soil, has contained the contamination to the upper ten feet of soil beneath the furnace room. Hnu levels and analytical levels of contaminants at the 10 foot level indicate that the forward edge of the plume has been removed some 24 feet above the groundwater table. All of the hot spots have been removed (over 50 ppmv headspace readings), nothing has reached the groundwater from information available today, no further migration or leaching can be expected, and the remaining threat to indoor air should be removed well within one year of its release. None of these conditions are present at the subject site. IRA Plan The original verbal IRA Plan of 150 cubic yards of contaminated soil removal should be more than enough to complete the project. Groundwater pumping or collection will not be necessary. SRT will excavate the offending corner in the 5 — 10 foot range and, upon laboratory confirmation, backfill and compact to the five foot level. After consultation with a structural engineer, the remaining contaminated soil under foundation walls, and interior walls, will be removed and recycled appropriately. Groundwater flow direction will be further determined, and monitoring of the groundwater will continue to completion. SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 Trask IRAP,N Andover RTN 3-20874 Oct. 17,2001 Please contact the undersigned ifY dli Lve any questions regarding the attached Immediate Response Action Plan. Sincerely, Subsurface Remediation Technologies, Inc. Timothy A Toomey LSP/ G President Enclosures cc: Town of North Andover BOH Town of North Andover Chief Municipal Officer Mr. & Mrs. Robert Trask SUBSURFACE REMEDIATION TECHNOLOGIES, INC. ` 355 Central Street • Rowley, Massachusetts 01969 Driveway I MW-3 I 1 15-80 ppm vapors beneath floor �2 Furnace Room I • J MW-2 Stockpiled Soil • • • Release/ I MW-1 • $- Soil Rei ioval Area Garage • I ,� a RASK RESIDENCE I 04 I I � BASEMENT LEVEL AREA 0. I I I I I I Drinking water well I O I I I I I I BOXFORD STREET LEGEND Bar Scale(in feet): SITE MAP/IRA Removal Area N Sample Powered hand auger gas probe borings 0 10 20 312 Boxford Street-Trask Property Location SRT NORTH ANDOVER, MASSACHUSETTS Geoprobe Location Scale: NA-sketch SUBSURFACE REMEDIATION - Monitoring Well (conducted by SRT) Date: 10/17/01 TECHNOLOGIES,INC. Monitoring Well Drn B 355 CENTRAL STREET AST Location y ROWLEY, MA. 01969 X Release Point 0 Sob 948-3861 FIGURE 1 hole in feed line Ck By: ( ) 4 PAGE 1 OF 1 f SOIL SAMPLES Boring/ Soil Reg. EXTRACTABLE&VOLA TII EPETAOL at headspace Sampling Sample SolVG1V k9-C18 C19-C36 Cll-C22 ( Xylenes sample Notes Location Date Depth category** aliphatics aliphatics aromatics slip❑e Anu/OVA FGH 9/13/01 0'-10' S1-GW1 330 120 120 p 0.71 10 i HK 9/13/01 0'-10' S1-GW1 ' 1800 330 500 1 40 Acenahthene=1.6 p 99 IJK 9/13/01 0'-10' S1-GW1 1700 330 430 14.5 45 13.6 40 :Acena hthene-1.4 * - - p FI 9/13/01 0'10' SI GW1 3600 540 760 i Bottom 9/13/01 10' SI-GWI 62 ND ND r ND 5 Acenaphthene=7.1* ABottom 9/13/01 5' S1-GW1 110 ND ND l ND 4 ASidewalls 9/13/01 0'-4' S1-GW1 4300 720 920 p 12 40 Acenaphthene=7.8* FGMJK 10/2/01 0'-5' S1-GW1 2800 690 1100 10.2 45 Acenaphthene=1.9* FGHIJK 10/2/01 5'-10' S1-GWI 640 230 380 0.37 30 ... ...................................... ........ < c: Slfir�aBosc:sfElcf:afanda�cd:fi»sEfe::>::>:::i::>: � ............... ...... 56U:.; ......::::::::::::::::::::::::::::::::::::::::.::::::::::::::::.:::::::::::::::::::::::::::::::::::::::::::::::::::.:::::::::::::::: .:::.............'.::::: . ....:.:.::::::::....:::::::::..:...:._::::::::::::::::.::::::::::::::.::::::::::::::::::::::::::::::::::::::::::::::.::::::.::::::. .::.:::::. .. ........................................... ......................................................... d:G...:. :.....>::>::::>::::>.:: Se :::::::: .:. P U>:»:: bQ9:D6:>: »:> ITP&? 7i»#Es > >''> ' t'G 'E'Aa<;'>;';;y:.;:.;:,;, tld.;>5 09Ak>.:::::..:::::::::::::::::::::::::::::.::::::::::::::::::::::::::::::::::::::::::::.::::::::::::::::::::::::::::::::::::::::::::. .. :Yg:: : ......:..............�......:. ..:..:::::.:::::::::::.:.::::::.:::::::::::::::::::::::::: ::::::::::::::::::::.::.::::.:::.:::::::. ::::i::i::�". ..:::::::::.:::::::::::::: ::::i:< ::::::::::'' ::::.....0. ......::i::::i:........................ ;:i::::::::::::>':::.... ::::i;:i::::: i::::i ::>::::::i::i::::i:::2:::i:: iG3Y.2Area.......... ...... DSO...... ue .................................................................................................................................. 1.G1?Y.3Ar�a:;:;:;:;:;2 Ui;:<: <S Q9D::>::>:� 'Q:::>::...............:......::..:::.:::.::..::..::..:...:: :.::::.::.:::..::.:._:::::::::::::::::::::::::::::::::::::::::::::::::. r>:;::>:::>:>:>>:>: :::::::::::..::::.::::::: ..:::::::: :::::::::8.::. ... DEI?:. . a.......................................................................................................................... S3:Idm#s:»:<::::> »:>:lQWW Arra:;:>:>:>:>:S'�OP:> 509Q:> .::.. .......................................................................................................................... s:>:>:>:: :. ..............................1GY Area.:::::::...rsX119......5tldQ:::::.506U::: 5:::::.::::::::::::::::: :::::::::::::::::::::::::::::.:_:::::::::::::::::::::::::::::::::::::::::::::: . :::. is is...........>::c:::z>:;:;:i:: d► 2S NOTES: ND-Compound not detected above the minimum S-1 through S-3 Soil St concentration limit or method detection limit of MCP. Applicable coi the particular analytical procedure(See Analytical CMR 40.0975(6)(a, Report). GW-1 Standards-Drin TABLE 1 >-Indicates the detection limit GW-2 Standards-Regi NS-Not Sampled for Particular Chemical and where groundwat Bold/Italic print indicate values over MCP limits. surface. GW-3 Standards-Regi areas are subject to i ATTACHMENT 1 �, Bureau husetts Department of Environmental Protection BWSC-105 ff Waste Site Cleanup Release Tracking Number IMMEDIATE RESPONSE ACTION (IRA) TRANSMITTAL 0_ 20874 FORA Pursuant to 310 CAR 40.0424-40.0427(Subpaft Dj' I A. RELEASE OR THREAT OF RELEASEResidence 44 �R s idOCATI N. Release Name:(optio,a) street: 312 Boxford Stieet Location Aid: C'yrro rax ?North Andover ZIP Code: 01845 ❑ Check here if a Tier Classification Submi"al has been provided to DEP for this Release Tr ckin;Number. ❑ Check here if Lhis location is Adequately Regu!o ed,pws:.•ant to 310 CIJ,.R-3.0110.0114 Specify Program: ❑ CERCLA ❑ HS11VA Cone:in e Action ❑ Sol,-.d Waste Management ❑ RCRA State Program(2t C Facilities) Related Release Tracking Numbers That This IRA Addresses: B.THIS FORM IS BEING USED TO: (check all that app!.•) Submit an IRA Plan(complete Sections A.B,C,D.E,H.I,J and i). ❑ Check here i!this IRA Plan is an update or An'ia,.ion of a previousy approved vrrilen IRA Plan. Date Subrnhed: ❑ Sub.nit an Imminent Hazard Evaluation(complete Sections A.B,C,F.H.I,J and I). 1-1 Submit an IRA Status Report(=mple.e Sections A.B.C.E.H.1,J and Mir. 17 Submit a Request to Terminate an Active Remedial System and/or Terminate a Continuing Response Action(s)Taken to Address an Imminent Hazard(complete Sections A,B.C.D.E,H,1,J and f4. Submit an IRA Completion Statement(complete Sections A,B.C.D,E.G,H,1•J and K). You must attach all supporting documentation required for each use of form indicated,including copies of any Legal Notices and Notices to Public Officials required by 310 CIJR 40.1400. C. RELEASE OR THREAT OF RELEASE CONDITIONS THAT WARRANT IRA: Identify I.Wla and Receptors Affected: (check all 111--at ap;!r) XX Air ❑ Groundwaer ❑ Surface Water E] Sedirien'.s 1.X Soil ❑ Wetland ❑ Storm Drain ❑ Paved Surface 1 Private Well ❑ Public Water Supply ❑ Zone 2 Q. Residence ❑ School ❑ Uni=wn ❑ Other Specify. Spill o c c u r e d within 100 feet Dr i v a t e well Identify Conditions That Require IRA,Pursuant to 310 CIJ,R 40.0:12: (check alt that app!.•) 2 Hour Rego ting Condi ions) ❑ 72 Hour Reporting Condition(s) ❑ Substsntial Release!✓ig*ation ❑ Other Condi:icn(s) Describe: Identify Oils and Hazardous Materials Released: (check all that app.) ( Oils ❑ Chlorinated So!ven:s ❑ Heavy 1t4e:a15 ❑ Others Specify. D. DESCRIPTION OF RESPONSE ACTIONS: (check all that appy.) ❑ Assessment and/or l&-iftoring Only ❑ Deployment of Absoruent or Containment IJateria!s iX Excavation of Contaminated Soils Tempora..Covers or Caps © Re-use,Recy.,fung or Treatment ❑ Bioremation 0 On She at Off Site Est.Vol.:' 15 0 _cubic yards ❑ Sea Vapor Extraction Describe: pcs disposal at recycling facility Structure Venting System ❑ Store O On Site O Off Site Est Vol.: cubic yards ❑ Product or NAPL Recovery ❑ Landfill O Cover O Disposal Est'Vol" cubic yards ❑ Groundwater Treatment Systems Removal of Drums.Tanks or Containers ❑ Air Sparging Descnbe: ❑ Temporary Water Supplies SECTION 0 IS CONTINUED ON THE NEXT PAGE Revised 2124GS Supersedes Forms BWSC=005,DOS,010(In part)and 011 Page 1 of 3 M Mnl d Haw Tlwe Amin i I f _ Massachusetts Department of Environmental Protection BWSC-105 i r • .. DJCE'2U Of 111=c",1 cafe Cle=nup Release Track-rig Number ;K IP, MEDIATE RESPONSE ACTION (IRA) TRANSMITTAL ' FOR(,d Pursuant to 310 CM.R 40.0424- 0.042 (Subpart D),. �3 ' 20874 D. DESCRIPTION OF RESPONSE ACTIONS(continued): U Removal of Other Con.'zmirz e:hem, Te-poraryE�acu�ion or Relozation of Residents Specify Type and Volume: 1 d r!im o i 1 r)abxr i c Fencing and Sign Posting OtM-a Response Actions �'-n'�: —n a t-a n t i a l o 17 Check here if this IRA involves the ase of lnno-.atioe T echnolories"DEP is interested in:.sing this info:nation to aid in creating an Innovative Technologies Clearingho:.se). Dmribe Technologies: E. TRANSPORT OF REh4ED1ATION V%'ASTE: (if Remed'a ion V'as'e has been sent to an c f-site facility,ans•,er the following questions) gameRFace y. - none tO- 04-o to Town and State: Ovantity of Remediation 1Nasle Transpofled to Cate:�• F. IMMINENT HAZARD EVALUATION SUTAtIA,ARY: (check one of the followin;,) Based upon an evaluation,an Imminent exists in connection v4uh this Release or Thte t of Release. Based upon an evaluation,an imminent Hazard does nit exist in connection vrh this Release or Threat of Release. J� Eased upon an e�alurtion,it is unknown wf-rether an Imminent Hazard exists in conntezl ion v.Ih This Release or Threat of Release,and further assessment activities will be undertaken. Based upon an evaluation,it is unknown whether an Imminent X"ard exists in connection w th this Release or Threat of Release. However, response actions v4ll address ftse condtions that could pose an Imminent Hazard. G. IRA COMPLETION STATEMENT: 17 Check here ff future response 2--lions addressing this Release or Threw of Release will be conduce ed as part of the Resp:,nse Actions planned for a Site that has already been Tier Classified under a d;iferenl Release Tracking Number,or a Ste that is identified on the Trans:ion List as described in 310 CIA,R 40.0300(.e.,a Transeion She,which inclj, es Sees Yth approved Waivers). These adds Tonal response actions must occur acoordiny to the deadlines applicable tc the earlier Release Tracking Number(.e.,See 10 Number). State Release Tracking Number(,e.,She ID Number)of Tier Classified See or Transition Sive: If any Remediation Waste will be stored,treated,managed,recycled or reused at the site following submission of the IRA Completion Statement,you must submit either a Release Abatement Measure(RAN,)Plan or a Phase N Remedy Implen•entation Flan,along with the appropriate transmittal form,as an attachment to the IRA Completion Statement H. LSP OPINION: 1 a"est under the pains and penalties of perjury that I hay*personally examined aid am familiar with this Lansmit"tal form,including any and all documents ac companyin;this submhal. In my professional opinion and Judgment based upon application of n the standard of care in 306 CMR 4.02(1),(ii)the applicable provisions of 306 CMR 4.02(2)and(3),and u: the provisions of 306 CMR 4.03;5),to the best of my knov.edge, information and belief, > b Section B of this form indcafes that an Immediate Response Action Plan is being submi.".ed,the response actions)that is(are)the subject of I his submittal n has(have)been developed in accordance v&h t1he ap;rauble provisions of fA,.G.L.c.21 E and 310 CMR 40.0000, u)is(are) appropriate and reasonable to accomplish the purposes of such response actim(s)as set forth in the applicable provisions of 1A.G.L.e.21 E and 310 CIA,R 40.00t00 andw complies(y)with the identified provisions of at orders,perm s,and appro%als identified in this submtU; > if SecSon B of this form indcates that an Imminent Hazard Evaluation is being submi"ed,this Imminent Hazard Evaluation was developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CIJR 40.0000,and the assessment acth y(es)undertaken to support this Imminent Hazard Evaluation complies(y)with the applicable provisions of M.G.L.e.21 E and 310 CtAtR 40.0000; > Q Section B of this form indcates that an Immediate Response Status Report is being submitted,the response action(s)that is(are)the subject of this submittal n is(are)being implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CZAR 40.0000, a is(are) appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the apprrcabte provisions of M.G.L.e.21 E and 310 CN,R 40.0000 andur complies(y)with the identified provisions of all orders,permits,and approvals identified in this submittal; > it SecSon B of this form indcates Mat an Immediate Response Action Completion Statement ora Request to Terminate an Active Remedial System and/or.Terminate a Continuing Response Action(s)Taken to Address an Imminent Hazard is being submitted,the response action(s) that is(are)the subject of this submittal n has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.e.21 E and 310 CMR 40.0000, a is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and nr compriesM with the identified provisions of all orders,permits,and approvals identified in this submktaL SECTION H IS CONTINUED ON THE NEXT PAGE Revised 224% Supersedes Forms BWSC-005,006, 010(in pari)and 011 Page 2 of 3 M NAJ AXtar Th;e Fnrrn. Massachusetts Department of Environmental Protection BWSC-105 Bureau of Waste Site Cleanup Release Tracking Number IMMEDIATE RESPONSE ACTION (IRA) 3 -) 20874 TRANSMITTAL FORM Pursuant to 310 CMR 40.0424-40.0427(Subpart D) H. LSP Opinion(continued): 1 am awe that significant penalties may result,including,but not limited to,possible fires and imprisonment,if 1 submit information which I know to be faiee.Inaccurate or materially incomplete. Chadic here it the Response Actions)on which this opinion is based.-if any,are(were)subject to any order(s),perfnk(s)and/or approva(s)issued by DEP or EPA. If the boot is checked,you MUST attach a statement identifying the applicable previsions the LTH OF LSPName: Timothy A. Toomey LSP x: 2891 Stamp: 0�� ass Telephone: (9 7 8) 948-3861 Ext.: T1Mp rHy 9�sN FAX(conal) No 68ey - pti C 91 SIW*h+e' STEP�O Q.. Data: t /Z O/ FPROFESS 1. PERSON UNDERTAKING IRA: Name of organization: Trask Residence Name of Contact Deborah Trask Title: owner Street: 312 Boxford Street Ctyfrown: North Andover State: MA ZIP Code: 01845 Te+ephae: (978) 557-1147 Ext.: FAX:(optional) Check hero if there has been a change in the person undertaking the IRA. J. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING IRA: (check one) ® RP or PRP Specify: C owner O Operator 0 Generator 0 Transporter Other RP or PRP: _ E] Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21E,s.2) Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) Any Other Person Undertaking IRA Specify Relationship: K. CERTIFICATION OF PERSON UNDERTAKING IRA: 1, Deborah Trask ,attest under the pains and penalties of perjury(i)that I have personally examined and am farmer with the Moan ation contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,be on my inquiry d these Individuals knrnedistaly resporuible for obtaining the information,the material information contained in this submittal is,to the best of my ionowledge and belief,true,accurate and complete,and(iii)that I am fully authorized to make this attestation on behalf of the entity bgalty responsible for pis submltit. IRM person or entity on whose behalf this submittal is made arta awarethat there are significant penalties,including,but not limited to, poaeli- and Imprisormmfor wWtL*y submitting false,inaccurate,or incomplete information. �Jw Title: Owner For. Trask Residence Date: 10 7 Z01- (print name of person or witty recorded in Section 1) Enter sddrsss at the person pmvideng certifiicsoon,if different from address recorded in Section 1: Street CWrown: State: ZIP Code: Telephone: Ext.: FAX.(optional) YOU MUST COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Revised 2r24o95 Supersedes Forms BWSC-005, o06, o1 o(in part)and 011 Page 3 of 3 Do Not Alter This Form Y, I ATTACHMENT 2 v EXETER ENVIRONMENTAL ASSOCIATES, INC. Test Boring Log P.O. Box 451, Exeter, NH 03833 (603) 778-3988 Boring Number MW-1 Pr 'ed Trask property,312 Boxford Street,North Andover,MA Sheet No. 1 of 2 Cr�errt Insurance Company ect No. 1294.13 BoringContractor NH Boring Casing Elevation NA Location see Figure 2 Ground Elevation NA Well Construction D - ate 8-1 3 to 8 14 201 Screen Length10' 30.2-20.2 T of Bentonite 14.0; Driller Bob Doherty Top of Sand 17.0 Standpipe: flush mount Inspector Tim Warr Sample Sample Descriptions Well VOC No. Blow Count and Classification Const. Remarks (ppm) NA 0-0.3 Asphalt. " 1 S-1 Brown, Gravelly fine to coarse Sand, " Bkg little Silt. Dry. 2 2"PVC riser pipe 3 " 4 5 S-2 16 Very Dense, brown, Gravelly fine to Bkg 52 coarse Sand,little Silt. Dry. Till. native back fill 6 100/3" 7 " cored through boulder from 6.5-9.0 feet 8 9 S-3 Very Dense, brown, Silty fine to coarse Bk 10 56 Sand, little fine to coarse Gravel. Dry. Till. �^ g 76 11 78 12 13 14 15 S-4 103/3" No recovery. 16 C-1 9 min bentonite seal Cored from 15.5-21.0. Highly fractured 4 min Diorite. Took 7 runs to get to 21 feet. 17 High angle fractures present. 3 min ROD=0%. 18 Minor iron staining on fracture faces. 19 3 min 20 5 min 21 C-2Y 5 min 21.0-25.5. Competent Diorite. r 22 Weathered fracture at 23.1 feet. 6 min ROD=93%. 2"PVC well screen 23 6 min `` measured water EXETER ENVIRONMENTAL ASSOCIATES, INC. Test Boring Log P.O. Box 451, Exeter, NH 03833 (603) 778-3988 Boring Number MW-1 Project Trask property,312 Boxford Street,North Andover,MA Sheet No. 2 of 2 Client Safety Insurance CompanyProject No. 1294.13 Boring Contractor NH Boring Casing Elevation NA Location see Rgure 2 Ground Elevation NA Well Construction Date 8-13 to 8-14, 201 Screen Len 10' 30.2-20.2 To of Bentonite 14.0 Driller Bob Dohertv Top of Sand 17.0 Standpipe: flush mount Inspector Tim Warr t Sample Sample Descriptions Well VOC No. Blow Count and Classification Const Remarks (ppm) 25 C-3 6 min Diorite from 25.55 to 27.5. ROD=90%. silica sand X. 26 Quartz vein: 27.5 to 30.2. ROD=50%. 6 min Vertical fractures in quartz with minor 27 minerlization. 2" PVC well screen 5 min 28 9 min 29 8 min 30 31 I 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 v SUBSURFACE REMEDIATION TECHNOLOGIES,INC. Page: 1 355 Central Street, Rowley, MA.01969 Boring No. MW-2 508 948-3861 SRT Job No. 235 Project Name: IRA Assessment-Trask Property Well Elevation: 100.41 arb. Client Name: Deborah Trask Well Elevation: George Boring Location: 312 Boxford Street North Andover jSRTGeoIogist Toomey Drilling Contractor: Soil Exploration IStart Date: 9/5/01 Drilling Method: HOLLOW STEM AUGER/Coreing CasinglAuger Size: I Date End: 9/6/01 Standard Sampler: Unless noted,sampler consists of a 2"split-spoon driven using a D SAMPLE Penetration 140 Ib hammer falling 30 in. N E Type Range Test Casing: Unless noted,casing driven using 300 ib hammer falling 24 in. O Well P & From Headspace Strata Field Classification T Diagram T No. I Blows per 6" Pen Rec OVA Change and E H To on split-spoon (in) (in) Reading Depth Drilling Information S (ppm) S-1 0 Tan very dense silty SAND&GRAVEL 7 some boulders TILL 5 S-2 5 1 SAME 10' 10 SS-3 15 35 120 7 SAME 16 20' SS-4 25 42 120 0 SAME 26 I 30' SS-5 30 38 120 0 SAME 31 40' End of Exploration 0 39 GRANULAR SOILS COHESWE SOILS NOTES: Blows/Ft Density Blows/Ft Density Screen at 29 to 39 feet 0-4 v.loose<2 v. soft 0.010 slot 2"PVC screen 4 - 10 loose 2-4 soft Bentonite seal at 25'to 27' 10 - 30 m.dense 4-8 m. stiff Roadbox-1.5 concrete approx 1 foot diameter 30 - 50 dense 8- 15 stiff GROUNDWATER READINGS SRT > 50 v.dense 15 - 30 v. stiff DATE TIME WATER AT CASING AT STABILIZATION BORING > 30 hard 6-Sep 33 ves NUMBER OA/OC CHECKED BY: 16-Octj 1 37.621 1yes MW-2 SUBSURFACE REMEDIATION TECHNOLOGIES,INC. Page: 1 355 Central Street,Rowley, MA.01969 Boring No. MW-3 508 948-3861 SRT Job No. 235 Project Name: IRA Assessment-Trask Property Well Elevation: 100.00 arb. Client Name: Deborah Trask Well Elevation: George Boring Location: 312 Boxford Street North Andover 1SRTGeologist Toomey Drilling Contractor: Soil Exploration IStart Date: 9/7/01 Drilling Method: HOLLOW STEM AUGER/Coreing Casing/Auger Size: jDate End: 9/10/01 Standard Sampler: Unless noted,sampler consists of a 2"split-spoon driven using a D SAMPLE Penetration 140 Ib hammer falling 30 in. N EjNo ange Test Casing: Unless noted,casing driven using 300 Ib hammer falling24 in. O Well Prom Headspace Strata Field Classification T Diagram T1 Blows per 6" Pen Rec OVA Change and E HTO on split-spoon (in) (in) Reading Depth Drilling Information S (Ppm) 0 Tan very dense silty SAND&GRAVEL 0 some boulders TILL 5 5 0 SAME 10' 10 SS-3 10 0 SAME 15 0 SAME NX1 17.5 Boulder 18.4 20' Till SS-4 25 120 no recovery 25.3 28 NX2 28 top of rock ® 28.0' 30' Granitic Gneiss 32 its. 1" to 1', some along foliation planes NX3 32 100%Recovery on all runs jts./foliation planes very tight 36 NX4 36 SAME 40' 41 NX5 41 43 End of Exploration @ 39 GRANULAR SOILS COHESIVE SOILS NOTES: Blows/Ft Density Blows/Ft Density Screen at 33 to 43 feet 0-4 v.loose<2 v. soft 0.010 slot 2"PVC screen 4- 10 loose 2-4 soft Bentonite seal at 28' to 31' 10- 30 m.dense 4-8 m. stiff Roadbox-1.5 concrete approx 1 foot diameter 30- 50 dense 8- 15 stiff GROUNDWATER READINGS SRT > 50 v.dense 15 - 30 v. stiff DATE TIME WATER AT CASING AT STABILIZATION BORING > 30 hard 10-Sep 23 no NUMBER OA/OC CHECKED BY: 11-2e 31.78 no MW-3 16-Oct 34.46 yes I ATTACHMENT 3 Y OCT.17.2001 2:52PM NO.737 P.5 Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO Environm ntal Laboratories Corporation LAB#:01100072-03 JOB NAME:Trask Residence JOB#:0110043 LOCATION:NIA SAMPLE IDENTITY: Drinking V later Well CONTROL#: 38651 DATE SAMPLED:10/02/01 DATE RECD:10/05/01 DATE ANALYZED:10/11/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER, (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROSENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUEN E BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DISROMO-3-CHLOROPRO' ANE BOL 0.5 1,2-DISROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BOL 0.5 1,1-DICHLOROETHANE BOL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BOL 0.5 CIS-1,2-DICHLOROETHENE BOL 0.5 TRANS-1,2•DICHLOROETHEMI BDL 0.5 1,2-DICHLOROPROPANE BOL 0.5 1,3-DICHLOROPROPANE BOL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-QICHLOROPROPENE BDL 0,5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROP NE BDL 0.5 ETHYLSENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1.2.2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BOL 0,5 TOLUENE BDL 0.5 CONTINUED;1 OF 2 PAGES Y OCT.17.2001 2:52PM NO.737 P.6 Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO Environmlater tal Laboratories Corporation LAB#:01100072-03 JOB NAME:Trask Residence LOCATION:N/A SAMPLE IDENTITY: Drinking Well CONTROL M 38651 DATE SAMPLED:10/02/01 DATE RECD:10/05/01 DATE ANALYZED: 10/11/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2.3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL E HER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLSENZENE BDL 0.5 tart-BUTYLSENZENE BDL 0.5 ISOPROPYLBI=NZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROSENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 Di-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUM ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD OCT.17.2001 2:50PM NO.737 P.1 Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO EnVironme ntal Laboratories Corporation LABM 01100072-01 JOB NAME:Trask Residence JOB 9:0110043 LOCATION:WA SAMPLE IDENTITY: MW-2 CONTROL#: 38651 DATE SAMPLED:10/02/01 DATE REC'D: 10/05/01 DATE ANALYZED:10/11/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DISROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPRO ANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0-5 TRANS-I,2-DICHLOROETHEN BDL 0.5 1,2-DICHLOROPROPANE SOL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-0ICHLOROPROPANE BDL 0.5 1,1-DiCHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPE E BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 i,1,1,2-TETRACHLOROETHANE BDL 0.5 1.1,2,2.TETRACKLOROETHAN E BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED:1 OF 2 PAGES rI . OCT.17.2001 2:51PM NO.737 P.2 Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO Environmc ntal Laboratories Corporation LABA 01100072-01 JOB NAME:Trask Residence LOCATION:N/A SAMPLE IDENTITY: MW-2 CONTROL M 38651 DATE SAMPLED:10/02/01 DATE RECD: 10/05/01 DATE ANALYZED:10/11/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UGIL) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL E7 HER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROSENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BOL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUM ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD (�l�u, 3 OCT.17.2001 2:51PM NO.737 P.3 i Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER AMRO Environmf ntal Laboratories Corporation LABM 01100072-02 JOB NAME:Trask Residence JOB#0110043 LOCATION:N/A SAMPLE IDENTITY: MW-3 CONTROL M 38651 DATE SAMPLED:10/02101 DATE RECD:10/05101 DATE ANALYZED:10/11/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROM ETHANE BDLL, 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM SOL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPRO ANE SOL 0.5 1,2-DISROMOETHANE BDL 0.5 DISROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMET E BDL 0.5 1,1-DICHLOROETHAN E BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-0ICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHEME BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROP NE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROET E BDL 0.5 1,1,2.2-TETRACHLOROETFW E SDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED:1 OF 2 PAGES i OCT.17.2001 2:52PM NO.737 P.4 ChemServe VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO EnvironmE Mal Laboratories Corporation LAB#:01100072-02 JOB NAME:Trask Residence LOCATION:NIA SAMPLE IDENTITY: MW-3 CONTROL#: 38651 DATE SAMPLED:10/02/01 DATE RECO:10/05/01 DATE ANALYZED:10/11/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL E HER BDL 0.5 CARBON DISULFIDE 8DL 0.5 n-BUTYLSENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BOL 0.5 n-PROPYLBENZENE BDL 0.5 1.2,3-TRICHLOROSENZENE BDL 0.5 1,2,4-TRI CHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLSEN7ENE BOL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTAOIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL-BELOW DETECTION LIMIT ANALYZED BY:TO OCT.17.2001 2:53PM NO.737 P.7 CHEMSERVE VOA SPIKE RECOVERY FORM EPA METHOD 524.2 CUSTOMER:AMRO Environmental Laboratorles Corporation LAB#01100072 JOB NAME:Trask Residenoe LOCATION:NIA SAMPLE IDENTITY:MATRIX SPIK 01100086-02 CONTROL#: 38651 DATE ANALYZED:10111101 COMPOUND CONC ADDED AMT REC DUP AMT REC %REC DUP%REC RPD (UG/L) (UG/L) (UCIL) 1,1-DICHLOROETHENE 4 4.3 106% BENZENE 4 4.1 103% TRICHLOROETHENE 4 3.7 93% CHLOROBENZENE 4 4.0 100% 1,2-DICHLOROBENZENE 6 3.8 95% 1,3,5-TRIMETHYLSEN2ENE 4 3.8 95% 1,2,4-TRICHLOROSENZENE 4 3.5 88% duplicate not available due to matrix Interference VOA MATRIX SPIKE REC 5 ■CONCADDED 4 I 3 I OLW RECOVERY 2! OLD RECOVERY 11 04 — 1 2 3 4 5 6 7 SPIKE RECOVERY LIMITS 70430% AMRO Environmental Labor,,atories Corporation CHAIN-OF-CUSTODY RECORD40382 Office:(603)424-2022 111 Herrick Street 4 a.*3 8 2 Fax:(603)429-8496 Merrimack,NH 03054 Y Project No.: Project Name: �,r �_ Project Manager: tnRlers fgnatui_.SAMRO Project No.: 31 Project State: Sample ID Date/Time Matrix Total# Analysis Required Remarks Sampled A=Air of Cont. a S=Soil &Size GW=Ground W. 'U y WW=Waste W. w DW=Drinking W. 0=Oil /,D v Other—Specify Oki � Lm4el t✓-Cf l N 'Vis' 0 Preservative: a E(, - NO3,S-H2SO4,Na-NaOH, -Other :.ontamerType: P-Plastic,G-Glass, - is, -Te on,O-Other Please print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will not start until any FAX No.: ambiguities are resolved. Send Results To: S19 WC, C, 3 �5+Cern( Seal Intact? GW-I GW-2 GW-3 Yes No"-N/A MCP Level Needed: ' - Relinquished By Date!Time Received By-' Date/Time P.O.No: PRIORITY TURNAROUND TIME AUTHORIZATION Before submitting samples for expedited TAT,you must have requested Results Need in advance and received a coded TAT AUTHORIZATION NUMBER ` By: -� � AUTHORIZATION No. BY: SHEET OF White:Lab Copy Yellow:Accompanies Report Pink:Client Copy IF ESE = = Environmental zi AMRO Environmental Laboratories Corp. Date: 30-Aug-01 CLIENT: Subsurface Remediation Technologies Project: Trask Residence Work Order Sample Summary Lab Order: 0108217 Date Received: 8/23/01 Lab Sample ID Client Sample ID Collection Date 0108217-01 A Drinking Water Well 8/22/01 0108217-02A Exeter MW 8/22/01 1' � 2 AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 Client: " AMRO 10: QO$a;ZF7 �v J� `_, •^~ Project Name: �[rra sV Date Rec.: `a—QS—O t Snip via: (circle one) Fed Ex.. UPS owner, Date Due: t Hand Del.. Other Courier. Other. Items to be Checked Upon P.eceiet Yes No NA I Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? 3. Custody Seals Intact? 4. Air Bill included in folder if.received? 5. Is COC included with samples? ✓ 6. Is COC signed and dated by client? o 7. Laboratory receipt temperature. TEMP = Samples rec with ice ✓ice`pff'cks_neither 8. Were samples received the same day they were sampled? Is client temperature 4•C ±2'C? ✓ If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC tilled out correctly and completely? 10. Does the info on the COC match the samples? ✓ 11.Were samples rec.within holding time? ✓ 12.Were all samples properly labeled? ✓ 13.Were all samples properly preserved? 14.Were proper sample containers used? ✓ 15.Were all samples received intact?(none broken or leaking) 16.Were VOA vials rec.with no air bubbles? ✓ 17. Were the sample volumes sufficient for requested analysis? ✓ 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH (circle one): M=Methanol, E=EnCore(air-tight container) Sampling Method VOA(circle one): M=Methanol. S6=Sodium Bisulfate, E=EnCore. S=Bulk If M or SB: Does preservative cover the soil? I I If NO then client must be faxed. Does preservation level come dose to the fill line on the vial? If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: ✓ What samples sent: Al l Where sent:C1n_m5e.v-ve- Date: $ Analysis: TAT: —7 21. Information entered into. Internal Tracking Log? ✓ Ory Weight Log? Client Log? Composite Log? ✓ Filtriation Log? Received By: j�Y� Oate: �a3101 Logged in By: NL_w` Oate: �ol2u}!ol Labeled By: LV-x. Date: (o2cf/01 Checked By: Date: 2 4,e_,9 NA= Not Applicable gc/gcmemos/forms/samplerec Rev.18 06/00 AMRO Environmental 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 • (603) 424-2022 Please Circle if: Sample= Soil Sample=Waste I List Preserv. Volume Final volume Preserv. Initial Acceptable? Added by Solution ID t Preservative adjusted Sample ID Analysis I Sample I Listed pH Y or N AMRO of Preserv. Added pH I i I - I I ih I I i I i i i i I I I I pH Checked B�. Date: pH adjusted By: Date: 4 gclgcmemos/forms/samplerec Rev.18 06100 AMRO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORD Office:(603)424-2022 ' 111 Herrick Street 40381 Fax:(603)429-8496 ,. Merrimack,NH 03054 ,. i Project No.: Project Name: T •e Project Manager: Samplers(Si re): AM Project No.: Yrj Project State: e+'�.• �. •..,_. 1 Sample ID Date/Time Matrix Total# 'Analysis:Re'uired �^� ""• Remarks Sampled A=Air of Cont. a ? S=Soil &Size -- " ., GW=Ground W. WW=Waste W. i DW=Drinking W. O=Oil Other—Specify WA(1 01 9 Vol 6 Gt/ . I f1. l ncsr.�.✓c� a tc� 6 G 3vd t LZ h t.v t N'X"o; .�. Q<< G reservatrve: a H,N- NO ,S- Na-NaOH, -Other `! ontamerType: -P antic, - as - to, -Teflon, - ter Please print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will not start until any FAX No.: ambiguities are resolved. Send Results To: * '• ,. . Sea[Intact? GW71GW-2 GW-3 [ Yes No N/A MCP LevelINeeded: elfin uish By Date/Time eived By ate/Time P.O.No: t d G�, PRIORITY TURNAROUND TIME AUTHORIZATION Before submitting samples for expedited TAT,you mint have requested Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER r' / By: AUTHORIZATION No. BY: QA1 -`^ti SHEET OF i 62ZY1Wh . ab Copy ello r Accompani RepgrL..--/ Pink:Client Cop T 317 Elm Street e Milford NH 03055 lerve Tel(603)673-5440 Fax(603)673-0366 August 28, 2001 Ms. Nicole Borduz AMRO Environmental Laboratories Corp 111 Herrick Street Merrimack, NH 03054 -" Job Name: WA Laboratory#: 01080190 Job#: 0108217 Purchase Order#: N/A Location: N/A Control#: 38118 Dear Ms. Borduz Enclosed please find the laboratory results for the above reference samples that were received by the ChemServe sample custodian, under chain of custody control number 38118 on 08/27/01: Samples were collected on 08/22/01. Any abnormalities to the samples on receipt would be noted on the enclosed chain of custody document. This report is not valid without a completed ChemServe chain of custody with the corresponding control number, attached. All samples analyzed by ChemServe are subject to quality standards. These standards are either as stringent or more stringent that those established under 40 CFR Part 136, state certification programs, and corresponding methodologies. ChemServe has written QA/QC Procedures Manual that outlines these standards, and is available, upon request, for your reference. Unless otherwise stated on the Chain of Custody or within the report, all holding times, preservation techniques, container types, and analytical methods are analogous with those outlined by them U.S. EPA. I certify that I have reviewed the above referenced analytical data and state forms, and I have found this report within compliance with the procedures outlined in the ChemServe QA/QC Procedures Manual. Ellen Abrams-QA/QC Manager Jay Chrystal- re i e La ry rato Director This report contains 8 pages. \N ACCpgOq't' a _ Y • t Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-01 JOB NAME: 0108217 JOB#: N/A LOCATION: N/A SAMPLE IDENTITY:01A Drinking Water Well CONTROL#:38118 DATE SAMPLED:08/22/01 DATE REC'D:08/24/01 DATE ANALYZED:08/27/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) i (UG/L)X 1 BENZENE -BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-D IBROMO-3-CHLOROPROPAN E BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHAN E BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED:1 OF 2 PAGES E G Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-01 JOB NAME: 0108217 LOCATION: N/A SAMPLE IDENTITY:01A Drinking Water Well CONTROL#:38118 DATE SAMPLED:08/22/01 DATE RECD:08/24/01 DATE ANALYZED:08/27/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: 1;1,1 TRICHLOROETHANE`" ^-BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZEN E BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD � 3 Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-02 JOB NAME: 0108217 JOB#: N/A LOCATION: N/A SAMPLE IDENTITY:02A Exeter MW CONTROL#:38118 DATE SAMPLED:08/22/01 DATE RECD:08/24/01 DATE ANALYZED:08/27/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE « . •ADL f� ;,,� .. - _ 0.5-, - BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPAN E BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHEN E BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED:1 OF 2 PAGES i Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-02 JOB NAME: 0108217 LOCATION: N/A SAMPLE IDENTITY:02A Exeter MW CONTROL M 38118 DATE SAMPLED:08/22/01 DATE REC'D:08/24/01 DATE ANALYZED:08/27/01 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1.1.1-TRICHLOROETHANE -BDL -. ,,, -..:..k .. - 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZEN E BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD CHEMSERVE VOA SPIKE RECOVERY FORM EPA METHOD 524.2 CUSTOMER:AMRO LAB#:01080190-01 JOB NAME: 0108217 LOCATION: N/A SAMPLE IDENTITY:MATRIX SIPKES 01080169-01 &01080190-01 CONTROL#:38118 DATE ANALYZED:08/27/01 COMPOUND CONC ADDED AMT REC DUP AMT REC %REC DUP%REC %RPD (UG/L) (UG/L) (UG/L) 1,1-DICHLOROETHENE 4 3.3 4.7 83% 118% 9% BENZENE 4 4.8 4.4 120% 110% 2% TRICHLOROETHENE 4- - 4.3 4:0 N :•:1108°k";�. '" " -100% = = 2% CHLOROBENZENE 4 3.6 3.4 90% 85% 1% 1,2-DICHLOROBENZENE 4 4.3 4.0 108% 100% 2% 1,3,5-TRIMETHYLBENZENE 4 3.9 3.7 98% 93% 1% 1,2,4-TRICHLOROBENZENE 4 4.8 4.4 120% .110% 2% VOA MATRIX SPIKE REC 6 5 - 4 - ■CONC ADDED UG/L 3 - 0 L RECOVERY 2 ❑LD RECOVERY 0 = - 1 2 3 4 5 6 7 SPIKE RECOVERY LIMITS 70-130% Chain of custody No. 2 Multiple COC's Yes No 7 �'e/'Ve .317 Elm Street Milford, NH 03055 CHAIN OF CUSTODY (603) 673-5440/Fax (603) 673-0366 CUSTOMER INFORMATION II c SAMPLE INFORMXHON CUSTOMER: ]?!( JOB NAME: TURNAROUND TIME•(CIRCLE ONE:) ADDRESS: JOB NUMBER: STANDARD /RUSH- 7 d..'� a• CITY/STATE/ZIP LOCATION: RUSH T.A.T. (CHECK w/LAB) TELEPHONE: TELEPHONE: AMBER GLASS(AG) / GLASS(G) / PLASTIC(P) 4 REPORT TO: CONTACT: P O NUMBER: QUOTE NUMBER: SAMPLE MATRIX p I SAMPLE IDENTIFICATION&LOCATION COLLECTED CQ TYPE n' SOLIDLIQUID (S) c I'R D � C) COMBINED(C) " o ® ANALYSIS O © © ® IIAZARU(H) O 8 1 a DATE TIME fir G f�tP G DATE TIME )LATE UBE + DATE IImE DATE I mE s DATE ILME DATE LIME DATE nME ® CUSTODY SAMPLER: MILITARY SAMPLE CHECK LIST: FIELD READING(S): TJ (print name) DATE mE RECEIVED WITHIN HOLD TIME &6�OR NO SIGNATURE: RECEIVED IN GOOD CONDITIONS/OR NO TEMPBLAN C ec t-o DATE TJME SHIPPED O HAN ELIVERED RELINQUISHED: SAMPLES WERE PROPERLY PRESERVED YE N N_/A DATE ILME SAMPLES WERE FILTERED IN FIELD B N/A RECEIVED: IF NO EXPLAIN: Q DATE T1mE RELINQUISHED: IImE GROUP# RBIFEIVED FOR LAB: <,I<r `4 5j AI\1RO Environmental Laboratories Corporation CHAIN-0F-CUSTODY RECORD Office:(603)424-2022 111 Herrick Street 41 376 Fax:(603)429-8496 Merrimack,NH 03054 Project No.: Project Name: Q 1 O t7a A Project Manager: Samplers(Signature); AMRO Project No.: Project State:, r Sample ID Date/Time. Matrix Total# Analysis Required IFRemarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. WW=Waste W. DW=Drinking W. !f) - i O=Oil Q U.. Othe—Specify W e. l �► a ✓ 19alo\, :�0 3x�-ic7rltL Wkl\ t Preservative:. -H ,Me f , N—0 S-H2SO4, Na—a -Other ontamer Type: -P ashc, - ass, - to, -Te pn, -Other Please print clearly,legibly and completely.Sampoes can not beNOTES:Preservatives,Special reporting limits,Known Contamination,etc; �0logged in and the turnaround time clock will not start until any FAX No.: Q 4 91— ambiguities are resolved. Send Results To: 2 C t SealIntact? G1V-I GW-2 GW-3 MoSll Yes No N/A MCP Level Needed: Relinquished By Date/Time gceived By Date/Time P.O.No: �►" i !1 rdj(�O ��i� PRIORITY TURNAROUND TIME AUTHORIZATION O �I Before submitting samples for expedited TAT,you must have requested r Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER Ir n—UL 41 If r By: AUTHORIZATION No. BY: SHEET OF White: Lab Copy Yellow:Accompanies Report Pink:Client Copy ?1's.I11 H�l 1 NEW HAMPSHIRE ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM Laboratory:Chemserva.Inc.,317 Elm Street,Millord,NH 03055 16031673-5440 Paye 1 of 4 1:: I Cartilicate Number: 100800-E Date of Issue: June 25,2001 Expiration Date:December 2,2001 •;twat ACCREDITS THE A80VED MENTIONED LABORATORY FOR THE FOLLOWING ANALYSES: &tate of-O,.eW 3'nmp.51)ire DRINKING WATER MICRO DRINKING WATER INORGANIC CONTAMINANTS iCerAa t Mt '�tM1k. Cltbirorunelltat 3Caborntorp ��ureaittttiolt iprograttt � � i�F :'�Y� •K 1 E.Coe Moment SM 9223 B.VV Mldte•N: EPA 300.0 H.to,ott rro Pl.a Com1: SM 921 S a Sulfate. EPA 300.0 "•�' t op •. 1 C� rota coKlw.a: sM 9221 s scalae: EIA 376.4 ^.,1,''� Total Caaorm: SM 9222 5 Tota FYI.Residue ITOSI: SM 25MC ' 1 Tota C.Iifonn: SM 9223 a TurbWtyf EPA 180.1 Awards Primary Accfeditation to \ DRINKW40 WATER METALS I L AR.rdnwn: DRINKING WATER TRIHALOMETHANES EPA 200.7 AMkmr.r: EPA 200.9 0,-dkhloromah.m: EPA 524,2 t �fjenlgerbr lttt. Anorak: EPA 200.7 B=form EPA$24.2 i 8arfwn: EPA 200.7 CMorodlb .sthsm- EPA 524.2 Or a.ryehrrt: EPA 200.7 Chkrororm: EPA 524.2 AMINO, Cadr..wn: ' EPA 200.7 Told ma TMalohema: EPA$24.2 Cack.n; EPA 200.7 \ Cfrornk". EPA 200.7 . 1 Coops: EPA 200,7 DRINKING WATER VOLATILE ORGANICS k". EPA 200.7 Leal: EPA 200.9 1.1,1.2-TotteeNometham: EPA 524.2 For the analyses listed on the attached`page(s) in accordance with M.nW.m..: EPA 200.7- 1,1,1-TrkNoroahana EPA$24.2 ' the provisions of tate NELAC Standards and Env-C 300. 1 Ma,cury: EPA 247.1 1,1.2.2•Twochloro.th.m: EPA 824.2 Nickel: EPA 200.7 1,1.2-Trkhtoroa0um: EPA 924.2 Sotardum: EPA 200.9 1.1-Dkhtoroethanst EPA 524.2 1 Sero: EPA 200.7 1,1.Okhloroathylanot EPA$24.2 F Sodh.n: EPA 200.7 1.1.Okhloroproperte: EPA$24.2 Tltaawn: EPA 200.9 1,2,3-Tdchlombentsm: EPA 524.2 + Here EPA 200.7 1.2,3•Trkhlaoprop"s EPA 524.2 f \ 1.2.4 ,10dwobantons: '• EPA$24.2 1 DRINKING WATER INORGANIC CONTAMINANTS 1.2.4-TrlmHhylb.nt.m: EPA 5244.2 ., 1.2•DIcNorobantam: EPA 524,2 f o AA.K,rry: EPA 3 10 1.2.01chloroahana EPA$24.2 ! AAak Yy: SM 2320 O 1.2.01cNorowopam: EPA$24.2 ,If q Certificate Number. 100800 1 ar wade: EPA 300.0 1,3.01cNorob.ntons: EPA 524.2 CMarbo: EPA 300.0 1.3.OkMeropropam: EPA 524.2 1 Condueu+MylSo.edk Cond.I: ►E A 120.1 1.3.9•TA sthylbont.ne: EPA 524.2 Date of Issue:January 24,2001 Cor.dwc:t-tvISP-,rtc Cond.I:SM 2S 10 B 1,4Okh1wobtimew. EPA 524.2 Clttwkta,M.dua Fro. SM 6300-Cl C 2.2.Okhlmopopomt EPA$24.2 Cy.rdda,Teta: EPA 335.2 2•CNorotoluom: EPA$24.2 Expiration Date:December 2,2001 4CNaotolvons: EPA$24.2 Ce, Toth: $M 4500•CN C Program Mamgcf Cy-"s.Tota., SM 4500-CH E 4 sopropyltoluone: VA$24.2 t F1wMda: EPA 300.0 Bantam: EPA 524.2 Muala•N: EPA 300.0 Bmmm roobae : EPA$24.2 • Jaw,ugae k dp,d.4 a.mRd ena"p.M,r.1..1.a.Poll • � , Lti+a.�sa.7 roily ar l.b.rrQy'.oar...��yo0natfOl)T7I.2»t�(60)127t•29fs \ z o TNs conlre.le woom dos as paviously Issued canlrkaa.. _ Program M of I AMRO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORD Office:(603)424-2022 I I I Herrick Street 4"'40:385 Fax:(603)429-8496 Merrimack,NH 03054 , Project No.: Project Name: Ti7.A.5 Project Manager: ^ Sam Icrs(Sig ature) AMRO Project No.: V j Project State: %^V1.t3/.trNws.c.IT ,' •• , Sample ID Date/Time Matrix Total# Analysis Required Remarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. WW=Waste W. DW=Drinking W. O=Oil 1� Other-Specify 1 / I I Preservative: e - - Na-NaOH, ter Contamer ype: Plastic,G-Glass, is, eon, - ter Please print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will not start until any FAX No.: ,ambiguities are resolved. Send Results To: Lf s /-fir,= p .'� j' Seal Intact? GW-I GW-2 GW-3 L4.4 A Yes No N/A MCP Level Needed: Relin wished By Date/Time Received By Date/Time P.O.No: / VU/0 PRIORITY TURNAROUND TIME AUTHORIZATION 014 ` "r Before submitting samples for expedited TAT,you must have requested Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER By:, AUTHORIZATION No. BY: SHEET OF White:Lab Copy Yellow:Accompanies Report Pink:Client Copy APPENDIX 4 I OCT.11.2001 3:05PM NO.550 P.4 AMRO Environ ental Laboratories Corp. Date: 11-Oct-01 CLIENT: Subsu ce Remediation Technologies Client Sample ID: EXC.FGI-117(0-5) Lab Order: 01100 3 Tab Number: Project: ##•WJASK RESIDENCE Collection Date: IOP-101 Lab ID: 0110043-05B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst!AKRK' C9-C18 Aliphatic Hydrocarbons 2,800 510 mg/N-dry 10 10/9101 10:40:00 AM C19-C36 Aliphatic Hydrocai bons 690 51 mg/Kg-dry 1 10/8101 9:36:00 PM C11-C22 Aromatic Hydroca bons 1,100 51 mg/Kg-dry 1 1018/01 9:36:00 PM Naphthalene 5,1 0.25 mg/Ka,-dry 1 10/8/01 9:36:00 PM 2-Mathyinaphthalene 23 0.25 mgMg-dry 1 10/8/01 9:36:00 PM Acenaphthylene ND 0.25 mg/Kg-dry 1 1018/01 9:36.0 PM Acenaphthene 1.2 0.25 mg/ICg-dry 1 108/01 9:36:00 PM Fluorene 3.8 0.25 mgN-dry 1 101=1 9:36:00 PM Phenanthrene 5.4 0.25 mgXg-dry 1 10/8/01 9:$6:00 PM Anthracene 0.82 0.25 mg/K9-dry 1 10/8101 9:36;00 PM Fluoranthene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Pyrene 0.66 0.25 mgXg-dry 1 10/8/01 9:36:00 PM Benz(a)anthrscene ND 0.25 mg/Kg-dry 1 10/8/01 9:36:00 PM Chrysene NO 0.25 mgffg-dry 1 1018/01 8:36:00 PM Benzo(b)fluoranthene ND 0.25 mg/Kg-dry 1 1018/01 9:36:00 PM BenzoMfluoronthene ND 0.25 mg/Kg-dry 1 1018/01 9:36:00 PM Benzo(a)pyrene ND 0.25 mg/l(q-dry 1 10/6/01 9:36:00 PM Dibenz(a,h)anthracene ND 0.25 mgfKg-dry 1 10/6!01 9:36:00 PM Indeno(1,2,3-od)pyrene ND 025 mg/Kg-dry 1 10/8/01 9:36:00 PM Benzo(g,h,i)perylene ND 0.25 mg/I(q-dry 1 1018/01 9:36:00 PM Surr.1-Chlorooctadecane 65.2 40-140 %REG 1 10/8/01 9:36:00 PM Surr:2-Bromon2phthale 103 40-140 %REC 1 10/8/01 9:36:00 PM Sun.2-Fiuorobiphenyl 93.6 40-140 %REC 1 10/8/01 9:36:00 PM Surr:o-Terphenyl 79.8 40-140 %REC 1 10/8101 9:36:00 PM Hydrocarbon range data excli de concentrations of any surrogate($)and/or internal standards elutin In that ren e. EPH; C11=C22 AromaticHydrocarbons exclu the concan 9 g pe tretion of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes luting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentratlon of target analytes eluting in this range and concentration f C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures uired by the VPH or EPH method followed: — Yes _ No-If No,See Case Narrative Were all performance/acceo me standards for required QA/QC procedures achieved: ' Yes _ No-If No,See Case Narrative Were any significant modifiea ions made to the method as specified in section 11.3: ` No _ Yes-Details enclosed I attest under the pains and i naf fos of pedury that based upon my inquiry of those individuals immediately naspons/ble for obtaining the Intimation,the materfaloanh iined in this)*port is,to the best of my knowkadpe and belief,accurate and compfeta. SIGNATURE: DATE; PRINTED NAME Nancy St It POSITION: Laboratory Director(or designee) Qualirscrs: RL• t co 0 o a rate qu- ND-Not Detected at tt 5-Mike Re oo r IAP obo tkatioa range 7-Anal)tc detected g Is d c vt B-Analyte detected in The assoo ated Method Blank 11•Method prescribed holding time cxceeded Y OCT.11.2001 3:e4PM NO.550 P.2 A 4RO Environmental Laboratories Corp. Date: H-04t-al CLIENT; Subs ace Remediation Technologies Client Sample ID: EXC.FGHIJ(0-5) Lab Order: 01100 3 Tag Number: Project: *** SK RESIDENCE Collection Date: 10/2/01 Lab ID: 01100 3-05A Matrix: SOIL Analysts Result RL, Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK CS-C8 Atiphatle HydrocarboIns 45 33 mg/Kg-dry 10 10/10/01 3;02:00 AM Cg-C12 Aliphatic Hydrocart�ons 60 8.3 mg/Kg-dry 10 10/10/01 3:02;00 AM C9-C10 Aromatic Hydrocadws 480 8.3 mg/Kg-dry 10 10/10/01 3:02:00 AM Methyl tert-butyl ether ND 0.66 mg/Kg-dry 10 10/ID/01 3:02:00 AM Benzene ND 0.65 mg/Kg-dry 10 1011010113:02-00 AM Toluene 0.86 0.68 mg/Kg-dry 10 10110/013:02.-00 AM Ethylbenzene 1.8 0.66 mo/Kg-dry 10 10/10/01 3:02:00 AM m.p-Xylene 6.6 0.66 mg1Kg-dry 10 10/10/013:02:OOAM o-Xylene 3.6 0.66 mg/kg-dry 10 10/10/01 3:02;00 AM Naphthalene 9.9 1.7 mgXg-dry ID 10/10/01 3:02:00 AM Sun:Dibromoffuorometh ne 106 70-150 %REC 10 10/10/01 3:02:00 AM Sun:1,2-Dichlowsthane113 70-130 %REC 10 10/10/013:02:00 AM Surr:Toluene-dB I 98.9 70.130 %REC 10 10/10/01 3:02:00 AM Surr:4-Bronwfluorobenz ne 101 70.130 %REC 10 10/10/01 3:02:00 AM Surr.2,5-Dibromotoluen 86.3 70-130 %REC 10 10/10/01 3:02:00 AM Hydrocarbon range data exclude concentrations of any surrogato(s)and/or Internal standards eluting In that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-M Aliphatic Hydrocarbons exclude the con- centration of target analytes aluting in this range, C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting In this range end concentration of C9-C10 Aromatic Hydrocarbons, CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: — Yes _ No-If No,See Case Narrative Were all performancrJaCCepi anee standards for required QA1QC procedures achieved: _ Yes _ No-If N0,See Case Narrative Were any significant modifitions made to the method as specified in section 11.3: _ No _ Yes-Details enclosed I attest under the pains and na/ties of pedury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the materlal con wined in this report Is,to the best of my knowledge and baWf,accurate and oWWWe. SIGNATURE: DATE PRINTED NAME: Nancy S ewart POSITION: Laboratory Dtreator(or designee) Qualificnt RL- r r e St w nMao-, 9 ttram quan c.ND-N�Dctectcd at�I t S ikc] c � ur�ii abo araitation ranee 7•AnN detectod u U u ee a tive 8-Antalytc dctcored in dtc assc dated Medtod Blank H•Method prescribed holding time exceeded OCT.11.2001 3:e3PM NO.550 P.1 AMMO Environmental Laboratories Corp. Date: 17-0c,-01 CLTENT: Subs cc Remediation Technologies Client Sample ID: EXC.FGH[7(5-10) Lab Order: 01100 II3 Tag Number: Project: 0**TT ASK RESIDENCE Collection Date: 10/2/01 Lab ID: 0110043-04A ii2atria: SOIL Analyses Result RL Qua[ tints DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK"7 C5-C8 Aliphatic Hydrocarbdns 3.5 3.0 mg/Kg-dry 1 1019101 10:27:00 PM C9-012 Aliphatic Hydrocarbons 7,9 0.75 mg/l(q-dry 1 10/9101 10:27:00 PM C9-C10 Aromatic Hydrocarbons 47 0.75 mgn(q-dry 1 10/9101 10:27:00 PM Methyl tert-butyl ether NO 0.060 rrg/Kgdry 1 1019101 10:27:00 PM Benzene ND 0.060 m9,'Kg-dry 1 10/9/01 10:27:00 PM Toluene NO 0.060 mg/Kg-dry 1 10/9/01 10:27;00 PM Ethylbenzene NO 0.060 mg/Kg-dry 1 1019101 10:27:00 PM m,p-Xylene 0.23 0.060 mg/Kg-dry 1 10/9/01 10:27:00 PM o-Xylene 0.1d 0.060 mg/Kg-dry 1 10/9101 10:27:00 PM Naphthalene 0.93 0.15 mg/Kg-dry 1 1019/01 10:27:00 PM Surr,Drbromofluorometh i ne 104 70-130 %REC 1 10/9/01 10:27:00 PM Surra 1,2-Dichloroeth2n 102 70-130 %REC 1 10/9/01 10:27:00 PM Surr Toluanod8 100 70.130 %REC 1 10/9101 10:27:00 PM Surr.4-Sromofluorobenz ne 107 70.130 %REC 1 10/9/01 10:27:00 PM Surr.2,5-Dlbromotoluene 79.3 70-130 %REC 1 10/9101 10:27:00 PM Hydrocarbon range data exclde concentrations Of any sum393te(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH; C5-Cll Aliphatic Hydrocarbons exclude the con- oentration of target analytes elluting in this range, 09-C12 Aliphatic Hydrocarbons exclude the concenttation of target ansytes eluting In this range and concentration bf C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures raquired by the VPH or EPH method followed: _- Yes No•If No,See Case Narrative Were nal performance/acoept nce standards for required QA/QC procedures achieved: _ Yes _ No-If No,See Case Narrative Were any significant modifies Ions made to the method as specffred to section 11.3: _ No _ Yes-Details enclosed I attest under the pains and na/ties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the information,the material conhtined in this report ts,to the best of my knowledge and belief,accurate and complete. SIGNATURE; DATE; PRINTED NAME: Nancy St wart POSITION: Laboratory Director(or designee) a_ QualiGcrs RL• t a he �Yst co t ffd , o, a AR,,,. ND-Arot Detected at t�o it S ike e$�� lbantitatien range J-Anal% detected rve B-Analyte detected in the assoc�imd Method Blank H-Method prescribed holding time exceeded I OCT.11.2001 3:04PM NO.550 P.3 AMRO Environ ental Laboratories Corp. Date: 11-Oct-01 CLIENT: Subsur Face Remediation Technologies Client Sample ID: EXC.FGlUJ(5-10) Lab Order: 0110043 Tag Number: Project: ---TI ASK RESIDENCE Collection Date: 10(2/01 f Lab ID: 0110013-04B /Matrix: SOIL Analyses II Result RL Qua[ Units DF Date Analyzed EXTRACTABLE PETRO �EUM HYDROCARBONS MAEPH Analyst: RKK'" C9-018 Aliphatic Hydroca Zs 640 53 mgfKg-dry 1 10110/012:50:00 AM C19-C36Aliphatic HydrocaIbons 230 53 mgfKg-dry 1 10110/012:50:00AM C11-C22 Aromatic Hydro Irbons 380 53 mgfK94ry 1 10/101012;50:00 AM Naphthalene 1.8 0.27 rngfKgil,ry 1 10/10/012:50:00 AM 2-Methyln2phth2lene 6.9 0.27 mg/Kg-dry 1 10110/012:50:00 AM Acenaphthylene NO 0.27 mg/4-dry 1 10/10/01 2:50:00 AM Acenaphthene 0.36 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Fluorene 0.85 027 mg/Kg-dry 1 10110/012:60:00 AM Phenanthrene 1.2 0.27 nhgft-dry 1 10/10/01 2:50:00 AM Anthracane NO 0.27 mg/Kg-dry 1 10110/012.50:00 AM Fluoranthens ND 0,27 mg/Kg-dry 1 10/10/01 2:50:00 AM Pyrene ND 0.27 mg/Kg-dry 1 10/10!01 2:50;00 AM Benz(a)anthmcena NO 0.27 mg/4-dry 1 10110/012,50:00 AM Chrysene ND 0.27 mgn-dry 1 10/10/01 2:50:00 AM Benzo(b)fluoranthene ND 0.27 mg/K"ry 1 10/101012:50:00 AM Senzo(k)Buoranthene ND 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Benzo(s)pyrene NO 0.27 mg/Kg-dry 1 10/10/012:50:00 AM Dibenz(a,h)anthraoane NO 0.27 mg1Kg-dry 1 10110/012:50:00 AM Indeno(1,2,&cd)pyrene NO 0.27 mg/Kg-dry 1 10/10/01 2:50:00 AM Senzo(g,h,l)perylene ND 0.27 mg/Kg-dry 1 10/10/012;50:00 AM Sum 1-Chloreootadeca 89.0 40-140 %REC 1 10/10/01 2:50:00 AM Sum 2-Bromonaphthalene 111 40-140 %REC 1 10/10/01 2:50:00 AM Sum2-Fluorobiphenyl 110 40-140 %REC 1 10/10/012:50:00AM Sum o-Terphenyi 81.5 40-140 0/.REC 1 10/10/01 2:50:00 AM Hydrocarbon re e data exclude concentrations of a surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Yd n9 r►Y 9 9 Aromatic Hydrocarbons exclde the concentration of target PAH analylec, VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes elating in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration f C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were at QA/QC procedures r qulred by the VPH or EPH method followed: ^ Yes No-If No,See Case Narrative pt�nc Were all perfDM1ance/2ocee standards for required QA1QCP rocedures achieved: Yes No-If No,See Case Narrative Were any significant nlodifi4om made to the method as speeded in section 1 i.3: No _ Yes-Details enclosed I attest under the pains and pl mal<ies of pedury that,based upon my inquiry of Mose individuals immediately responsible for obtaining the fifonnetion,the material contained in this report Is,to the best of my knowledge and be0d,,accurate and complete. SIGNATURE I DATE: PRINTED NAME: Nancy S art POSITION: Laboratory Director(or designee) ND-Not RL- hquitEEPTM )Nur>ae quan�VD-Not Daccud at lira E abohhnutation rfnge 1-Analyte detected b i Ss we A-Analyte detected in the use iatod Method Blank H-Method prescribed holding time exceeded I I � AMBO Environmental Laboratories Corporation CHAIN-Or-CUSTODY RECORD Office:(603)424-2022 111 Herrick Street 40382 Fax:(603)429-8496 Merrimack,NH 03054 Project No.: Project Name: !.,�.r C. Project Manager: emRlcrs,('ignatuTy t0 Project No.: Project State: J'" Sample ID Date/Time Matrix Total# Analysis Required Remarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. WW=Waste W. \ DW=Drinking W. p �; O=Oil 1\ /L' � o I Other=Specify -Irl.- )&P ; . reservative;C 1,KI.C5FI, ,S-090T,Na-Na0R,T Otfier :ontamer ype: - ast,c, - ass, - to, - eon, - ter be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; lease print clearly,legibly and completely.Samples can not ; )gged in and the turnaround time clock will not start until any FAX No.: ' mbiguities are resolved. cnd Results To: /it/G rscal►nlact? GW-1 GLV-2 GW-3 '2 / kus No—N/A MCP Level Needed: Relin wished B Date/Time Received Daterrime P.O.No: _ ,,`// /��• r PRIORITY TURNAROUND TIME AUTHORIZATION du� /V/�I Before submitting sampicifor expedited TAT,you must have requested Results Need in advance and received a Coded TAT AUTHORIZATION NUMBER By: -✓ � AUTHORIZATION No. BY: SHEET OF ,Vhite:Lab Copy Yellow:Accompanies Report Pink:Client Copy A Environmental Laboratories Corporation 111 Herrick Street,Merrimack, NH 03054 TEL:(603)424-2022•FAX: (603)429-8496 September 24,2001 Tim Toomey Subsurface Remediation Technologies 355 Central St. =� Rowley, MA 01969 TEL: (978)948-3861 FAX: (978)948-3861 RE: TRASK RESIDENCE Order No.: 0109079 Dear Tim Toomey: AMRO Environmental Laboratories Corp. received 7 samples on 9/14/01 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference(NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s) upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time, AMRO will properly dispose of the remaining sample(s). If you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of pages. This letter is an integral part of your data report. If you . have any questions regarding this project in the future, please refer to the Order Number above. Sincerely, Nancy Stewart Vice President/Lab Director3:. t I I AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Project: TRASK RESIDENCE Work Order Sample Summary Lab Order: 0109079 Date Received: 9/14/01 Lab Sample ID Client Sample ID Collection Date _- - 0109079-OIA FGH 9/13/01 0109079-01 B FGH 9/13/01 0109079-02A HK 9/13/01 0109079-02B HK 9/13/01 0109079-03A JKI 9/13/01 0109079-03B JKI 9/13/01 0109079-04A FI 9/13/01 0109079-04B FI 9/13/01 0109079-05A BOTTOM 9/13/01 0109079-05B BOTTOM 9/13/01 0109079-06A A BOTTOM 9/13/01 0109079-06B A BOTTOM 9/13/01 0109079-07A A SIDEWALL 9/13/01 0109079-07B A SIDEWALL 9/13/01 1_. 2 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Project: TRASK RESIDENCE CASE NARRATIVE Lab Order: 0109079 GENERAL 1.The samples were received in the laboratory at 15 degrees C above the recommended teperature of 4 degrees C. MADEP-VPH 1.The surrogate 2,5-Dibromotoluene recovered below the QC limits (70-130%) in sample 0109079- 07A. MADEP-EPH 2.The duplicate sample 0109079-04B had %RPD's outside the QC limits due to sample non- homogeniety. -01 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FGH Lab Order: 0109079 Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-OIB Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: JSL "'Sample receipt problems were observed for this test method. See Case Narrative for details. Percent Moisture 2.6 0 wt% 1 9/18/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded ti -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. .. 4 i AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: HK Lab Order: 0109079 Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-02B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: JSL "'Sample receipt problems were observed for this test method. See Case Narrative for details. Percent Moisture 3.3 0 wt% 1 9/18/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. rl I ` I AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: JKI Lab Order: 0109079 Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-03B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: JSL "'Sample receipt problems were observed for this test method. See Case Narrative for details. Percent Moisture 3.7 0 wt% 1 9/18/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. 6 AMRO Environmental Laboratories Corp. Date: 29-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FI Lab Order: 0109079 Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-04B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: JSL Sample receipt problems were observed for this test method. See Case Narrative for details. Percent Moisture 5.4 0 wt% 1 9/18/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. H i AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: BOTTOM Lab Order: 0109079 Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-05B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: JSL "'Sample receipt problems were observed for this test method. See Case Narrative for details. Percent Moisture 5.1 0 wt% 1 9/18/01 ate. Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits 1-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded # -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. _ _ AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: A BOTTOM Lab Order: 0109079 Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-06B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: JSL Sample receipt problems were observed for this test method. See Case Narrative for details. Percent Moisture 7.7 0 wt% 1 9/18/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits 7-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded N -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. 9 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: A SIDEWALL Lab Order: 0109079 Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-07B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed PERCENT MOISTURE D2216 Analyst: JSL "'Sample receipt problems were observed for this test method. See Case Narrative for details. Percent Moisture 4.8 0 wt% 1 9/18/01 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded ti -See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. 10 • II I I AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FGH Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-01A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK Sample receipt problems were observed for this test method. See Case Narrative for details. C5-C8 Aliphatic Hydrocarbons ND 29 mg/Kg-dry 10 9/21/01 5:17:00 PM C9-C12 Aliphatic Hydrocarbons 12 7.3 mg/Kg-dry 10 9/21/01 5:17:00 PM C9-C10 Aromatic Hydrocarbons 120 7.3 mg/Kg-dry 10 9/21/01 5:17:00 PM Methyl tert-butyl ether ND 0.58 mg/Kg-dry 10 9/21/01 5:17:00 PM Benzene ND 0.58 mg/Kg-dry 10 9/21/01 5:17:00 PM Toluene ND 0.58 mg/Kg-dry 10 9/21/01 5:17:00 PM Ethylbenzene NO 0.58 mg/Kg-dry 10 9/21/01 5:17:00 PM m,p-Xylene 0.71 0.58 mg/Kg-dry 10 9/21/01 5:17:00 PM o-Xylene ND 0.58 mg/Kg-dry 10 9/21/01 5:17:00 PM Naphthalene 2.6 1.5 mg/Kg-dry 10 9/21/01 5:17:00 PM Surr.Dibromofluoromethane 95.8 70-130 %REC 10 9/21/01 5:17.00 PM Surr: 1,2-Dichloroethane-d4 88.1 70-130 %REC 10 9/21/01 5.17.00 PM Surr:Toluene-d8 96.9 70-130 %REC 10 9/21/01 5:17:00 PM Surr:4-Bromofluorobenzene 98.8 70-130 %REC 10 9/21/01 5:17:00 PM Surr:2,5-Dibromotoluene 81.5 70-130 %REC 10 9/21/01 5:17:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Z"Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Yes _ No-If No,See,Cose Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Z Yes-Details enclosed i attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 11 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: HK Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-02A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK "'Sample receipt problems were observed for this test method. See Case Narrative for details. C5-C8 Aliphatic Hydrocarbons 37 30 mg/Kg-dry 10 9/21/01 5:53:00 PM C9-C12 Aliphatic Hydrocarbons 43 7.5 mg/Kg-dry 10 9/21/01 5:53:00 PM C9-C10 Aromatic Hydrocarbons 670 7.5 mg/Kg-dry 10 9/21/01 5:53:00 PM Methyl tert-butyl ether ND 0.60 mg/Kg-dry 10 9/21/01 5:53:00 PM Benzene ND 0.60 mg/Kg-dry 1'0 9/21/01 5:53:00 PM Toluene 2.2 0.60 mg/Kg-dry 10 9/21/01 5:53:00 PM Ethylbenzene 3.6 0.60 mg/Kg-dry 10 9/21/01 5:53:00 PM m,p-Xylene 13 0.60 mg/Kg-dry 10 9/21/01 5:53:00 PM o-Xylene 6.9 0.60 mg/Kg-dry 10 9/21/01 5:53:00 PM Naphthalene 14 1.5 mg/Kg-dry 10 9/21/01 5:53:00 PM %REC 10 9/21/01 5:53:00 PM i Surr:Dibromofluoromethane 103 70-130 /o Surr: 1,2-Dichloroethane-d4 88.7 70-130 %REC 10 9/21/01 5:53:00 PM Surr:Toluene-d8 107 70-130 %REC 10 9/21/01 5:53:00 PM Surr:4-Bromofluorobenzene 104 70-130 %REC 10 9/21/01 5:53:00 PM Surr.2,5-Dibromotoluene 101 70-130 %REC 10 9/21/01 5:53:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-Cl 0 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: VYes No-If No,See Cate Narrative Were any significant nificant modifications made to the method ass specified in section 11.3: No Yes-Details enclosed P — I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: �lv DATE: ! r PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits tl-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 7 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: JKI Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-03A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK —Sample receipt problems were observed for this test method. See Case Narrative for details. C5-C8 Aliphatic Hydrocarbons 36 30 mg/Kg-dry 10 9/21/016:28:00 PM C9-C12 Aliphatic Hydrocarbons 54 7.4 mg/Kg-dry 10 9/21/01 6:28:00 PM C9-C10 Aromatic Hydrocarbons 540 7.4 mg/Kg-dry 10 9/21/01 6:28:00 PM Methyl tert-butyl ether ND 0.59 mg/Kg-dry 10 9/21/01 6:28:00 PM Benzene ND 0.59 mg/Kg-dry 10 9/21/01 6:28:00 PM Toluene 1.2 0.59 mg/Kg-dry 10 9/21/01 6:28:00 PM Ethylbenzene 2.7 0.59 mg/Kg-dry 10 9/21/01 6:28:00 PM m,p-Xylene 9.4 0.59 mg/Kg-dry 10 9/21/01 6:28:00 PM o-Xylene 5.1 0.59 mg/Kg-dry 10 9/21/01 6:28:00 PM Naphthalene 12 1.5 mg/Kg-dry 10 9/21/01 6:28:00 PM Surr.Dibromofluoromethane 95.3 70-130 %REC 10 9/21/01 6:28:00 PM Surr.1,2-Dichloroethane-d4 92.9 70-130 %REC 10 9/21/01 6:28:00 PM Surr:Toluene-d8 102 70-130 %REC 10 9/21/01 6:28:00 PM Surr:4-Bromofluorobenzene 104 70-130 %REC 10 9/21/01 6:28:00 PM Surr.2,5-Dibromotoluene 97.6 70-130 %REC 10 9/21/01 6:28:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is,to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: PRINTED NAME: Nancy Stewa POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery Iimits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded - 12 + i AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FI Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-04A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK ***Sample receipt problems were observed for this test method. See Case Narrative for details. C5-C8 Aliphatic Hydrocarbons 32 29 mg/Kg-dry 10 9/21/01 7:04:00 PM C9-C12 Aliphatic Hydrocarbons 55 7.3 mg/Kg-dry 10 9/21/01 7:04:00 PM C9-C10 Aromatic Hydrocarbons 630 7.3 mg/Kg-dry 10 9/21/01 7:04:00 PM Methyl tert-butyl ether ND 0.59 mg/Kg-dry 10 9/21/01 7:04:00 PM Benzene ND 0.59 mg/Kg-dry 10 9/21/01 7:04:00 PM Toluene 1.0 0.59 mg/Kg-dry 10 9/21/01 7:04:00 PM Ethylbenzene 2.4 0.59 mg/Kg-dry 10 9/21/01 7:04:00 PM m,p-Xylene 8.7 0.59 mg/Kg-dry 10 9/21/01 7:04:00 PM o-Xylene 4.9 0.59 mg/Kg-dry 10 9/21/01 7:04:00 PM Naphthalene 13 1.5 mg/Kg-dry 10 9/21/01 7:04:00 PM Surr:Dibromofluoromethane 98.6 70-130 %REC 10 9/21/01 7:04:00 PM Surr: 1,2-Dichloroethane-d4 94.7 70-130 %REC 10 9/21/01 7:04:00 PM Surr:Toluene-d8 101 70-130 %REC 10 9/21/01 7:04:00 PM Surr:4-Bromofluorobenzene 102 70-130 %REC 10 9/21/01 7:04:00 PM Surr:2,5-Dibromotoluene 81.6 70-130 %REC 10 9/21/01 7:04:00 PM I Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-G10 Aromatic Hydrocarbons. CERTIFICATION / Were all QA/QC procedures required by the VPH or EPH method followed: ✓ Yes — No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No _ Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accuratte�and complete. SIGNATURE: \ f `�7 50L� DATE: PRINTED NAME: Nancy StewartPOSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits N-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded i4 i AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: BOTTOM Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-05A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK "'Sample receipt problems were observed for this test method. See Case Narrative for details. C5-C8 Aliphatic Hydrocarbons ND 3.2 mg/Kg-dry 1 9/18/01 7:10:00 PM C9-C12 Aliphatic Hydrocarbons ND 0.80 mg/Kg-dry 1 9/18/01 7:10:00 PM C9-C10 Aromatic Hydrocarbons 3.4 0.80 mg/Kg-dry 1 9/18/01 7:10:00 PM Methyl tert-butyl ether ND 0.064 mg/Kg-dry 1 9/18/01 7:10:00 PM Benzene ND 0.064 mg/Kg-dry 1 9/18/01 7:10:00 PM Toluene ND 0.064 mg/Kg-dry 1 9/18/01 7:10:00 PM Ethylbenzene ND 0.064 mg/Kg-dry 1 9/18/01 7:10:00 PM m,p-Xylene ND 0.064 mg/Kg-dry 1 9/18/01 7:10:00 PM o-Xylene ND 0.064 mg/Kg-dry 1 9/18/01 7:10:00 PM Naphthalene ND b.16 mg/Kg-dry 1 9/18/01 7:10:00 PM Surr:Dibromofluoromethane 94.8 70-130 %REC 1 9/18/01 7:10:00 PM Surr: 1,2-Dichloroethane-d4 87.8 70-130 %REC 1 9/18/01 7:10:00 PM Surr:Toluene-d8 101 70-130 %REC 1 9/18/01 7:10:00 PM Surr:4-Bromofluorobenzene 97.2 70-130 %REC 1 9/18/01 7:10:00 PM Surr:2,5-Dibromotoluene 77.1 70-130 %REC 1 9/18/01 7:10:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: i7Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: PRINTED NAME: Nancy Stewart f POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: A BOTTOM Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-06A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK Sample receipt problems were observed for this test method. See Case Narrative for details. C5-C8 Aliphatic Hydrocarbons ND 2.5 mg/Kg-dry 1 9/18/01 7:45:00 PM C9-C12 Aliphatic Hydrocarbons 0.86 0.63 mg/Kg-dry 1 9/18/01 7:45:00 PM C9-C10 Aromatic Hydrocarbons 15 0.63 mg/Kg-dry 1 9/18/01 7:45:00 PM Methyl tert-butyl ether NO 0.050 mg/Kg-dry 1 9/18/01 7:45:00 PM Benzene ND 0.050 mg/Kg-dry 1 9/18/01 7:45:00 PM Toluene ND 0.050 mg/Kg-dry 1 9/18/01 7:45:00 PM Ethylbenzene ND 0.050 mg/Kg-dry 1 9/18/01 7:45:00 PM m,p-Xylene ND 0.050 mg/Kg-dry 1 9/18/01 7:45:00 PM o-Xylene ND 0.050 mg/Kg-dry 1 9/18/01 7:45:00 PM Naphthalene 0.40 0.13 mg/Kg-dry 1 9/18/01 7:45:00 PM Surr:Dibromofluoromethane 94.7 70-130 %REC 1 9/18/01 7:45:00 PM Surr: 1,2-Dichloroethane-d4 88.2 70-130 %REC 1 9/18/01 7:45:00 PM Surr:Toluene-d8 99.0 70-130 %REC 1 9/18/01 7:45:00 PM Surr:4-Bromofluorobenzene 98.9 70-130 %REC 1 9/18/01 7:45:00 PM Surr:2,5-Dibromotoluene 77.5 70-130 %REC 1 9/18/01 7:45:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: _ZYes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: Yes _ No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No _b Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: �/� _ _ �-� DATE: ( ' v(, __0/ PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 16 AMRO Environmental Laboratories Corp. Date: 29-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: A SIDEWALL Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-07A Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed VOLATILE PETROLEUM HYDROCARBONS MAVPH Analyst: SK ***Sample receipt problems were observed for this test method. See Case Narrative for details. C5-C8 Aliphatic Hydrocarbons ND 20 mg/Kg-dry 10 9/21/01 7:40:00 PM C9-C12 Aliphatic Hydrocarbons 41 5.0 mg/Kg-dry 10 9/21/01 7:40:00 PM C9-C10 Aromatic Hydrocarbons 430 5.0 mg/Kg-dry 10 9/21/01 7:40:00 PM Methyl tert-butyl ether ND 0.40 mg/Kg-dry 10 9/21/01 7:40:00 PM Benzene ND 0.40 mg/Kg-dry 10 9/21/01 7:40:00 PM Toluene 1.2 0.40 mg/Kg-dry 10 9/21/01 7:40:00 PM Ethylbenzene 2.2 0.40 mg/Kg-dry 10 9/21/01 7:40:00 PM m,p-Xylene 7.7 0.40 mg/Kg-dry 10 9/21/01 7:40:00 PM o-Xylene 4.3 0.40 mg/Kg-dry 10 9/21/01 7:40:00 PM Naphthalene 12 1.0 mg/Kg-dry 10 9/21/01 7:40:00 PM Surr:Dibromofluoromethane 94.4 70-130 %REC 10 9/21/01 7:40:00 PM Surr: 1,2-Dichloroethane-d4 91.9 70-130 %REC 10 9/21/01 7:40:00 PM Surr:Toluene-d8 95.8 70-130 %REC 10 9/21/01 7:40:00 PM Surr:4-Bromofluorobenzene 90.7 70-130 %REC 10 9/21/01 7:40:00 PM Surr:2,5-Dibromotoluene 57.5 70-130 S %REC 10 9/21101 7:40:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C,10 Aromatic Hydrocarbons. CERTIFICATION / Were all QA/QC procedures required by the VPH or EPH method followed: ✓ YesNo-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is,to the best of my knowledge and belief, accurate and complete. SIGNATURE: -f DATE: _21y__0__0 1 PRINTED NAME: Nancy StewartPOSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 1. 7 AMRO Environmental Laboratories Corp. Date: 29-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FGH Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-01B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK "'Sample receipt problems were observed for this test method. See Case Narrative for details. C9-C18 Aliphatic Hydrocarbons 330 50 mg/Kg-dry 1 9/19/01 1:12:00 AM C19-C36 Aliphatic Hydrocarbons 120 50 mg/Kg-dry 1 9/19/01 1:12:00 AM C11-C22 Aromatic Hydrocarbons 120 50 mg/Kg-dry 1 9/19/01 1:12:00 AM Naphthalene 0.47 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM 2-Methyinaphthalene 2.5 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Acenaphthylene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Acenaphthene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Fluorene 0.53 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Phenanthrene 0.61 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Anthracene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Fluoranthene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Pyrene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Benz(a)anthracene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Chrysene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Benzo(b)fluoranthene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Benzo(k)fluoranthene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Benzo(a)pyrene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Dibenz(a,h)anthracene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Indeno(1,2,3-cd)pyrene ND 0.25 mg/Kg-dry 1 9/19/011:12:00 AM Benzo(g,h,i)perylene ND 0.25 mg/Kg-dry 1 9/19/01 1:12:00 AM Surr. 1-Chlorooctadecane 82.3 40-140 %REC 1 9/19/01 1:12:00 AM Surr.2-Bromonaphthalene 109 40-140 %REC 1 9/19/01 1:12:00 AM Surr:2-Fluorobiphenyl 111 40-140 %REC 1 9/19/01 1:12:00 AM Surr.o-Terphenyl 66.5 40-140 %REC 1 9/19/01 1:12:00 AM I Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: V/Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes �No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range 1-Analyte detected below quantitation limits R-RPD outside accepted recovery limits !1-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded '� Q AMRO Environmental Laboratories Corp. Date: 29-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: HK Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-02B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK Sample receipt problems were observed for this test method. See Case Narrative for details. C9-C18 Aliphatic Hydrocarbons 1,800 510 mg/Kg-dry 10 9/19/01 1:26:00 PM C19-C36 Aliphatic Hydrocarbons 330 51 mg/Kg-dry 1 9/19/01 1:47:00 AM C11-C22 Aromatic Hydrocarbons 500 51 mg/Kg-dry 1 9/19/01 1:47:00 AM Naphthalene 5.4 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM 2-Methylnaphthalene 17 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Acenaphthene 1.6 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Fluorene 2.9 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Phenanthrene 3.1 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Anthracene 0.60 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Pyrene 0.52 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM I'I Chrysene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Dibenz(a,h)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 9/19/011:47:00 AM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry 1 9/19/01 1:47:00 AM Surr: 1-Chlorooctadecane 98.5 40-140 %REC 1 9/19/01 1:47:00 AM Surr:2-Bromonaphthalene 101. 40-140 %REC 1 9/19/01 1:47:00 AM . Surr:2-Fluorobiphenyl 108 40-140 %REC 1 9/19/01 1:47:00 AM Surr:o-Terphenyl 93.4 40-140 %REC 1 9/19/01 1:47:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required b the VPH or EPH method followed: Yes _ No-If No,See Case Narrative P q Y _ Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No _ Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range 7-Analyte detected below quantitation limits R-RPD outside accepted recovery limits q-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 19 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: JKI Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-03B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK —Sample receipt problems were observed for this test method. See Case Narrative for details. C9-C18 Aliphatic Hydrocarbons 1,700 510 mg/Kg-dry 10 9/19/01 2:01:00 PM C19-C36 Aliphatic Hydrocarbons 330 51 mg/Kg-dry 1 9/19/01 2:22:00 AM C11-C22 Aromatic Hydrocarbons 430 51 mg/Kg-dry 1 9/19/01 2:22:00 AM Naphthalene 4.5 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM 2-Methylnaphthalene 15 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Acenaphthene 1.4 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Fluorene 2.6 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Phenanthrene 2.9 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM 'Anthracene 0.30 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Pyrene 0.47 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Chrysene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Dibenz(a,h)anth race ne ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM lndeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry 1 9/19/01 2:22:00 AM Surr:1-Chlorooctadecane 118 40-140 %REC 1 9/19/01 2:22:00 AM Surr:2-Bromonaphthalene 102 40-140. %REC 1 9/19/01 2:22:00 AM Surr:2-Fluorobiphenyl 110 40-140 %REC 1 9/19/01 2:22:00 AM Surc o-Terphenyl 97.9 40-140 %REC 1 9/19/01 2:22:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: _.-4es _ No-If No,See Case Narrative Were all performance/acceptance standards for required CA/QC procedures achieved: _ Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: — No 7Z Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. SIGNATURE: �ic--, DATE: PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range 7-Analyte detected below quantitation limits R-RPD outside accepted recovery limits tl-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 20 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: FI Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-04B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK ""Sample receipt problems were observed for this test method. See Case Narrative for details. C9-C18 Aliphatic Hydrocarbons 3,600 530 mg/Kg-dry 10 9/19/01 2:36:00 PM C19-C36 Aliphatic Hydrocarbons 540 53 mg/Kg-dry 1 9/19/01 3:32:00 AM C11-C22 Aromatic Hydrocarbons 760 53 mg/Kg-dry 1 9/19/01 3:32:00 AM Naphthalene 9.0 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM 2-Methylnaphthalene 25 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Acenaphthene 7.1 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Fluorene 6.0 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Phenanthrene 6.6 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Anthracene 0.56 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Pyrene 0.90 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Chrysene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Dibenz(a,h)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry 1 9/19/01 3:32:00 AM Surr: 1-Chlorooctadecane 116 40-140 %REC 1 9/19/01 3:32:00 AM Surr:2-Bromonaphthalene 101 40-140 %REC 1 9/19/01 3:32:00 AM Surr:2-Fluorobiphenyl 106 40-140 %REC 1 9/19/01 3:32:00 AM Surr:o-Terphenyl 108 40-140 %REC 1 9/19/01 3:32:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: _ZYesNo-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes V, No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Z Yes-Details enclosed I attest under the pains and penalties of pedury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: ? .7-y-0 l PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 21 AMRO Environmental Laboratories Corp. Date: 29-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: BOTTOM Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-05B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK "'Sample receipt problems were observed for this test method. See Case Narrative for details. C9-C18 Aliphatic Hydrocarbons 62 52 mg/Kg-dry 1 9/19/01 4:42:00 AM C19-C36 Aliphatic Hydrocarbons ND 52 mg/Kg-dry 1 9/19/01 4:42:00 AM C11-C22 Aromatic Hydrocarbons ND 52 mg/Kg-dry 1 9/19/01 4:42:00 AM Naphthalene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM 2-Methylnaphthalene 0.32 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Acenaphthene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Fluorene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Phenanthrene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Anthracene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Pyrene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Chrysene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Dibenz(a,h)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry 1 9/19/01 4:42:00 AM Surr:1-Chlorooctadecane 64.8 40-140 %REC 1 9/19/01 4:42:00 AM Surr.2-Bromonaphthalene 108 40-140 %REC 1 9/19/01 4:42:00 AM Surr.2-Fluorobiphenyl 113 40-140 %REC 1 9/19/01 4:42:00 AM Sum o-Terphenyl 58.2 40-140 %REC 1 9/19/01 4:42:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes _ No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes '_Z No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No V/ Yes-Details enclosed I attest under the pains and Penalties of Pegurthat based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. SIGNATURE: DATE: " 2_t1__6/ PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded, 22 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: A BOTTOM Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-06B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK Sample receipt problems were observed for this test method. See Case Narrative for details. C9-C18 Aliphatic Hydrocarbons 110 53 mg/Kg-dry 1 9/19101 5:17:00 AM C19-C36 Aliphatic Hydrocarbons ND 53 mg/Kg-dry 1 9/19/01 5:17:00 AM C11-C22 Aromatic Hydrocarbons NO 53 mg/Kg-dry 1 9/19/01 5:17:00 AM Naphthalene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM 2-Methylnaphthalene 0.58 0.26 mg/Kg-dry 1 9119/01 5:17:00 AM Acenaphthylene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Acenaphthene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Fluorene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Phenanthrene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Anthracene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Pyrene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Chrysene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Benzo(a)pyrene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Dibenz(a,h)anthracene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 9/19/015:17:00 AM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry 1 9/19/01 5:17:00 AM Surr: 1-Chlorooctadecane 72.1 40-140 %REC 1 9/19/01 5:17:00 AM Surr.2-Bromonaphthalene 115 40-140 %REC 1 9/19/01 5:17:00 AM Surr:2-Fluorobiphenyl 118 40-140 %REC 1 9/19/01 5:17:00 AM Surr:o-Terphenyl 56.5 40-140 %REC 1 9/19/01 5:17:00 AM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C,10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: _ZYes No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes No-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief, accurate and complete. SIGNATURE: DATE: PRINTED NAME: Nancy Stewak POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recoverylimits #-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 23 AMRO Environmental Laboratories Corp. Date: 24-Sep-01 CLIENT: Subsurface Remediation Technologies Client Sample ID: A SIDEWALL Lab Order: 0109079 Tag Number: Project: TRASK RESIDENCE Collection Date: 9/13/01 Lab ID: 0109079-07B Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed EXTRACTABLE PETROLEUM HYDROCARBONS MAEPH Analyst: RKK —Sample receipt problems were observed for this test method. See Case Narrative for details. C9-C18 Aliphatic Hydrocarbons 4,300 520 mg/Kg-dry 10 9/19101 3:46:00 PM C19-C36 Aliphatic Hydrocarbons 720 52 mg/Kg-dry 1 9/20/01 5:00:00 PM C11-C22 Aromatic Hydrocarbons 920 52 mg/Kg-dry 1 9/20/01 5:00:00 PM Naphthalene 8.2 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM 2-Methylnaphthalene 25 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Acenaphthylene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Acenaphthene 7.8 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Fluorene 10 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Phenanthrene 9.0 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Anthracene 1.1 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Fluoranthene 0.56 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Pyrene 1.2 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Benz(a)anthracene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Chrysene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Benzo(b)fluoranthene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Benzo(k)fluoranthene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Senzo(a)pyrene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Dibenz(a,h)anth racene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Indeno(1,2,3-cd)pyrene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Benzo(g,h,i)perylene ND 0.26 mg/Kg-dry 1 9/20/01 5:00:00 PM Surr. 1-Chlorooctadecane 81.0 40-140 %REC 1 9/20/01 5:00:00 PM Sum 2-Bromonaphthalene 93.9 40-140 %REC 1 9120/01 5:00:00 PM Sun-2-Fluorobiphenyl 91.0 40-140 %REC 1 9/20/01 5:00:00 PM Sum o-Terphenyl 81.9 40-140 %REC 1 9/20/01 5:00:00 PM Hydrocarbon range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. EPH: C11-C22 Aromatic Hydrocarbons exclude the concentration of target PAH analytes. VPH: C5-C8 Aliphatic Hydrocarbons exclude the con- centration of target analytes eluting in this range. C9-C12 Aliphatic Hydrocarbons exclude the concentration of target analytes eluting in this range and concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures required by the VPH or EPH method followed: Yes No-If No,See Case Narrative Were all performance/acceptance standards for required QA/QC procedures achieved: _ Yes 140-If No,See Case Narrative Were any significant modifications made to the method as specified in section 11.3: _ No Yes-Details enclosed 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is, to the best of my knowledge and belief,accurate and complete. SIGNATURE: V PRINTED NAME: Nancy Stewart POSITION: Laboratory Director(or designee) Qualifiers: RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits E-Value above quantitation range J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits tl-See Case Narrative B-Analyte detected in the associated Method Blank H-Method prescribed holding time exceeded 24 AMBO Environmental Laboratories Corporation I I I Herrick Street Merrimack.NH 03054 Volatile Petroleum Hydrocarbons (VPH) Massachusetts Department of Environmental Protection (MADEP) Method 1.0 -January 1998 AMBO Modifications This modification is based on the use of a purge and trap gas chromatography mass spectrometer(GC/MS) system to analyze samples for VPH. The hydrocarbon ranges are quantified using predominant mass fragmentation ions which are characteristic for the range being measured. This approach eliminates potential false positives for the target analytes while providing accurate hydrocarbon range data. The chromatographic column is an HP-624 capillary column which has been validated by GCIMS analysis of a gasoline standard to correctly identity the marker compounds and elution order of specific gasoline components. Batch quality control includes, at a minimum, method blank, laboratory control sample, and duplicate analysis. A matrix spike and/or matrix spike duplicate is analyzed if sufficient sample is submitted to the laboratory. The Reporting Limit(RL) of this method for each of the collective aliphatic and aromatic ranges is approximately 0.6-2.2 mg/kg in soil and 25-110 ug/L in water. The RL of this method for the target analytes ranges from approximately 0.05-0.13 mg/kg in sail and 2.0- 5.0 ug/L for water samples. * Extractable Petroleum Hydrocarbons (EPH) Massachusetts Department of Environmental Protection (MADEP) Method 1.0 -January 1998 AMBO Modifications This modification is based on a solvent extraction and gas chromatography mass j spectrometer (GC/MS) analysis. The hydrocarbon uan 'fi are ranges 9 q � ed using mass fragmentation ions which are characteristic for the range bung measured. This approach eliminates the silica gel solid-phase fractionation step. False positives for targeted PAH analytes are eliminated by using GC/MS as the primary analysis technique. Th e chromatographic column is a J&W Scientific DB-Sms capillary column. Internal standard calibration is performed using Sa-Androstane at a concentration of �. 40 ng/µL. a-Terphenyl and 1-Chlorooctadecane are added as surrogate compounds at 20 ng/uL in the sample extract. These two surrogates monitor the effects of the sample matrix and extraction efficiency. Two additional surrogates, 2-Fluorobiphenyl and 2- 8romonaphthalene, are added to the finished extract prior to analysis to monitor instrument performance. Batch quality control includes, at a minimum, a procedure blank, laboratory control sample and duplicate sample analysis. A matrix spike is analyzed if sufficient sample is submitted to the laboratory. The Reporting Limit (RL) of this method for each of the collective aliphatic and aromatic ranges is approximately 2-15 mg/kg in sail and 10-50 ug/L in water. The RL of this method for the Target PAH analytes ranges from approximately 0.25 to O.Smg/kg in sail; 1.0ug/L for water when operating the GC/MS in full scan mode, and 0.1 to 1.0ug/L when operating the GC/MS in SIM mode. For sites requiring the lowest levels cited in the Massachusetts Contingency Plan for water. GC/MS in the Selected Ion Monitoring (SIM) made is used. adacrnemo-;/rnr-,0.'1i,."k R-" i i rm,2 5 AMRO Environmental Laboratories Corp. 24-Sep-01 Lab Order: 0109079 Client: Subsurface Remediation Technologies DATES REPORT Project: TRASK RESIDENCE Sample ID Client Sample ID Collection Date Matrix Test Name TCLP Date Prep Date Analysis Date 0109079-01A FGH 9/13/01 Soil Volatile Petroleum 1-lydrocarbons 9/13/01 9/21/01 0109079-OIB EPH,Soil,Full List 9/17/01 9/19/01 Percent Moisture 9/18/01 0109079-02A HK Volatile Petroleum Hydrocarbons 9/13/01 9/21/01 0109079-02B EI'11,Soil,Full List 9/17/01 9/19/01 EMI,Soil,Full List 9/17/01 9/19/01 Percent Moisture 9/18/01 0109079-03A JKI Volatile Petroleum Ilydrocarbons 9/13/01 9/21/01 0109079-03B EI'I I,Soil,[:oil List 9/17/01 9/19/01 EPI 1,Soil,Full List 9/17/01 9/19/01 Percent Moisture 9/18/01 0109079-04A FI Volatile Petroleum Ilydrocarbons 9/13/01 9/21/01 0109079-04B EPI I,Soil,Full List 9/17/01 9/19/01 EPI 1,Soil,Full List 9/17/01 9/19/01 Pcrccnt Moisture 9/18/01 0109079-05A BOTTOM Volatile Petroleum Ilydrocarbons 9/13/01 9/18/01 0109079-05B E111 1,Soil,Full List 9/17/01 9/19/01 Pcrccnt Moisture 9/18/01 0109079-06A A BOTTOM Volatile Petroleum Hydrocarbons 9/13/01 9/18/01 0109079-06B EPH,Soil,Full List 9/17/01 9/19/01 Percent Moisture 9/18/01 0109079-07A A SIDEWALL Volatile Petroleum Hydrocarbons 9/13/01 9/21/01 0109079-07B EI'11,Soil,Full List 9/17/01 9/19/01 EI'l1,Soil,Full List 9/17/01 9/20/01 Percent Moisture 9/18/01 Q� AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 Client: 7— 603 424-2022 AbIR01D: 7 Project Name: TQ/�S G�i,Q[�eG Date Rec.: _ Ship via:(circle one) Fed Ex., UP 1R0 Courier, Date Due: _ -0 Hand Del., Other Courier, Other. Items to be Checked Upon Receipt Yes No NAT-:: Comments 1. Army Samples received in individual plastic bags? V-11 2. Custody Seals present? 3. Custody Seals Intact? 4. Air Bill included in folder if received? 5. Is COC included with samples? 6. Is COC signed and dated by client? 7. Laboratory receipt temperature. TEMP= �a Samples rec.with ice_ice packs_2neither 8. Were samples received the same day they were sampled? Is client temperature 4•C±2'C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? 10. Does the info on the COC match the samples? ✓ 11.Were samples rec.within holding time? 12.Were all samples properly labeled? 13.Were all samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact?(none broken or leaking) 16.Were VOA vials rec.with no air bubbles? 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH(circle one. =Methano, E=EnCore(air-tight container) Sampling Method VOA(circle one): M=Methanol,SB=Sodium Bisulfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? r/ If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained fro client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into: Internal Tracking Log? Dry Weight Log? Client Log? Composite Log? Filtration Log? Received By: aC• Date: —� — Logged in By: �� Date: GI ?_ Labeled By: Date: 9--�7—Qr Checked By: M Date: _ J _ 27 AMRO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORD Office: (603)424-2022 111 Herrick Street 40387 Fax: (603)429-8496 Merrimack,NH 03054 + ti Project No.: Project Name: IC Project Manager: AMRO Project No.: Project State: WIA— o'- Sample ID Date/Time Matrix Totalo# i Analysis Required Remarks Sampled A=Air of Cont. $=Soil &.Size i GW=Ground W. WW=Waste W. DW=Drinking W. 0=Oil Other-Specify I 14 10 1=90� e s 1 b Au MPIA Vo Preservative:CkHC1,MeOH,N-H 03,S-H2SO4,Na-NaOH,O-Other ContainerType: P-Plastic,G-Glass,V-Via,T-Teflon,O- ter Please print clearly,legibly and completely.Samples can not be �� NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will not start until any FAX No.: ?l :ambiguities are resolved. Send Results To: rti Su,, /rfr-` / " ;•./,. �'C.. < <<.N(rn T— Seal Intact? GW-1 GW-2 GW-3 V:n —r- Yes No N/A MCP Level Needed: , Relinquished By Date/Time Received By Date/Time P.O.No: O .. PRIORITY TURNAROUND TIME AUTHORIZATION ./z Before submitting samples for expedited TAT,you must have requested Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER 0,3 B AUTHORIZATION No. BY: SHEET OF White:Lab Copy Yellow:Accompanies Report Pink:Client Copy = = = Environmental Laboratories Corporation 111 Herrick Street,Merrimack, NH 03054 TEL: (603)424-2022- FAX: (603)429-8496 September 10,2001 Tim Toomey Subsurface Remediation Technologies 355 Central St. Rowley,MA 01969 TEL: (978)948-3861 FAX: (978)948-3861 RE: TRASK,312 Boxford St.,N. Andover Order No.: 0108297 Dear Tim Toomey: AMRO Environmental Laboratories Corp. received 1 sample on 8/31/01 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference(NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s) upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time, AMRO will properly dispose of the remaining sample(s). If you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of 0� pages. This letter is an integral part of your data report. If you have any questions regarding this project in the future, please refer to the Order Number above. Sincerely, 1 Nancy Stewart Vice President/Lab Director 1 I AMRO Environmental Laboratories Corp. Date: 10-sep-01 CLIENT: Subsurface Remediation Technologies Project: TRASK,312 Boxford St.,N.Andover Work Order Sample Summary Lab Order: 0108297 Date Received: 8/31/01 Lab Sample ID Client Sample ID Collection Date 0108297-OIA Stockpile 8/30/01 .. i 2 f AMRO Environmental Laboratories Corp. Date: 10-sep-oI CLIENT: Subsurface Remediation Technologies Client Sample ID: Stockpile Lab Order: 0108297 Tag Number: Project: TRASK,312 Boxford St.,N.Andover Collection Date: 8/30/01 Lab ID: 0108297-OIA Matrix: SOIL Analyses Result RL Qual Units DF Date Analyzed TPH BY GC/FID(MODIFIED 8015B) SW8015B Analyst: KD Gasoline ND 51 mg/Kg-dry 1 9/7/01 11:00:00 PM Mineral Spirits ND 51 mg/Kg-dry 1 917/01 11:00:00 PM Kerosene ND 51 mg/Kg-dry 1 9/7/01 11:00:00 PM Diesel Fuel/Fuel Oil#2 15,000 51 mg/Kg-dry 1 917/01 11:00:00 PM Motor Oil/Hydraulic Oil ND 100 mg/Kg-dry 1 9/7/01 11:00:00 PM Unidentified Hydrocarbons NO 51 mg/Kg-dry 1 9/7/01 11:00:00 PM PERCENT MOISTURE D2216 Analyst: JSL Percent Moisture 4.0 0 wt% 1 9/5/01 Gasoline cannot be accurately determined by this method. Purge and trap sample introduction into a GC or GCMS is the recommended approach for gasoline. Due to the physical,chemical,and biological processes which affect the chemical composition of fuel mixtures exposed to the environment,the qualitative identity of a hydrocarbon mixture as a fuel product is not always conclusive by this method due to the method's reliance on chromatographic pattern recognition. A result provided for a specific fuel indicates that the mixture present in the sample has a chromatographic pattern similar to the laboratory's reference standard for that fuel mixture under specific GC operating conditions utilized at the time of analysis. A result identified as Unidentified Hydrocarbons is based upon the detector response obtained for the laboratory's Fuel Oil#2 reference standard and includes the entire chromatographic response for the sample between n-Alkanes of carbon numbers C9 to C36. Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits J-Analyte detected below quantitation limits R-RPD outside accepted recovery limits B-Analyte detected in the associated Method Blank E-Value above quantitation range H-Method prescribed holding time exceeded. #-See Case Narrative RL-Reporting Limit;defined as the lowest concentration the laboratory can accurately quantitate. 7 i AMRO Environmental Laboratories Corp. 10-Sep-01 Lab Order: 0108297 Client: Subsurface Remediation Technologies DATES REPORT Project: TRASK,312 Boxford St.,N. And Sample ID Client Sample ID Collection Date Matrix Test Name TCLP Date Prep Date Analysis Date 0108297-01 A Stockpile 8/30/01 Soil Percent Moisture 9/5/01 'r111-1 by GC/FlD(modified 801513) 9/6/01 9/7/01 i I AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick S;ree Laboratories Corporation Merrimack, NH 0305 Client 603) 424-202. S�T AMRO ID: (J fra9 7 Project Name: 7 ?AS6t Date Rec.: Ship via:(circle ore) Fed Ex., UP ,AMRO Courier, Date Due: —/D_D Hand Del., Other Courier, Other. Items to be Checked Upon Receipt Ye?; No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? 3. Custody Seals Intact? t/ 4. Air Bill included in folder if received? 5. Is COC included with samples? 6. Is COC signed and dated by client? 7. Laboratory receipt temperature. TEMP= Samples rec.with ice L,11'ce packs_neither 8. Were samples received the same day they were sampled? Is client temperature 4'C±2'C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? t/ 10. Does the info on the COC match the samples? 11.Were samples rec.within holding time? 12.Were all samples properly labeled? 13.Were all samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact?(none broken or leaking) 16.Were VOA vials rec.with no air bubbles? 17. Were the sample volumes sufficient for requested analysis? ✓ 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH (circle one): M=Methanol, E=EnCore(air-tight container) Sampling Method VOA(circle one): M=Methanol,SB=Sodium Bisulfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: 21. Information entered into: Internal Tracking Log? Dry Weight Log? Client Log? Composite Log? e/ Filtration Log? ✓ Received By: Date: _ _ �T .3/—O Logged in By: C� Date: g 0 5 Labeled By: C Date: �� 3/-� Checked By: ti Date: �j-Y Of AMRO Environmental Laboratories Corporation CHAIN-OF-CUSTODY RECORD 0 Office:(603)424-2022 t 111 Herrick Street Fax:(603)429-8496 Merrimack,NH 03054 Project No.: Project Name: 2>7 S Project Manager: .�J Sam Icrs(Sig aturc) AMRO P o`ject No. f O kvn./1 tiP,f_ /hNQdv[ „ (J/ Project State: (Ntn SiA('HZ-a-,&1T J Sample ID Date/Time Matrix Total# Analysis Required Remarks Sampled A=Air of Cont. S=Soil &Size GW=Ground W. WW=Waste W. DW=Drinking W. c, 0=Oil Other-Specify ,\ Preservative: Cl-H ,Me H,N-H 0 ,-S--H—TS-04, a-Na H, -Other Container Type: P-Plastic,G- ass, -Via,T-Teflon,O-Other Please print clearly,legibly and completely.Samples can not be NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will not start until any FAX No.: ambiguities are resolved. Send Results To: Ii As A n J, /1' N Seal Intact? GW-1 GW-2 GW-3 JCj 02O Yes No N/A MCP Level Needed: Relinquished By Date/Time Received By Date/Time P.O.No: � PRIORITY TURNAROUND TIME AUTHORIZATION ��)p �— Before submitting samples for expedited TAT,you must have requested f J�/a/ 0 / P ;!Y Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER i By:. AUTHORIZATION No. BY: SHEET OF i e:Lab Copy Yellow: Accompanies Report Pink:Client Copy i COMMONWEALTH OF MASSACHUSETTS w _ EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS ' DEPARTMENT OF ENVIRONMENTAL PROTECTION Metropolitan Boston—Northeast Regional Office O JANE SWIFT GovernorBOB DURAND t i Secretary OCT 2 9 2001 LAUREN A.LISS Commissioner Mr. &Mrs.Robert Trask RE: NORTH ANDOVER 312 Boxford Street Residential Property North Andover,MA 01845 312 Boxford Street RTN: #3-20874 Revised Immediate Response Action Plan Approval, M.G.L. c. 21E& 310 CMR 40.0000 Dear Mr. &Mrs. Trask: On October 19, 2001, the Department of Environmental Protection (the Department and/or DEP) received a revised "Immediate Response Action (IRA) Plan" (dated October 17, 2001) from you for approval pursuant to 310 CMR 40.0420 of the Massachusetts Contingency Plan(the MCP). The purpose of this letter is to approve the revised IRA Plan. The revised IIIA Plan was developed by Mr. Timothy A. Toomey (LSP - #2891) of Subsurface Remediation Technologies, Inc. of Rowley, MA in response to the sudden release of approximately one hundred fifty (150) gallons of #2 heating fuel oil to above and below the concrete basement floor as the result of the oil feed line becoming damaged during a "lightning strike". This incident was reported to the Department on July 3,2001. In general,the revised IRA Plan indicates that further excavation of petroleum contaminated soil will be conducted to address residual#2 heating fuel oil contamination, and will not exceed the one hundred fifty (150) cubic yard volume previously verbally approved by the Department on August 15,2001. This information is available in alternate format by calling our ADA Coordinator,at(617)5746872. 205A Lowell St. Wilmington,MA 01887 * Phone(978)661-7600 . Fax(978)661-7615 • TTD#(978)661-7679 Za Printed on Recycled Paper ,ta B this s 1 etter, the Department approves the subject revised Immediate Response Action Plan. f If you have any questions relative to this matter, you should contact Mr. Steven S. Ross at the letterhead address or (978) 661-7600. All future communications regarding this release must reference the Release Tracking Number (RTN # 3-20874) contained in the subject block of this ' letter. f Sincerely, f teven S. Ross Environmental Analyst Emergency Response Branch ngsley B.Ndi 11 Emergency Response Chief Bureau of Waste Site Cleanup ' CC. Subsurface Remediation Technologies,Inc., 355 Central Street,Rowley,MA 01969; ATTN: Timothy A. Toomey North Andover Board of Health North Andover Fire Department DEP File/Data Entry i I I Page 2 of 2 x COMMONWEALTH OF MASSACHUSETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS DEPARTMENT OF ENVIRONMENTAL PROTECTION 4 Metropolitan Boston—Northeast Regional Office JANE SWIFT BOB DURAND Governor c Secretary S E 2 1 G 200LAUREN A.LISS J 1 Commissioner i Mr. &Mrs.Robert Trask RE: NORTH ANDOVER 312 Boxford Street Residential Property North Andover,MA 01845 312 Boxford Street i RTN: #3-20874 Immediate Response Action Plan Denial• M.G.L. c. 21 E& 310 CMR 40.0000 vi OvFkFiL, �•.. i20 Dear Mr. &Mrs. Trask: r On September 5,2001,the Department of Environmental Protection(the Department and/or DEP) received an "Immediate Response Action (IRA) Plan" (dated September 4, 2001) from you for approval pursuant to 310 CMR 40.0420 of the Massachusetts Contingency Plan (the MCP). The purpose of this letter is to deny the IRA Plan and to provide you with an opportunity to submit a revised IRA Plan to the Department. The IRA Plan was developed by Mr. Timothy A. Toomey (LSP - #2891) of Subsurface Remediation Technologies, Inc. of Rowley,MA in response to the sudden release of approximately one hundred fifty (150) gallons of#2 heating fuel oil to above and below the concrete basement floor as the result of the oil feed line becoming damaged during a"lightning strike". This incident was reported to the Department on July 3,2001. In general, the subject submittal indicates that additional assessment activities, in the form of the installation of groundwater monitoring wells and soil sampling, will be conducted to further evaluate site conditions. This information is available in alternate format by calling our ADA Coordinator at(617)574-6872.. 205A Lowell St. Wilmington,MA 01887 • Phone(978)661-7600 • Fax(978)661-7615 • TTD#(978)661-7679 C� Printed on Recycled Paper I It is important to note that on August 15, 2001 the Department verbally approved an IRA consisting of(a) the excavation, proper management and disposal of no greater than one hundred fifty (150) cubic yards of petroleum contaminated soil, and (b) the temporary storage of petroleum contaminated groundwater in an on-site frac-tank in the event dewatering became necessary to facilitate the excavation of petroleum contaminated soil. Section 310 CMR 40.0414 - Scope and Types of Immediate Response Actions states that IRAs shall be presumed to require the initiation of one or more containment or removal actions, unless it can be demonstrated, substantiated by a preponderance of evidence, that in general, an Imminent Hazard does not exist, and/or the unmitigated migration of non-aqueous phase liquid (NAPL) is not occurring. The IRA Plan does not provide adequate information supporting the position that an Imminent Hazard does not exist on site. Based upon site assessment activities conducted to date,the unmitigated migration of NAPL cannot be determined. Section 310 CMR 40.0424(1) of the MCP describes what items an IRA Plan must include. The Department has reviewed the IRA Plan and has determined that it does not meet the regulatory requirements of 310 CMR 40.0424 - Immediate Response Actions Plans. Specifically, the Department has determined the following items to be inadequate, missing, incomplete, and/or deficient: • a description of the release or threat of release, site conditions and surrounding receptors; The IRA Plan does not include sufficient information regarding site conditions and how they relate to potential Imminent Hazard M, Substantial Release Migration (SRM), and Critical Exposure Pathway(CEP)conditions. The IRA Plan indicates that the private on-site water supply was tested, however, does not provide specific details regarding purge volume or purge duration prior to collecting the water sample. In light of this, it is unclear whether the drinking water supply sample � represented ac foal aquifer conditions or well water storage tank conditions. • the reason why an Immediate Response Action is required; • the objective(s), specific plan(s) and proposed schedule for the Immediate Response Action, including, as appropriate, plans and/or sketches of the site and any proposed investigative and/or remedial installations; • where appropriate, a proposed environmental monitoring plan, for implementation during and/or after the Immediate Response Action; The IRA Plan does not include response actions necessary to evaluate the potential for petroleum vapors to.impact indoor air quality within the residential dwelling. Page 2 of 3 i On September 25, 2001, Department personnel verbally rejected the IRA Plan during a telephone conversation with LSP-of-Record Timothy A. Toomey, and discussed the technical deficiencies of the IRA Plan with him. During the conversation Mr. Toomey indicated that j approximately ninety (90) cubic yards of petroleum impacted soil has been excavated from the source area, and petroleum concentrations in subsurface soils remain above the applicable MCP clean-up standards. Mr. Toomey also indicated that groundwater depression has not been required due to the depth of the groundwater table at approximately twenty four(24)feet below grade. By this letter, the Department denies the subject Immediate Response Action Plan, and requests the submittal of a revised IRA Plan addressing the issues raised above. The Department reminds you that the revised IRA Plan must include assessment activities necessary to evaluate potential Imminent Hazard (IH), Substantial Release Migration (SRM), and Critical Exposure Pathway (CEP) conditions. Additional Immediate Response Actions will be required in, the event an IH, SRM, or CEP conditions are observed. The revised IRA Plan shall include sufficient assessment activities designed to evaluate the potential for this release to impact indoor air quality and the private on-site drinking water supply well. If you have any questions relative to this matter, you should contact Mr. Steven S. Ross at the letterhead address or (978) 661-7600. All future communications regarding this release must reference the Release Tracking Number (RTN # 3-20874) contained in the subject block of this letter. Sincerely, teven S.Ross Environmental Analyst Emergency Response Branch t gsley B.Ndi Emergency Response Chief Bureau of Waste Site Cleanup cc: Subsurface Remediation Technologies,Inc.,355 Central Street,Rowley,MA 01969; ATTN: Timothy A.Toomey North Andover Board.of Health North Andover Fire Department DEP File/Data Entry Page 3 of 3 SUBSURFACE REMEDIATION TECHNOLOGIES, INC. ENVIRONMENTAL CONSULTING & REMEDIATION SERVJ%So � 355 Central Street • Rowley, Massacftistt3© µA�jK.. BOA ---f�""� , (978) 948-3861 sk 5 2002 , JUP� Iwo May 28, 2002 Massachusetts Department of Environmental Protection North East Regional Office 205A Lowell Street Wilmington, MA 01887 RE: Trask Residence, 312 Boxford Street, North Andover, MA 01845 Immediate Response Action Completion and Remedial Action Outcome Statements, RTN 3-20874 Dear Sir/Madam: On behalf of Deborah and Robert Trask, owners of the subject residence, Subsurface Remediation Technologies, Inc. (SRT) is submitting the following Immediate Response Action (IRA) Completion Report and Remedial Action Outcome Statement in conformance with Department of.Environmental Protection (DEP) and the Massachusetts Contingency Plan (MCP) requirements. The original IRA Completion and RAO transmittal forms are enclosed and copies are included as Attachment 1. Also, since this is submitted after 120 days, a copy of the IRA payment check is also enclosed. Background The release of approximately 150 gallons of heating oil occurred at this site on July 3, 2001. The Trask family returned home after being away, to find that lightning had struck a tree located approximately 15 to 20 feet from the rear corner of their house. They also found that their #2 fuel oil tank had emptied through a ruptured furnace feed line and had seeped onto and below the concrete floor, through cracks. Information regarding nofificafion, verbal IRA approval, soil borings, monitoring well installations, soil and groundwater testing, and excavation of contaminated soil in the furnace room and garage areas of the residence, were all described and submitted to the DEP with the written IRA Plan on October 18, 2001. 1 t � I i The aboveground 330-gallon storage tank is estimated to have lost approximately 150 gallons of fuel oil based on available records. The site is in.a hilly, glacial till area of single family homes, with on-site septic systems and private wells. The surrounding receptors most at risk due to this release are the Trask's own drinking water well, and indoor air at the residence itself. Immediate Response Action As described in the IRA Plan, hand excavation of the room in question began on August 22, 2001, under a verbal IRA, and had continued up to the re-submittal of the IRA Plan on October 18, 2001. Progress was very slow because the underlying glacial till was so dense it had to be jack hammered prior to removing by hand shovel. It also contained numerous, relatively large, rocks. At the time of the IRA Plan submittal, the bottom of the contamination had been found at a 10 foot depth in the furnace room and at a 5 foot depth in the affected part of the garage. Jar headspace readings recorded on October 16, 2001 in the 5 to 10 foot depth range of the furnace room had shown that three grids of sidewall area (JKM) still had high headspace readings. Sidewall location FGHIL (5 to 10 foot depth) was also screened (2 ppmv) and sampled on October 16, 2001 for EPH and was found to meet the required S1/GW-1, Method 1, soil standard. Sample analyses confirmed that the JKM sidewall exceeded EPH parameters but not VPH parameters. The JKM sidewall had previously passed Method 1 standards for VPH (October 2, 2001, FGHIJK). Picking up where the work described in the IRA Plan left off, SRT continued the excavation of the still contaminated sidewalls in the 5 to 10 foot depth. SRT separated the furnace room into grids, as shown on the enclosed Figure 1, and used the lettering sequences to track the sidewall samples. Removal efforts were directed at the 5 to 10 foot depth range in order to backfill to a 5 foot depth and then work on the sidewalls and beneath the foundation in the 0 to 5 foot depth range. Removal on of soils on the JKM sidewalls on October 18 and October 22, 2001, was again directed by jar headspace readings. Approximately 2 1/2 feet of soil were removed from these sidewalls, reducing soil jar headspace readings from the 28 to 50 ppmv range to the 2 to 12 ppmv range. Two composite soil samples were collected from the JKM sidewalls, one from a depth of 0 to 5 feet and another from a depth of 5 to 10 feet. These two samples were designated as J1K1M1, 0 to 5 feet/5 to 10 feet. SRT submitted the samples to AMRO Environmental Laboratories (AMRO) of Merrimack, NH for EPH analysis. Analytical results showed that these sidewalls were now well below MCP Method 1 Standards. These results are summarized in the enclosed Table 1 and 2 SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 t s Attachment 2 of the previously submitted report. On October 29, 2001, clean sand backfill was placed and compacted in 1 foot lifts from the bottom of the excavation to the 5 foot level. Sidewall JKM was also cleaned from 0 to 5 feet by October 22, 2001. Once all affected soils beneath the 5 foot depth were removed and the excavation backfilled, efforts were directed at affected soils at the 0 to 5 foot depth. Screening and further hand excavation and removal of the 0 to 5 foot sidewalls continued on October 30, 2001 until SRT reached a point where further excavation jeopardized the stability of the foundation. Two composite samples (sidewall locations LAI IA A and FGH LF ALF A) were collected and sent to AMRO for both EPH and VPH analysis. Figure 2 and Figure 3 show the lettering sequences used to track the'subject sidewall samples, all taken as composites. Both of the samples collected on October 30, 2001 had exceedances of MCP Method 1 S1/GW-1 soil standards. A structural evaluation to determine underpinning requirements was conducted on November 7, 2001. Underpinning was put in place on November 13, 2001 with excavation of the still contaminated sidewalls in the 0 to 5 foot range continuing from the November 13, 2001 through November 15, 2001. On November 15, 2001, after achieving jar headspace readings in the 0 to 5 foot range of 8 to 14 ppmv, two additional composite soil samples (AFGH and IA) were collected and sent to the lab for EPHNPH analyses. Results were well below MCP Method 1 Standards. Table 1 summarizes all soil laboratory analytical results. The laboratory analytical reports were included as Attachment 2 of the previously submitted report, dated February 20, 2002. On November 28 and 29, 2001, after receiving laboratory analytical results indicating soil concentrations well below applicable Method 1 Standards, the 0 to 5 foot excavation was backfilled, and compacted in 1 foot lifts to grade. Since that time, the concrete floors have been replaced and the basement has been restored to usable condition. Copies of the Bills of Lading for the contaminated soil removal to Brox Industries of Dracut, Massachusetts for recycling are included as Attachment 3 of the previously submitted report. A total of 120.04 tons were removed on September 20 and 21, and November 9 and 16, 2001. The original Bill of Lading was also included in this IRA Status submittal, dated February 20, 2002. Also enclosed in the IRA Status submittal was the copy of the manifest, dated September 14, 2001, for one drum of oily solids/debris generated during the initial response action. On December 31, 2001, the remaining monitoring well (MW-4), proposed as part of the IRA Plan, was installed. The boring log was included in Attachment 4 of 3 SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 f t the IRA Status submittal, dated February 20, 2002. On February 7, 2002, MW-4 and the drinking water well were bailed and evacuated as previously described, and water samples were delivered to AMRO for Volatile Organic analyses by EPA Method 524 (drinking water). Nothing was detected in the drinking water well above the 0.5 µg/l (micrograms per liter or parts per billion) detection limit for the vast majority of compounds. MW-4 showed only 3.1 µg/1 carbon disulfide. Laboratory analytical reports are included as Attachment 2. On May 11, 2002, all monitoring wells were bailed and evacuated, as previously described, including the drinking water well. All groundwater samples were delivered to AMRO for Volatile Organic analyses by EPA Method 524 (drinking water). Results,from all of the monitoring wells did not show any contamination that can be attributed to the 92 fuel oil release. Laboratory analytical reports are included as Attachment 2. The following table shows what was found in the monitoring wells: MW-1 MW-2 MW-3 MW-4 1,4-dichlorobenzene 2.5 µg/1 4.0µg/1 2.1 µg/1 0.8 µg/1 MTBE 3.5 µ 4.O µ 4.4 µ 4.O µ 1 carbon disulfide <0.5 µ <0.5 µ <0.5 1 1.9 1,4-dichlorobenzene is used as a general insecticide, fumigant, and germicide, and is common in moth balls. Its GW-1 Reportable Concentration is 5 µg/1. MTBE is a gasoline additive with a GW-1 RC of 70 µg/1. Carbon disulfide is used in the manufacturing of viscose rayon, cellophane, and flotation agents; soil disinfectants; electric vacuum tubes; herbicides; grain fumigants; and as a solvent for fats, resins, phosphorus, sulfur, bromine, iodine, and rubber. Its GW-1 RC is 1 µ/1. None of these compounds are associated in any way with 42 fuel oil. Nothing was detected in the drinking water well above the 0.5 µg/1 detection limit for the vast majority of compounds. As shown on the groundwater flow map included as Figure 4, the groundwater at the site flows in a south-southeasterly direction. If contamination from the 92 fuel oil release had impacted groundwater, related contaminants would surely have been detected in the monitoring wells surrounding the release area, especially MW-4 which is located immediately downgradient. RISK CHARACTERIZATION The site is in a hilly, glacial till area of widely spaced single family homes, with on-site septic systems and private wells. The Trask residence sits on a relatively 4 SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street - Rowley, Massachusetts 01969 steep hill. The surrounding receptors most at risk due to this release were the Trask's own drinking water well, and indoor air at the residence itself. Figure 2 shows the areal extent of the fuel oil migration within the residence. When the oil seeped through the floor it spread in the six inches of sand underlying the cement floor, then began to seep into the glacial till. The underlying glacial till was so dense it had to be jack hammered to be removed. It also contained numerous, relatively large, rocks. By screening the soils as they were excavated, SRT realized stark reductions in headspace readings when the bottom and sidewall area excavations encountered the limits of the extent of the spill migration. Exposure point concentrations are "0" for groundwater, which is not unexpected given"the depths to the groundwater table (23 feet +), and the extremely dense glacial' ill. No trace of any contaminant was found in the drinking water well after five tests. Exposure point concentrations for soil are considered very conservatively as the last composites collected from the bottom and sidewalls of the excavation. The residence will remain a residence for the foreseeable future. The only possible human receptor will be if someone excavates the areas under the foundation where these concentrations were left. The results of the EPH and VPH testing was on composite sidewalls and bottom samples that have already been averaged by testing the composites put together from each particular area. These concentrations are all below Method 1 standards at their respective locations. If someone does indeed excavate these areas in the distant future, the plane with these concentrations will be mixed with the soils outside the excavation, which are rapidly decreasing in concentration from the Exposure Point Concentrations used, and also with the clean sand used to fill the excavation. CONCLUSIONS/LSP OPINION FOR RESPONSE ACTION OUTCOME The location is classified as GW-1 and GW-3 groundwater since the water table is greater than 15 feet beneath an occupied structure and there are drinking water wells located on the property. SRT based its soil sampling locations on both obvious and likely affected areas as indicated by field screening procedures. The soils classification would be an S3, given their inaccessible location beneath the footing of the building. The preferred cleanup Method 1 standard was selected in consideration of the owner's desire to not have an Activity and Use Limitation (AUL) on the property. Therefore, SRT removed soils to below the S 1 Method 1 MCP standard. 5 SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 t � The reportable conditions of sudden release were eliminated during the initial response by others and do not exist today. The oil and affected media were contained and some of the released product was recovered and placed in drums that were later disposed of by SRT. Seventy-five cubic yards, or 120.04 tons, of affected soils were recovered by SRT and disposed of at Brox Industries, a licensed recycling facility. Confirmation testing indicates no exceedances of the S 1/GW 1 Method 1 applicable MCP standard. This, along with groundwater sampling of four monitoring wells and one private drinking water well, was used as a standard for evaluation of whether or not further MCP action was required for the release site. Based on this IRA, the soil and groundwater samples' laboratory analytical results and visual observations by SRT, the release site presents a condition of No Significant Risk to human health and the environment and a Class A-2 Response Action Outcome is appropriate. Remaining soil concentrations are above the assumed background EPH concentrations which are below analytical method detection limits. JUSTIFICATION FOR NOT ACHIEVING A CLASS A-1 RAO It has been confirmed through the results of several sampling events, that groundwater and drinking water at the site has been determined to contain no substances attributable to the #2 fuel oil spill. Detected non-related substances are below the Method 1 GW-1 Standards. Class A-1 classification The justification for not achieving a C , to meet an assumed background concentration in the soil to below detection limits, is as follows: Based upon the location of the remaining contamination beneath the residence, it P is infeasible to remove the contamination due to the threat which would be presented to the structural integrity of the house. In addition, the existence of the remaining contamination does not pose an immediate threat to the household occupants or the environment. Cleanup standards were a desired S 1 soil classification and not the likely S3 classification as it would be very well inaccessible and beneath a foundation. SRT's cleanup standard for soil on this property for #2 fuel oil is presented in the MCP Method 1 standards and presented in this report. A comparison of these standards with the results reviewed from the sampling program indicated all concentrations of#2 fuel oil remaining at the release area are under the Method 1 S 1/GW 1 standard. This is a desired standard to negate the placement of an AUL. Exposure Point Concentrations are significantly below the S 1 soil standards which are the most strict standards in the MCP. Therefore, it is SRT's opinion that no further remedial or investigative operations would be required regarding this release. Further recovery and remedial operations to obtain background 6 SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 e. concentrations (assumed to be below detection limits) [as defined in 310 CMR 40.0006 (12)] for soil would not be feasible due to the potential impact to the structural integrity of the residence and would not provide proportional health, safety, public welfare or environmental benefits [310 CMR`40.0860 (7)]. An estimated cost for the removal of additional soils beneath the building, to achieve non-detectable petroleum concentrations, would over $100,000 and would not provide a proportional benefit. LIMITATIONS The investigation procedures reported herein were conducted to assess the site at the 92 oil release which occurred at the Trask Residence located at 312 Boxford Street, North Andover, MA, as defined by Massachusetts General Laws Chapter 21E and the..Massachusetts Contingency Plan (MCP 310 CMR 40.0000). The conclusions stated are based on observations of the site made by the writer, review of available public records at the time services were conducted, and interpretation of all data collected. This report was prepared for the Responsible Party for use in an environmental evaluation of the subject property. Future events may alter these findings. Should additional research and/or field investigation reveal inconsistent findings, sections of this report may require modification. No other warranty is expressed, written, or implied. Please contact me at (978) 948-3861 if you have any questions. Sincerely, S�ubsurfac Remediation Technologies, Inc. Timothy A Toomey L /C G President Enclosures cc: Town of North Andover BOH Town of North Andover Chief Municipal Officer Mr. & Mrs. Robert Trask Exeter Environmental 7 SUBSURFACE REMEDIATION TECHNOLOGIES, INC. 355 Central Street • Rowley, Massachusetts 01969 s a TABLES PAGE 1 OF I SOIL SAMPLES Boring/ Soil Reg. EXTRACTABLE&VOLA11LE PMOLI Tar headspacd. Sampling Sample So1VGW C9-C18 ('19-C361 Cll-C221 Xylenes Sample Notes Location Date Depth catagory** aliphatics ahphaticsjaromatics jalipe Hnu/OVA FGH 9/13/01 0'-10' Sl-GWI 330 120 120 0.71 10 HK 9/13/01 0'-10' SI-GWI 1800 330 Soo 19.9 40 Acenaphthene=1.6* IJK 9/13/01 01-10, S1-GW1 1700 330 430 14.5 45 Fl 9/13/01 0'-10' Sl-GW1 3600 540 760 13.6 40 Acenaphthene--l.4* Bottom 9/13/01 10, SI-GWI 62 ND ND ND 5 Acenaphthene-7.1* ABottom 9/13/01 5' SI-GW1 110 ND ND ND 4 A Sidewalls 9/13/01 0--4- SI-GWI 4300 720 920 12 40 Acenaphthene=7.8* FGI-1lJK 10/2/01 0'-5' Sl-GWI 2800 690 1100 10.2 45 Acenaphthene=1.9* FG1-1IJK 10/2/01 5'-10' Sl-GWI 640 230 380 0.37 30 FGFUL 10/16/01 5'-10' Sl-GWI ND ND ND NS 2 JKM 10/16/01 5'-10' S1-GW1 3700 430 780 NS 50 Acenaphthene=3.8* J1K1M1 10/22/01 5'-10' Sl-GWI 230 84 ND NS 10 J1K1M1 10/22/01 0'-5' Sl-GWI 180 70 64 NS 8 LAI IA*A 10/30/01 0'-5' Sl-GWI 3800 1600 1800 1 2.12 6 to 70 Acenaphthene=2.1* (*I,in FGH LF* ALF A 10/30/01 0'-5' Sl-GWI 2400 880 1200 1 4.4 0-70 Acenaphthene=2* *1'in AFGH 11115101 0'-5' SI-GWI 140 NTD 52 ND 14 1A 11/15/01 Q'-51 SI-GWI ND ND ND ND [-6 ......................... ........................................... ....... .............. ....... ..........I............... TAWARPS: ............I................................... ...........................XX ......... ....................................................... X2. ....... OM.0 ... A6k:*—** ........84W him ifila iffiai"r .... .......... ...... ........... ........ . ...... . . ....... ........... GW.W.* ':I SW .......... .... ........ ........................... ............. . .................. X ........ ;:>.«»:<»:>:>: ....... ........... . ............................................. ..................... K.04 . .......... .. . ............... . ..... X: Iwo ... .... ............................. ...................... ............................... ....................... ...................... 00 ..... ...................... ........................... xxm-iij .... ..100.0 ............................ ........... ........................::.............I.................................................... ..........................................................................................I.......... .......................................I..I................................... ................:..:..:.............. .. W..... ......................... ............. .............. rxx.x. " o ....... ..... ....... .............................. ............ ........... . . ...... . . ..... ..... . .00.................... .......... ................... .......... 4ArW........ .. . ........... ................................ .......... . .......... ........ ..... .... ........... ....... .... ........ .....WOO NOTES: ND-Compound not detected above the minimum S-1 through S-3 Soil concentration limit or method detection limit of MCP. Applicable o the particular analytical procedure(See Analytical CMR 40.0975(6)(E Report). GW-1 Standards-Dri TABLE I >-Indicates the detection limit GW-2 Standards-Rej NS-Not Sampled for Particular Chemical and where groundw, Bold/Italic print indicate values over MCP limits. surface. GW-3 Standards-Rej areas are subject to I FIGURES Bottom Garage(A) &Bottom furnace room met AICP Standards on 9/13/01 MW-3 Sidem•all Sample FGHIL Met Standards on 10/16/01 40- IRA Soil F G rLRemoval c'. a 10 A 7 Furnace Room 4— MW-2 I T K JIMM1 Sides;•all met AJCP Standards on Garage 10/22/01 TRUSK RESIDENCE � MW-4 5 - 10 foot ran depth e g 10/22/01 LEGEND 10/22/01 IRA SOIL REMOVAL MAP N 312 Boxford Street NORTH ANDOVER, MASSACHUSETTS SUBSURFACE REMEDIATION Chimney TECHNOLOGIES,INC. 355 CENTRAL STREET :::. Drn By: PDM ROWLEY, MA. 01969 Ck By: TAT (508) 948-3861 ` Date: 20 Jan 02 Bar Scale 0 20 40 FIGURE 1 Scale: 1-in=40-ft (in feet): MW-3 Sidea•all Sample FGH LF* ALF A (*-1'in) 4— IRA Soil Removal F OPP OPPm 4•. 7 P 35PPm i�po .35ppm - 28 L Furnace Room 4— PP A MW-2 6ppm N1 0-50ppm Sample LAI IA* A (*-Vin) I J K J1 K1 J1K1;�11 Sidewalls met MCP Standards on 10/22/01 Garage I TRaSK RESIDENCE MW-4 0 - 5 foot depth range 10130101 LEGEND N 10/30/01 IIIA SOIL REMOVAL MAP 312 Boxford Street NORTH ANDOVER, MASSACHUSETTS SUBSURFACE REMEDIATION Chimney TECHNOLOGIES, INC. 355 CENTRAL STREET ;; Drn B M Y• PD ROVVLEY, ),4A. 01969 Ck By: TAT (508) 948-3861 Date: 20 Jan 02 Bar Scale 0 '-0 40 . . FIGURE 2 Scale: 1-in=40-ft (in feet): I MW-3 Confirmation Sidewall Sample AFGH IIIA Soil Removal F F G H ' Furnace Room A Li4MW-2 K JIK1M1 Sidewalls Confirmation Side«•all met MCP Standards Sample Al on 10/22/01 Garabe '.\4W-4 TR4SK RESIDENCE 0 - 5 foot depth range 11/15/01 LEGEND N 11/15/01 IRA SOM REMOVAL MAP Underpin 312 Boxford Street Temporary Support For NORTH ANDOVER, MASSACHUSETTS Foundation SUBSURFACE REMEDIATION Chimney TECHNOLOGIES, INC. 355 CENTRAL STREET ce Dm By: PDM ROWLEY, MA. 01969 Ck By: TAT (508) 948-3861 Date: 20 Jan 02 Bar Scale 0 20 40 FIGURE 3 Scale: 1-in=40-ft (in feet): i Driveway I MW-3 / P1 4- (68.60) 2 IRA Release/ Soil Removal Area Furnace Rooml MW-2 / (64.76) O MW-1 (68.78) 4- arage X05 MW-4 rR RESIDENCE (64.12) ASEMENT LE V AREA C a a Q Drinking water well O (61.72) B OXFORD STREET LEGEND Bar Scale(in feet): SITE GROUNDWATER FLOW MAP 4/4/02 N 0 10 20 312 Boxford Street-Trask Property MW-1 Groundwater Elevation ofy NORTH ANDOVER, MASSACHUSETTS (66.69) 4/4/02 groundwater elevation COntOur Scale: 1"=20' SUBSURFACE REMEDIATION -�- Monitoring Well (proposed) Date: 5/26/02 TECHNOLOGIES, INC. Monitoring Well o furnace 355 CENTRAL STREET AST Location Drn By: tat ROWLEY, MA. 01969 FIGURE 4 X Release Point —� (508) 948-3861 hole in feed line Ck B :ies L s' I` ATTACHMENT 1 Massachusetts Department of Environmental Protection BWSC-105 Bureau of Waste Site Cleanup IMMEDIATE RESPONSE ACTION (IRA) Release Tracking Number--� � — TRANSMITTAL FORM Pursuant to 310 CMR 40.0424-40.0427 (Subpart D) ! J 201 874 A. RELEASE OR THREAT OF RELEASE LOCATION: Release Name:(optional) T r aqlr R P a i rl a n r P Street: 312 Boxford Street Location Aid: City/Town: Nnrt-h Andover ZIP Code: 01845 ❑ Check here if a Tier Classification Submittal has been provided to DEP for this Release Tracking Number. ❑ Check here if this location is Adequately Regulated,pursuant to 310 CL)IR 40.0110-0114. Specify Program:❑ CERCLA ❑ HSWA Corrective Action ❑ Solid Waste Management ❑ RCRA State Program(21C Facilities) Related Release Tracking Numbers That This IRA Addresses: B.THIS FORM IS BEING USED TO: (check all that apply) Submit an IRA Plan(complete Sections A,B,C,D.E.H.I,J and K). ❑ Check here if this,IRA Plan is an update or modification of a previously approved writlen IRA Plan. Date Submitted: ❑ Submit an Imminent Hazard Evaluation(cornplele Sections A.B,C.F,H,I,J and In. ❑ Submit an IRA Status Report(complete Sections A,B.C.E,H,I,J and I). ❑ Submit a Request to Terminate an Active Remedial System andlor Terminate a Continuing Response Action(s)Taken to Address an Imminent Hazard(complete Sections A.B,C,D.E.H.I,J and K). I Submit an IRA Completion Statement(complete Sections A.B.C.D,E.G,H.I,J and K). You must attach all supporting documentation required for each use of form indicated,including copies of any Legal Notices and Notices to Public Officials required by 310 CMR 40.1400. C. RELEASE OR THREAT OF RELEASE CONDITIONS THAT WARRANT IRA: Identify Media and Receptors Affected: (check all that appy) U'll Air ❑ Groundvater ❑ Surface Water L _ Sedimen!s ® Soil ❑ Wetland ❑ Storm Drain ❑ Paved Su:•faCe ❑ Prhale Well ❑ Public Water Supply ❑ Zone 2 ® Residence ❑ School ❑ Unknown ® other specify. Spill occured within 100 feet of private well Identify Conditions That Require IRA,Pursuant to 310 CA4R 40.0412: (check all that apply) 2 Hour Reporting Condition(s) ❑ 72 Hour Reporting Condition(s) ❑ Substantial Release Migration ❑ Other Condition(s) Describe: Identify Oils and Hazardous Materials Released: (check all Lhat apply) ® Oils ❑ Chlorinated Solvents ❑ Heavy Metals ❑ Others Specify.' D. DESCRIPTION OF RESPONSE ACTIONS: (check all that apply) ❑ Assessment and/or Monitoring Only ❑ Deployment of Absorbent or Containment Materials Excavation of Contaminated Soils ❑ Temporary Covers or Caps Re-use,Recycling or Treatment ❑ Bioremediation O On Site Off Site Est.Vol: 8 0 -0 3 cubic yards ❑ Soil Vapor Extraction Describe: p e s disposal a t recycling faeility❑ Structure Venting System ❑ Store L On site O Off Site Est.Vol.: cubic yards ❑ Product or NAPL Recovery ❑ Landfiti () Cover O Disposal Est.Vol.: cubic yards ❑ Groundwater Treatment Systems Removal of Drums.Tanks or Containers ❑ Air Sparging Describe: ❑ Temporary Water Supplies SECTION D IS CONTINUED ON THE NEXT PAGE. Revised 224195 Supersedes Forms BWSC-005, 006, 010(in pari)and 011 Page 1 of 3 Massachusetts Department of Environmental Protection BWSC-105 Bureau of Waste Site Cleanup Release Tracking Number IMMEDIATE RESPONSE ACTION (IRA) TRANSMITTAL FORM Pursuant to 310 CMR 40.0424-40.0427 (subpart D) 3 '1'2 0 8 7 4 D. DESCRIPTION OF RESPONSE ACTIONS (continued): Removal of Other Contaminated Media !J Temporary Evacuation or Relocation of Residents Specify Type and Volume:1 drum o i 1 debris Ej Fencing and Sign Posting u Other Response Actions Describe: Check here if this IRA involves the use of Innovative Technologies(DEEP is interested in using this information to aid in creating an Innovative Technologies Clearinghouse). Describe Technologies: E. TRANSPORT OF REMEDIATION WASTE: (it Remediation Waste has been sent to an off-site facility,answer the following questions) NameofFacility: Brox industries Town and Stale: D r a c u t;' MA OuanlityofRemediation Waste Transported toDate: 120 . 04 tons F. IMMINENT HAZARD EVALUATION SUMMARY: (check one of the following) 17 Based upon an evaluation,an Imminent Hazard ex?sts in connection with this Release or Threat of Release. 17 Based upon an evaluation,an Imminent Hazard does not exist in connection w h this Release or Threat of Release. Based upon an evaluation,it is unknov,"n whether an Imminent Hazard exists in connection with this Release or Threat of Release,and further assessment activities will be undertaken. GBased upon an evaluation,h is unknown whether an Imminent Hazard exists in connection vrilh this Release or Threat of Release. However, response actions will address those conditions that could p✓se an Imminent Hazard. G. IRA COMPLETION STATEMENT: Check here if future response actions addressing this Release or Threat of Release will be conducted as part of the Response Actions planned for a She that has already been Tier Classified under a different Release Tracking Number,or a Site that is identified on the Transition List as described in 310 CMR 40.0500(i.e.,a Transition Site,which includes Sees rich approved Waivers). These additional response actions must occur according to the deadlines applicable to the earlier Release Tracking Number(i.e.,Site ID Number). State Release Tracking Number(i.e.,Site ID Number)of Tier Ciassified Site or Transition Site: If any Remediation Waste will be stored,treated,managed,recycled or reused at the site following submission of the IRA Completion Statement,you must submit either a Release Abatement Measure(RAI,1)Plan or a Phase N Remedy Implementation Plan,along with the appropriate transmittal form,as an attachment to the IRA Completion Statement. H. LSP OPINION: I attest under the pains and penalties of perjury that I have personalty examined and am familiar Nyhh this transmittal form,including any and all documents accompanying this submetal. In my professional opinion and judgment based upon application of(i)the standard of care in 3D9 CMR 4.02(1),()the applicable provisions of 309 CN,R 4.02(2)and(3),and(iii)the provisions of 309 CMR 4.03(5),to the best of my knowledge.'.. information and belief;— _ > if Section B of this form indicates that an Immediate Response Action Plan is being submi7ed,the response action(s)that is(are)the subject of this submittal(i)has(have)been developed in accordance with the applicable provisions of M.G.L.c.21E and 310 CIAR 40.0DD0,(ii)is(are) . appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(ii)complies(y)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B of this fonn indicates that an Imminent Haiard Evaluation is being submitted,this Imminent Hazard Evaluation was developed in accordance vAth the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,and the assessment activhy(ies)undertaken to support this Imminent Hazard Evaluation complies(y)with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.ODDO; > if SecDon B of this form indicates that an Immediate Response Status Report is being submitted,the response action(s)that is(are)the subject of this submittal(i)is(are)being implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are):.. appropriate and reasonable to accomplish the purposes of such response action(s)as set forth inlhe applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)complies(y)with the identified provisions of all orders,permits,and approvals identified in this submittal.......' > if Section B of this form indicates that an Immediate Response Action Completion Statement or a Request to Terminate an Active Remedial•_ System and/or Terminate a Continuing Response Action(s) Taken to Address an Imminent Hazard is being submitted,the response actions) that is(are)the subject of this submittal(i)has(have)been deYeloped and implemented in accordance with the applicable provisions of M.G.L.c.-21 E.-7 and 310 CMR 40.0DD0,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.ODDD-and(ii)"complies(y)with,the identified provisions of all orders,permits,and approvals identified in this submittal. t_:.a, :,r __ SECTION H IS CONTINUED ON THE NEXT PAGE. . Massachusetts Department of Environmental Protection BWSC-105 - -Bureau-of Waste Site Cleanup Release Tracking Number IMMEDIATE RESPONSE ACTION (IRA) 13.I _ 20874 TRANSMITTAL FORM Pursuant to 310 CMR 40.0424-40.0427(Subpart D) L I t_� H. LSP Opinion (continued): I am aware that significaht penalties may result,including,but not limited to,possible fines and imprisonment,if I submit information which I know to be false,inaccurate or materially incomplete. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),per pproval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable provisions ther �(kA OF I,t qSS• �• qc LSP Name: Timothy A. Toomey LSP#: ?/391 Stamp: r TIMOTHY Telephone: 978-948-3861 Ext.: A. TOOMEY y FAX(optional) No.2891 GISI Signature: Date: r� /, I. PERSON UNDERTAKING IRA: Name of Organization`. T r a c k R a c i rl 2 n C 2 Name of Contact: Ilp hi rah T r g c k Title: Own p r . Street: 112 Boxford Str et City/Town: North Andover State: MA ZIP Code: 01845 Telephone: 978-557-1147 Ext.: FAX:(optional) E] Check here if there has been a change in the person undertaking the IRA. J. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING IRA: (check one) ® RP or PRP Specify: ® Owner O Operator O Generator O Transporter Other RP or PRP: 0 Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E,s.2) Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21E,s.50)) Any Other Person Undertaking IRA Specity Relationship: K. CERTIFICATION OF PERSON UNDERTAKING IRA: 1, 1]_ phr)r ah Track ,attest under the pains and penalties of perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowiedge and belief,true,accurate and complete,and(iii)that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. Vlhe person or entity on whose behalf this submittal is made amts aware that there are significant penalties,including,but not limited to, possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. Y B W ic>�1 w1/ Title: l� (signature) Date: (print / r. j1d?bot� 1°s� /1�4jZ�s�C �� I �� -z— For (print name of person or entity recorded in Section 1) Enter address of the person providing certification,if different from address recorded in Section I: Street: City/Town: State: ZIP Code: Telephone: Ext.: FAX:(optional) YOU MUST COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Revised 2124/95 Supersedes Forms BV✓SC-005, 006, 010(in part) and 011 Page 3 of 3 Massachusetts Department of Environmental Protection 6WSC-104 Bureau of Waste Site Cleanup .. !_:,�!_,, RESPONSE ACTION OUTCO1t1,E (RAO) STATEMENT & Release Tracking Number DOWNGRADIENT PROPERTY STATUS TRANSMITTAL FORM Pursuant to 310'C141140.0180(Subpart B),•:0.C550(Subpart E)E 40,105S(Subpart J) ,ffim ]3 _J 20874 A. SITE OR DOWNGRADIENT PROPERTY LOCATION: She Name:(op!icna!) T I'2 c 1< Ren 4 rl n p,-ig - - Street: 312 Boxford Street Location Aid: ciy/To++n: North Andover zIP Code: 01845 Check here if this Ste localion is Tier Classified. If a i t�1assachusetts Department of Environmental Protection of Waste Site Cleanup f - Release Tracking Number ' RESPONSE ACTION OUTCOME (RAM-STATEMENT & DOWNGRADIENT PROPERTY STATUS TRANSt,41TTAL FORM ;3 20874 ' 1 40.D5W(Subpart E)b 40.1055(Sub;.arl J) Pursuant to 310 CMR 40.0150(Subpart E), C. DESCRIPTION OF RESPONSE ACTIONS: (continued) Chcck here 11 any Response Aclion(s)that serve asthe.zsis for Ly:s RAO Statement invo!ve the use of Innovative 7echnol��e5. (DEP Is Lnterested in using lhis Information to crease an Innolla:i:t Tethnal>ties G1ear nghouse.) Dcs:.'ibe 7er•,hna�ies: D. TRANSPORT OF REMEDIATION WASTE: (it Re-ediation 1';as:e was sent to an o!f-see lzcilr y,ansAtr t`.e tollaving questions) of FacMf. B I Tc+r�amstaie: Dracut MA QrE. RESPONSE tiyofRemerizl;onWzs!eTransporiOI.00a:e: 120 .04 tOt1S ACTION OUTC-Oh;E CLASS: y the Czss of Res nse Action OJcome that apples to ane Si:e or Disp:5.21 5'e. Se1ea ONLY one Crass: V Class A-1 RAO: Specify one of the folh.ing: ' O A Thceat of Relerse hzs b^en eliminated. COntamina`Jon tmS bean:E-Jx!c:z k; e ^.d leve's. : X Class A•2 RSO: You MUST prcvde jstif L n reducing c-D7..inzsic-to backg^round k'se's is in!ersibe. ! rroq• � h an i-n-ecCP_n!ed AC.r ana Use(j-,-z:iOn(AUL)and)---Slj '..atiOn that reducing CAn:oi:11n2:i?1 Cass A-3 f.ACr You h UST ' '�• 'y to a}yr,Jnd lea's is i-!ersi>t t ft zpp,''cable.preside U»carter of a AuL ion Cz:e a Case Lie desi,n 1;'e of L`,e rer�e:y vitt er>:: D Clio f3-1 RAO: Spec�"y oe,.e of dx foflrring: OCtr am:-ztion is .o ase>;wth`a:ky.o-* levels O Coma=.z ion is NOT coals enc v'h ba kgrrJ k�,e'.s. Class f3 2 RAO: You MUST P v,-',k i-imps r':e:'AUL 11 zp,rz:e,prL`x AUL op -Dn e : Class C RAO: CN-ck tx t N you v,Rl Gx,J.K;pcs FiAO C�e-a;>n,F.'ai^f erance a-.:Na^mor='�at L`x See. El Spes"y O.-).e: O ?trs,t Ope ra'i>',and},'ai-Lerz rx O Only 0.- Awve Cpez�x a-�1:air'era•�x(def,-.ed zt 310 C!.!R 40.0.1Jc) ' F. RESPONSE ACTION OUTCOME INFORMATION: of ^ ^-Ow ® 1f ari ft1.0 Corp! '+-e Fee is required,e•'xck!�ere tc ccr:ify L`z Lx fec 1zs b suY�'ed. You h!US7 z"ah a Ry:tx=�' " Gfx c 2,e a i!subcnCing one a more AULs. You n. ea--h an AUL 7ransnh'al Form(Bv,,SC-113)and a cost'of each iT,Pler'rrn:ed AUL + re'.-,e_-d to L.s RAO S'.a:err+enL Speedy Vte 1)7 of AUL(s)txlo+r. (required for an Class A-3 RAGS and Cass B-2 RAOs) , Number of AULs a;.aehed: Notice of Adi.`y ani^itatian O d Use tGm-E of.Ernionmen'al Restriction Sper�!y Vie Risk Gra xder ration McLhod(s)used to acti evt L'x RAO described abave and an Soz and GroundA-*dACategories tpp icabk to the S'f e, " apply at'a511e. . a1 may y ndwatet C y PP . • Groundwater e9«y ' More than one Soil Category and more than one r • stringent soil and groundwater slandards were meL 1!more stn 9 . . . o ' even 9 Be sure to check ori all l.PPUCf.B1 E uteg nes; _ _ Mel; 2 p Method 3 . Risk CharadelionyMeuwd(s)Used TJcthod 1 ' ® S 1 . ® S-2 ®. S-3 --.- Soll Cate2ory(Ks)AP,'�licat�te GW-2 - -' Grou-KN%aler Calegory(ies)APpficabk:. ® GYJ-t > When submitting any Class A-1 RAO or a Class B-1 RAO wtwe contaminatlon is consistent with background Ieveis.do NOT specify A. _ Rlsk Chadcrisstlon Method.• _ _ cannot >'tfihcn submltting any Class A-2 RAO of a Class B-1 RAO wlxre contaminatlon is NOT consistcnl wish background ingRlkC levels,you u 3 use an AUL to malntaln a level of no signifiunt risk Therefore,you must meet 5.1 soil Standards,if using RJsk Charaeteritstlon, Method 1.. _ _.. .. 111 .11♦ VI �I•�• `� '�-�Ilul 1 I V 1�.V�1 VI I LJ��V V 1 V1 I • Bureau of Waste Site Cl- enup. _ RESPONSE ACTION OUTCOME(RAO) STATEMENT & Release Tracking Number DOWNGRADIENT PROPERTY STATUS TRANSMITTAL FORM [3] _1 20874 Pursuant to 310 CMR 40.0180(Subpart B),40.0590(SuSpaA E)b 10.1055(Su5parl J)_ G. DOWNGRADIENT PROPERTY STATUS SUBMITTAL:- - - L tf a Down;radient F.-oper!y, Status Sv_ "a1 Cc r:f anw Fre is re;.r:ted,C' ;It-:k here to certify tha!the fet has been submY ed. You MUST a"ach a photocopy of the payment. Check here If a Rekese(s)of Oil or Hazardo;:s l,Ive.ial(s),other than Ir-al Ankh is the sutjCt OI this s lbmlilBl,has occurred at this property, Release Tracking Number(s): C1 Check here If the Rekases identified a5ove require funzer Response Actions pursuant 10 310 CIVA 10.0000. Required docurrxntation for a Downgradienl Property status Subrllttal includes,but is not Iirrite-d to,copies of notices provided to owners and operators of both upgradient and downgradient aburiing properties and of any known or suspected source properties, H. LSP OPINION: I a"esl under the puns and penalties of perjury that I have persorzfy mrnined and am familiar with this t a^srni"at form,i•+cluding any and all documents accompanying this s654iral, In my prolessio-al opinion a:-/d iud^ymenl based upon application of(i)Lhe standard of care in 309 VAR :.02(1),{ii)the appl�51e prop cions of 3x09 CII!R 4.02(2)z�d(3),and(i ij the pro+isixs of 3a3 CM5 1.03(5),to the best of my kncv,'ed;e,iniorrna ion and belief, > if SecDon B indcates that a Dcwngradient Property S'afus Subris of is txing p�vided,the resvonse zc5on(s)that is(are)the subject of 1, submittal(i)has(have)been developed and impleMeME-d in accordzn:•e nilh 1'e applL=Ne p;visions of M.G.L e.21 E and 310 CIAR 10.DDOO,(ii) is(are)appropizte and reasonable to s camptish the pja-�of such response aera'(s)as set forth in 310 CN.R 43.01 Em 3(2)(b),and(iii)cap!ws(y) rr.1h the identified 7tv:sions of all orders,permits,and zpprcals i e-Lfwd in ris su�•�l: > if SecDon B iodcafes teat ether an RAO S.atemenL Phase f Ca:.?te tars Sjicrnent and/or Periodic Reyiew Opinlon is teing yavided,the response acton(s)t'tat is(are)t'x sub!erl of this su5rn:�J()has ChZa )been deyel -and imp;e-nenI in a rdan a wth the n pli P s prath;n's of M,.G.L e.21 E and 310 CMR 10.0000.(i)is(are)app r7 ale and re25a rhe to s�rnpGsh the p rpo-ses d such respor•ae&c. (s)es set forth in the zppFrrabe•Urv,s+ons of M.G.L e.21E and 310 CI,r,R 40.0D00,and nu =r9besb')v h the identified prc,-' i°rs of all ordars,permits,and apprffais identified in this sUSrrli:tal. I am 2-Awe t`�at pry ties rzy result.in.^luding,5aj,nd rrn- .ed to,p::!K fres and ^,ent,e I su5mil inforr.atian%sohich 11:ttiv tr be !a!se,ina�.rrate or rssa:e.�I.y cx:arnTeta_ ._ . . - , Check lire tf t'tt Respnrse AC;71(s)on which th:•s opinion is✓st- r sTl,L-1(wee)su*ec-4 to arty order(s),pCrr�s)and'or ap^,�^.a1(s) issued by DEP or EPA if the basis checked,you MUST a t a sheer rt�`)�'g t e a•pp'1�5e pr-,>.ti5ia5 L'x-sof. LSPName: Timothy A- Tnr)mPv LSP s: 28 l— Stamp: �THOFr{�SS Te;e�: 978-948-3861 _ E)d-= 17M077iY9`tiN 1 FAX:(oy;xzD �' TOM � 9 No.2891 y siy - CC7� - ��i GID P �rztu e. / /STEP Dale: ! 4-- - FPROFS 11. PERSON MAKING SUBMITTAL:' Name of organization: Trask Residence NarnedCona<t Deborah Trask = T-6e: Owner Street312 Boxford Street Sisie:.--M -- ZJe code: 0184 Cityrrcwn: North-Andover Telephone: 978- 78-557-1147 EA-:,. _ FAx(opt"D J. RELATIONSHIP TO SITE OF PERSON MAKING SUBMITTAL• (chone k ) RP or PRP Spcdfy. Owner. -0pentot`t� -Q Timet CrJw RP a PRP: F-1 Fiduciary,Secured Leader or MuniclpaGty ve h Exempt Status(as ddrxd by kG,L C.21 E-,s.2) Agerxy of PubGe Utility on a Rigid of Wry(as defrxd by NLG.L a 21 E.s.5% _ Any Other Person SuSRir.;r,�7tvs Form Spey Rct> orsNp I . .,.0 I..------ r_—. r"nnrf 010 fin narfl — - Page 3of 4. massachusetts Department of Environmental Protection 6WSC-104 r Bureau d Was!e Site Cleanup RESPONSE ACTION OUTCOME (RAO) STATEMENT & Re;zitseTraclonq Numbef DOWNGRADIENT PROPERTY STATUS TRANSMITTAL FORM r-?_; i Pursuant to 310 CMR 40.0180(Subpar%B),40.0593(Subpart E)d 40.1056(Sum J) It 3 20874 J K. CERTIFICATION OF PERSON SUBMITTING DOWNGRADIENT PROPERTY STATUS SUBMITTAL: i Deborah Trask attest under the pains and penallies of perjury(i)that I have personalty ermined and am familiar wilh the information contained in this submi;:at,including any and all documents accompanying this transml"al for (ii)the, asd on my inquiry _ of IhO.hose individual(s)immediately responsible for obtaining the information.the material information conlarrred herein is,to the best of my k.o edge, information and wief,true,accurate and complete:(iii)that,to the best of my knoMedge.Information and belitf.Me person(s)or eray(es)on whose behalf lhls submirtai is made satisfy('les)the criteria in 310 CMR 40.01&3(2):(!v)that ine person(s)or entity()on w1 re behalf trs subrttiral is made have provided nolice in accordance m1h 310 CMR 40.01 E3(5):and(v)that I am fully author;Zed to make this=lfeslalion on behalf of the person(s)or entcy(lis)legalty responsible for this submitlal. Vibe persons)or en:'y(ies)on"hose behalf this submittal is made islare aware thx Dere are significant penalties,including,bul not limded to,possible fines and imprisonment,for%6ZIully submitting false,inaccurate,or incomp;,-e informa5on. By Title: (signature) For: Dale: (print name of,person or.entry recorded in Seclion I) Enter address of the person provldiny certification,if d;t'erenl from adccess recorded in Setlion I: Strut: Ci'y,'Torvn: Slate: ZIP Code: Telephaoe: ESC.: FAX:(oplival) L. CERTIFICATION OF PERSON MAKING SUBIYJTT.tl-: if you are completing only a Downgradienf Properly Stalus Submitral,you do not need to cc>rn?lefe Lhis section of the form 1, D phclr ah Trask ares;ur-4-- L`ie;tins and penarjes of perjury()t at i have pe:sa-.alty e)carni•-,ed and am !a^.ar vrth Uu c',o-ration eau^le in Lhs subm'�J, idiny L-y and at documen's acc�r'ary*g Lh s tar.&M-=tat form,(iii)that.besed m my inquiry of L'iose ivJi.iC as imr-�ediale!y resporsibte for o ri-ry the info,-72-51n,LY rraleral'cnfoCr ,15on grztai ed'61 L'is s-uh-,:=-at is,10 t1�e best of rTy kin,tie, dge and befit,true,a=z �!e ar.d cmp;e:e,and(E Val I 2--n`--y a Y.�ed to rake Urre Urs atalion on be''�aff of rile-try y resporz ''e for Uyxis s: l'W. V,!-,epecan or "y on wmt behalf tis s br ra!is.lade ar..ra a,sare that Ux a are sig vfranl peraues,inC awing,but rut Fu-�d to, poss!_bse frees and imp-isaru-lent,for wilift0y sun.lj."fa'se,i�a�-rz e,Or i. npie a intarmalion. (s�;ratu,e) For 1. Ot�� - Dale: / (print name of person or errtily recorded in Se-'ion f) Enter address of U-e person prodding certification,if C fcent tram address recorded in Sex--ion 1: Seel: ChlTov,1: Stale: Z1P Code: Tdcphone: F)d: FAX:(optical) YOU MUST COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP ),LAY RETURN THE DOCUMENT AS INCOMPLETE. IF YQU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PE AL1ZED FOR WSSING A REQUIRED DEADLINE,AND YOU MAY INCUR ADDITIONAL COMPLIANCE FEES, ATTACHMENT 2 i _= Environmental Laboratories Corporation 111 Herrick Street, Merrimack, NH 03054 TEL: (603)424-2022 FAX:(603)429-8496 February 25,2002 Tim Toomey Subsurface Remediation Technologies 355 Central St. Rowley, MA 01969 TEL: (978)948-3861 FAX: (978)948-3861 RE: Trask Residence Order No.: 0202053 Dear Tim Toomey: AMRO Environmental Laboratories Corp. received 2 samples on 2/8/02 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference (NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s)upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of thirty(30) days from this report date. After this time,AMRO will properly dispose of the remaining sample(s). If you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of 6 pages. This letter is an integral part of your data report. If you have any questions regarding this project in the future, please refer to the Order Number above. Sincerely, Nancy Stewart Vice President/Lab Director I 1 A AMRO Environmental Laboratories Corp. Date: 25-Feb-02 CLIENT: Subsurface Remediation Technologies Project: Trask Residence Work Order Sample Summary Lab Order: 0202053 Date Received: 2/8/02 Lab Sample ID Client Sample ID Collection Date 0202053-OIA MW-4 2/7/02 0202053-02A Drinking Water Well 2/7/02 1 2 i AMBO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 Client: T- AMROID: 603 424-2022 Project Name: Date Rec.: Ship via: (circle one) Fed Ex., UP ,AMRO Courier, Date Due: Hand Del., Other Courier, Other. Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? f/ 3. Custody Seals Intact? 4. Air Bill included in folder if received? 5. Is COC included with samples? f/ 6. Is COC signed and dated by client? 7. Laboratory receipt temperature. TEMP =�4 Samples rec.with ice V-ice packs ✓neither 8. Were samples received the same day they were sampled? Is client temperature 4°C±2°C? r� If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? 10. Does the info on the COC match the samples? t/ 11.Were samples rec.within holding time? 12.Were all samples properly labeled? 13.Were all samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact?(none broken or leaking) 16.Were VOA vials rec.with no air bubbles? 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH (circle one): M=Methanol, E=Encore(air-tight container) Sampling Method VOA(circle one): M=Methanol, SB=Sodium Bisutfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: TAT: i 21. Information entered into: Internal Tracking Log? Dry Weight Log? Client Log? Composite Log? Filtration Log? Received By: 14C- Date: C Logged in B Labeled 8 gg y: CL Date: Y CL Date: —/l—D Checked By: 1116, Date: NA= Not Applicable gc/gcmemos/forms/samplerec Rev.18 0100 ' AMRO Environmental 111 Herrick Street Laboratories Corporation Merrimack. NH 03054 (603) 424-2022 Please Circle if: Sample= Soil Sample=Waste List Preserv. Volume Final Volume Preserv. Initial Acceptable? Added by Solution 10 Preservative adjusted Sample ID Analysis Sample Listed pH Y or N AMRO of Preserv. Added pH c�l — owl I I i I I I I I I i i i I i i I t I i I I I i t I I I I I I I i i I i I PH Checked By: Date: pH adjusted By: Date: gc'gcmemcs/forms/samplerec Rev.18 06100 4 j. i AMRO Environmental Laboratories Corporation 111 Herrick Street 3 5 7 5 Merrimack, N.H.03054 Office: 603-424-2022 Fax:603-429-8496 CHAIN OF.CUSTODY RECORD i Proj.No. Project Name - r Project State MATRIX PAGE OF Water-A 01 Soil/Solid-S Samplers(Signature) �� ?' / Type Waste-W Size, Other-0 &No.of Containers Explain �^ Sta.No. Date Time Comp Grab Station Location Remarks 3 4.L Gli � Please print clearly, legibly and completely. Samples cannot be logged PRIORITY TURNAROUND TIME AUTHORIZATION in and the turnaround time clock will not start until any ambiguities are Before submitting samples for expedited T.A.T., you must have requested in advance and resolved. received a coded T.A.T.AUTHORIZATION NUMBER. AUTHORIZATION NO. T.A.T. authorized by: Relin uished b (Signaturgl.— ate Tim ]b v J Receiv ( nature) ❑Fax to(phone) Send Results to: Results needed Relinquished by(Signature) Date Time Received by(Signature) P0# Relinquished by(Signature) Date Time Received by(Signature) AMBO Project No. Remarks Seal Intact? ; Iinq d y Signature) at Ti Received Ved�for Lab Yatoryp�j igna use ,/�/,� J Yes No N/A White:Lab copy Yellow:Accompanies report _- m : ient copy a '�.�•i'i .• :•i•ii':. �i/i•/i�: •:�iii�iL. ..,��';. \.\�:. %///i•� �•�i�iii'7i//iii//ii' .�i��iii�; 1�/iijiii• •ii��i•�\. •�•/• \:\:i..•rl%I •�l♦ ♦\.' \:i..�l:i �,• `\.• �\:i..i�I i• �•i'r •`�•• \:i•.•i%I�• '.i'" •�\�•' \:�..'i11• ./'i••. �IIi •i•I ••\\1`i\�..ilil i•%/I•. i\\\\iii\r rl•%i///;.,::'. r`\\11\.\r rl i%i/I//•ri\\\\i\ilr i%II//I�/;rr: ��\��1;;1.rl lli////•r •`\\�. The Commonwealth of Massachusetts T.a Department of Environmental Protection Division of Environmental Analysis Senator William X. Wall Experiment Station - certifies 'Z M-NH012 AMRO ENVIRONMENTAL LAB 111 HERRICK ST MERRIMACK, NH 03054-0000 — Laboratory Director: Nancy Stewart for the analysis of NON POTABLE WATER(CHEMISTRY) ZZ ' POTABLE WATER(CHEMISTRY) NIX pursuant to 310 CMR 42.00 This certificate supersedes all previous Massachusetts certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CNLR 42.00. This certificate is valid only when accompanied by the latest dated Certified Parameter List as issued by the Massachusetts D.E.P. Contact the Division of Environmental Analysis to verb the current certification status of the laboratory. Certification is no guarantee of the validity of the data. This certification is subject to z unannounced laboratory inspections. Issued- 01 JUL 2001 f-Ypires: 30 JUN 2002 Director, Division of Environmental Analysis , ;�:: p i i•i ::;:� p S�iii q ;iii•%9•pr ::�: ':i iii i'Y,' ;;.;;:,t�:7. 'i r•i :�:�:t f ,��t�: •:.��.�iia::.' %.�i/�i•�'::�iiCiQi�}` :�/�fii�i 1:�4ii��+�j:/ .�.�iii�;;1';�iCi���i`/ ':�i�ii�%"'.'��ii��i�i: ii�i�iiiil'1;',C�i��i•� :�,�// i::fr ..!!!. .�iiit:; '•:�,\i���. '.�.iii/��. •I...i!!. .,�iiiiN '•�:��!.• '.iii i/iSY'r:��.��.!. .,�iij%'...' �?i�i!,' ''4iiiji�. COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of: 10 FEB 2002 M-NHO12 AiMRO ENVIRONMENTAL LAB N ERRIMACK NH NON POTABLE WATER(CHEMISTRY) Effective 10 FEB 2002 Expiration 30 JUN 2002 Date Date Analytes and Methods ' ALUMINUM EPA 200.7 ORTHOPHOSPHATE EPA 300.0 ANTIMONY EPA 200.7 TOTAL PHOSPHORUS EPA 365.2 ANTIMONY EPA 204.2 CHEMICAL OXYGEN DEMAND EPA 410.4 . ARSENIC EPA 200.7 BIOCHEMICAL OXYGEN DEMAND EPA 405.1 ARSENIC EPA 206.2 TOTAL CYANIDE EPA 335.2 ARSENIC ASTM D2972-93(C) NON-FILTERABLE RESIDUE EPA 160.2 BERYLLIUM EPA 200.7 TOTAL RESIDUAL CHLORINE SM 4500-CL-G CADMIUM EPA 200.7 OIL AND GREASE EPA 413.1 CHROMIUM EPA 200.7 TOTAL PHENOLICS EPA 420.1 COBALT EPA 200.7 VOLATILE HALOCARBONS EPA 624 COPPER EPA 200.7 VOLATILE AROMATICS EPA 624 LEAD EPA 200.7 CHLORDANE EPA 608 LEAD EPA 239.2 ALDRIN EPA 608 MANGANESE EPA 200.7 DIELDRIN EPA 608 MERCURY EPA 245.1 DDD EPA 608 MOLYBDENUM EPA 200.7 DDT EPA 608 . NICKEL EPA 200.7 HEPTACHLOR EPA 608 SELENIUM EPA 200.7 HEPTACHLOR EPDXIDE EPA 608 SELENIUM EPA 270.2 POLYCHLORINATED BIPHENYLS(WATEF EPA 608 SILVER EPA 200.7 POLYCHLORINATED BIPHENYLS(OIL) EPA 600/4-81-045 STRONTIUM EPA 200.7 THALLIUM EPA 200.7 THALLIUM EPA 279.2 ZINC EPA 200.7 PH EPA 150.1 SPECIFIC CONDUCTIVITY EPA 120.1 TOTAL DISSOLVED SOLIDS EPA 160.1 TOTAL HARDNESS(CAC03) EPA 200.7 CALCIUM EPA 200.7 MAGNESIUM EPA 200.7 SODIUM EPA 200.7 POTASSIUM EPA 200.7 TOTAL ALKALINITY EPA 310.1 CHLORIDE EPA 325.3 CHLORIDE EPA 300.0 FLUORIDE EPA 300.0 SULFATE EPA 300.0 AMMONIA-N EPA 350.2 NITRATE-N EPA 300.0 NITRATE-N EPA 353.2 KJELDAHL-N EPA 351.1 ORTHOPHOSPHATE EPA 365.2 January 18,2002 *Provisional Certification Page 1 of 2 COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of: 10 FEB 2002 M-NHO12 AMRO ENVIRONMENTAL LAB MERRIMACK NH POTABLE WATER(CHEMISTRY) Effective 10 FEB 2002 Expiration 30 JUN 2002 Date Date Analvtes and Methods ANTIMONY EPA 200.9 ARSENIC EPA 200.7 ARSENIC EPA 200.9 BARIUM EPA 200.7 BERYLLIUM EPA 200.7 CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COPPER EPA 200.7 LEAD, EPA 200.9 MERCURY EPA 245.1 NICKEL EPA 200.7 SELENIUM EPA 200.9 THALLIUM EPA 200.9 NITRATE-N EPA 353.2 NITRITE-N EPA 353.2 FLUORIDE EPA 300.0 SODIUM EPA 200.7 SULFATE EPA 300.0 CYANIDE SM 4500-CN-C,E TURBIDITY EPA 180.1 CALCIUM EPA 200.7 TOTAL ALKALINITY SM 23208 TOTAL DISSOLVED SOLIDS SM 2540C PH EPA 150.1 1,2-DIBROMOETHANE EPA 504.1 1,2-DIBROMO-3-CHLOROPROPANE EPA 504.1 January 18,2002 *Provisional Certification Page 2 ofi �2 I d CAr" � 4 ,er ve 317 Elm Street Milford NH 03055 Tel(603)673-5440 Fax(603)673-0366 February 21, 2002 Ms. Nicole Borduz AMRO Environmental Laboratories Corp 111 Herrick Street Merrimack, NH 03054 Job Name: Trask Residence Laboratory#: 02020078 Job#: 02020053 Purchase Order#: N/A Location: N/A Control#: 39950 Dear Ms. Borduz Enclosed please find the laboratory results for the above reference samples that were received by the ChemServe sample custodian, under chain of custody control number 39950 on 02/12/02. Samples were collected on 02/07/02. Any abnormalities to the samples on receipt would be noted on the enclosed chain of custody document. This report is not valid without a completed ChemServe chain of custody with the corresponding control number, attached. All samples analyzed by ChemServe are subject to quality standards. These standards are either as stringent or more stringent that those established under 40 CFR Part 136, state certification programs, and corresponding methodologies. ChemServe has written QA/QC Procedures Manual that outlines these standards, and is available, upon request, for your reference. Unless otherwise stated on the Chain of Custody or within the report, all holding times, preservation techniques, container types, and analytical methods are analogous with those outlined by them U.S. EPA. certify that I have reviewed the above referenced analytical data and state forms, and I have found this report within compliance with the procedures outlined in the ChemServe QA/QC Procedures Manual. Ellen Abrams -QA/QC Manager Jay Ch7co Laboratory Director This rens 8 pages. �N ACCOA Altp -ilk rr, 0r, . 1 Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO ENVIRONMENTAL LAB LAB#:02020078-01 JOB NAME:Trask Residence LOCATION:N/A SAMPLE IDENTITY:MW-4 CONTROL#:39950 DATE SAMPLED:02/07/02 DATE RECD:07/12/02 DATE ANALYZED:02/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE 3.1 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 NOTE.NON TARGET COMPOUNDS PRESENT BDL=BELOW DETECTION LIMIT ANALYZED BY:TD Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO ENVIRONMENTAL LAB LAB#:02020078-02 JOB NAME:Trask Residence JOB#:0202053 LOCATION: NIA SAMPLE IDENTITY:Drinking water well CONTROL#:39950 DATE SAMPLED:02/07/02 DATE RECD:07/12/02 DATE ANALYZED:02/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHAN E BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO ENVIRONMENTAL LAB LAB#:02020078-01 JOB NAME:Trask Residence JOB#:0202053 LOCATION:N/A SAMPLE IDENTITY:MW-4 CONTROL#:39950 DATE SAMPLED:02/07/02 DATE RECD:07/12/02 DATE ANALYZED:02/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 6ROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES a - a Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO ENVIRONMENTAL LAB LAB#:02020078-02 JOB NAME:Trask Residence LOCATION:N/A SAMPLE IDENTITY:Drinking water well CONTROL*39950 DATE SAMPLED:02/07/02 DATE RECD:07/12/02 DATE ANALYZED:02/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE'! BDL 0.5 1,2,3-TRICHLOROPROPANE,',. BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD rC00 , x CHEMSERVE VOA SPIKE RECOVERY FORM EPA METHOD 524.2 CUSTOMER:AMRO ENVIRONMENTAL LAB LAB#:02020078 JOB NAME:Trask Residence LOCATION:NIA` SAMPLE IDENTITY:MATRIX SPIKE 02020095-01 CONTROL#:39950 DATE ANALYZED:02/16/02 COMPOUND CONC ADDED AMT REC %REC (UG/L) (UG/L) 1,1-DICHLOROETHENE 4 4.4 110% BENZENE 4 4.2 105% TRICHLOROETHENE 4 4.2 105% CHLOROBENZENE 4 3.3 83% 1,2-DICHLOROBENZENE 4 4.3 108% 1,3,5-TRIMETHYLBENZENE 4 3.3 83% 1,2,4-TRICHLOROBENZENE 4 4.0 100% VOA MATRIX SPIKE REC 6 5 4 ■CONC ADDED UG/L 3 0 LW RECOVERY 2 OLD RECOVERY 01 1 2 3 4 5 6 7 SPIKE RECOVERY LIMITS 70-130% A111RO Environmental Laboratories Corporation ..CHAIN-OF-CUSTODY RECORD7 L Office:(603)424-2022 I 111 Herrick Street J V Fax: (603)429-8496 Merrimack,NH 03054 Project No.: Project Name: '714 $, E.512j Project Manager. Samplers(Signature): AMRO Project No.: Project State: _ Sample ID Date/Time Matrix Total# Analysis Required Remarks Sampled A=Air of Cont. S=Soil &Size ` GW=Ground W. WW=Waste W. DW=Drinking W. O ' O=Oil - Other—Specify 7o? /0 3- o UUf>�71 WEc-L- Preservative: -HCI;McOH,N-HNO ,S-H2SO4,Na-NaOH,O-Other C Container Type: P-Plastic, -G ass,V-Via,T-Teflon,O-Other G. Please print clearly,legibly and completely.Samples can not be // NOTES:Preservatives,Special reporting limits,Known Contamination,etc; logged in and the turnaround time clock will not start until any FAX No.: ambiguities are resolved. Send Results To: / OA S> Seal Intact? GW-I GW-2 GW-3 0-5 l„f.. .. ` Yes No N/A MCP Level Needed: Relinquished By Date/Time Received By Date/Time P.O.No: 02 W • e--t"u PRIORITY TURNAROUND TIME AUTHORIZATION Before submitting samples for expedited TAT,you must have requested Results Needed in advance and received a coded TAT AUTHORIZATION NUMBER `9 Y: AUTHORIZATION No. BY: 1,7 V, i tri ,:. G; SHEEN OF i' White:Lab Copy Yellow:Accompanies eport Pink:Client Copy Chain of Custody No. 39,950 Multiple COC's Yes No (�hemtlerve 317 Elm Street Milford, NH 03055 (603) 673-5440/Fax (603) 673-0366 CHAIN OF CUSTODY A --'CUSTOMER WORMATION11INFORMATIONc CUSTOMER: i JOB NAME: TURNAROUND TIME:(CIRCLE ONE:) ac ADDRESS: JOB NUMBER: STANDARD RUSH CITY/STATE/ZIP LOCATION: RUSH T.A.T. (CHECK w/LAB) TELEPHONE: TELEPHONE: AMBER GLASS(AG) / GLASS(G) / PLASTIC(P) 4 cz REPORT TO: CONTACT: O��w tiJ4 P O NUMBER: QUOTE NUMBER: G� w4 SAMPLE I MATRIX Q4 p SAMPLE IDENTIFICATION&LOCATIONQ COLLECTED to TYPE a SOLID(S) c 0 ["[BIND F:D D( 0 COMBINED _ ® ANALYSIS CJ HAZARD(11) O Pj DAIE TIME PALE UME DATE TIME .. PACE TIME DATE TIME DATE TIME DATE TIME DATE TIME MILITARY SAMPLE CHECK LIST: _ FIELD READING(S): ® CUSTODY SAMPLER: PA1E 11ME RECEIVED WITHIN HOLD TIME CS-'OR NO (print name) RECEIVED IN GOOD CONDITION(:�q OR NO SIGNATURE: TEMP BLANI(----- 'C e C:--g DACE nm SHIPPED O AND LIVERED RELINQUISHED: SAMPLES WERE PROPERLY PRESERVED 'E$.) NO /A DATE TIME SAMPLES WERE FILTERED IN FIELD LAB /A' RECEIVED: IF NO EXPLAIN: DATE TIME RELINQUISHED: RECEIVED FOR LAB: DATE IVAL ?.. / ( GROUP# C-)7c7_ U 6 2/l7 '�".•4.''.,:�:L...�Y 4.'r;.,.d..�.� `�: ;F;,.L3y:•;,�'•'Yti,E:L..'„.,.:fr,.E,1:'1.::a.V.,.l:.,(.r.w..y71s.Et��..,tJJ�,•'••:r...:,Tfhi^:;:).'•.1::-.••.;rH.,+4;ti:. t �`.rT,,;,^�!: •� : 1• NEW HAhPSE1RE ENVIRONMENTAL LABORATORY ACCRt7 tT ATION PROGRAM 1 :: V r � A F n v C e ev,,e. Inc . 317 Elm Sueel.Md1oW.NH 03055 16031 673 5440 PJye 1 of 4 _ ,IE' a::�l �'�`M M -� Laooralor n m Cer1,I,CJle NurT:cer 100601 A Dale of Issue December 3. 2001 EKpgat.on Dote: December 2. 2001 ACCREDITS THE ABOVE MENTIONED LABORATORY FOR THE FOLLOWING ANALYSES. L•"a .. SES. 1'&ii• ( I� DRINKING WATER MICRO DRINKING WATER INORGANIC CONTAMINANTS tCon1 I a State of J\1'ev,YrIrrr1751r_ir"e f :,• 511 9112 R C.,i It Iu141 Sr.,4500 Coo E IEn-r-IironmentafLaGonitc�ry��ccrLl�fitEitivrr �I rc��r��rrr srl�::,d II��;cs EPA IOU J :. 5r.1 1111 R Ha• SM 2140 B ^l - ;` ,. Y,.}�9.' �% ac•ar..la.a PI,Ir:.unl SIA y115 R N•U JIC N EPA]OU U /bc I ur _In_. 4 Sr,1911t a N,Lne N EPA 3000 51./9:11 0 UnnoP....Pn... EPA 30011 Sed 9111 R 0.Uwynua.r"1c EPA 365 2 ��•� P.. EPA 1501 !,ra - DRI/IKI/IG WATER/.1E TAl5 , 1�\\-Ards P1ln zirl Acc eL limI011 to) `. _N SwI,Ie EPA 3000 rh; iia S,.IUIr EPA 315 4 !. _ EPs 20.11 IuI,I/,n H,•s.d,.c,tOS, Sr•17541;C y\ ,'a `�•- - EP^_.iJY Iu1n,JJ, EPA 1801 EPA IUO 7 �'~s'•'' (/�� (• r ':-•j EPs 1�iG 7 1 T "ll J t-lrce/ Inc. -- a`'' '-'• (;a DRINKING WATER IgINAIOMETHANEs d..r EP ,-,-•.,;` u l or. _ EPA IVv 7 RIJI„Jena r,lunlmeIhanr EPA 524 2 il(.: ; �l•1 i�/clrlf '\'JL Ease.'J3 7 R........l,,.rn EPA 524 2 r ✓ F dJ; CnWIUJ,nmmun,etl,J^i EPA 514 1 EPA 514 2 EPs,.;0 7 LInnamrcuunrs EPA 514. EPA:CJ 7 EPA eco 7 For the .11T.11yses 1IstCd 011 the.111,IeheLI page(s) in accordance \\ith u •J,-IJ��r+• EPA IUU 7 DRINKING WATER votnTlfE ORGANICS '_'•`'�a r<: } the pros isions of the NLL1�(' Standards and Enl-C 31111. �';`_� •' EPA:JS 1 r / !.1_•.ur.•_m (Ps;a.J 7 1 1 I 1 leu4anlorortnanr EPA 52-'2 N•C•eI/ EPA 1JU 7-;ii.:�•a � 1.1 1 Tntmorormane EPA SN 2 L Pip Nmm EPA 1JU 7 1 1 2 2 te—Colnuueth4ne EPA 524 2 \``: aI ir.•` j Sr t.,.m EPA 100 9 1 t 2 Ir,,.m,n oerhane EPA 524 2 5.. (PA 1UJ/ 1 1 G•,,hl,✓,rinal,r EPA 524: "S + `' _..1_-• EPA 100 1 I 1 U.o,�.un.Irne EPA 524 1 .:.i' I';: '.PA•r.rr A u'.....Pc , EPA 514 1 JJ. i 7 1 1 1 Ir„r nhcnlene EPA 514. ;,,.u��1! �`.1:.1�♦ (�, `A r....... ..nr.P.,nr EPA 1 J Ir„r,.,,•In.,nrr.,e IPA 514Number: 100101 ORINKING rATER INORGANIC CONTAMINANTS J 57Jnela�po EPL 514 2 11sEIL: December t. 2011 EPA S24Date III - t r,�o a.j / -::D. d •< U'A i ! ; 1 U.—. JuruP,ne EPA 514 2 1 i // / + AJJ : f..A _ )O,r.m.,r..ncnra•ne EPs 514 1 I. l _1111_ENIMIM1011 Date: December-. [PA5: '..ua t•1oa'II In\6-c / ., �•.•:• .. t 3 a 1„u.......n...,:.r,. EAG 5:4 ry;.; EPA S1:. 1. ,n(J..r.1,Ian•,n u...,l.P.nJa„1.•n.u..a�..lul.,n.,,,,, ,.n., ,,,.n,n '���"'a 1u,L•n.r,m,.a.rlr.n,.I,n,r,L.r...,,n.rn.I,I�.n..,n 1 .�r:•I.P.n.r. - elap _.!. =? A /�s 'w n. R1., A .1' �•. .I T. � 1: .rr 1_.. .a_ef 4n e.e.,J,.aI, ��/;lti4r✓ /�, /� o ---� • . _"� �__ •1. •:;i ,E�••,_,.s+��`�y,+;�a�11•'.•�'_•�'•: .`•'6•,.. `/�. >:•:~' ;.,�,;i''.::' M d I Rte\ <, le�9a Sonoec EACH ,Aver M AARK ton= m S S` \ ti TfEAWO rH r I a` ct` •f, r•, Sv osarra �°i Lx. S, cn,a. P ul -Farm d CLARK 1P _ t° m • 1 5 r ti © C Ea .4s - i POi'LCfI Yu v0 O fpr HILL y F NAIIC'®� "1 a ° D f USHING W CE ERAL �ty D y S LO 6 P '':Wil \'° to^ ♦ = T f Z 1.. SC: F t YEY rO r°Sr m l e R �;'.�. - °a BLDG S C` eay°� G �J Q0 LONGS o r C KEEFE PN 1,QD yd 6�N 4'o m 0 O O VOCA rIONaL ,'FR a O y �4LLAR0 l r SCH LOR/ G� O e Rd { °(a\' JIY r 6 135 J ° �r 1 ..... 8� \ P S', .....JB. p .II _ P'd r$ fyP m C'Gt s A p ar o ` y sl rJ PI r .....C4 ....E7 r DeSo Av CnaNei q n \ my m \T. .....D8" � / < .. .. '^' rt o T ....H7 Mansfield St........H7 I '< as D Sr..:,. 9y sc '° ° e q0, r� V .....G6 Maple La.............GS Merle Ros q ° << ARRCIS11 sue F4 Maple St..............GS Ld See _ Coburnville 0 ANNA O Q C St ....E4 Maplewood St.....07 SODe. = ��p\d``O MURPH ° ° o r^m g e e .....JS Marble Sl.............J7 r• m Qr' PLG ° eo e s a\ ....E8 Marfan Rd............J7 to ° ....KS Mark Rd..............C7 Nixon Rd.............C2 c ° c� _...D8 Mary Agnes Rd..C6 Nob Hill Dr........... 44 CS a° _ y •�aY'v�HaY .....E8 Massachusetts Normal Hill Rd....GS -. -'_` `. St res o6�` Brook ...K5 Tnpk(Toll).......G 1 Norman Or..........E7 A _ :.—a ....E8 Maureen Rd........E7 Normandy Rd.....G6 shakam f e ( r ....E4 Mayflower Cir......GS Normandy Rd Ext OiR(� =- � 1 � ...C6 Mayflower Rd......EB .........................G6 N°tm° 3 y - - 4 a' Framingham ...G7 Mayhew St..........G4 North La..............E6 P m ,, ' / ....H4 Mayhew Sl Ext...G4 North Rd.............H4 Framinghar• ,P J 0Framinghar _.. E2 Maymont Of........E8 North St..............08 Pinewood Or.......D7 ro� da I tr ° �<`' Framingham . .H3 Maynard Rd........F4 Oak Crest Or......G3 Pitt RO..............._F6 w ; a rm°Y 9a m Go Framinghar ...07 Mayo St....._........E6 Oak PI..................J6 Pleasant St.........F2 o i Framinghar ...C7 McAdams Rd......04 Oak St.................F5 Pleasant St ` O�dOyh ° Rd 3: Framingham ...J5 McAfee AV...........K6 Oaks Rd..............G6 Connector.......G1 ,�qy aa4 ° Medical r ....E8 McCarthy Cir......H2 Oakvale Rd.........C6 Pleasantview Ter..F2y 1 i Garden in!r' _..04 McDonald La......H3 Oakwood Ct........C7 Pond St...............H7 ° C^e ° ' Hemenway°- ...E4 McLaughlin St.....G6 Old Central Tnpk..J5 Poplar St.............E5 Royce Rd............F7Thai°\/�✓ Whittier St...........F8 Winter St.............H5 Juniper HSL ...O6 McPhee Rd.........F7 Old Connecticut Portmore La........H4 Russell Cir...........G4 �. //�I,� 1 Upland Rd........... F7 Wickford Rd........E6 Winter Ter...........G4 Keefe Vocal ....H6 MCQuinn Cir........F2 Path.................F8 Poskus Rd...........F6 Russell Rd...........G4 �° Upper Joclyn Av.. E7 Wild Oak Rise.....E6 Winthrop St..........J5 Lake Coch,. ....H6 Meadow La.........D8 Old Wood Rd......G4 Potter Rd.............06 Russin AV............D8 Stillman St............J8 Upper Rd.............G1 Wilde AV...............J5 Winthrop Ter........J5 Learned Po-- ...E2 Meadow St..........08 Old Worcester Rd Powder Mill Rd....E4 Ruth Or................ F7 Stones Ct............07 Upton Rd.............C7 Wildewood Ter....E2 Wood Av...............J6 Libraries Mechanic St........07 ........................G4 Pratt St.................J6 Ruthellen Rd.......E4 Stony Brook Rd.. G6 Vaillencourt Or.... F3 William J Heights..J4 Wood Ter.............G5 Centrat to. FB Mellen St..............J6 Oliver St..............H6 Prescott St..........G5 Sage La...............D4 Sturgis Rd...........G7 Valentine Rd.......G7 William Welch Wy Woodland Or.......E5 Saxonv,ll, ...ES Melrose Sl..........H6 Olympic St..........E7 Primo Or..............G4 Saint Lo St..........G6 Sudbury Landing..07 Valley Rd.............HIS .. H6 Woodleigh Rd.-...G4 Longs Play_' .....J7 Merchant Rd.......K7 Oran Rd..............G7 Prindiville AV.......H6 Salem End La.....G4 Sullivan Ter...-.....E3 Vanderventer Av..E8 Williams St..........G7 Woodmere Rd....F3 Loring Arent. v..E3 Meredith Cir........E5 Ordway St...........G7 Prior Or...............E7 Salem End Rd....H2 Summer La......... F6 Vernon St............F5 Willis Av...............K6 Woodside Rd......C6 McCarthy S ....F6 Merlin St..............E7 Oriole AV.............H5 Proctor St...........H6 Salmi Rd .............08 Summer St......... F6 Victor Rd..............J8 Willis St...............H7 Woodstock Or.....C3 MCI-Fram. ....G6 Merriam Rd.........F4 Otey Wy..............G2 Prospect St.........F6 Salvi Or................E6 Summit Path.......D8 Victor Rd Ext.......J8 Willowbrook Or...H2 Woodward Rd.....F7 Memorial B,. ....H6 Merrill Or.............C5 Otis St.................H6 Purchase St........07 Sandra Or...........C6 Summit St............J6 Victory St............J5 Wilmont Rd......... F7 Worcester Rd.....03 Melrowesl I: ...J4 Michael Rd..........C7 Overlook Or East Pusan Rd.............J7 Sanger St............H6 Sun Dial Pf..........F4 Vigue Cir.............E3 Wilson AV.............J5 Yorks Rd..............E6 Union Ho ... FS Michaud Or.........F5 .........................C7 Queens Wy.........E8 Saucier St............J6 Sun Valley Or...... F4 Vincent AV...........H5 Wilson St.............H7 1st St....................J7 Millwood Fa ..F5 Middle St..............J7 Overlook Or West Quinlan Or........... F7 Savoy Rd.............C6 Sunset Or............ F6 Vose St.................J4 Winch Pk Rd.......E7 2nd St...................J7 Nobscot Co- F5 Middlesex St.......G6 .........................C6 Raleigh Rd..........E4 Sax Rd................E4 Surro Or..............E4 Wakefield Or.......H2 Winch St .............03 3rd St....................J7 Park....... ....H6 Mill St..................F4 Palmer Rd...........G7 Randy Rd.....:......F7 Saxony Rd..........D8 Susan Or..............J4 Walker's Wy........02 Windsor Or..........05 Pinefield S ..E6 Miller AV..............K6 Palmetto AV.........JS Ransom Rd..........JS Saxony Ter..........D8 Swanson Rd.......D6 Walkup Cir..........D4 Winifred Rd.........ES Numbered Streets Police Stalk' ....H7 Millwood Cir........E3 Pamela Rd..........D6 Raymond St........H6 Saybrook Rd.......F7 Swift Rd...............G5 Walnut AV............06 Winter La............G4 1 Danforth Cl....D8 Post Offices ...H6 Millwood St.........E3 Park AV................D7 Redcoat Rd.........F2 School St ............E8 Sylvester Or........F7 Walnut St............G6 Winter Park Rd...H5 2 Kings Ct..........08 Center St. ...J6 Milton St..............H6 Park PI..................J6 Reed St................J5 Scott Or...............E5 Tally Ho La..........E2 Walsh St.............. F7 Framingh ....H2 Mohawk Or..........C4 Park Rd...............H5 Reni La................F4 Sealtest Or..........ES Tara Rd............... F6 Ward Farm Cir....E5 Points of Interest Saxonvdie ...C7 Monterey La.......F3 Park St.................J6 Reservoir Ridge..G4 Second St............J7 Taralli Ter.............H7 Warren PI............F5 Anna Murphy Playground............................J5 South Fra' ..F4 Montgomery Or..D5 Parker Rd............H2 Rhubena St..........J5 Seminole AV.........J5 Tartufi Cir............D6 Warren Rd..........G6 Armo y:........................................................G6 Potter Road ...D4 Moran Rd............E7 Parker St.............E7 Richardson Cir....H6 Sewell St.............G7 Taylor St...............J6 Water St..............D5 Athenaum Hall..............................................D7 Reardon Pay ..F6 Morse Rd...........F7 Parmenler Rd.....B2 Richardson Cl.....H6 Shady La.............F5 Temi Rd...............C7 Watson PI............D7 Barbieri School................ .................... H5 School Adm' ... F6 Morse Rd Ext.....F7 Partridge Rd.......E8 Richwood St........G7 Shawmut Ter.......H6 Temple PI............G4 Waushakum Blvd..K6 Bowditch Field.............................................G6 Shopper;VV ..G7 Morton St............H7 Patony Rd...........E6 Ricky Or..............H4 Sheehan Cir.. E2 Temple St............ F4 Waushakum St....J6 Brophy Elementary School..........................F3 Shopping C= ...D5 Moulton Park Rd..G5 Patricia Rd..........06 Ridgefield Or.......F6 Sheffield Rd........C6 Terri Rd...............E5 Waveney Rd....... F2 Burbank Circle Playground..........................C6 Simpson Po ...D5 Mountainview Dr..C3 Paul St.................G4 Riner St...............D6 Sherwin Ter.........H5 Thayer St............K6 Waveney Wy.......F2 Butterworth Park..........................................H7 St George s J.E6 Mt Wayte AV.......H5 Pavia PI................J4 Ring Rd...............F8 Simpson Or.........E6 The Mountain Rd..F2 Waverley Ct.........J6 Callahan State Park...............................C4,132 St Stephens ...H5 Murphy Cir.........C6 Paxton Rd...........E7 River St...............G5 Singletary La......G4 Thelma Rd..........G7 Waverley La.,.......J4 Church Hill Cemetery.................................G5 St Tarcisius ...F7 Murray Rd...........F6 Pearl Harbor Rd..G7 Riverpath Or.......D8 Skinner Rd..........H2 Third St................J7 Waverley St.........JS Cochituate State Park .................................E8 Stapleton E-t ...J7 Myrna Rd............E5 Pearl Sl...............H6 Riverview Rd.......D6 Skyline Or............F7 Thomas Gr..........F1 Wayside AV.........06 Commuter Rail Station(Framingham).......J6 State Civil D ...H4 Myrtle St.............H6 Pelham AV...........G7 Robert Rd...........H4 Sloane Or............C6 Thompson St......H6 Wayside Inn Rd..B3 Costanza Park..............................................07 State Police Or Nadine Rd...........D6 Pennsylvania AV.F2 Robertson Rd.....H6 Snow St................J7 Thurber St...........H6 Webster St..........H6 Cushing General Hospital...........................H5 Town Hall . ..H3 Nancy La.............D4 Perry H Henderson Rock St................J5 South Rd.............H5 Tomkins La.........H3 Weld St.................J7 Danforth Museum........................................H6 Walsh Middf: ...E8 Naples St.............J6 Or.....................E6 Rockridge Rd......G2 South St...............J6 Torrey St.............H6 Wellington AV.......J6 Danforth Street Playground........................D8 Waushakum .. 06 Neal Wy...............D4 Pershing AV..........J5 Rolling Or............E2 Speen St.............E8 Tower St..............F4 Wesley Rd...........E6 Dennison Playground...................................J7 Wilson Scho;_ ...C7 Nelson St............H6 Phelps Rd...........G7 Rolling La............C6 Spring La............D6 Townsend Ter......07 West Rd..............H5 Dunning Elementary School........................E5 Winch Park F ..E7 Neville Rd............G5 Philip Rd..............E7 Rose Kennedy La Spring St.............G5 Trafton Rd...........GS West St...............G4 Edgell Grove Cemetery...............................F5 Woodfield P,' ..06 New York AV........F1 Phipps St.............J7 .........................G6 Springhill Rd.......E8 Travis Or..............H4 Western AV..........J7 Edwards Cemetery..,...................................D7 ...E4 Newbury St.........F8 Picard Ter.............J7 Rose La...............G3 Spruce St............E5 Treeland Or.........C5 Westgate Rd.......F3 Fairbanks Road Playground.......................G6 Community f ..E4 Newton Pk Rd.....H5 Pierce St.............G7 Ross St................J4 Stalker La............H2 Tripp St.................J6 Westview Rd.......05 Fire Stations County....... ...E4 Newton PI............He Pin Cushion Rd....J4 Rosslare Rd........F6 Stanley Or...........E2 Turner Rd............C6 Weybossett AV.....J5 Centre......................................................G5 Area(Sq.Mie ...ES Nicholas Rd........D7 Pine Hill Rd.........Ft Roundtop Rd......C5 State St...............G5 Underwood AV....G7 Wheeler AV.........G5 Concord St..............................................G7 Population ..F7 Nipmuc Rd..........K6 Pine La................E5 Roxanna St..........J7 Stearns St...........DB Union AV..............G5 Whiting Rd..........D5 Hollis Sl....................................................J6 Form of Go,' ..G5 Nipmuc Rd Ext....J6 Pine St..................J6 Royai Ct..............G4 Stedmen Rd.........J5 Union AV Ter.......G5 Whitney AV .........K6 Nobscot....................................................DS Area Code ..E3 Nipmuc Ter..........K6 Pinecrest Rd.......E8 Royal Meadow La..F3 Stevens Rd.........G5 Universal St.........J7 Whittemore Rd...DS Saxonville..........................................Ir.........D7 Zip Code ... Z - 4.` M INDIAN C I 1 'JAD � ech 0 CEM �> LL : 6 ® Copyright A OW MAP,INC • ...._. • r .. 26 • .7 � V�i•�i' r I •r 28 27 25 �• , ' '_ ' �� �3-1 2123 lw Wit • O 23 • 'i .�221 .� • ` r �• ,6�Qf w �� • • )a ® 4 is a r� ,► , •, . � � , • 1 ted , AMRO Environmental Laboratories Corporation 111 Herrick Street - ' Merrimack, N.H.03054 Office: . Office: 603-424-2022 Fax: 603-429-8496 CHAIN OF CUSTODY RECORD Proj.No. Project Name t�1. 61v&)Ve,Z Project State MATRIX PAGE I OF Water-A Soil/Solid-S i t Samplers(Signa tu Type Waste-W &iNo.of Other-0 i . Containers Explain I Sta.No. Date Time Com Grab Station.Location Remarks eo it r? 2:10 J- 04 iF i tr /•)t) kw- S Please print clearly, legibly,and completely. Samples cannot be logged PRIORITY TURNAROUND TIME AUTHORIZATION in'agd the turnaround time clock will not start until any ambiguities are Before submitting samples for expedited T.A.T.,you must have requested in.advance and resolved. received a coded T.A.T.AUTHOR IZATION.NUMBER. AUTHORIZATION NO. T.A.T. authorized by: '` a f' ❑Fax to(phone) Send Results to: inquis y(Sig:i tur Da Ti ;I r Received by(Sig ature) I Results needed Relinquished b Si nature Date ime Received b (Signature) q Y 1 9 ) Y PO# / Relinquished by(Signature) Date Time Received by(Signature) AMRO Project No. Remarks Seal Intact. V; Relinquished by(Signature) Date Time Received for Laboratory by:(Signature) i r Yes No N/A r White:Lab copy Yellow:Accompanies report Pink:Client copy a t 1 _= = Environmental Laboratories Corporation 111 Herrick Street, Merrimack, NH 03054 TEL: (603)424-2022-FAX: (603)429-8496 April 19,2002 Tim Toomey Subsurface Remediation Technologies 355 Central St. Rowley, MA 01969 TEL: (978)948-3861 FAX: (978)948-3861 RE: Trask Property:- Workorder No.:0204149 Dear Tim Toomey: AMRO Environmental Laboratories Corp. received 5 samples on 4/12/02 for the analyses presented in the following report. AMRO operates a Quality Assurance Program which meets or exceeds National Environmental Laboratory Accreditation Conference(NELAC), state, and EPA requirements. A copy of the appropriate state and/or NELAC Certificate is attached. The enclosed Sample Receipt Checklist details the condition of your sample(s)upon receipt. Please be advised that any unused sample volume and sample extracts will be stored for a period of 60 days from = sample receipt date (90 days for samples from New York). After this time,AMRO will properly dispose of the remaining sample(s). If you require further analysis, or need the samples held for a longer period, please contact us immediately. This report consists of a total of G pages. This letter is an integral part of your data report. All results in this project relate only to the sample(s)as received by the laboratory and documented in the Chain-of-Custody. This report shall not be reproduced except in full,without the written approval of the laboratory. If you have any questions regarding this project in the future, please refer to the Workorder Number above. Sincerely, Nancy Stewart Vice President/LabDirector a AMRO Environmental Laboratories Corp. Date: 19-Apr-02 CLIENT: Subsurface Remediation Technologies Project: Trask Property Work Order Sample Summary Lab Order: 0204149 Date Received: 4/12/02 Lab Sample ID Client Sample ID Collection Date 0204149-OIA Drinking Water Well 4/11/02 0204149-02A MW-1 4/11/02 0204149-03A MW-2 4/11/02 0204149-04A MW-3 4/11/02 0204149-05A MW-4 4/11/02 1 AMRO Environmental Laboratories Corporation y 111 Herrick Street E 35708 Merrimack, N.H. 03054 Office: 603-424-2022 Fax: 603-429-8496 CHAIN OF CUSTODY RECORD Proj.No. Project Name AJ. Project State MATRIX I 1 nnPAGE OF Jird r0 "'" 4 X Water-A Soil/Solid-S Samplers(Signatur Type Waste-W y ;t Size, Other-0 &No.of Containers Explain Sta.No. Date Time Comp Grab Station Location Remarks ri o z I2 SD ,c l�W-I 3 VOA 111, OZ 2: a VOA A It D� q;oo x \JDA t' �q< W VbV� 4 I =� I i t Please print clearly, legibly and completely. Samples cannot be logged PRIORITY TURNAROUND TIME AUTHORIZATION in ar?d the turnaround time clock will not start until any ambiguities are Before submitting samples for expedited T.A.f�you must have requested in advance and resolved. received a coded T.A.T.AUTHORIZATION NUMBER. AUTHORIZATION NO. T.A.T.authozed by: L/ ❑Fax tohSend Results to: t y(Sig{ tur Da Ti 3 d ReUeivedSi`ature (pone) enResults needed -� •�� ���'� rT_ /'tOfit�l� a' -�, Relinquished by(Signature) Date ime Received by(Signature) POff / V ` Relinquished by(Signature) Date Time Received by(Signature) ��AMRRO Project No. Remarks C/ L i Seal Intact? R inquuii d y Signature) to Ti e Received for Laboratory by:(Signature) _It Yes No NIA White:Lab copy Yellow:Accompanies report Pi6k:Client copy ¢ ` AMRO Environmental SAMPLE RECEIPT CHECKLIST 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 Client: r AMRO ID: 603 424-2022 Project Name: crcl Date Rec.: nW Ship via: (circle one) Fed Ex., OPS,eavlRu Courtgc:> Date Due: [� O Hand Del., Other Courier, Other. Items to be Checked Upon Receipt Yes No NA Comments 1. Army Samples received in individual plastic bags? 2. Custody Seals present? 3. Custody Seals Intact? 4. Air Bill included in folder if received? 5. Is COC included with samples? 6. Is COC signed and dated by client? o __ 7. Laboratory receipt temperature. TEMP= Samples rec.with ice�ce packs_neither 8. Were samples received the same day they were sampled? Is client temperature 4°C+_2°C? If no obtain authorization from the client for the analyses. Client authorization from: Date: Obtained by: 9. Is the COC filled out correctly and completely? 10. Does the info on the COC match the samples? 11.Were samples rec.within holding time? 12.Were all samples properly labeled? 13.Were all samples properly preserved? 14.Were proper sample containers used? 15.Were all samples received intact? (none broken or leaking) 16.Were VOA vials rec.with no air bubbles? 17. Were the sample volumes sufficient for requested analysis? 18. Were all samples received? 19. VPH and VOA Soils only: Sampling Method VPH(circle one): M=Methanol, E=EnCore(air-tight container) Sampling Method VOA(circle one): M=Methanol, SB=Sodium Bisulfate, E=EnCore, B=Bulk If M or SB: Does preservative cover the soil? If NO then client must be faxed. Does preservation level come close to the fill line on the vial? If NO then client must be faxed. Were vials provided by AMRO? If NO then weights MUST be obtained from client Was dry weight aliquot provided? If NO then fax client and inform the VOA lab ASAP. 20. Subcontracted Samples: What samples sent: Where sent: Date: Analysis: sa TAT: 21. Information entered into: Internal Tracking Log? Dry Weight Log? Client Log? Composite Log? , Filtration Log? Received By:,�Z Date: 4 —0 Logged in By: Date: CS4_/.5=�� Labeled By: CC_ Date: 4_ p a— Checked By: Date: _l� --� NA= Not Applicable gc/gcmemos/forms/samolerec Rev 1R nrinn AMRO Environmental 111 Herrick Street Laboratories Corporation Merrimack, NH 03054 (603) 424-2022 Please Circle if: Sample= Soil Sample= Waste List Preserv. Volume Final Volume Preserv. Initial Acceptable? Added by Solution ID# Preservative adjusted Sample ID Analysis Sample Listed pH Y or N AMRO of Preserv. Added pH U I —05A I I, x 40--L I I - I • I i f I I i H Checked B : Date: H adjusted B : Date: P Y P 1 Y 5 gclgcmemos/forms/sam lerec Rev. 6100 p e .18 0 ;. .;;�.,r :,,►�•;::,: .',.s.s;'�'% �'�►.•:::;:%:::;'fir r ;�.�::•';,,'S:�%S'.:;'�'' �'�''�:`�2;"%S::'•r': �'�►►�.'.:;;�:;;;10�..,� .;:►►.,\.. ,:%i•.�• ``•.•�\►t:�i..i��i;i�•'i•'• •�,�:•�\:\:�..irli;i•.;�•• �`••'�\:\ii..::%:;:•r��i�I• ,•`:•,•�\:\:i. 'ii:ij;r;'��•.• :•`.��;.;;:\:;..'ir%:j;r, �•1%•I,..••�.Ii'.' `,,\,�•�1\�.i11i;I;��..:' .�.,\;i:i:i II: , . •, ,, •, 01! '.!i�,.. ,,,'�.,♦•"-� ��. The Commonwealth of Massachusetts • i F � C .;�.: ; ;. Department of Environmental Protection Division of Environmental Analysis Senator William X. Wall Experiment Station certifies ;?•' M-NH012 AMRO ENVIRONMENTAL LAB 111 HERRICK ST MERRIMACK, NH 03054-0000 Laboratory Director: Nancy Stewart =s = for the analysis of NON POTABLE WATER(CHEMISTRY) POTABLE WATER(CHEMISTRY) pursuant to 310 CMR 42.00 This certificate supersedes all previous Massachusetts certificates issued to A,is •.:•. laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CMR 42.00. This certificate is valid only when accompanied by the latest dated Certified Parameter List as issued by the Massachusetts D.E.P. Contact the Division of Environmental Analysis to ' verify the current certification status of the laboratory. .r Certification is no guarantee of the validity of the data. This certification is subject to unannounced laboratory inspections. Issued: 01 JUL 2001 Expires: 30 JUN 2002 Director, Division of Environmental Analysis ,..; ; `::�111. •.�.�r�/I,/!%. '?�,\��!►!!. .��i/i!I/i. 1�;:,�.�1. •Ariii�!i.' '.:Q�i�!!.' ••!��iii/I;, i�\,.�.►.►►1. .�,.,.,SII�. .:\\�:.►�!. .�,iii i�!<�. COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of: 10 FEB 2002 M-NHO12 AMRO ENVIRONMENTAL LAB MERRIMACK NH NON POTABLE WATER(CHEMISTRY) Effective 10 FEB 2002 Expiration 30 JUN 2002 Date Date Analytes and Methods ALUMINUM EPA 200.7 ORTHOPHOSPHATE EPA 300.0 ANTIMONY EPA 200.7 TOTAL PHOSPHORUS EPA 365.2 ANTIMONY EPA 204.2 CHEMICAL OXYGEN DEMAND EPA 410.4 ARSENIC - EPA 200.7 BIOCHEMICAL OXYGEN DEMAND EPA 405.1 ARSENIC EPA 206.2 TOTAL CYANIDE EPA 335.2 ARSENIC ASTM D2972-93(C) NON-FILTERABLE RESIDUE EPA 160.2 BERYLLIUM EPA 200.7 TOTAL RESIDUAL CHLORINE SM 4500-CL-G CADMIUM EPA 200.7 OIL AND GREASE EPA 413.1 CHROMIUM EPA 200.7 TOTAL PHENOLICS EPA 420.1 COBALT EPA 200.7 VOLATILE HALOCARBONS EPA 624 COPPER EPA 200.7 VOLATILE AROMATICS EPA 624 LEAD EPA 200.7 CHLORDANE EPA 608 LEAD EPA 239.2 ALDRIN EPA 608 MANGANESE EPA 200.7 DIELDRIN EPA 608 MERCURY EPA 245.1 DDD EPA 608 MOLYBDENUM EPA 200.7 DDT EPA 608 NICKEL EPA 200.7 HEPTACHLOR EPA 608 SELENIUM EPA 200.7 HEPTACHLOR EPDXIDE EPA 608 SELENIUM EPA 270.2 POLYCHLORINATED BIPHENYLS(WATEF EPA 608 ; SILVER EPA 200.7 POLYCHLORINATED BIPHENYLS(OIL) EPA 600/4-81-045 STRONTIUM EPA 200.7 THALLIUM EPA 200.7 THALLIUM EPA 279.2 ZINC EPA 200.7 PH EPA 150.1 SPECIFIC CONDUCTIVITY EPA 120.1 TOTAL DISSOLVED SOLIDS EPA 160.1 TOTAL HARDNESS(CAC03) EPA 200.7 CALCIUM EPA 200.7 MAGNESIUM EPA 200.7 SODIUM EPA 200.7 POTASSIUM EPA 200.7 TOTAL ALKALINITY EPA 310.1 CHLORIDE EPA 325.3 CHLORIDE EPA 300.0 FLUORIDE EPA 300.0 SULFATE EPA 300.0 AMMONIA-N EPA 350.2 NITRATE-N EPA 300.0 NITRATE-N EPA 353.2 KJELDAHL-N EPA 351.1 ORTHOPHOSPHATE EPA 365.2 January 18,2002 * Provisional Certification Page 1 of 2 r , s COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of: 10 FEB 2002 i M-NHO12 AMRO ENVIRONMENTAL LAB MERRIMACK NH POTABLE WATER(CHEMISTRY) Effective 10 FEB 2002 Expiration 30 JUN 2002 Date Date Analytes and Methods ANTIMONY EPA 200.9 ARSENIC EPA 200.7 ARSENIC EPA 200.9 BARIUM - EPA 200.7 -- BERYLLIUM EPA 200.7 CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COPPER EPA 200.7 LEAD EPA 200.9 MERCURY EPA 245.1 NICKEL EPA 200.7 SELENIUM EPA 200.9 THALLIUM EPA 200.9 NITRATE-N EPA 353.2 NITRITE-N EPA 353.2 FLUORIDE EPA 300.0 SODIUM EPA 200.7 SULFATE EPA 300.0 CYANIDE SM 4500-CN-C,E TURBIDITY EPA 180.1 CALCIUM EPA 200.7 TOTAL ALKALINITY SM 23208 TOTAL DISSOLVED SOLIDS SM 2540C PH EPA 150.1 1,2-DIBROMOETHANE EPA 504.1 1,2-DIBROMO-3-CHLOROPROPANE EPA 504.1 January 18,2002 * Provisional Certification Page 2 of 2 317 Elm Street CAi" e er Ve Milford03055 Tel(603))673-5440 Fax(603)673-0366 April 17, 2002 Ms. Nicole Borduz AMRO Environmental Laboratories Corp 111 Herrick Street Merrimack, NH 03054 -- Job Name: Trask Property Laboratory#: 02040166 Job#: 0204149 Purchase Order#: N/A Location: N/A Control#: 40305 Dear Ms. Borduz Enclosed please find the laboratory results for the above reference samples that were received by the ChemServe sample custodian, under chain of custody control number 40305 on 04/16/02. Samples were collected by CC on 04/11/02. Any abnormalities to the samples on receipt would be noted on the enclosed chain of custody document. This report is not valid without a completed ChemServe chain of custody with the corresponding control number, attached. All samples analyzed by ChemServe are subject to quality standards. These standards are either as stringent or more stringent that those established under 40 CFR Part 136, state certification programs, and corresponding methodologies. ChemServe has written QA/QC Procedures Manual that outlines these standards, and is available, upon request, for your reference. Unless otherwise stated on the Chain of Custody or within the report, all holding times, preservation techniques, container types, and analytical methods are analogous with those outlined by them U.S. EPA. I certify that I have reviewed the above referenced analytical data and state forms, and I have found this report within compliance with the procedures outlined in the ChemServe QA/QC Procedures Manual. I1L.-- 1 Ellen Abrams-QF QC Manager J y C:repo sta 'dent/Laboratory Director T 's contains 14 pages. 0� \,g ACC0,9 v .. Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-01 JOB NAME: Trask Property JOB#: N/A LOCATION: MA SAMPLE IDENTITY:Drinking Water Well 01A CONTROL M 40305 DATE SAMPLED:04/11/02 DATE RECD:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER_ : - (UG/L) (UG/L)X 1 -- BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 B ROMODICH LOROM ETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE BDL 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-01 JOB NAME: Trask Property LOCATION: MA SAMPLE IDENTITY:Drinking Water Well 01A CONTROL#:40305 DATE SAMPLED:04/11/02 DATE REC'D:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: - (UG/L) (UG/L)X 1 -- 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE' BDL 0.5 1,2,3-TRICHLOROPROPANE . BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER BDL 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD . 11 a Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-02 JOB NAME: Trask Property JOB#: N/A LOCATION: MA SAMPLE IDENTITY:MW-1 02A CONTROL#:40305 DATE SAMPLED:04/11/02 DATE RECD:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE 2.5 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-1,2-DICHLOROETHENE BDL 0.5 12-DIC HLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-1,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES PCU �' 4 Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-02 JOB NAME: Trask Property LOCATION: MA SAMPLE IDENTITY:MW-1 02A CONTROL#:40305 DATE SAMPLED:04/11/02 DATE RECD:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER 3.5 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 - NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD r � , Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-03 JOB NAME: Trask Property JOB#: N/A LOCATION: MA SAMPLE IDENTITY:MW-2 03A CONTROL M 40305 DATE SAMPLED:04/11/02 DATE RECD:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE 4.0 0.5 - DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1 DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-03 JOB NAME: Trask Property LOCATION: MA SAMPLE IDENTITY:MW-2 03A CONTROL#:40305 DATE SAMPLED:04/11!02 DATE RECD:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE;i BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER 4.0 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 10.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-04 JOB NAME: Trask Property JOB#: N/A LOCATION: MA SAMPLE IDENTITY:MW-3 04A CONTROL M 40305 DATE SAMPLED:04/11/02 DATE REC'D:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- BENZENE BDL 0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROM ETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE 2.1 0.5 - DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-1,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES � ' 8 Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-04 JOB NAME: Trask Property LOCATION: MA SAMPLE IDENTITY:MW-3 04A CONTROL M 40305 DATE SAMPLED:04/11/02 DATE RECD:04/16/02 DATE ANALYZED:-04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER 4.4 0.5 CARBON DISULFIDE BDL 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 - NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD I 6 Chemserve VOLATILE ORGANIC ANALYSIS EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-05 JOB NAME: Trask Property JOB#: NIA LOCATION: MA SAMPLE IDENTITY:MW-4 05A CONTROL M 40305 DATE SAMPLED:04/11/02 DATE RECD:04/16/02 DATE ANALYZED:04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- BENZENE BDL .0.5 BROMOBENZENE BDL 0.5 BROMOCHLOROMETHANE BDL 0.5 BROMODICHLOROMETHANE BDL 0.5 BROMOFORM BDL 0.5 BROMOMETHANE BDL 0.5 CARBON TETRACHLORIDE BDL 0.5 CHLOROBENZENE BDL 0.5 CHLOROETHANE BDL 0.5 CHLOROFORM BDL 0.5 CHLOROMETHANE BDL 0.5 2-CHLOROTOLUENE BDL 0.5 4-CHLOROTOLUENE BDL 0.5 DIBROMOCHLOROMETHANE BDL 0.5 1,2-DIBROMO-3-CHLOROPROPANE BDL 0.5 1,2-DIBROMOETHANE BDL 0.5 DIBROMOMETHANE BDL 0.5 1,2-DICHLOROBENZENE BDL 0.5 1,3-DICHLOROBENZENE BDL 0.5 1,4-DICHLOROBENZENE 0.8 0.5 DICHLORODIFLUOROMETHANE BDL 0.5 1,1-DICHLOROETHANE BDL 0.5 1,2-DICHLOROETHANE BDL 0.5 1,1-DICHLOROETHENE BDL 0.5 CIS-1,2-DICHLOROETHENE BDL 0.5 TRANS-I,2-DICHLOROETHENE BDL 0.5 1,2-DICHLOROPROPANE BDL 0.5 1,3-DICHLOROPROPANE BDL 0.5 2,2-DICHLOROPROPANE BDL 0.5 1,1-DICHLOROPROPENE BDL 0.5 CIS-1,3-DICHLOROPROPENE BDL 0.5 TRANS-I,3-DICHLOROPROPENE BDL 0.5 ETHYLBENZENE BDL 0.5 METHYLENE CHLORIDE BDL 0.5 STYRENE BDL 0.5 1,1,1,2-TETRACHLOROETHANE BDL 0.5 1,1,2,2-TETRACHLOROETHANE BDL 0.5 TETRACHLOROETHENE BDL 0.5 TOLUENE BDL 0.5 CONTINUED: 1 OF 2 PAGES 0 Chemserve VOLATILE ORGANIC ANALYSIS PAGE 2 OF 2 EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166-05 JOB NAME: Trask Property LOCATION: MA SAMPLE IDENTITY:MW-4 05A CONTROL#:40305 DATE SAMPLED:04/11%02 DATE RECD:04/16/02 DATE ANALYZED:-04/16/02 MATRIX:LIQUID DETECTION LIMIT BASED ON PQL COMPOUND CONCENTRATION DETECTION LIMIT MULTIPLIER: (UG/L) (UG/L)X 1 -- 1,1,1-TRICHLOROETHANE BDL 0.5 1,1,2-TRICHLOROETHANE BDL 0.5 TRICHLOROETHENE BDL 0.5 TRICHLOROFLUOROMETHANE BDL 0.5 1,2,3-TRICHLOROPROPANE BDL 0.5 VINYL CHLORIDE BDL 0.5 TOTAL XYLENES BDL 0.5 METHYL-TERTIARY-BUTYL ETHER 4.0 0.5 CARBON DISULFIDE 1.9 0.5 n-BUTYLBENZENE BDL 0.5 sec-BUTYLBENZENE BDL 0.5 tert-BUTYLBENZENE BDL 0.5 ISOPROPYLBENZENE BDL 0.5 4-ISOPROPYLTOLUENE BDL 0.5 n-PROPYLBENZENE BDL 0.5 1,2,3-TRICHLOROBENZENE BDL 0.5 1,2,4-TRICHLOROBENZENE BDL 0.5 1,2,4-TRIMETHYLBENZENE BDL 0.5 1,3,5-TRIMETHYLBENZENE BDL 0.5 HEXACHLOROBUTADIENE BDL 0.5 NAPHTHALENE BDL 0.5 TERTIARY-AMYL METHYL ETHER BDL 0.5 ETHYL TERTIARY-BUTYL ETHER BDL 0.5 DI-ISOPROPYL ETHER BDL 0.5 TERTIARY-BUTYL ALCOHOL BDL 20 BDL=BELOW DETECTION LIMIT ANALYZED BY:TD i rN 1 � n CHEMSERVE VOA SPIKE RECOVERY FORM EPA METHOD 524.2 CUSTOMER:AMRO LAB#:02040166 JOB NAME: Trask Property LOCATION: MA SAMPLE IDENTITY:MATRIX SPIKE 02040091-03 CONTROL#:40305 DATE ANALYZED:04/16/02 COMPOUND CONIC ADDED AMT REC %REC (UG/L) (UG/L) 1,1-DICHLOROETHENE 4 4.3 108% BENZENE - 4 4.5 113% -- TRICHLOROETHENE 4 4.4 110% CHLOROBENZENE 4 4.6 115% 1,2-DICHLOROBENZENE 4 4.5 113% 1,3,5-TRIMETHYLBENZENE 4 4.3 108% 1,2,4-TRICHLOROBENZENE 4 4.4 110% VOA MATRIX SPIKE REC 6 5 4 ■CONIC ADDED UG/L 3 ❑LW RECOVERY 2 - OLD RECOVERY 1 , 0 1 2 3 4 5 6 7 SPIKE RECOVERY LIMITS 70-130% �� C 0 12 AMRO Environmental Laboratories Corporation 111 Herrick Street 3621 1 Merrimack, N.H. 03054 1 Office: 603-424-2022 Fax: 603-429-8496 CHAIN OF CUSTODY RECORD Proj.No. Project Name y Project State MATRIX PAGE OF S�C Water A SoiVSolid-S Samplers(Signature) Type Waste-W j Size, Other &No.of Containers Explain - Sta.No. Date Time Com Grab Station Location Remarks 00 ' �- 10 M110 �- i/ Please print clearly, legibly and completely. Samples cannot be logged PRIORITY TURNAROUND TIME AUTHORIZATION in and the turnaround time clock will not start until any ambiguities are Before submitting samples for expedited T.A.T.,you must have requested in advance and resolved. received a coded T.A.T.AUTHORIZATION NUMBER. AUTHORIZATION NO. T.A.T. authorized by: Relinquished by(Signature) Date Timb 1/1,5- Received by(Signature) ❑Fax to(phone) R' Send Results to: Results needed Relinquished by(Signalud Date Time Received by(Signature) PO# elinquished by(Signature) Date Time Reced (Signature) AMBO Project No. Remarks C Relinquis by(Signature) Date Time Receiv a r Laboratory b�' f"Le Seal Intact? Yes No N/A ( ,1 9/- /1--;7Z 4. /a. l ✓� . G White:Lab copy Yello :Ac mpanies report Ain :Clien t opy - lr Chain of Custody No. 40305 �rVe Multiple COC's Yes No C�11 ei�"LG• 317 Elm Street Melford, NH 03055 P (603) 673-5440/Fax (603) 673-0366 CHAIN OF CUSTODY CUSTOMER INFORMATION G PROJECT INFORMATION SAMPLE INFORMATION CUSTOMER: r� 'l l, JOB NAME: TURNAROUND TIME:(CIRCLE ONE:) ADDRESS: JOB NUMBER: STANDARD RUSH CITY/STATE/ZIP LOCATION: RUSH T.A.T. (CHECK w/LAB) TELEPHONE: AMBER GLASS(AG) / GLASS(G) / PLASTIC(P) TELEPHONE: C1 C 4 L . REPORT TO: CONTACT: P O NUMBER: QUOTE NUMBER: LOw4 SAMPLE [ MATRIX 44 p SAMPLE IDENTIFICATION&LOCATION® COLLECTED W TYPE a SOLID(S) o F Q LIQUID ® ANALYSIS Q p( O COMBINEDD((C) vFOD © © O ® V HAZARD(11) Q J I DATE TIME st C. G.. 1 1`'? �•' C f DATE TIME DATE 11ML DATE IIME DATE TIME DATE TIME DATE TIME I DAIS IM MILITARY SAMPLE CHECK LIST: rid FIELD READING(S): ® CUSTODY SAMPLER: DATE TIME RECEIVED WITHIN HOLD TIME Y�S' OR NO (print name) RECEIVED IN GOOD CONDITION (LES) OR NO SIGNATURE: TEMPBLANK 'c tC� � DATE TIME SHIPPED OR 4E6t7ELIVERED RELINQUISHED: SAMPLES WERE PROPERLY PRESERVED YES NO N/A DATE TIME SAMPLES WERE FILTERED IN FIELD LAB /A RECEIVED: IF NO EXPLAIN: DATL TIME RELINQUISHED: TIME RECEIVED FOR LAB: . GROUP# C f G �, [J 3E po 'i �� EALTII OF.%1.\SSA('IIItSE'ITS :j1fiL=. } 'ii :tr..!i: •r, :�i:. is;;:�•::•. :r. •t, r t.,•:c.. DI:P.%Rt\IENTOFENVIRONMENI'AI.PRO rt:("1'll)N sa cl. ..i;.i •:;ir l•jt;.i:: :'! , :it:s:i:;•.. :til r...;i;t,,; 1:';•: W, :,1:.r: .ri.:.t..•,y '�•;}t-i;,.� Cmifitil Parameter 1.1.1 as uf: 10 FELL 2002 The Commonwealth of Massachusetts �1..HB2J rHE�ISI:R�E •,:;;:;^. MILFORD VII i VON POTABLE\5'AtER 1('IMMISTRY) Effective 10 PINI:00.2 EcpiraNnn JO JUN 2002 Dale ZJr Anals les anJ\ttlhn.h ALUMINUM EPA 200 r DDD EPA 606 ANTIMONY EPA 200 T DOE EPA 606 "•" ARSENIC EPA 200 t DDT EPA 606 BERYLLIUMEPA 200 r HEPTACHLOR EPA We De artment o Environ►nental Protection I CADMIUM EPA 200) HEPTACHLOR EPDXIDE EPA 606 •�•,' �fVlSlOn a/'E11VIrannlentQl Analysis CHROMIUM EPA 200/ POLYCHLORINATED B+PHENrl510111 EPA 6oa'4.61•o4S J y COBALT EPA 200 T Senator William X. {Nall Experiment Station COPPER EPA 200 t IRON EPA 200 r LEAD EPA 200 T ^w4� certifies =y MANGANESE EPA 200 1 G ESE ?rj M•NH023 CIIEMSERVE MERCURY EPA N51 317 ELM ST NICKEL EPA 200 t /._ MILFORD, NII 03055-0000 SELErnurt EPA 200 T SILVER EPA 200 l Laboratory Director: Jay W.Crysu1 v"n"D1uPa EPA 200 •."I,,'r ZINC FPA 200 i =` for the anal}•sis of NON POTABLE WATER(CHEMISTRY) P. EPA i50 1 f POTABLE WATER ICIIENIISTRY) SPEc+r+c CONDUCTIVITY EPA 4201 :'tr{ TOTAL pS50lvED SOlr05 Su 25400 pursuant to 110 C.1I11 42.00 TOTAL HARDNESS 1CACO31 SM 23408 .. y\\ rhis certificate auperaedet all previous Ahastichuxtn«rfificuftj issued to this %%,{; tattluM EPA 200 luboratory. rhe laboratory is regululed by and shall be responsible for bring in MAGNESIUM EPA 200 T r Yn� compliance with r1lassachuseus regulaT tions ut J I0 C.IIR 42.00. -• POTASSIUM AAi EPA 2a0 t L TOTAL ALKALINITY Ski 23208 '/ �.i' CHLORIDE EPA 325 2 17Pis certificate is valid ants,when uccompunted hs,the latest dated Certified Porumerer List NITRATE N EPA 3000 us issued by the Massachusetts D.E.P. Cuntuct the Division of Enrlrnnn/enful.tnuhsIs to verify the current certification stunts of the luhorutorl K.EIoAHL N EPA 351 3 •�1 ORTHOPHOSPHATE EPA 3652 t ('ertification is no guarantee of the vulitlitl•a/the dorti. Tliii certlfcannn N flthject to TOTAL PHOSPHORUS EPA 365 2 �4'tit unannounced laboratory inspections. (±' CHE'.bCAI OAvGEN OEP}ANO EPA 4x04 B.00HE.uCAI O.YGEr/OEMANO EPA 405 4 i� � TOTAL C r AraOE FPA 335 2 Issued: 01 JUL 2001 NON.r ALTERABLE RESIDUE SPA 25-000 Eipires: JO JUN 2002 tOral RESIDUAL CHLORINE EPA 330 S 04 AND GREASE EPA 1664 Director.Division of E,rvtronmental Anahsis Y TOTAL PHENOLICS EPA 410 t �•' VOLATILE HALOCARBONS EPA 624 VOLATILE AROMATICS EPA 624 CHLOROANE EPA 606 ALDRIN r EPA 606 DWELDRIN EPA606 jiilid '•//liiip° iiiili 'Ihiii'::} !iit:'t. ?rt�iil.: ;;i iih l '!hiii':: 'iVl1 i'•' ilii°:: ±a.lr;` ��ltl,..}( �. .;L:a%;'1. r r ti:• �:J�t u:.rrrrtr ii:� ;t::::: r/j .i••:+. r tr 1. •{t 1P' •,} !iltttl• iS.:r..r:::J'+._ 'iltrlli�' '.���},I:irfrtrl!;.• 'iil::vt[iirttj 1t: .;t.;•1t•:: t: t:,�•• .its::•. Januan Is.2002 'ProvisinnalCertification Pagt I of 2 4 v ,