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HomeMy WebLinkAboutMiscellaneous - 384 OSGOOD STREET 4/30/2018 (3)00 a O N M O N o E o o i r E cn e ° 0 a � o cts c .E o a N� 0 C ow L > a� 7 y 00 c M tj �t d C c �, bq a CY, o C �sC7 �a N G O V VO � abi 4. � x E U CO w 00 0Cd M Cc0 +.i O C/1 y N o a C D .4 O o -� O O oc O O O 4 k c U V O Z U Q Y O 6) ° d 8 8 a U d A U G7 a A U U� • •� fl� • w tl N Grant, Michele From: Grant, Michele Sent: Friday, May 24, 2013 7:45 AM To: Carney, John; Sawyer, Susan Cc: Foulds, Eric; Blackburn, Lisa; Rillahan, Deb Subject: RE: dumpster pick up Good Morning, Apparently they are picking up between 5:30 and 7:00am Thanks MG -----Original Message ----- From: Carney, John Sent: Thursday, May 23, 2013 6:54 PM To: Sawyer, Susan Cc: Foulds, Eric; Blackburn, Lisa; Grant, Michele; Rillahan, Deb Subject: Re: dumpster pick up What time are they coming? Sent from John Carney On May 23, 2013, at 5:15 PM, "Sawyer, Susan"<ssawyer(@townofnorthandover.com> wrote: > I just spoke with this gentlemen. I told him that we will speak with CVS or whomever IRM is servicing and tell them they need to stop the pick-ups by calling their provider. Apparently it is Friday morning. > Secondly, he feels that he will not get respect if he calls the NAPD in the early morning as I suggested. I told him that would not be the case. > Do you think your officers would be against following this type of complaint up? Or maybe there is some history with this person; as he said he is a retired police officer. > There is discretion of a fine,.if someone is seen dumping prior to 7 > AM as in the code they can be cited by the PD citing the following > TOWN OF NORTH ANDOVER DUMPSTER REGULATIONS > 3.2 The emptying of the contents of the dumpster(s) by the contractor > shall not commence before 7:00 A.M. and not continue after 9:00 P.M. > authority is... > The Board of Health at its discretion may levy fines upon the > authorized agent/property owner in accordance with M.G.L. Section 40 > Chapter 21D. Fines will be fifty dollars ($50) per violation. Each day > that the violation remains uncorrected constitutes a separate violation. > -----Original Message----- > From: Sawyer, Susan > Sent: Thursday, May 23, 2013 4:55 PM > To: 1carney(@napd.us; Foulds, Eric > Cc: Blackburn, Lisa(LBlackburn(townofnorthandover.com); Grant, I >'Milthele; Rillahan, Deb(drillaha(@townofnorthandover.com) > Subject: dumpster pick up > Hi EJ and John, > Not sure who to send this too. > We received this complaint. The trash company is well aware that dumpsters are not to be picked up prior to 7:00AM. > We have had these complaints in the past and it has worked to have the complainant contact the NAPD to try to approach the driver to deliver the message at the time of the offense. Us doing a random stake out, is just a waste of time. > This dumpster is a IRM dumpster at the rear of CVS. The complainant lives in the housing authority buildings just behind, Bingham Way. > Just want to give you all a heads up. If you have other ideas, please let us know. > Thank you > Susan > -----Original Message----- > From: noreply(@townofnorthandover.com >[mailto:noreply@townofnorthandover.com] > Sent: Thursday, May 23, 2013 12:15 PM > To: Sawyer, Susan > Subject: > This E-mail was sent from "RNPOA428C" (Aficio MP C5000). > Scan Date: 05.23.2013 12:14:57 (-0400) Queries to: > noreply@townofnorthandover.com > Please note the Massachusetts Secretary of State's office has determined that most emails to and from municipal offices and officials are public records. For more information please refer to: http://www.sec.state.ma.us/pre/preidx.htm. > Please consider the environment before printing this email. a 2 Commonwealth of Massachusetts North Andover, Massachusetts System Pumninz Record System Owner & Address: Lisa Jackson 68 Tucker Farm Road North Andover, MA 01845 Location of system: Rear yard Date of Pumping: May 17, 2013 Type of system: Septic Tank Gallons Pumped: 1500 gallons System pumped by: Service Pumping & Drain Co., Inc. S Hallberg Park North Reading, Ma License #: BHP -2013-0098,0100,0765,0096,0097,0099,0101 Contents transferred to: Greater Lawrence Sanitary District RECEIVE® 1`A 2 3 2013 TOWN OF 4ORTtf ANDOVER u�eC tkt &PARIIAEWT Date: May '17, 2013 Pumping Technician. DM This is PROPRIETARY and CONFIDENTIAL information that may be used only by the Board of Health for regulatory purposes 3,r,�p p.5. o�� s -t F I `� fiY- C- -� _ _�_ --, ./� I �r ri ' r i Ll� / V� r S TOWN OF NORTH ANDOVER DIVISION OF PUBLIC WORKS 384 OSGOOD STREET NORTH ANDOVER, MASSACHUSETTS 01845-2909 BRUCE D. THIBODEAU, P.E. DIRECTOR Eugene P. Willis, PE Director of Engineering May 23, 2013 MassDEP Northeast Regional Office 205B Lowell Street Wilmington, Massachusetts 01887 Re: X256058 — B.U.D. for Cyr Recycle Center Telephone (978) 685-0950 Fax (978) 688-9573 To Whom It May Concern: Please find enclosed an Application for Beneficial Use Determination, transmittal #X256058, for the Town of North Andover's Cyr Recycle Center on Sharpeners Pond Road. A copy of this application has been sent to the North Andover Board of Health Sin ly Eu (e�.Willis P.E. Di ctor of.Engineering Enc. Cc file, North Andover Board of Health Massachusetts Department of Environmental Protection ? Bureau of Waste Prevention — Solid Waste Management i� Application for Beneficial Use Determination BWP SW 39 Commercial Products - BWP SW 40 Regulated Systems BWP SW 41 Restricted Applications - BWP SW 42 Unrestricted Applications BWP SW 44 Modifications Important: When filling out forms on the computer, use only the tab key to move your cursor - do not use the return key. naso A. Applicant Information Town of North Andover Name 384 Osgood Street Street Address North Andover City/Town Telephone Eugene P. Willis, P.E. Contact Person Directions: B. Project Information Complete A and B, as well as the applicable section Which permit category are you applying for? of C. Specify the plan/report and page numbers where the information is located. Enter "N/A" if information requested is not applicable. MA State 978-685-0950 Contact Telephone ❑ BWP SW 39 ❑ BWP SW 40 ® BWP SW 41. ❑ BWP SW 42 1. Summary of the secondary material's proposed use & handling 2. Description of how the proposed utilization will result in a viable & beneficial substitution for a commercial product or commodity a. Description of the feedstock or product the secondary material is replacing b. Description of the proposed use of secondary material 3. Detailed description of the proposed facility that stores, processes, or otherwise handles the secondary material proposed for use a. Source or origin of secondary material b. Processing methods used in the preparation of secondary material Plan/Report # Attachment 1 A++ --I, , --+ 1 A++.,.,h.,-,n.,+ 1 A++.,.,h..,.,..+ 4 Page # Page 1 Page 1 Page 1 Page 1 Page 1 Page 1 Page 1 X256058 Transmittal Number Facility ID# (if known) 01845 Zip Code ❑ BWP SW 44 Page # DEP Use Only Application for Beneficial Use Determination • Revised 11/06 BWP SW 39 40 4142 • Page 1 of 6 1. Please type or print. A separate Transmittal Form must be completed for each permit application. 2. Make your Enter your transmittal number 10 X256058 Transmittal Number Your unique Transmittal Number can be accessed online: http://mass.gov/dep/service/online/trasmfrm.shtml Massachusetts Department of Environmental Protection Transmittal Form for Permit Application and Payment A. Permit Information BWP-SW 41 1. Permit Code: 7 or 8 character code from permit instructions Beneficial Use Determiantion - Restricted Appl 3. Type of Project or Activity Beneficial Use Determination 2. Name of Permit Category ications checkpayableto B. Applicant Information -Firm or Individual the Commonwealth of Massachusetts Town of North Andover and mail it with a 1. Name of Firm - Or, if party needing this approval is an individual enter name below: copy of this form to: DEP, P.O. Box 4062, Boston, MA 2. Last Name of Individual 3. First Name of Individual 4. MI 02211. 384 Osgood Street 3. Three copies of this form will be needed. Copy 1 - the original must accompany your permit application. Copy 2 must accompany your fee payment. Copy 3 should be retained for your records 4. Both fee -paying and exempt applicants must mail a copy of this transmittal form to: MassDEP P.O. Box 4062 Boston, MA 02211 * Note: For BWSC Permits, enter the LSP. 5. Street Address North Andover MA 01845 978-685-0950 6. City/Town 7. State 8. Zip Code 9. Telephone # 10. Ext. # Eugne P. Willis, P.E. gwillis@townofnorthandover.com 11. Contact Person 12. e-mail address (optional) C. Facility, Site or Individual Requiring Approval Cvr Recvcle Center 1. Name of Facility, Site Or Individual Sharpner's Pond Road 2. Street Address North Andover MA 01845 3. City/Town 4. State 5. Zip Code 6. Telephone # 7. Ext. # 8. DEP Facility Number (if Known) 9. Federal I.D. Number (if Known) 10. BWSC Tracking # (if Known) D. Application Prepared by (if different from Section B)* Woodard & Curran, Inc. 1. Name of Firm Or Individual 40 Shattuck Road 2. Address Andover 3. City/Town Alan Benevides, P.E. 8. Contact Person E. Permit - Project Coordination MA 01810 978-557-8150 3663 4. State 5. Zip Code 6. Telephone # 7. Ext. # 9. LSP Number (BWSC Permits only) 1. Is this project subject to MEPA review? ❑ yes ® no If yes, enter the project's EOEA file number - assigned when an Environmental Notification Form is submitted to the MEPA unit: EOEA File Number F. Amount Due DEP Use Only Special Provisions: 1. ® Fee Exempt (city, town or municipal housing authority)(state agency if fee is $100 or less). Permit No: There are no fee exemptions for BWSC permits, regardless of applicant status. 2. ❑ Hardship Request - payment extensions according to 310 CMR 4.04(3)(c). Rec'd Date: 3. ❑ Alternative Schedule Project (according to 310 CMR 4.05 and 4.10). 4. ❑ Homeowner (according to 310 CMR 4.02). Reviewer: Check Number Dollar Amount Date tr-formw.doc • rev. 1/07 Page 1 of 1 Massachusetts Department of Environmental Protection Bureau of Waste Prevention — Solid Waste Management Application for Beneficial Use Determination BWP SW 39 Commercial Products - BWP SW 40 Regulated Systems BWP SW 41 Restricted Applications - BWP SW 42 Unrestricted Applications BWP SW 44 Modifications B. Project Information (continued) Plan/Report # Page # c. Description of similar products currently & Attachment 1 Page 1 historically produced by facility d. Annual quantities, by weight and/or Attachment 1 Page 1 volume, of the secondary material proposed for beneficial use e. Storage requirements necessary for Atatchemnt 1 Page 1 maintaining sufficient inventory to meet market demand 4. Proposed location of use, if applicable, or Attachment 1 Page 2 types of locations where the secondary material will be used (e.g. highway rights-of- way, industrial zoned properties, etc.) 5. Detailed physical & chemical Attachment 1 Page 2 characterization of both the secondary material proposed for beneficial use & the final product a. Physical properties: size, density, particle Attachment 1 Page 2 size and gradation, percent solids, organic fraction, moisture content/moisture capacity, etc. b. Biological properties: pathogens, etc. Attachment 1 Page 2 c. Chemical characterization Attachment 1 Page 2 i. Detailed list of chemical constituents found in the secondary material and the Attachment 1 Page 2 derived beneficial use product(s) ii. Identification of Critical Contaminants Attachment 1 Page 2 of Concern (CCCs) d. Description of sampling & analysis Attachment 1 Page 2 methods i. Quality assurance & quality control Attachment 1 Page 2 plan X256058 Transmittal Number Facility ID# (if known) Page # DEP Use Only Application for Beneficial Use Determination • Revised 11/06 BWP SW 39 40 4142 • Page 2 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Prevention — Solid Waste Management r Application for Beneficial Use Determination BWP SW 39 Commercial Products - BWP SW 40 Regulated Systems BWP SW 41 Restricted Applications - BWP SW 42 Unrestricted Applications BWP SW 44 Modifications B. Project Information (continued) Plan/Report # Page # 6. Evaluation & control of potential adverse Attachment 1 Page 2 health, safety or environmental impacts a. Toxics Use Reduction Plan (TURP), if Attachment 1 Page 2 applicable b. Risk management techniques being used Attachment 1 Page 2 (e.g. deed/use limitations, location restrictions, engineering controls, etc.) c. Best Management Practices (BMPs) Attachment 1 Page 3 employed C. Category -Specific Information Complete only the applicable section. Plan/Report # Page # 1. BWP SW 39: Use in Commercial Products, 310 CMR 19.060(14) a. Physical characterization of the commercial product b. Constituents (including hazardous materials) contained in the product manufactured using traditional materials or products c. Comparative analysis of the product manufactured using the secondary material versus the traditionally used material it is replacing i. Hazardous materials, including CCCs (on a weight & concentration basis) ii. Processing required for use iii. Storage & handling before actual use X256058 Transmittal Number Facility ID# (if known) Page # DEP Use Only Page # DEP Use Only Application for Beneficial Use Determination • Revised 11/06 BWP SW 39 40 4142 • Page 3 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Prevention — Solid Waste Management Application for Beneficial Use Determination BWP SW 39 Commercial Products - BWP SW 40 Regulated Systems BWP SW 41 Restricted Applications - BWP SW 42 Unrestricted Applications BWP SW 44 Modifications C. Category -Specific Information (continued) Complete only the applicable section iv. Actual use v. Management or processing during its lifecycle, including, but not limited to, any destructive practices that reasonably may be expected to be employed in recycling or disposing of the material at the end of its useful life Plan/Report # Page # 2. BWP SW 40: Use of Secondary Materials in Regulated Systems, 19.060(15) a. Operative DEP permit, order, or approval for the facility/site i. Terms and conditions of any such permit, order or approval relevant to the proposed use b. General description of the facility/site activities c. Appropriate numerical standards, risk management criteria and other applicable requirements as identified by DEP d. Identification, evaluation and control of potential significant risks from the storage, transfer, processing, treatment activities and use of the secondary material 3. BWP SW 41: Use of Secondary Materials in Restricted Applications, 19.060(16) a. Concentrations of hazardous materials of Attachment 1 concern in the material proposed for use b. Upper concentration limits (UCLs) for Attachment 1 those hazardous materials Page 3 Page 3 X256058 Transmittal Number Facility ID# (if known) Page # DEP Use Only Application for Beneficial Use Determination • Revised 11/06 BWP SW 39 40 4142 • Page 4 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Prevention — Solid Waste Management Application for Beneficial Use Determination BWP SW 39 Commercial Products - BWP SW 40 Regulated Systems BWP SW 41 Restricted Applications - BWP SW 42 Unrestricted Applications BWP SW 44 Modifications C. Category -Specific Information (continued) Complete only the applicable section. Plan/Report # Page # c. Background concentrations of those Attachment 1 Page 3 hazardous materials i. Statewide NA ii. Site-specific Attachment 1 Page 3-4 d. Release and exposure pathways e. Risk management techniques used to prevent adverse impact or significant risks to public health, safety & the environment, including nuisance conditions i. Engineering controls ii. Use limitations iii. Other techniques f. Hazardous materials concentrations above UCLs g. Hazardous materials concentrations not below background i. Demonstration that these are within acceptable limits through (a) Numerical Standards or (b) Total Waste Reuse Risk h. Evaluation and control of significant risks to public health and safety i. Evaluation and control of significant risks to the environment j. End of use management k. Deed notification Attachment 1 Page 4-5 NA NA Attachment 1 Page 5 Attachment 1 Page 5 Attachment 1 Page 5 Attachment 1 Page 5 Attachment 1 Page 5 Attachment 1 Page 5 Attachment 1 Page 5 Attachment 1 Page 5 X256058 Transmittal Number Facility ID# (if known) Page # DEP Use Only Application for Beneficial Use Determination • Revised 11/06 BWP SW 39 40 4142 • Page 5 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Prevention — Solid Waste Management Application for Beneficial Use Determination BWP SW 39 Commercial Products - BWP SW 40 Regulated Systems BWP SW 41 Restricted Applications - BWP SW 42 Unrestricted Applications BWP SW 44 Modifications C. Category -Specific Information (continued) Complete only the applicable section. Plan/Report # Page # 4. BWP SW 42: Use of Secondary Material in Unrestricted Applications, 19.060(17) a. Description of proposed use b. Conservative, unrestricted general exposure assumptions c. Complete Section 3 (BWPSW41) on page 4 of this form 5. BWP SW 44: Modification a. Description of Change b. Attach existing BUD c. Summation of data collection under existing BUD, if any d. Identification and submission of information needed to process requested modification D. Certification: 310 CMR 19.011 Any person, required by these regulations or any order issued by the Department, to submit papers shall identify themselves by name, profession, and relationship to the applicant and legal interest in the facility, and make the following certification: "I certify under penalty of law that I have personally examined and am familiar with the information submitted in this document and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the information is true, accurate and complete. I am aware that there are significant penalties both civil and criminal for submitting false information including possible fines and imprisonment." X256058 Transmittal Number Facility ID# (if known) Page # DEP Use Only Application for Beneficial Use Determination • Revised 11/06 BWP SW 39 40 4142 • Page 6 of 6 .-4 WOODARD &CURRAN ATTACHMENT 1- PROJECT INFORMATION B. Project Information 1. Summary of the secondary material's proposed use and handling The proposed material is catch basin cleanings and street sweepings to be combined with compost and reused along the edge of town roads or islands within the public right of way. The catch basin cleanings and street sweepings are collected with mechanical equipment by Public Works personnel and transported to the Cyr Recycle Center on Sharpener's Pond Road for storage. At the Cyr Recycle Center the catch basin cleanings and street sweepings are combined together and will be mixed with compost at a minimum mix ratio of one part catch basin cleaning/street sweeping to six parts compost. The final material will be transported as needed and detailed in this BUD. 2. Description of how the proposed utilization will result in a viable & beneficial substitution for a commercial product or commodity. a. Description of the feedstock or product the secondary material is replacing The proposed material will replace natural soil needed as surface cover along road edges or islands within public right of ways. b. Description of the proposed use of the secondary material The proposed use of the secondary material is use as a surface cover to be left bare or seeded as needed to maintain roadway shoulders and islands within the Town of North Andover. 3. Detailed description of the proposed facility that stores process, or otherwise handles the secondary material proposed for use. a. Source or origin of secondary material The proposed material is catch basin cleanings and street sweepings collected from the Town of North Andover owned and maintained catch basins and streets respectively. Street sweepings primarily consist of sand and soil generated during routine cleaning of roadways and may also include some leaves and other miscellaneous material collected during the sweeping. Catch basin cleanings typically consist of leaves, sand and twigs removed from separated storm water collection systems during cleaning operations. b. Processing methods used in the preparation of the secondary material The catch basin cleanings and street sweepings are combined together and will be mixed with compost at a minimum mix ratio of one part catch basin cleaning/street sweeping to six parts compost utilizing a front end loader, excavator or similar equipment. The mixing process will take place at the Cyr Recycle Center. c. Description of similar products currently & historically produced by the facility Historically mulch for Town use has been produced by the facility. d. Annual quantities, by weight and/or volume, of the secondary material proposed for beneficial use Approximately 150 Tons of the material is anticipated to be generated on an annual basis. e. Storage requirements necessary for maintaining sufficient material inventory to meet market demand. An approximate 12,000 sf area is available for storage of catch basin cleanings, street sweepings, and compost at the Cyr Recycle Center. Town of North Andover (225073.12) 1 Woodard & Curran Attachment 1 —Project Information May 2013 AD- { fit toDARD &xGURRAN 4. Proposed location of use, if applicable, or types of locations where the secondary material will be used. The proposed use of the secondary material is use as a surface cover to be left bare or seeded as needed to maintain roadway shoulders and islands within the Town of North Andover. 5. Detailed physical & chemical characterization of both the secondary material proposed for beneficial use and the final product a. Physical & chemical characterization, percent solids, organic fraction, moisture content/moisture capacity The proposed BUD material will consist of a mixture at a ratio of one part catch basin cleanings and street sweeping to two part compost. Based on the laboratory data collected (See Attachment 2: Summary of Analytical Data for the North Andover Catch Basin Cleanings BUD Application) the catch basin cleanings and street sweepings had an average moisture content of 21% and was comprised of an average of 79% solids. Since these materials will be mixed with compost and used as a mulch the percent organics will be significant. b. Biological properties: pathogens, ect. Due to the nature of the material, this is not applicable. c. Chemical characterization Attachment 2 contains a summary table comparing the analytical results to the applicable Method 1 BUD standards. A copy of the certified laboratory analytical report is presented in Attachment 3. As shown in the Summary Table included in Attachment 2, there was one detection of benzo(a)pyrene at a concentration of 2,400 ppb in sample CB -1 that slightly exceeded the applicable S-2/GW-2 and S-2/GW-3 standards of 2,100 ppb. However, the average concentrations for the two samples collected were all below the applicable Method 1 BUD standards. In addition, besides the detection of benzo(a)pyrene in sample CB -1, there were no other Critical Contaminants of Concern that exceeded the applicable BUD standards in either sample. d. Description of sampling & analysis methods On June 7, 2012, John Borgesi of Woodard & Curran, Inc., collected two samples from stockpiles of catch basin cleanings and street sweepings that had been combined at the Cyr Recycle Center. The samples were picked up via courier service by TestAmerica Laboratories, Inc. from Woodard & Curran's office at 35 New England Business Center, Andover, MA and delivered under a chain of custody to TestAmerica's Westfield, MA laboratories. Please refer to Attachment 3 for copies of the attached analytical data, QA/QC, and chain of custody. 6. Evaluation & control of potential adverse health, safety or environmental impacts. a. Toxics Use Reduction Plan (TURP), if applicable A Toxics Use Reduction Plan (TURP) is not applicable. b. Risk management techniques being used (e.g. deed/use limitations, location restrictions, engineering controls, etc.) The proposed BUD material will be used in restricted locations and will mimic the requirements of the Massachusetts Street Sweeping policy, Policy# BWP-94-092: Reuse & Disposal of Street Sweepings. These restrictions will include the following: • The street sweepings will not have been collected from Urban Center Roads; • The BUD materials will be used under the road surface or as fill along the side of the road within the public way; • The BUD materials will not be used in residential areas; Town of North Andover (225073.12) 2 Woodard & Curran Attachment 1 — Project Information May 2013 Ab.- WOODARD &CURRAN • The BUD materials will be kept above the level of the groundwater; • The BUD materials will not be used in designated "No Salt Areas"; • The BUD materials will not be used within the 100 foot buffer zone of a wetland or within wetland resource area including bordering vegetative wetlands and riverfront areas; • The BUD materials will not be used within 500 feet of a ground or surface drinking water supply or within a potential drinking water source area. Primary commercial roads within the Town of North Andover are owned and maintained by the Massachusetts Department of Transportation. In addition, based on the groundwater and soil categories as defined in 310 CMR 40: Massachusetts Contingency Plan, (see section C.1.d below) the proposed BUD materials will not be used in the following areas: • Areas categorized as GW -1 which include the following: o Areas within a current or potential drinking water source; or • Areas categorized as S-1 which include the following: • Areas where both adults and children reside and are located for long periods of time (eight hours or more a day); and • Areas where there is the potential to disturb the soil with activities such as gardening and playing recreational sports. Based on the locations where the BUD material is being proposed for reuse (surface cover along road edges, shoulders, or islands within public right of ways) none of these areas are categorized as an S-1 as identified above. Best Management Practices (BMPs) Proper erosion controls and dust prevention measures are proposed during transport of the material and at the storage facility. C. Category -Specific Information 1. BWP SW 41: Use of Secondary Materials in Restricted Applications, 19.060(16) a. Concentrations of hazardous materials of concern in the material proposed for use Based on the laboratory analysis performed concentrations of metals, volatile organic compounds and semi -volatile organic compounds were detected; however with the exception of benzo(a)pyrene in sample CB -1, all of the concentrations detected were below the applicable Method 1 BUD standards. In addition, the average concentration of benzo(a)pyrene for the two samples collected was below the applicable Method 1 BUD standard. b. Upper concentration limits (UCLs) for those hazardous materials Based on the laboratory analysis performed, no UCLs were exceeded in either of the two samples collected (See Attachment 2). c. Background concentrations of those hazardous materials L Statewide ii. Site-specific Since the BUD material is being proposed to be used along the shoulders of asphalt roadways or within islands within the asphalt roadway the background fill within these areas would be expected to contain coal and coal type constituents. In addition, the majority of fill used throughout the Commonwealth over the years has contained some Town of North Andover (225073.12) 3 Woodard & Curran Attachment 1 —Project Information May 2013 A. WOODARD &CURRAN bi-product of either coal or wood ash; therefore the MA DEP Identified Background Levels in Soil Containing Coal Ash or Wood Ash Associated with Fill Material was considered to be the applicable background standard for comparison. As summarized in Attachment 2, there were no exceedences of the background concentrations in soil containing coal ash or wood ash associated with fill material. d. Release and exposure pathways In accordance with the MCP (310 CMR 40.00), this section identifies and documents the soil and groundwater categories applicable to the Site, as described in 310 CMR 40.0930. Based on the soil and groundwater categories, the applicable Method 1 BUD standards will be used for comparison of the COC's and characterize the risk. Soil The MCP specifies three soil categories (S-1, S-2, and S-3). Category S-1 soil represents the highest potential for exposure because it assumes the unrestricted use of the soil (i.e., residential), whereas Category S-3 soil represents the lowest potential for exposure. As previously discussed, the proposed reuse for the BUD material is being restricted for use along roadway edges, shoulders, and islands within the public right of way. With these restrictions the areas proposed for reuse do not fall within any of the S-1 categories for adult and children intensity and frequency therefore the S-1 category is not applicable. Even with the proposed restricted use, and the low intensity and low frequency that either adults or children will be present within these areas, the BUD material will potentially be located within 0-3 feet below the ground surface and will be accessible (e.g. unpaved), therefore the S-2 category is applicable. In addition, over time and the continued reuse of the proposed BUD material, although unlikely, the potential exists for the material to be accessible and located greater than 3 feet below the ground surface. With the same potential exposure intensities and frequencies for both adults and children and the material being located greater than 3 feet below the ground surface the S-3 category is also applicable. In summary, soil is classified as S-2 and S-3. Groundwater MassDEP has established three categories for groundwater, which may apply to a specified volume of groundwater at a Site or to an aquifer taken as a whole. These groundwater categories were established to identify groundwater associated with the following three distinct types of exposures: • GW -1 applies to groundwater that currently is or assumed to be a potential source of drinking water. • GW -2 applies to groundwater considered to be a potential source of vapors that could migrate through the subsurface and concentrate in indoor air of on-site buildings. • GW -3 applies to groundwater that is assumed to discharge to surface water. As identified under the proposed restrictions, the BUD material will not be used in any areas within 500 feet of a ground or surface drinking water supply or within any potential drinking water source areas; therefore the GW -1 category is not applicable. Town of North Andover (225073.12) 4 Woodard & Curran Attachment 1 — Project Information May 2013 WOODARD cCURRAN Since the depth to groundwater will vary in different areas within the Town, the depth to groundwater may be within 15 feet below the ground surface. In addition, the shoulder or roadways may be within 30 feet or an occupied building; therefore the GW -2 category is applicable. All groundwater in the Commonwealth is classified as GW -3, which assumes that groundwater will ultimately migrate and discharge to a surface water body. In summary, groundwater is classified as GW -2 and GW -3. e. Risk management techniques used to prevent adverse impact or significant risks to public health, safety & the environment, including nuisance conditions L Engineering Controls ii. Use limitations iii. Other techniques Refer to the above response to question 6.b for a detailed discussion on proposed Risk Management techniques. f. Hazardous materials concentrations above UCLs Not Applicable. No UCLs were exceeded in the material samples. g. Hazardous materials concentrations not below background i. Demonstration that these are within acceptable limits through (a) Numerical Standards or (b) Total Waste Reuse Risk As previously discussed, the only exccedence of the Method 1 BUD standards was the slightly elevated concentration of benzo(a)pyrene in sample CB -1 which exceeded the standard of 2,000 ppb with a detection of 2,400 ppb. All other compounds detected were below the applicable Method 1 BUD standards, below the UCL's, and below the background concentrations (including benzo(a)pyrene) for soil containing coal ash or wood ash associated with fill material. In addition, the average concentration of benzo(a)pyrene for the two samples collected was below the applicable Method 1 BUD standard. (See Attachment 2: Summary of Analytical Data for the North Andover Catch Basin Cleanings BUD Application) h. Evaluation and control of significant risks to public health and safety The proposed average BUD material concentrations were all below the applicable BUD Method 1 categories for S- 2/GW-2, S-2/GW-3, S-3/GW-2, and S-3/GW-3; therefore, the reuse of the BUD material will not pose a risk to the public health, safety, welfare or the environment. i. Evaluation and control of significant risks to the environment Refer to response to C. 1.h above. j. End of use management Secondary material applied along the edge of town roads, shoulders, or islands within the public right of ways will be maintained in accordance with the Towns routine right of way maintenance including but not limited to the application of vegetation (as necessary) and periodic mowing. k. Deed notification Not Applicable. The secondary material is proposed to be reused with public right of ways. Town of North Andover (225073.12) 5 Woodard & Curran Attachment 1 — Project Information May 2013 WOODARD &CURRAN ATTACHMENT 2 - SUMMARY OF ANALYTICAL DATA Town of North Andover (225073.12) Woodard & Curran Attachment 1 — Project Information May 2013 ATTACHMENT 2 - SUMMARY OF ANALYTICAL DATA FOR THE NORTH ANDOVER CATCH BASIN CLEANINGS BUD APPLICATION OIL OR HAZARDOUS MATERIAL Proposed S- Proposed S- Proposed S- Proposed S- 2, GW -2 BUD 2, GW -3 BUD 3, GW -2 BUD 3, GW -3 BUD Values Values Values Values ug/Kg ug/Kg ug/Kg ug/Kg UCLs ug/Kg Background Concentration in Soil Containing Coal Ash or Wood Ash Associated with Fill Material ug/Kg CB -1 61712012 ug/Kg CB -2 61712012 I ug/Kg Average 61712012 ug/Kg VOCs ACETONE 50,000 350,000 50,000 350,000 10,000,000 NS <46000* <35000* ND BENZENE 76,000 76,000 330,000 540,000 9,000,000 NS <460 <350 ND BROMOFORM 700 520,000 700 800,000 10,000,000 NS <460 <350 ND BROMOMETHANE 10 32,300 10 32,000 10,000,000 NS <910 <700 ND BUTANONE-2 MEK 50,000 350,000 50,000 350,000 10,000,000 NS <4600* <3500* ND CARBON TETRACHLORIDE 4,500 31,000 4,500 220,000 4,000,000 NS <460 <350 ND CHLOROBENZENE 490 110,000 500 1 110,000 10,000,000 NS <460 <350 ND CHLORODIBROMOMETHANE 17 48,000 17 340,000 5,000,000 NS <460 <350 ND CHLOROFORM 38 410,000 38 410,000 8,000,000 NS < 460 < 350 ND DICHLOROBENZENE, 1,2- (o -DCB) 15,000 330,000 15,000 330,000 10,000,000 NS <460 <350 ND DICHLOROBENZENE, 1,3- (m -DCB) 21,000 500,000 21,000 500,000 5,000,000 NS <460 <350 ND DICHLOROBENZENE, 1,4- (p -DCB) 1,200 170,000 1,200 1,200,000 10,000,000 NS <460 <350 ND DICHLOROBROMOMETHANE 8 66,000 8 460,000 5,000,000 NS <460 <350 ND DICHLOROETHANE, 1,1- 2,700 1,000,000 2,700 1,300,000 10,000,000 NS <460 <350 ND DICHLOROETHANE,1,2- 6 45,000 6 310,000 6,000,000 NS <460 <350 ND DICHLOROETHYLENE,CIS-1,2- 220 500,000 220 500,000 5,000,000 NS <460 <350 ND DICHLOROETHYLENE, TRANS -1,2- 640 1,000,000 640 2,500,000 10,000,000 NS 390J 330J 360J DICHLOROPROPANE,1,2- 5 52,000 5 280,000 6,000,000 NS <460 <350 ND DICHLOROPROPENE,1,3-* 42 35,000 42 140,000 NS NS <460 <350 ND DIOXANE, 1,4- 2,700 300,000 2,700 450,000 5,000,000 NS <46000 <35000 ND ETHYLBENZENE 230,000 230,000 230,000 230,000 10,000,000 NS <460 <350 NO ETHYLENEDIBROMIDE EDB)* 5 48 5 1 330 300,000 NS <460 <350 ND HEXACHLOROBUTADIENE 45,000 45,000 54,000 54,000 1,000,000 NS <460 <350 ND METHYL ISOBUTYL KETONE 50,000 400,000 50,000 400,000 10,000,000 NS <46000* <35000* ND METHYL TERT BUTYL ETHER** 100,000 500,000 100,000 500,000 5,000,000 NS < 460 < 350 ND NAPHTHALENE 14,000 1,000,000 14,000 3,000,000 10,000,000 500 <4600 <3500 ND STYRENE 1,800 120,000 1,800 630,000 10,000,000 NS <460 <350 ND TETRACHLOROETHANE, 1,1,1,2- 25 52,000 25 150,000 3,000,000 NS <460 <350 ND TETRACHLOROETHANE, 1,1,2,2- 9 6,800 91 19,000 400,000 NS <460 1 <350 ND TETRACHLOROETHYLENE 5,000 80,000 5,000 370,000 10,000,000 NS <460 <350 ND TRICHLOROBENZENE, 1,2,4- 33,000 450,000 30,000 450,000 9,000,000 NS <460 <350 ND TRICHLOROETHANE, 1,1,1- 320,000 1,000,000 320,000 1,400,000 10,000,000 NS <460 <350 ND TRICHLOROETHANE, 1,1,2- 530 30,000 530 91,000 2,000,000 NS <460 <350 ND TRICHLOROETHYLENE 250 370,000 250 810,000 10,000,000 NS <460 <350 ND TOLUENE 130,000 520,000 130,000 520,000 10,000,000 NS <460 <350 ND VINYL CHLORIDE 660 1,800 660 1 12,000 300,000 NS <460 <350 ND SVOCs ACENAPHTHENE 3,000,000 3,000,000 5,000,000 5,000,000 10,000,000 2,000 <2200 <2000 ND ACENAPHTHYLENE 110,000 14,000 110,000 14,000 10,000,000 1,000 < 2200 < 2000 ND ANTHRACENE 3,000,000 3,000,000 5,000,000 5,000,000 10,000,000 4,000 < 2200 < 2000 ND BENZO(a)ANTHRACENE 21,000 21,000 160,000 160,000 3,000,000 9,000 2000J 1600 J 1800 J BENZO a PYRENE** 2,100 2,100 16,000 16,000 300,000 7,000 2400 1700 J 2,050 J BENZO b FLUORANTHENE 21,000 21,000 160,000 1 160,000 3,000,000 8,000 3600 1 2400 3,000 BENZO g,h,i PERYLENE 3,000,000 3,000,000 5,000,000 5,000,000 10,000,000 1 3,000 1100 J 700 J 900 J BENZOkFLUORANTHENE 210,000 210,000 1,600,000 1,600,000 10,000,000 4,000 1700J 1500J 1,600J BIS2-CHLOROETHYLETHER 660 1,500 660 4,700 90,000 NS <4400 <4000 ND BIS 2-ETHYLHEXYL PHTHALATE 230,000 230,000 230,000 230,000 10,000,000 NS <4400 <4000 ND CHLOROPHENOL, 2- 2,300 310,000 2,300 312,000 10,000,000 NS <4400 <4000 ND CHLOROANILINE, - 100,000 3,300 100,000 3,300 3,000,000 NS <8900 <7900 ND CHRYSENE 2,100,000 2,100,000 3,400,000 1 3,400,000 10,000,000 7,000 2800 1 1900J 2,350J DIBENZO a,h ANTHRACENE 2,100 2,100 16,000 16,000 300,000 1 1,000 <2200 <2000 ND DICHLOROBENZENE, 1,2 -(o -DCB) 15,000 330,000 15,000 330,000 10,000,000 1 NS <4400 <4000 ND DICHLOROBENZENE, 1,3 -(m -DCB) 21,000 500,000 21,000 500,000 5,000,000 NS <4400 <4000 ND DICHLOROBENZENE, 1,4 -(p -DCB) 1,200 170,000 1,200 1,200,000 10,000,000 NS <4400 <4000 ND DICHLOROBENZIDINE, 3,3'- 5,000 5,000 20,000 20,000 400,000 NS <8900 <7900 ND DICHLOROPHENOL,2,4- 49,000 40,000 49,000 40,000 1,000,000 NS <4400 <4000 ND DI ETHYL PHTHALATE 200,000 290,000 200,000 290,000 10,000,000 NS <4400 <4000 ND 51METHYLPHENOL, 2,4- 64,000 1,250,000 64,000 1,300,000 10,000,000 NS <4400 <4000 ND DIMETHYL PHTHALATE 50,000 1 550,000 50,000 1 550,000 1 10,000,000 NS <4400 <4000 ND DINITROPHENOL,2,4- 45,200 1 45,200 1 45,200 1 45,000 1 900,000 NS <4400 <4000 ND DINITROTOLUENE,2,4- 5,700 1 5,700 1 15,000 1 36,000 1 700,000 NS <4400 <4000 ND ATTACHMENT 2 - SUMMARY OF ANALYTICAL DATA FOR THE NORTH ANDOVER CATCH BASIN CLEANINGS BUD APPLICATION OIL OR HAZARDOUS MATERIAL Proposed S- Proposed S- Proposed S- Proposed S- 2, GW -2 BUD 2, GW -3 BUD 3, GW -2 BUD 3, GW -3 BUD Values Values Values Values ug/Kg ug/Kg ug/Kg ug/Kg UCLs uglKg Background Concentration in Soil Containing Coal Ash or Wood Ash Associated with Fill Material uglKg CB -1 61712012 ug/Kg CB -2 6/7/2012 uglKg Average 617/2012 ug/Kg FLUORANTHENE 3,000,000 3,000,000 5,000,000 5,000,000 10,000,000 10,000 4700 3400 4,050 FLUORENE 3,000,000 3,000,000 5,000,000 5,000,000 10,000,000 2,000 < 2200 < 2000 ND HEXACHLOROBENZENE 2,400 2,400 15,000 15,000 300,000 NS <4400 <4000 ND HEXACHLOROBUTADIENE 45,000 45,000 54,000 54,000 1,000,000 NS <4400 <4000 ND HEXACHLOROETHANE 1,700 74,000 1,700 74,000 1,000,000 NS <4400 <4000 ND INDEN 01,2,3 -cd PYRENE 21,000 21,000 160,000 160,000 3,000,000 3,000 970 J 690 J 830 J METHYLNAPHTHALENE, 2- 12,000 240,000 12,000 240,000 5,000,000 1,000 <2200 <2000 ND NAPHTHALENE 14,000 1,000,000 14,000 3,000,000 10,000,000 1,000 <2200 <2000 ND PENTACHLOROPHENOL* 33,000 13,000 230,000 10,000 5,000,000 NS <22000 <20000 NO PHENANTHRENE 1,000,000 1,000,000 3,000,000 3,000,000 10,000,000 20,000 2200 18001 2,000 J PHENOL 50,000 15,500 50,000 20,000 10,000,000 NS <4400 <4000 ND PYRENE 3,000,000 3,000,000 5,000,000 5,000,000 10,000,000 20,000 4500 3200 3,850 TRICHLOROBENZENE,1,2,4- 33,000 450,000 30,000 450,000 9,000,000 NS <4400 <4000 ND TRICHLOROPHENOL, 2,4,5- 1,000,000 580,000 1,000,000 580,000 10,000,000 NS <4400 <4000 ND TRICHLOROPHENOL 2,4,6- 7,800 18,900 7,800 19,000 10,000,000 NS <4400 <4000 ND TPH PETROLEUM HYDROCARBONS 500,000 500,000 500,000 500,000 10,000 NS 700 B 710 B 705 B PCBs _ _. _.. POLYCHLORINATED BIPHENYLS (PCBs) 1,600 1,600 1,600 1,600 NS NS <120 <120 ND METALS ARSENIC* 11,000 11,000 11,000 11,000 200,000 20,000 6,600 5,500 6,050 BARIUM 2,100,000 2,100,000 2,100,000 21100,000 10,000,000 50,000 30,000 32,000 31,000 CADMIUM 16,000 16,000 16,000 16,000 300,000 3,000 200J 290 290 CHROMIUM TOTAL 570,000 570,000 570,000 570,000 2,000,000 40,000 26,000 35,000 30,500 LEAD 110,000 110,000 110,000 110,000 3,000,000 600,000 31,000 44,000 37,500 MERCURY 16,000 16,000 16,000 16,000 300,000 1,000 < 120 430 275 SELENIUM 390,000 390,000 390,000 390,000 8,000,000 1,000 <710 <640 ND SILVER 110,000 110,000 1 110,000 107,000 2,000,000 5,000 < 710 < 640 ND ZINC 3,000,000 3,000,000 1 5,000,000 5,000,000 10,000,000 300,000 82000 B 94000 B 88,000 B Notes Bold indicates exceedance of MADEP BUD standard Detection limit too high to confirm MADEP Identified Background Levels in Soil standard met Detection limit too high to confirm MADEP BUD standard met * - LCS or LCSD exceeds the control limits B - Compound was found in blank and sample J - Result is less than to RL but greater than or equal to the MDL and the concentration is an approximate value. ug/kg - micrograms per kilogram NS - No Standard ND - Not Detected WOODARD &CURRAN ATTACHMENT 3 - LABORATORY REPORT Town of North Andover (225073.12) Woodard & Curran Attachment 1 — Project Information May 2013 THE LEADER IN ENVIRONMENTAL TESTING TestAmerica Laboratories, Inc. TestAmerica Westfield Westfield Executive Park 53 Southampton Road Westfield, MA 01085 Tel: (413)572-4000 TestAmerica Job ID: 360-41013-1 Client Project/Site: North Andover For: Woodard & Curran Inc 35 New England Business Center Andover, Massachusetts 01810 Attn: John Borgesi �44' Mx�j Authorized for release by. - 611812012 y.6/18/2012 5:01:10 PM Joe Chimi Report Production Representative joe.chimi@testamericainc.com Designee for Becky Mason Project Manager II becky.mason@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Woodard & Curran Inc Project/Site: North Andover Table of Contents TestAmerica Job ID: 360-41013-1 Cover Page .............................................. 1 Table of Contents ......................................... 2 Case Narrative ........................................... 3 Detection Summary .........................:.............. 6 Method Summary ......................................... 7 Sample Summary ......................................... 8 Client Sample Results ...................................... 9 Definitions/Glossary....................................... 17 QC Association Summary ................................... 18 Surrogate Summary ....................................... 21 QC Sample Results ........................................ 23 Lab Chronicle ............................................ 41 Certification Summary ..................................... 42 Receipt Checklists ......................................... 44 Chain of Custody .......................................... 45 TestAmerica Westfield Page 2 of 45 6/18/2012 Case Narrative Client: Woodard & Curran Inc Project/Site: North Andover Job ID: 360-41013-1 Laboratory: TestAmerica Westfield Narrative TestAmerica Job ID: 360-41013-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required. Calculations are performed before rounding to avoid round -off errors in calculated results. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. TestAmerica's Reporting Limits (RLs) for this report may not always meet client specified method reporting limits due to various reasons such as methodology, dilutions, matrix or moisture content (soils). TestAmerica's pivot table EDD documents which compound(s) exceed certain regulatory standards. If not included with your deliverables, please contact your Project Manager about the availability of this EDD for your report. Receipt The samples were received on 6/8/20126:20 PM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 5.7° C. GC/MS VOA Method 8260C: The calibration curve uses quadratic regressions for Dichlorodifluoromethane, Acetone and Hexachlorobutadiene as allowed by the method. The laboratory control sample (LCS) and the laboratory control sample duplicate (LCSD) for batch 91862 exceeded control limits for one or more compounds. The data is flagged accordingly. Please reference the QC report for details. The method blank for batch 91862 contained Methylene Chloride above the method detection limit (MDL). Associated samples were re -analyzed due to suspected laboratory contamination of this compounds. Both sets of results for Methylene Chloride are reported. The following samples were provided to the laboratory with a significantly different initial weight than that required by the reference method: CB -1 (360-41013-1), CB -2 (360-41013-2). The method requires 1:1 ratio of soil to methanol. The amount provided was below this range. The laboratory control sample (LCS) and the laboratory control sample duplicate (LCSD) for high level batch 91954 exceeded control limits for one or more compounds. The data is flagged accordingly. Please reference the QC report for details. Methylene Chloride was detected above the reporting limit (RL) in the method blank associated with batch 91954 as well as in the following samples: CB -1 (360-41013-1), CB -2 (360-41013-2). These are the re -analyses of the associated samples. Both sets of results are reported for Methylene Chloride. No other analytical or quality issues were noted. GC/MS Semi VOA Method 8270D: The calibration curve uses quadratic regressions for Aniline as allowed by the method. The method blank for batch 91885 contained Di -n -butyl phthalate above the method detection limit (MDL). This target analyte concentration was less than the reporting limit (RL); therefore, re -extraction and/or re -analysis of samples was not performed. The laboratory control sample (LCS) and the laboratory control sample duplicate (LCSD) for batch 91885 exceeded control limits for one or more compounds. The data is flagged accordingly. Please reference the QC report for details. The following samples were diluted due to the abundance of target analytes: CB -1 (360-41013-1), CB -2 (360-41013-2). Elevated reporting limits (RLs) are provided. No other analytical or quality issues were noted TestAmerica Westfield Page 3 of 45 6/18/2012 Case Narrative Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Job ID: 360-41013-1 (Continued) O Laboratory: TestAmerica Westfield (Continued) GC Semi VOA Method 801513: The method blank for preparation batch 91884 contained Total Petroleum Hydrocarbons (C9 -C36) above the reporting limit (RL). The associated samples contained detects for this analyte at concentrations greater than ten times the value -found in the method blank; therefore, re -extraction and/or re -analysis of samples was not performed. The following samples were diluted due to the abundance of target analytes: CB -1 (360-41013-1), CB -2 (360-41013-2). Elevated reporting limits (RLs) are provided. For sample CB -2 (360-41013-2), due to the level of dilution required, surrogate recoveries were diluted outside control limits. No other analytical or quality issues were noted. Metals Method 6010C: The method blank for preparation batch 91916 contained Zinc above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re -extraction and/or re -analysis of samples was not performed. At the request of the client, an abbreviated MCP analyte list was reported for this job. No other analytical or quality issues were noted. TestAmerica Westfield Page 4 of 45 6/18/2012 MassDEP Analytical Protocol Certification Form Laboratory Name: TestAmerica Westfield Project #: 360-41013-1 Project Location: North Andover RTN: This form provides certifications for the following data set: list Laboratory Sample ID Number(s): 360-41013-(1-2) Matrices: ❑ Groundwater/Surface Water ® Soil/Sediment ❑ Drinking Water ❑Air ❑ Other: CAM Protocols (check all that apply below): 8260 VOC 7470/7471 Hg Mass DEP VPH 8081 Pesticides 7196 Hex Cr Mass DEP APH CAM II A ® CAM III B ® CAM IV A ❑ CAM V B ❑ CAM VI B ❑ CAM IX A ❑ 8270 SVOC 7010 Metals Mass DEP EPH 8151 Herbicides 8330 Explosives TO-15 VOC CAM IIB CAM III C ❑ CAM IV B ❑ CAM V C ❑ CAM VIII A ❑ CAM IX B ❑ 9014 Total 6010 Metals 6020 Metals 8082 PCB Cyanid /PAC 6860 Perchlorate CAM IIIA CAM III D ❑ CAM V A ® CAM VI A ❑ CAM VIII B ❑ Affirmative Responses to Questions A through F are required for "Presumptive Certainty" status Were all samples received in a condition consistent with those described on the Chain-of-Custody, A properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding time. ® Yes ❑ No 13 Were the analytical method(s) and all associated QC requirements specified in the selected CAM protocol(s) followed? ®Yes ❑ No C Were all required corrective actions and analytical response actions specified in the selected CAM ❑ tocol(s) implemented for all identified performance standard non-conformances? X❑Yes No Does the laboratory report comply with all the reporting requirements specified in CAM VII A, D "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical ❑ Data"?X❑ Yes No a. VPH, EPH and APH Methods only: Was each method conducted without significant ❑ Yes ❑ No E modification(s)? (Refer to the individual method(s) for a list of significant modifications). IE]Yes b. APH and TO-15 Methods only: Was the complete analyte list reported for each method? ❑ No F Were all applicable CAM protocol QC and performance standard non-conformances identified and ❑ evaluated in a laboratory narrative (including all "No" responses to Questions A through E)? I X❑Yes No Responses to Questions G, H and I below are required for "Presumptive Certainty" status Ere the reporting limits at or below all CAM reporting limits specified in the selected CAM Gttocol(s)? X ❑ ❑ Yes No Data User Note: Data that achieve 'Presumptive Certainty" status may not necessarily meet the data usability and representativeness requirements described in 310 CMR 40. 1056 (2)(k) and WCS-07-350 H Were all QC performance standards specified in the CAM protocol(s) achieved? ❑Yes No' Were results reported for the complete analyte list specified in the selected CAM protocol(s) ? ❑ YesX❑ No' All negative responses must be addressed in an attached laboratory narrative. 1, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief, is accurate and complete. Signature: Position: Technical Manager Printed Name: James Wickham Date: 6/18/12 16:44 his form has been electronically signed and approved Page 5 of 45 6/18/2012 Detection Summary Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Client Sample ID: C13-1 Lab Sample ID: 360-41013-1 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Methylene Chloride 2500 B 1800 370 ug/Kg 1 8260C Total/NA trans-1,2-Dichloroethene 390 J 460 260 ug/Kg 1 8260C Total/NA Methylene Chloride - RA 1200 J B 1800 370 ug/Kg 1 8260C Total/NA Benzo[a]anthracene 2000 J 2200 660 ug/Kg 10 8270D Total/NA Benzo[a]pyrene 2400 2200 660 ug/Kg 10 8270D Total/NA Benzo[b]fluoranthene 3600 2200 660 ug/Kg 10 8270D Total/NA Benzo[g,h,i]perylene 1100 J 2200 660 ug/Kg 10 8270D Total/NA Benzo[k]fluoranthene 1700 J 2400 660 ug/Kg 10 8270D Total/NA Chrysene 2800 2200 660 ug/Kg 10 8270D Total/NA Fluoranthene 4700 2200 660 ug/Kg 10 8270D Total/NA Indeno[1,2,3-cd]pyrene 970 J 4400 660 ug/Kg 10 8270D Total/NA Phenanthrene 2200 2200 660 ug/Kg 10 8270D Total/NA Pyrene 4500 2200 660 ug/Kg 10 8270D Total/NA Arsenic 6.6 1.4 0.16 mg/Kg 1 6010C Total/NA Barium 30 0.71 0.16 mg/Kg 1 6010C Total/NA Cadmium 0.20 J 0.28 0.0093 mg/Kg 1 6010C Total/NA Chromium 26 0.71 0.17 mg/Kg 1 6010C Total/NA Zinc 82 B 3.5 0.30 mg/Kg 1 6010C Total/NA Lead 31 0.71 0.069 mg/Kg 1 6010C Total/NA Analyte Result Qualifier RL RL Unit Dil Fac D Method Prep Type Total Petroleum Hydrocarbons 700 B 43 43 mg/Kg 10 80156 Total/NA (C9 -C36) Diesel Range Organics [C10 -C28] 310 43 43 mg/Kg 10 80158 Total/NA Specific Conductance 700 3.9 3.9 umhos/cm 1 SM 2510B Soluble Client Sample ID: C13-2 Lab Sample ID: 360-41013-2 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Methylene Chloride 2100 B 1400 280 ug/Kg 1 82606 Total/NA trans-1,2-Dichloroethene 330 J 350 200 ug/Kg 1 8260C Total/NA Methylene Chloride - RA 1100 J B 1400 280 ug/Kg 1 8260C Total/NA Benzo[a]anthracene 1600 J 2000 590 ug/Kg 10 8270D Total/NA Benzo[a]pyrene 1700 J 2000 590 ug/Kg 10 8270D Total/NA Benzo[b]fluoranthene 2400 2000 590 ug/Kg 10 8270D Total/NA Benzo[g,h,i]perylene 700 J 2000 590 ug/Kg 10 8270D Total/NA Benzo[k]fluoranthene 1500 J 2100 590 ug/Kg 10 8270D Total/NA Chrysene 1900 J 2000 590 ug/Kg 10 8270D Total/NA Fluoranthene 3400 2000 590 ug/Kg 10 8270D Total/NA Indeno[1,2,3-cd]pyrene 690 J 4000 590 ug/Kg 10 8270D Total/NA Phenanthrene 1800 J 2000 590 ug/Kg 10 8270D Total/NA Pyrene 3200 2000 590 ug/Kg 10 8270D Total/NA Arsenic 5.5 1.3 0.15 mg/Kg 1 6010C Total/NA Barium 32 0.64 0.15 mg/Kg 1 6010C Total/NA Cadmium 0.29 0.26 0.0085 mg/Kg 1 6010C Total/NA Chromium 35 0.64 0.15 mg/Kg 1 6010C Total/NA Zinc 94 B 3.2 0.27 mg/Kg 1 6010C Total/NA Lead 44 0.64 0.063 mg/Kg 1 60106 Total/NA Mercury 0.43 0.067 0.016 mg/Kg 1 7471A Total/NA Analyte Result Qualifier RL RL Unit Dil Fac D Method Prep Type Total Petroleum Hydrocarbons 710 B 79 79 mg/Kg 20 80156 Total/NA (C9 -C36) Diesel Range Organics [C10 -C28] 280 79 79 mg/Kg 20 8015B Total/NA Specific Conductance 420 4.0 4.0 umhos/cm 1 SM 2510B Soluble TestAmerica Westfield Page 6 of 45 6/18/2012 Method Summary Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Method Method Description Protocol Laboratory 8260C Volatile Organic Compounds (GC/MS) MA DEP TAL WFD 8270D Semivolatile Organic Compounds (GC/MS) MA DEP TAL WFD i 80158 Diesel Range Organics (DRO) (GC) SW846 TAL WFD ' 8082 Polychlorinated Biphenyls (GC/ECD) MA DEP TAL WFD 6010C Metals (ICP) SW846 TAL WFD 7471A Mercury (CVAA) SW846 TAL WFD Moisture Percent Moisture EPA TAL WFD SM 25108 Conductivity, Specific Conductance SM TAL WFD Protocol References: EPA= US Environmental Protection Agency MA DEP = Massachusetts Department Of Environmental Protection SM = "Standard Methods For The Examination Of Water And Wastewater", SW846 ='Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL WFD = TestAmerica Westfield, Westfield Executive Park, 53 Southampton Road, Westfield, MA 01085, TEL (413)572-4000 TestAmerica Westfield Page 7 of 45 6/18/2012 Client: Woodard & Curran Inc Project/Site: North Andover Lab Sample ID 360-41013-1 360-41013-2 Client Sample ID CB -1 CB -2 Sample Summary TestAmerica Job ID: 360-41013-1 Matrix Collected Received Solid 06/07/1214:30 06/08/1218:20 Solid 06/07/1214:30 06/08/1218:20 TestAmerica Westfield Page 8 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Client Sample ID: C13-1 Lab Sample ID: 360-41013-1 Date Collected: 06/07/1214:30 Matrix: Solid Date Received: 06/08112 18:20 Percent Solids: 74.6 Method: 8260C - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2 -Tetrachloroethane ND 460 220 ug/Kg * 06/12/1216:11 06/13/1204:10 1 1,1,1 -Trichloroethane ND 460 330 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 1 1,1,2,2 -Tetrachloroethane ND 460 180 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 1,1,2 -Trichloroethane ND 460 180 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 I 1,1-Dichloroethane ND 460 330 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 1,1-Dichloroethene ND 460 290 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 1,1-Dichloropropene ND 460 260 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,2,3-Trichlorobenzene ND 460 200 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,2,3-Trichloropropane ND 460 200 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,2,4-Trichlorobenzene ND 460 180 ug/Kg 06/12/1216:11 06/13/12 04:10 1 1,2,4-Trimethylbenzene ND 460 220 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,2-Dibromo-3-Chloropropane ND 4600 260 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,2 -Dichlorobenzene ND 460 180 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,2-Dichloroethane ND 460 380 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,2-Dichloropropane ND 460 270 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,3,5-Trimethylbenzene _ ND 460. 240 ug/Kg 06/12/12 1 1. 6:11 06/13/12 0410 1 r 1,3 -Dichlorobenzene ND 460 180 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,3-Dichloropropane ND 460 210 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,4 -Dichlorobenzene ND 460 180 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 1,4 -Dioxane ND 46000 20000 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 2,2-Dichloropropane ND 460 370 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 2-Butanone (MEK) ND * 4600 2100 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 2-Chlorotoluene ND 460 220 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 2-Hexanone ND 4600 2500 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 4-Chlorotoluene ND 460 200 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 4-Isopropyltoluene ND 460 270 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 4-Methyl-2-pentanone (MIBK) ND 4600 1800 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Acetone ND 46000 18000 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Benzene ND 460 310 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Bromobenzene ND 460 270 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Bromoform ND 460 290 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Bromomethane ND 910 420 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Carbon disulfide ND 460 350 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Carbon tetrachloride ND 460 310 ug/Kg * . 06/12/12 16:11 06/13/12 04:10 1 Chlorobenzene ND 460 200 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Chlorobromomethane ND 460 250 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Chlorodibromomethane ND 460 220 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Chloroethane ND 910 290 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Chloroform ND 460 270 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Chloromethane ND 910 260 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 cis-1,2-Dichloroethene ND 460 220 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 cis-1,3-Dichloropropene ND 460 180 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Dibromomethane ND 460 230 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Dichlorobromomethane ND 460 240 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Dichlorodifluoromethane ND 910 380 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Ethyl ether ND 460 190 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Ethylbenzene ND 460 290 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Ethylene Dibromide ND 460 200 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Hexachlorobutadiene ND 460 260 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Isopropyl ether ND 460 200 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 Isopropylbenzene ND 460 290 ug/Kg * 06/12/12 16:11 06/13/12 04:10 1 TestAmerica Westfield Page 9 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc Project/Site: North Andover Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac TestAmerica Job ID: 360-41013-1 Client Sample ID: CB -1 1800 370 ug/Kg 06/14/12 15:20 06/15/12 02:39 1 Surrogate Lab Sample ID: 360-41013-1 Date Collected: 0610711214:30 Prepared Analyzed Dil Fac 4-Bromofluorobenzene 103 70-130 Matrix: Solid Date Received: 06/0811218:20 1 Dibromofluoromethane 98 70-130 06/14/12 15:20 06/15/12 02:39 Percent Solids: 74.5 Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) 96 70-130 06/14/12 15:20 06/15/12 02:39 1 1,4 -Dichlorobenzene ND Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac m -Xylene & p -Xylene ND 910 550 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 Methyl tert-butyl ether ND 460 270 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 Methylene Chloride 2500 B 1800 370 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 n-Butylbenzene ND 460 180 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 I N-Propylbenzene ND 460 180 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 Naphthalene ND 4600 430 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 o -Xylene ND 460 240 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 sec-Butylbenzene ND 460 260 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 Styrene ND 460 180 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 Teri -amyl methyl ether ND 460 270 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 Teri -butyl ethyl ether ND 460 270 ug/Kg 06/14/1212:23 06/12/12 16:11 06/13/12 04:10 1 teri-Butylbenzene ND 460 240 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Tetrachloroethene ND 460 290 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Tetrahydrofuran ND 9100 5200 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Toluene ND 460 310 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 _ trans-1,2-Dichloroethene 390 J 460 260 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 trans-1,3-Dichloropropene ND 460 370 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Trichloroethene ND 460 370 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Trichlorofluoromethane ND 910 280 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Vinyl chloride ND 460 290 ug/Kg 06/12/12 16:11 06/13/12 04:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Brom6fluorobenzene 104 70-130 06/12112 16:11 06/13/12 04:10 1 Dibromofluoromethane 99 70-130 06/12112 16:11 06/13112 04:10 1 Toluene -0 (Surr) 97 70-130 06/12112 16:11 06/13/12 04:10 1 Method: 8260C - Volatile Organic Compounds (GC1MS) - RA Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac Methylene Chloride 1200 J B 1800 370 ug/Kg 06/14/12 15:20 06/15/12 02:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene 103 70-130 06/14/12 15:20 06/15/12 02:39 1 Dibromofluoromethane 98 70-130 06/14/12 15:20 06/15/12 02:39 1 Toluene -d8 (Surr) 96 70-130 06/14/12 15:20 06/15/12 02:39 1 Method: 8270D - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4-Trichlorobenzene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 1,2 -Dichlorobenzene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 1,3 -Dichlorobenzene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 1,4 -Dichlorobenzene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,2'-oxybis[l-chloropropane] ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,4,5 -Trichlorophenol ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,4,6 -Trichlorophenol ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,4-Dichlorophenol ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,4 -Dimethylphenol ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,441nitrophenol ND 4400 730 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,4-Dinitrotoluene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2,6-Dinitrotoluene ND 4400 660 ug/Kg * 06/13/1218:29 06/14/1212:23 10 2-C61oronaphthalene ND 4400 660 ug/Kg * _ 06/13/1218:29 06/14/1212:23 10 2 -Chlorophenol ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 2 -Methylnaphthalene ND 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 TestAmerica Westfield Page 10 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Client Sample ID: CB -1 Lab Sample ID: 360-41013-1 Date Collected: 06/0711214:30 Matrix: Solid Date Received: 06/08/1218:20 Percent Solids: 74.5 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 2-Methylphenol ND 4400 660 ug/Kg 30-130 06/13/1218:29 06/14/1212:23 10 2-Nitrophenol ND 4400 660 ug/Kg 10 06/13/1218:29 06/14/1212:23 10 3 & 4 Methylphenol ND 4400 660 ug/Kg 30-130 06/13/12 18:29 06/14/12 12:23 10 3,3'-Dichlorobenzidine ND 8900 660 ug/Kg 10 06/13/1218:29 06/14/1212:23 10 4-13romophenyl phenyl ether ND 4400 660 ug/Kg 06/13/12 18:29 06/14/12 12:23 10 4-Chloroaniline ND 8900 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 4-Nitrophenol ND 22000 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Acenaphthene ND 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Acenaphthylene ND 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Acetophenone ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Aniline ND 22000 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Anthracene ND 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Azobenzene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Benzo[a]anthracene 2000 J 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Benzo[a]pyrene 2400 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Benzo[b]fluoranthene 3600 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Benzo[g,h,i]perylene 1100 J 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Benzo[k]fluoranthene 1700 J 2400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Bis(2-chloroethoxy)methane ND 4400 660 ug/Kg _ 06/13/1218:29 05/14/1212:23 10 Bis(2-chloroethyl)ether ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Bis(2-ethylhexyl) phthalate ND 4400 660 ug/Kg 06/13/12 18:29 06/14/12 12:23 10 Butyl benzyl phthalate ND 4400 660 ug/Kg 06/13/12 18:29 06/14/12 12:23 10 Chrysene 2800 2200 660 ug/Kg' 06/13/1218:29 06/14/1212:23 10 Di -n -butyl phthalate ND 4400 690 ug/Kg 06/13/12 18:29 06/14/12 12:23 10 Di-n-octyl phthalate ND 4400 660 ug/Kg 06/13/12 18:29 06/14/12 12:23 10 Dibenz(a,h)anthracene ND 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Dibenzofuran ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Diethyl phthalate ND 4400 660 ug/Kg _ 06/13/12 18:29 06/14/12 12:23 10 Dimethyl phthalate ND 4400 660 ug/Kg 06/13/12 18:29 06/14/12 12:23 10 Fluoranthene 4700 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Fluorene ND 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Hexachlorobenzene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Hexachlorobutadiene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Hexachloroethane ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Indeno[1,2,3-cd]pyrene 970 J 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Isophorone ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Naphthalene ND 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Nitrobenzene ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Pentachlorophenol ND 22000 1200 ug/Kg 06/13/1218:29 06/14/1212:23 10 Phenanthrene 2200 2200 660 ug/Kg . .. 06/13/1218:29 . 06/14/1212:23 10 Phenol ND 4400 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Pyrene 4500 2200 660 ug/Kg 06/13/1218:29 06/14/1212:23 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2, 4, 6-Tribromophenol 43 30-130 06/13/12 18:29 06/14/12 12:23 10 2-Fluorophenol 69 30-130 06/13/12 18:29 06/14/12 12:23 10 Nitrobenzene -d5 64 30-130 06/13/12 18:29 06/14/12 12:23 10 Phenol -d5 66 30-130 06/13/12 18:29 06/14/12 12:23 10 Terphenyl-04 73 30-130 06/13/12 18:29 06/14/12 12:23 10 2-Fluorobiphenyl 56 30-130 06/13/12 18:29 06/14/12 12:23 10 TestAmerica Westfield Page 11 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Client Sample ID: C13-1 Date Collected: 06!07/1214:30 Date Received: 06/08/1218:20 RL MDL Unit D Prepared Lab Sample ID: 360-41013-1 Matrix: Solid Percent Solids: 74.5 Method: 8016B - Diesel Range Organics (DRO) (GC) 6.6 1.4 0.16 mg/Kg 06/14/1210:47 06/15/1214:15 Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Petroleum Hydrocarbons 700 B 43 43 mg/Kg 06/14/1210:47 06/13/12 18:22 6/1203-.32 10 (C9 -C36) 0.17 mg/Kg 06/14/1210:47 06/15/1214:15 1 ND 0.71 Diesel Range Organics [C10 -C28] 310 43 43 mg/Kg 1 06/13/12 18:22 06/16/12 03:32 10 Surrogate %Recovery Qualifier Limits 06/15/1214:15 1 82 B Prepared Analyzed Dil Fac I o-Terphenyl 79 40 - 140 1 31 0.71 06/13/12 18:22 06/16/12 03:32 10 Method: 8082 - Polychlorinated Biphenyls (GC/ECD) 06/15/1214:15 1 Result Qualifier RL MDL Unit D Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac PCB -1016 ND 120 36 ug/Kg Unit 06/13/1218:43 06/14/1212:06 1 PCB -1221 ND 120 71 ug/Kg 06/13/1218:43 06/14/1212:06 1 PCB -1232 ND 120 110 ug/Kg 06/13/1218:43 06/14/1212:06 1 PC6-1242 ND 120 43 ug/Kg Analyzed 06/13/1218:43 06/14/1212:06 1 PCB -1248 ND 120 120 ug/Kg 1 06/13/1218:43 06/14/1212:06 1 PCB -1254 ND 120 71 ug/Kg 0611 3/1 2 18:43 06/14/1212:06 1 PCB -1260 ND 120 52 ug/Kg 06/13/1218:43 06/14/1212:06 1 PCB -1262 ND 120 65 ug/Kg 06/13/1218:43 06/14/1212:06 1 PCB -1268 ND 120 59 ug/Kg 06/13/1218:43 06/14/1212:06 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro-m-xylene 93 30-150 06/13/12 18:43 06/14/12 12:06 1 Tetrachloro-m xylene 103 30-150 06/13/12 18:43 06/14/12 12:06 1 DCB Decachlorobiphenyl 88 30-150 06/13/12 18:43 06/14/12 12:06 1 DCB Decachlorobiphenyl 113 30-150 06/13/12 18:43 06/14/12 12:06 1 Method: 6010C - Metals (ICP) Analyte Arsenic Barium Cadmium Chromium Silver Selenium Zinc Lead Method: 7471A - Mercury (CVAA) Analyte Mercury General Chemistry Analyte Percent Moisture Percent Solids General Chemistry - Soluble Arialyte LSpecific Conductance Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 6.6 1.4 0.16 mg/Kg 06/14/1210:47 06/15/1214:15 1 30 0.71 0.16 mg/Kg 06/14/1210:47 06/15/1214:15 1 0.20 J 0.28 0.0093 mg/Kg 06/14/1210:47 06/15/1214:15 1 26 0.71 0.17 mg/Kg 06/14/1210:47 06/15/1214:15 1 ND 0.71 0.037 mg/Kg 06/14/1210:47 06/15/1214:15 1 ND 0.71 0.34 mg/Kg 06/14/1210:47 06/15/1214:15 1 82 B 3.5 0.30 mg/Kg 06/14/1210:47 06/15/1214:15 1 31 0.71 0.069 mg/Kg 06/14112 10:47 06/15/1214:15 1 Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 0.12 0.029 mg/Kg 06/13/12 08:53 06/13/12 12:14 1 Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac 25 1.0 1.0 % 06/11/1214:21 1 75 1.0 1.0 % 06/11/12 14:21 1 Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac 700 3.9 3.9 umhos/cm 06/13/1210:21 1 TestAmerica Westfield Page 12 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Client Sample ID: C13-2 Date Collected: 06/07/12 14:30 Date Received: 06/08/1218:20 Lab Sample ID: 360-41013-2 Matrix: Solid Percent Solids: 82.8 Method: 8260C - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2 -Tetrachloroethane ND 350 170 ug/Kg 06/12/1216:11 06/13/1204:33 1 1,1,1 -Trichloroethane ND 350 250 ug/Kg 06/12/1216:11 06/13/1204:33 1 1,1,2,2 -Tetrachloroethane ND 350 140 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,1,2 -Trichloroethane ND 350 140 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 I 1,1-Dichloroethane ND 350 250 ug/Kg 06/12/1216:11 06/13/12 04:33 1 1,1-Dichloroethene ND 350 230 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,1-Dichloropropene ND . 350 200 Ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,2,3-Trichlorobenzene ND 350 160 ug/Kg 06/12/1216:11 06/13/1204:33 1 1,2,3-Trichloropropane ND 350 160 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,2,4-Trichlorobenzene ND 350 140 ug/Kg ......... 06/12/12 16:11 .. .......... 06/13/12 04:33 1 1,2,4-Trimethylbenzene ND 350 170 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,2-Dibromo-3-Chloropropane ND 3500 200 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,2 -Dichlorobenzene ND 350 140 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,2-Dichloroethane ND 350 290 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,2-Dichloropropane ND 350 210 ug/Kg 06/12/1216:11 06/13/1204:33 1 1,3,5-Trimethylbenzene ND 350 180 ug/Kg 06/12/1216:11 ................ 06/13/1204:33 1 u 1,3 -Dichlorobenzene ND 350 140 ug/Kg 06/12/1216:11 06/13/1204:33 1 1,3-Dichloropropane ND 350 160 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,4 -Dichlorobenzene ND 350 140 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 1,4 -Dioxane ND 35000 15000 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 2,2-Dichloropropane ND 350 290 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 2-Butanone (MEK) ND * 3500 1600 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 2-Chlorotoluene ND 350 170 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 2-Hexanone ND * 3500 1900 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 4-Chlorotoluene ND 350 160 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 4-Isopropyltoluene ND 350 210 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 4-Methyl-2-pentanone (MIBK) ND 3500 1400 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Acetone ND 35000 14000 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Benzene ND 350 240 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Bromobenzene ND 350 210 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Bromoform ND 350 220 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Bromomethane ND 700 320 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Carbon disulfide ND 350 270 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Carbon tetrachloride ND 350 240 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Chlorobenzene ND 350 160 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Chlorobromomethane ND 350 190 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Chlorodibromomethane ND 350 17o ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Chloroethane ND 700 230 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Chloroform ND 350 210 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Chloromethane ND 700 200 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 cis-1,2-Dichloroethene ND 350 170 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 cis- 1,3-Dichloropropene ND 350 140 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Dibromomethane ND 350 170 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Dichlorobromomethane ND 350 180 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Dichlorodifluoromethane ND 700 300 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Ethyl ether ND 350 150 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Ethylbenzene ND 350 230 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Ethylene Dibromide ND 350 160 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Hexachlorobutadiene ND 350 200 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Isopropyl ether ND 350 160 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Isopropylbenzene ND 350 230 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 TestAmerica Westfield Page 13 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc Project/Site: North Andover %Recovery Qualifier Limits Prepared Analyzed Dil Fac TestAmerica Job ID: 360-41013-1 Client Sample ID: CB -2 70-130 06/12/12 16:11 06/13/12 04:33 1 Dibromofluoromethane Lab Sample ID: 360-41013-2 Date Collected: 06/07/1214:30 06/12112 16:11 06/13/12 04:33 1 Toluene -d8 (Surr) 98 70-130 Matrix: Solid Date Received. 06/08/1218:20 1 Dibromofluoromethane 100 70-130 06/14/1215:20 06/15/1203:02 Percent Solids: 82.8 Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) 98 70-130 06/14/12 15:20 06/15/12 03:02 1 1,4 -Dichlorobenzene ND Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac m -Xylene & p -Xylene ND 700 420 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 Methyl tert-butyl ether ND 350 210 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 Methylene Chloride 2100 B 1400 280 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 n-Butylbenzene ND 350 140 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 N-Propylbenzene ND 350 140 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 Naphthalene ND 3500 330 ug/Kg 06/14/1212:54 06/12/1216:11 06/13/1204:33 1 o -Xylene ND 350 180 ug/Kg 06/14/1212:54 06/12/1216:11 06/13/1204:33 1 sec -Butyl benzene ND 350 200 ug/Kg 06/14/1212:54 06/12/1216:11 06/13/1204:33 1 Styrene ND 350 140 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 Tert-amyl methyl ether ND 350 210 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 Tert-butyl ethyl ether ND 350 210 ug/Kg 06/14/1212:54 06/12/12 16:11 06/13/12 04:33 1 tert-Butylbenzene ND 350 180 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Tetrachloroethene ND 350 230 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Tetrahydrofuran ND 7000 4000 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Toluene ND 350 240 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 trans-1,2-Dichloroethene 330 J 350 200 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 trans-1,3-Dichloropropene ND 350 280 ug/Kg 06/12/1216:11 06/13/1204:33 1 Trichloroethene ND 350 280. ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Trichlorofluoromethane ND 700 220 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Vinyl chloride ND 350 230 ug/Kg 06/12/12 16:11 06/13/12 04:33 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene 102 70-130 06/12/12 16:11 06/13/12 04:33 1 Dibromofluoromethane 97 70-130 06/12112 16:11 06/13/12 04:33 1 Toluene -d8 (Surr) 98 70-130 06/12/12 16:11 06/13/12 04:33 1 Method: 8260C - Volatile Organic Compounds (GC/MS) - RA Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Methylene Chloride 1100 J B 1400 280 ug/Kg 06/14/12 15:20 06/15/12 03:02 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene 103 70-130 06/14/12 15:20 06/15/12 03:02 1 Dibromofluoromethane 100 70-130 06/14/1215:20 06/15/1203:02 1 Toluene -d8 (Surr) 98 70-130 06/14/12 15:20 06/15/12 03:02 1 Method: 8270D - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4-Trichlorobenzene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 1,2 -Dichlorobenzene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 1,3 -Dichlorobenzene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 1,4 -Dichlorobenzene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,2'-oxybis[1-chloropropane] ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,4,5 -Trichlorophenol ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,4,6 -Trichlorophenol ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,4-Dichlorophenol ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,4 -Dimethylphenol ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,4-Dinitrophenoi ND 4000 660 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,4-Dinitrotoluene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2,6-Dinitrotoluene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2-Chloronaphthalene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2 -Chlorophenol ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 2 -Methylnaphthalene ND 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 TestAmerica Westfield Page 14 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc Project/Site: North Andover %Recovery Qualifier Limits Prepared Analyzed Dil Fac TestAmerica Job ID: 360-41013-1 Client Sample ID: CB -2 30-130 06/13/12 18:29 06/14/12 12:54 10 2-Fluorophenol Lab Sample ID: 360-41013-2 Date Collected: 06/07/1214:30 06/13/12 18:29 06/14/12 12:54 10 Nitrobenzene -d5 68 30-130 Matrix: Solid Date Received: 06/08/1218:20 10 Phenol -d5 69 30-130 06/13/12 18:29 06/14/12 12:54 Percent Solids: 82.8 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) 30-130 06/13/12 18:29 06/14/12 12:54 10 2-Fluorobiphenyl 60 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 2-Methylphenol ND 4000 590 ug/Kg — 06/13/1218:29 06/14/1212:54 10 2-Nitrophenol ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 3 & 4 Methylphenol ND 4000 590 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 3,3'-Dichlorobenzidine ND 7900 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 I 4-Bromophenyl phenyl ether ND 4000 590 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 4-Chloroaniline ND 7900 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 4-Nitrophenol ND 20000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Acenaphthene ND 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Acenaphthylene ND 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 (i Acetophenone ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Aniline ND 20000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Anthracene ND 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Azobenzene ND 4000 590 ug/Kg 0 06/13/1218:29 06/14/1212:54 10 Benzo[a]anthracene 1600 J 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Benzo[a]pyrene 1700 J 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Benzo[b]fluoranthene 2400 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 1 Benzo[g,h,i]perylene 700 J 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Benzo[k]fluoranthene 1500 J 2100 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Bis(2-chloroethoxy)methane ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Bis(2-chloroethyl)ether ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Bis(2-ethylhexyl) phthalate ND 4000 590 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 Butyl benzyl phthalate ND 4000 590 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 Chrysene 1900 J 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Di -n -butyl phthalate ND 4000 620 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 Di-n-octyl phthalate ND 4000 590 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 Dibenz(a,h)anthracene ND 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Dibenzofuran ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Diethyl phthalate ND 4000 590 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 Dimethyl phthalate ND 4000 590 ug/Kg 06/13/12 18:29 06/14/12 12:54 10 Fluoranthene 3400 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Fluorene ND 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Hexachlorobenzene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Hexachlorobutadiene ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Hex achloro-ethane ND 4000 590 ug/Kg 06/13/121829 06/14/1212:54 10 Indeno[1,2,3-cd]pyrene 690 J 4000 590 ug/Kg, 06/13/1218:29 06/14/1212:54 10 Isophorone ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Naphthalene ND 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Nitrobenzene ND 4000 590 ug/Kg 06/1 311 2 18:29 06/14/1212:54 10 Pentachlorophenol ND 20000 1000 ug/Kg 06/13/1218:29 06/14/1212:54 10 Phenanthrene 1800 J 2000 590 ug/Kg . ... 06/13/1218:29 .......... 06/14/1212:54 10 Phenol ND 4000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Pyrene 3200 2000 590 ug/Kg 06/13/1218:29 06/14/1212:54 10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2,4, 6-Tribromophenol 47 30-130 06/13/12 18:29 06/14/12 12:54 10 2-Fluorophenol 64 30-130 06/13/12 18:29 06/14/12 12:54 10 Nitrobenzene -d5 68 30-130 06/13/1218:29 06/14/1212:54 10 Phenol -d5 69 30-130 06/13/12 18:29 06/14/12 12:54 10 Terphenyl-d14 81 30-130 06/13/12 18:29 06/14/12 12:54 10 2-Fluorobiphenyl 60 30-130 06/13/12 18:29 06/14/1212:54 10 TestAmerica Westfield Page 15 of 45 6/18/2012 Client Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Client Sample ID: C13-2 Lab Sample ID: 360-41013-2 Date Collected: 06/07/12 14:30 Matrix: Solid Date Received: 06/08/1218:20 Percent Solids: 82.8 Method: 8015B - Diesel Range Organics (DRO) (GC) Analyte Result Qualifier Total Petroleum Hydrocarbons 710 B (C9 -C36) Analyzed Diesel Range Organics [C10 -C28] 280 Surrogate %Recovery Qualifier o-Terphenyl 0 XD Method: 8082 - Polychlorinated Biphenyls (GC/ECD) Analyte Result Qualifier PCB -1016 ND PCB -1221 ND PCB -1232 ND PCB -1242 ND PCB -1248 ND PCB -1254 ND PCB -1260 _ ND PCB -1262 ND PCB -1268 ND Surrogate %Recovery Qualifier Tetrachloro-m-xylene 92 Tetrachloro-m-xylene 98 DCB Decachlorobiphenyl 87 DCB Decachlorobiphenyl 107 Method: 6010C -Metals (ICP) ug/Kg Analyte Result Qualifier Arsenic 5.5 Barium 32 Cadmium 0.29 Chromium 35 Silver ND Selenium ND Zinc 94 B Lead 44 Method: 7471A - Mercury (CVAA) 41 Analyte Result Qualifier Mercury 0.43 General Chemistry 120 Analyte Result Qualifier Percent Moisture 17 Percent Solids 83 General Chemistry - Soluble 68 Analyte Result Qualifier Specific Conductance 420 RL RL Unit D Prepared Analyzed Dil Fac 79 79 mg/Kg 06/13/12 18:22 06/16/12 04:04 20 79 79 mg/Kg 06/13/12 18:22 06/16/12 04:04 20 Limits Prepared Analyzed Dil Fac I 40-140 06/13/12 18:22 06/16/12 04:04 20 RL MDL Unit D Prepared Analyzed Dil Fac 120 35 ug/Kg 06/13/1218:43 06/14/1212:27 1 120 68 ug/Kg 06/13/1218:43 06/14/1212:27 1 120 100 ug/Kg 06/13/1218:43 06/14/1212:27 1 120 41 ug/Kg 06/13/1218:43 06/14/1212:27 1 120 110 ug/Kg 06/13/1218:43 06/14/1212:27 1 120 68 ug/Kg 06/13/1218:43 06/14/1212:27 1 120 50 ug/Kg 06/13/1218:43 06/14/1212:27 1 120 63 ug/Kg 06/13/1218:43 06/14/1212:27 1 1.20 56 ug/Kg 06/13/1218:43 06/14/1212:27 1 Limits Prepared Analyzed Dil Fac 30-150 06/13/12 18:43 06/14/12 12:27 1 30-150 06/13/12 18:43 06/14/12 12:27 1 30-150 06/13/12 18:43 06/14/12 12:27 1 30-150 06/13/12 18:43 06/14/12 12:27 1 RL MDL Unit D Prepared Analyzed Dil Fac 1.3 0.15 mg/Kg 06/14/1210:47 06/15/1214:17 1 0.64 0.15 mg/Kg 06/14/1210:47 06/15/1214:17 1 0.26 0.0085 mg/Kg 06/14/1210:47 06/15/1214:17 1 0.64 0.15 mg/Kg 06/14/1210:47 06/15/1214:17 1 0.64 0.033 mg/Kg 06114/1210:47 06/15/1214:17 1 0.64 0.31 mg/Kg 06/14/1210:47 06/15/1214:17 1 3.2 0.27 mg/Kg 06/14/1210:47 06/15/1214:17 1 0.64 0.063 mg/Kg 06/14/1210:47 06/15/1214:17 1 RL MDL Unit D Prepared Analyzed Dil Fac 0.067 0.016 mg/Kg 06713/12 08:53 06/13/12 12:16 1 RL RL Unit D Prepared Analyzed Dil Fac 1.0 1.0 % 06/11/12 14:21 1 1.0 1.0 % 06/11/12 14:21 1 RL RL Unit D Prepared Analyzed Dil Fac 4.0 4.0 umhos/cm 06/13/1210:22 1 TestAmerica Westfield Page 16 of 45 6/18/2012 Definitions/Glossary Client: Woodard & Curran Inc Project/Site: North Andover Qualifiers GC/MS VOA Qualifier Qualifier Description * LCS or LCSD exceeds the control limits B Compound was found in the blank and sample. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. TestAmerica Job ID: 360-41013-1 GC/MS Semi VOA Qualifier Qualifier Description * LCS or LCSD exceeds the control limits J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. B Compound was found in the blank and sample. GC Semi VOA Qualifier Qualifier Description B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D. X Surrogate is outside control limits Metals Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an B Compound was found in the blank and sample. Gloss Abbreviation These commonly used abbreviations may or may not be present in this report. E Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF Contains no Free Liquid DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re -extraction, or additional Initial metals/anion analysis of the sample EDL Estimated Detection Limit EPA United States Environmental Protection Agency MDL Method Detection Limit ML Minimum Level (Dioxin) ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RL Reporting Limit RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Westfield Page 17 of 45 6/18/2012 QC Association Summary Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover GC/MS VOA Prep Batch: 91800 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 CB -1 Total/NA Solid 5035 360-41013-2 CB -2 Total/NA Solid 5035 LCS 360-91800/2-A Lab Control Sample Total/NA Solid 5035 LCSD 360-91800/3-A Lab Control Sample Dup Total/NA Solid 5035 MB 360-91800/4-A Method Blank Total/NA Solid 5035 Analysis Batch: 91862 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 CB -1 Total/NA Solid 8260C 91800 360-41013-2 CB -2 Total/NA Solid 8260C 91800 I LCS 360-91800/2-A Lab Control Sample Total/NA Solid 8260C 91800 LCSD 360-91800/3-A Lab Control Sample Dup Total/NA Solid 8260C 91800 MB 360-91800/4-A Method Blank Total/NA Solid 8260C 91800 Prep Batch: 91911 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 - RA CB -1 Total/NA Solid 5035 360-41013-2 - RA CB -2 Total/NA Solid 5035 LCS 360-91911/2-A Lab Control Sample Total/NA Solid 5035 LCSD 360-91911/3-A Lab Control Sample Dup Total/NA Solid 5035 MB 360-91911/4-A Method Blank Total/NA Solid 5035 Analysis Batch: 91954 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 - RA CB -1 Total/NA - Solid 8260C 91911 360-41013-2 - RA CB -2 Total/NA Solid 8260C 91911 LCS 360-91911/2-A Lab Control Sample Total/NA Solid 8260C 91911 LCSD 360-91911/3-A Lab Control Sample Dup Total/NA Solid 8260C 91911 MB 360-91911/4-A Method Blank Total/NA Solid 8260C 91911 GC/MS Semi VOA Prep Batch: 91885 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 CB -1 Total/NA Solid 3546 360-41013-2 CB -2 Total/NA Solid 3546 LCS 360-91885/2-A Lab Control Sample Total/NA Solid 3546 LCSD 360-91885/3-A Lab Control Sample Dup Total/NA Solid 3546 MB 360-91885/1-A Method Blank Total/NA Solid 3546 Analysis Batch: 91895 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 CB -1 Total/NA Solid 8270D 91885 360-41013-2 CB -2 Total/NA Solid 8270D 91885 LCS 360-91885/2-A Lab Control Sample Total/NA Solid 8270D 91885 LCSD 360-91885/3-A Lab Control Sample Dup Total/NA Solid 8270D 91885 MB 360-91885/1-A Method Blank Total/NA Solid 8270D 91885 TestAmerica Westfield Page 18 of 45 6/18/2012 Client: Woodard & Curran Inc Project/Site: North Andover GC Semi VOA Matrix Prep Batch: 91884 Client Sample ID Lab Sample ID Client Sample ID 360-41013-1 CB -1 360-41013-2 CB -2 LCS 360-91884/2-A Lab Control Sample LCSD 360-91884/3-A Lab Control Sample Dup MB 360-91884/1 -A Method Blank Prep Batch: 91886 360-41013-1 Lab Sample ID Client Sample ID 360-41013-1 CB -1 360-41013-2 CB -2 LCS 360-91886/2-A Lab Control Sample LCSD 360-91886/3-A Lab Control Sample Dup MB 360-91886/1 -A Method Blank Analysis Batch: 91901 CB -1 Lab Sample ID Client Sample ID 360-41013-1 CB -1 360-41013-2 CB -2 LCS 360-91886/2-A Lab Control Sample LCSD 360-91886/3-A Lab Control Sample Dup MB 360-91886/1-A Method Blank Analysis Batch: 91988 Solid Lab Sample ID Client Sample ID 360-41013-1 CB -1 360-41013-2 CB -2 LCS 360-91884/2-A Lab Control Sample LCSD 360-91884/3-A Lab Control Sample Dup MB 360-91884/1-A Method Blank Metals Prep Batch: 91844 Matrix Lab Sample ID Client Sample ID 360-41013-1 CB -1 360-41013-2 CB -2 LCDSRM 360-91844/3-A LCDSF Lab Control Sample Dup LCSSRM 360-91844/2-A Lab Control Sample MB 360-91844/1-A Method Blank Analysis Batch: 91860 3546 Lab Sample ID Client Sample ID 360-41013-1 CB -1 360-41013-2 CB -2 LCDSRM 360-91844/3-A LCDSF Lab Control Sample Dup LCSSRM 360-91844/2-A Lab Control Sample MB 360-91844/1-A Method Blank Prep Batch: 91916 Prep Batch Lab Sample ID Client Sample ID 360-41013-1 CB -1 360-41013-2 CB -2 QC Association Summary TestAmerica Job ID: 360-41013-1 Prep Type Matrix Method Prep Batch Total/NA Solid 7471A Total/NA Solid 3546 Total/NA Solid 3546 Total/NA Solid 3546 Total/NA Solid 3546 Total/NA Solid 3546 Prep Batch Prep Type Matrix Method Prep Batch Total/NA Solid 3546 91844 Total/NA Solid 3546 I Total/NA Solid 3546 91844 Total/NA Solid 3546 91844 Total/NA Solid 3546 Prep Batch Prep Type Matrix Method Prep Batch Total/NA Solid 8082 91886 Total/NA Solid 8082 91886 Total/NA Solid 8082 91886 Total/NA Solid 8082 91886 Total/NA Solid 8082 91886 Prep Type Matrix Method Prep Batch Total/NA Solid 8015B 91884 Total/NA Solid 8015B 91884 Total/NA Solid 8015B 91884 Total/NA Solid 80156 91884 Total/NA Solid 8015B 91884 Prep Type Matrix Method Prep Batch Total/NA Solid 7471A Total/NA Solid 7471A Total/NA Solid 7471A Total/NA Solid 7471A Total/NA Solid 7471A Prep Type Matrix Method Prep Batch Total/NA Solid 7471A 91844 Total/NA Solid 7471A 91844 Total/NA Solid 7471A 91844 Total/NA Solid 7471A 91844 Total/NA Solid 7471A 91844 Prep Type Matrix Method Prep Batch Total/NA Solid 3050B Total/NA Solid 3050B TestAmerica Westfield Page 19 of 45 6/18/2012 QC Association Summary Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Metals (Continued) Prep Batch: 91916 (Continued) Analysis Batch: 91773 Lab Sample ID' Client Sample ID Prep Type Matrix Method Prep Batch LCDSRM 360-91916/3-A LCDSF Lab Control Sample Dup Total/NA Solid 3050B 6B-1 LCSSRM 360-91916/2-A Lab Control Sample Total/NA Solid 3050B 360-41013-2 MB 360-91916/1 -A Method Blank Total/NA Solid 3050B Analysis Batch: 91991 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 CB -1 Total/NA Solid 6010C 91916 360-41013-2 CB -2 Total/NA Solid 6010C 91916 LCDSRM 360-91916/3-A LCDSF Lab Control Sample Dup Total/NA Solid 6010C 91916 LCSSRM 360-91916/2-A Lab Control Sample Total/NA Solid 6010C 91916 I MB 360-91916/1 -A Method Blank Total/NA Solid 6010C 91916 General Chemistry Analysis Batch: 91773 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 6B-1 Total/NA Solid Moisture 360-41013-2 CB -2 Total/NA Solid Moisture Leach Batch: 91819 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 CB -1 Soluble Solid DI Leach 360-41013-2 CB -2 Soluble Solid DI Leach LCS 360-91819/2-A Lab Control Sample Soluble Solid DI Leach MB 360-91819/1-A Method Blank Soluble Solid DI Leach Analysis Batch: 91855 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 360-41013-1 CB -1 Soluble Solid SM 2510B 360-41013-2 CB -2, Soluble Solid SM 2510B LCS 360-91819/2-A Lab Control Sample Soluble Solid SM 2510B MB 36 0-91 81 9/1-A Method Blank Soluble Solid SM 2510B TestAmerica Westfield Page 20 of 45 6/18/2012 Surrogate Summary Client: Woodard & Curran Inc Project/Site: North Andover Method: 8260C - Volatile Organic Compounds (GC/MS) Matrix: Solid Lab Sample ID Client Sample ID BFB (70-130) 360-41013-1 CB -1 104 360-41013-1 - RA CB -1 103 360-41013-2 CB -2 102 360-41013-2 - RA CB -2 103 LCS 360-91800/2-A Lab Control Sample 103 LCS 360-91911/2-A Lab Control Sample 98 LCSD 360-91800/3-A Lab Control Sample Dup 99 LCSD 360-91911/3-A Lab Control Sample Dup 100 MB 360-91800/4-A Method Blank 102 MB 360-91911/4-A Method Blank 101 Surrogate Legend 69 Method Blank BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane TOL = Toluene -d8 (Surr) TestAmerica Job ID: 360-41013-1 Total/NA . i Method: 8270D - Semivolatile Organic Compounds (GC/MS) Matrix: Solid Prep Type: Total/NA Lab Sample ID 360-41013-1 360-41013-2 LCS 360-91885/2-A LCSD 360-91885/3-A MB 360-91885/1-A Surrogate Legend TBP = 2,4,6-Tribromopl- 2FP = 2-Fluorophenol NBZ = Nitrobenzene -d5 PHL = Phenol -d5 TPH = Terphenyl-d14 FBP = 2-Fluorobiphenyl Percent Surrogate Recovery (Acceptance Limits) Client Sample ID Percent Surrogate Recovery (Acceptance Limits) DBFM TOL (70-130) (70-130) 99 97 98 96 97 98 100 98 99 100 101 100 101 100 98 97 98 98 100 97 Total/NA . i Method: 8270D - Semivolatile Organic Compounds (GC/MS) Matrix: Solid Prep Type: Total/NA Lab Sample ID 360-41013-1 360-41013-2 LCS 360-91885/2-A LCSD 360-91885/3-A MB 360-91885/1-A Surrogate Legend TBP = 2,4,6-Tribromopl- 2FP = 2-Fluorophenol NBZ = Nitrobenzene -d5 PHL = Phenol -d5 TPH = Terphenyl-d14 FBP = 2-Fluorobiphenyl Percent Surrogate Recovery (Acceptance Limits) Client Sample ID TBP (30-130) 2FP (30-130) NBZ (30-130) PHIL (30-130) TPH (30-130) FBP (30-130) CB -1 43 69 64 66 73 56 CB -2 47 64 68 69 81 60 Lab Control Sample 67 72 73 76 91 72 Lab Control Sample Dup 64 76 74 72 89 69 Method Blank 63 82 77 82 97 70 Method: 80158 - Diesel Range Organics (DRO) (GC) Matrix: Solid OTPH1 Lab Sample ID Client Sample ID (40-140) 360-41013-1 CB -1 79 360-41013-2 CB -2 0 X D LCS 360-91884/2-A Lab Control Sample 75 LCSD 360-91884/3-A Lab Control Sample Dup 74 MB 360-91884/1-A Method Blank 84 Surrogate Legend L OTPH = o-Terphenyl Prep Tvoe: Total/NA Percent Surrogate Recovery (Acceptance Limits) TestAmerica Westfield Page 21 of 45 6/18/2012 Surrogate Summary Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Method: 8082 - Polychlorinated Biphenyls (GC/ECD) Matrix: Solid Prep Type: Total/NA TCX = Tetrachloro-m-xylene DCB = DCB Decachlorobiphenyl TestAmerica Westfield Page 22 of 45 6/18/2012 Percent Surrogate Recovery (Acceptance Limits) TCX1 TCX2 DCB1 DCB2 Lab Sample ID Client Sample ID (30-150) (30-150) (30-150) (30-150) 360-41013-1 CB -1 93 103 88 113 360-41013-2 CB -2 92 98 87 107 LCS 360-91886/2-A Lab Control Sample 91 102 92 106 LCSD 360-91886/3-A Lab Control Sample Dup 88 99 88 101 MB 360-91886/1-A Method Blank 96 110 97 111 Surrogate Legend TCX = Tetrachloro-m-xylene DCB = DCB Decachlorobiphenyl TestAmerica Westfield Page 22 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover Method: 8260C - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 360-91800/4-A Matrix: Solid Analysis Batch: 91862 Analyte 1,1,1,2 -Tetrachloroethane 1,1,1 -Trichloroethane 1,1,2,2 -Tetrachloroethane 1,1,2 -Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1, 2, 3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2 -Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3 -Dichlorobenzene 1,3-Dichloropropane 1,4 -Dichlorobenzene 1,4 -Dioxane 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl;2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis -1, 3-Dichloropropene Dibromomethane Dich lorobromomethane Dichlorodifluoromethane Ethyl ether Ethylbenzene Ethylene Dibromide Hexachlorobutadiene TestAmerica Job ID: 360-41013-1 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 91800 MB MB Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 130 60 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 90 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 90 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 80 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 70 u9/K9 06/12/12 16:11 06/13/12 02:37 1 ND 130 55 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 56 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 60 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 1300 70 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 100 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 75 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 65 u9/K9 06/12/12 16:11 06/13/12 02:37 1 ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 57 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 13000 5400 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 100 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 1300 570 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 60 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 1300 690 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 55 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 75 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 1300 490 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 13000 5000 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 85 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 75 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 79 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 250 120 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 95 ug/Kg 06/12/12 16:11 06/1 3/1202:37 1 ND 136 85 ug/Kg 66/12/12 16:11 06/13/12 02:37 1 ND 130 55 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 69 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 59 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 250 80 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 75 ug/Kg 06/12/12 16:11 06/13%12 02:37 1 ND 250 70 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 60 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 62 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 65 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 250 110 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 52 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 80 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 56 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 ND 130 70 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 TestAmerica Westfield Page 23 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 360-91800/4-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 91862 Prep Batch: 91800 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Isopropyl ether ND 130 56 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Isopropylbenzene ND 130 80 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 m -Xylene & p -Xylene ND 250 150 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Methyl tert-butyl ether ND 130 75 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Methylene Chloride 311 J 500 100 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 n-Butylbenzene ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 N-Propylbenzene ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Naphthalene ND 1300 120 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 o*lene ND 130 65 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 sec-Butylbenzene ND 130 70 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Styrene ND 130 50 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Tert-amyl methyl ether ND 130 75 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Tert-butyl ethyl ether ND 130 73 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 tert- Butyl benzene ND 130 65 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Tetrachloroethene ND 130 80 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Tetrahydrofuran ND 2500 1400 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Toluene ND 130 85 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 trans-1,2-Dichloroethene ND 130 71 ug/Kg 06/12/1216:11 06/13/1202:37 1 trans-1,3-Dichloropropene ND 130 100 ug/Kg 06/12/1216:11 06/13/1202:37 1 Trichloroethene ND 130 100 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 Trichlorofluoromethane ND 250 77 ug/Kg 06/12/1216 1 :11 06/13/120 1 2 :37 1 Vinyl chloride ND 130 80 ug/Kg 06/12/12 16:11 06/13/12 02:37 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene 102 70-130 06/12/12 16:11 06/13/12 02:37 1 Dibromofluoromethane 98 70-130 06/12/12 16:11 06/13/12 02:37 1 Toluene -d8 (Surr) 98 70-130 06/12112 16:11 06/13/12 02:37 1 Lab Sample ID: LCS 360-91800/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 91862 Prep Batch: 91800 Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,1,2 -Tetrachloroethane 5000 4840 ug/Kg 97 70-130 1,1,1 -Trichloroethane 5000 4990 ug/Kg 100 70-130 1,1,2,2 -Tetrachloroethane 5000 4620 ug/Kg 92 70-130 1,1,2 -Trichloroethane 5000 4510 ug/Kg 90 70-130 1,1-Dichloroethane 5000 5090 ug/Kg 102 70-1310 1,1-Dichloroethene 5000 5010 ug/Kg 100 70-130 1,1-Dichloropropene 5000 4880 ug/Kg 98 70-130 1,2,3-Trichlorobenzene 5000 5440 ug/Kg 109 70-130 1,2,3-Trichloropropane 5000 4610 ug/Kg 92 70-130 1 X2,4-Trichlorobenzene 5000 4840 ug/Kg 97 70-13 0 1,2,4-Trimethylbenzene 5000 5050 ug/Kg 101 70-130 1,2-Dibromo-3-Chloropropane 5000 4700 ug/Kg 94 70-130 1,2 -Dichlorobenzene 5000 4610 ug/Kg 92 70-130 1,2-Dichloroethane 5000 4640 ug/Kg 93 70-130 1,2-Dichloropropane 5000 4700 ug/Kg 94 70-130 1,3,5-Trimethylbenzene 5000 5170 ug/Kg 103 70-130 TestAmerica Westfield Page 24 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 360-91800/2-A Matrix: Solid Analysis Batch: 91862 Analyte 1,3 -Dichlorobenzene 1,3-Dichloropropane 1,4-6chlorobenzene 1,4 -Dioxane 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis- 1,2-Dichloroethene cis-1,3-Dichloropropene Dibromomethane Dichlorobromomethane Dichlorodifluoromethane Ethyl ether Ethylbenzene Ethylene Dibromide . Hexachlorobutadiene Isopropyl ether Isopropylbenzene m -Xylene & p -Xylene Methyl tert-butyl ether . Methylene Chloride n-Butyibenzene N-Propylbenzene Naphthalene o -Xylene sec -Butyl benzene Styrene Tert-amyl methyl ether Tert-butyl ethyl ether tert-Butylbenzene Tetrachloroethene Tetrahydrofuran Toluene Spike Added LCS LCS Result Qualifier Unit 5000 4960 ug/Kg 5000 4580 ug/Kg 5000 4780 ug/Kg 50000 48600 ug/Kg 5000 4620 ug/Kg 50000 30500 * ug/Kg 5000 4940 ug/Kg 50000 31800 * ug/Kg 5000 5070 ug/Kg 5000 5300 ug/Kg 50000 42700 ug/Kg 50000 20500 ug/Kg 5000 4880 ug/Kg 5000 4780 ug/Kg 5000 4750 ug/Kg 5000 5980 ug/Kg 5000 6140 ug/Kg 5000 5030 ug/Kg 5000 4950 ug/Kg 5000 4740 ug/Kg 5000 4650 ug/Kg 5000 6090 ug/Kg 5000 4730 ug/Kg 5000 4830 ug/Kg 5000 4980 ug/Kg 5000 4580 ug/Kg 5000 4580 u91K9 5000 4730 ug/Kg 5000 4510 ug/Kg 5000 5230 ug/Kg 5000 5050 ug/Kg 5000 4630 ug/Kg 5000 5340 ug/Kg 5000 4890 ug/Kg 5000 5210 ug/Kg 10000 10300 ug/Kg 5000 4850 ug/Kg 5000 5420 ug/Kg 5000 4930 ug/Kg 5000 5220 ug/Kg 5000 4650 ug/Kg 5000 5090 ug/Kg 5000 5120 ug/Kg 5000 5010 ug/Kg 5000 4760 ug/Kg 5000 4960 ug/Kg 5000 5010 ug/Kg 5000 4770 ug/Kg 50000 44500 ug/Kg 5000 4920 ug/Kg TestAmerica Job ID: 360-41013-1 Client Sample ID: Lab Control Sample TestAmerica Westfield Page 25 of 45 6/18/2012 T Prep Type: Total/NA Prep Batch: 91800 %Rec. D %Rec Limits 99 70-130 92 70-130 96 70-130 97 70-130 92 70-130 61 70-130 99 70-130 64 70-130 101 70-130 106 70-130 85 70-130 41 70-130 98 70-130 96 70-130 95 70-130 120 70-130 123 70-130 101 70-130 99 70-130 95 70-130 93 70-130 122 70-130 95 70-130 97 70-130 100 70-130 92 70-130 92 70 - 130 95 70-130 90 70-130 105 70-130 101 70-130 93 70-130 107 70-130 98 70-130 104 70-130 103 70-130 97 70-130 108 70-130 99 M - 130 104 70-130 93 70-130 102 70-130 102 70-130 100 70-130 95 70-130 99 70-130 100 70-130 95 M - 130 89 70-130 98 70-130 TestAmerica Westfield Page 25 of 45 6/18/2012 T QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) Prep Type: Total/NA Lab Sample ID: LCS 360-91800/2-A Prep Batch: Client Sample ID: Lab Control Sample Matrix: Solid %Rec. RPD Prep Type: Total/NA Analysis Batch: 91862 Limits RPD Limit ug/Kg Prep Batch: 91800 70-130 Spike LCS LCS ug/Kg 96 %Rec. Analyte Added Result Qualifier Unit D %Rec Limits trans-1,2-Dichloroethene 5000 4970 uglKg 99 70-130 trans-1,3-Dichloropropene 5000 4790 ug/Kg 96 70-130 Trichloroethene 5000 5020 ug/Kg 100 70-130 Trichlorofluoromethane 5000 5480 ug/Kg 110 70-130 Vinyl chloride 5000 4840 ug/Kg 97 70-130 Surrogate 4-Bromofluorobenzene Dibromofluoromethane Toluene -d8 (Surr) LCS LCS %Recovery Qualifier Lab Sample ID: LCSD 360-91800/3-A Matrix: Solid Analysis Batch: 91862 Analyte 1,1,1,2 -Tetrachloroethane 1,1,1 -Trichloroethane 1,1,2,2 -Tetrachloroethane 1,1,2 -Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-D1chloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichloro6enzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2 -Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethy1benzene 1,3 -Dichlorobenzene 1,3-Dichloropropane 1,4 -Dichlorobenzene 1,4 -Dioxane 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexahone 4-Chlorotoluene 4-Isopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide 103 99 100 Limits 70-130 70-130 Spike Added 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 50000 5000 50000 5000 50000 5000 5000 50000 50000 5000 5000 5000 5000 5000 LCSD LCSD Result Qualifier 4600 4800 4400 4380 4890 4720 4690 5000 4390 4520 4710 4630 4330 4670 4590 4820 4760 4580 4620 44900 4330 31300 4660 31200 4740 4850 42400 21400 4700 4460 4630 5660 5880 Page 26 of 45 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 91800 %Rec. RPD Unit D %Rec Limits RPD Limit ug/Kg 92 70-130 5 20 ug/Kg 96 70-130 4 20 ug/Kg 88 70-130 5 20 ug/Kg 88 70-130 3 20 ug/Kg 98 70-130 4 20 ug/Kg 94 70-130 6 20 ug/Kg 94 70 - 130 4 20 ug/Kg 100 70-130 8 20 ug/Kg 88 70-130 5 20 ug/Kg 90 70 - 130 7 20 ug/Kg 94 70-130 7 20 ug/Kg 93 70-130 1 20 ug/Kg 87 70-130 6 20 ug/Kg 93 70-130 1 20 ug/Kg 92 70-130 2 20 ug/Kg 96 70-130 7 20 ug/Kg 95 70-130 4 20 ug/Kg 92 70-130 0 20 ug/Kg 92 70-130 4 20 ug/Kg 90 70-130 8 20 ug/Kg 87 70'--130 7 20 ug/Kg 63 70-130 3 20 ug/Kg 93 70-130 6 20 ug/Kg 62 70-130 2 20 ug/Kg 95 70-130 7 20 ug/Kg 97 70-130 9 20 ug/Kg 85 70-130 1 20 ug/Kg 43 70-130 4 20 ug/Kg 94 70-130 4 20 ug/Kg 89 70-130 7 20 U09 93 70-130 2 20 ug/Kg 113 70-130 6 20 ug/Kg 118 70-130 4 20 TestAmerica Westfield 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 360-91800/3-A Matrix: Solid Analysis Batch: 91862 Analyte Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis- 1,3-D ichloropropene Dibromomethane Dich lorobromomethane Dichlorodifluoromethane Ethyl ether Ethylbenzene Ethylene Dibromide Hexachlorobutadiene Isopropyl ether Isopropyl benzene m -Xylene & p -Xylene Methyl tert-butyl ether Methylene Chloride n-Butylbenzene N-Propylbenzene Naphthalene o -Xylene sec -Butyl benzene Styrene Tert-amyl methyl ether Tert-butyl ethyl ether tert-Butyl benzene Tetrachloroethene Tetrahydrofuran Toluene trans-l,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride Surrogate 4-Bromofluorobenzene Dibromofluoromethane Toluene -d8 (Surr) LCSD LCSD %Recovery Qualifier 99 101 100 Spike Added 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 10000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 50000 5000 5000 5000 5000 5000 5000 Limits 70-135 70-130 70-130 LCSD LCSD Result Qualifier 4780 4600 4660 4520 6130 4630 4850 4830 4470 4480 4630 4580 5270 4670 4610 4780 4850 4850 9510 4870 5460 4570 4780 4480 4930 4670 4760 4800 4860 4890 4540 45500 4680 4780 4590 4850 5420 4680 Page 27 of 45 TestAmerica Job ID: 360-41013-1 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 91800 TestAmerica Westfield 6/18/2012 %Rec. RPD Unit D %Rec Limits RPD Limit ug/Kg 96 70.130 5 20 ug/Kg 92 70.130 7 20 ug/Kg 93 70.130 2 20 ug/Kg 90 70.130 3 20 ug/Kg 123 70-130 1 20 ug/Kg 93 70-130 2 20 ug/Kg 97 70.130 1 20 i ug/Kg 97 70_130 3 20 ug/Kg 89 70-130 2 20 U09 90 n - n*0 2 20 ug/Kg 93 70.130 2 20 8 ug/Kg 92 70.130 2 20 ug/Kg 105 70.130 1 20 ug/Kg 93 70.130 8 20 ug/Kg 92 70.130 0 20 ug/Kg 96 70.130 11 20 ug/Kg 97 70.130 1 20 ug/Kg 97 70-130 7 20 ug/Kg 95 70_130 8 20 ug/Kg 97 70.130 0 20 ug/Kg 109 70.130 1 20 ug/Kg 91 70-130 7 20 ug/Kg 96 70.130 9 20 ug/Kg 90 70_130 4 20 ug/Kg 99 70-130 3 20 ug/Kg 93 70-130 9 20 ug/Kg 95 70.130 5 20 ug/Kg 96 70-130 1 20 ug/Kg 97 70.130 2 20 ug/Kg 98 70.130 3 20 ug/Kg 91 70.130 5 20 ug/Kg 91 70.130 2 20 ug/Kg 94 70.130 5 20 u9/Kg 96 70.130 4 20 ug/Kg 92 70.130 4 20 ug/Kg 97 70.130 3 20 ug/Kg 108 70.130 1 20 ug/Kg 94 70.130 3 20 TestAmerica Westfield 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8260C -Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 360-91911/4-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 91954 Prep Batch: 91911 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2 -Tetrachloroethane ND 130 60 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,1,1 -Trichloroethane ND 130 90 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,1,2,2 -Tetrachloroethane ND 130 50 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,1,2 -Trichloroethane ND 130 50 ug/Kg 06/14/121520 06/15/1202:16 1 1,1-Dichloroethane ND 130 90 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,1-Dichloroethene ND 130 80 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,1-Dichloropropene ND 130 70 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,2,3-Trichlorobenzene ND 130 55 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,2,3-Trichloropropane ND 130 56 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,2,4-Trichlorobenzene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,2,4-Trimethylbenzene ND 130 60 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,2-Dibromo-3-Chloropropane ND 1300 70 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,2 -Dichlorobenzene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,2-Dichloroethane ND 130 100 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,2-Dichloropropane ND 130 75 ug/Kg 06/14/1215:20 06/15/1202:16 1 1,3,5-Trimethylbenzene ND 130 65 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,3 -Dichlorobenzene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,3-Dichloropropane ND 130 57 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,4 -Dichlorobenzene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 1,4 -Dioxane ND 13000 5400 ug/Kg 06/14/1215:20 06/15/1202:16 1 2,2-Dichloropropane ND 130 100 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 2-Butanone (MEK) ND 1300 570 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 2-Chlorotoluene ND 130 60 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 2-Hexanone ND 1300 690 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 4-Chlorotoluene ND 130 55 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 4-Isopropyltoluene ND 130 75 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 4-Methyl-2-pentanone (MIBK) ND 1300 490 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Acetone ND 13000 5000 u9/Kg 06/14/12 15:20 06/15/12 02:16 1 Benzene ND 130 85 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Bromobenzene ND 130 75 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Bromoform ND 130 79 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Bromomethane ND 250 120 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Carbon disulfide ND 130 95 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Carbon tetrachloride ND 130 85 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Chlorobenzene ND 130 55 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Chlorobromomethane ND 130 69 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Chlorodibromomethane ND 130 59 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Chloroethane ND 250 80 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Chloroform ND 130 75 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Chloromethane ND 250 70 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 cis-1,2-Dichloroethene ND 130 60 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 cis-1,3-Dichloropropene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Dibromomethane ND 130 62 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Dichlorobromomethane ND 130 65 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Dichlorodifluoromethane ND 250 110 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Ethyl ether ND 130 52 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Ethylbenzene ND 130 80 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Ethylene Dibromide ND 130 56 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Hexachlorobutadiene ND 130 70 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 TestAmerica Westfield Page 28 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 360-91911/4-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 91954 Prep Batch: 91911 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Isopropyl ether ND 130 56 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Isopropylbenzene ND 130 80 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 m -Xylene & p -Xylene ND 250 150 ug/Kg _ 06/14/12 15:20 06/15/12 02:16 1 Methyl tert-butyl ether ND 130 75 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Methylene Chloride 559 500 100 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 n-Butylbenzene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 N-Propylbenzene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Naphthalene ND 1300 120 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 - o -Xylene ND 130 65 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 sec-Butylbenzene ND 130 70 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Styrene ND 130 50 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Tert-amyl methyl ether ND 130 75 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Tert-butyl ethyl ether ND 130 73 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 tert-Butylbenzene ND 130 65 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Tetrachloroethene ND 130 80 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Tetrahydrofuran ND 2500 1400 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Toluene ND 130 85 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 trans-1,2-Dichloroethene ND 130 71 ug/Kg 06/14/1215:20 ... 06/15/1202:16 1 trans-1,3-Dichloropropene ND 130 100 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Trichloroethene ND 130 100 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Trichlorofluoromethane ND 250 77 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 Vinyl chloride ND 130 80 ug/Kg 06/14/12 15:20 06/15/12 02:16 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene 101 70-130 06/14112 15:20 06/15/12 02:16 1 Dibromofluoromethane 100 70-130 06/14/12 15:20 06/15/12 02:16 1 Toluene -d8 (Surr) 97 70-130 .06/14/12 15:20 06/15/12 02:16 1 Lab Sample ID: LCS 360-91911/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 91954 Prep Batch: 91911 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,1,2 -Tetrachloroethane 5000 4620 ug/Kg 92 70-130 1,1,1 -Trichloroethane 5000 4850 ug/Kg 97 70-130 1,1,2,2 -Tetrachloroethane 5000 4680 ug/Kg 94 70-130 1,1,2 -Trichloroethane 5000 4530 ug/Kg 91 70 - 130 1,1-Dichloroethane 5000 5040 ug/Kg 101 70-130 1,1-Dichloroethene 5000 4710 ug/Kg 94 70-130 1,1-Dichloropropene 5000 4700 ug/Kg 94 70-130 1,2,3-Trichlorobenzene 5000 5220 ug/Kg 104 70-130 1,2,3-Trichloropropane 5000 4330 ug/Kg 87 70-130 1,2,4-Trichlorobenzene 5000 4710 ug/Kg 94 70-130 1,2,4-Trimethylbenzene 5000 4690 ug/Kg 94 70-130 1,2-Dibromo-3-Chloropropane 5000 4680 ug/Kg 94 70-130 1,2 -Dichlorobenzene 5000 4440 ug/Kg 89 70-130 1,2-Dichloroethane 5000 4810 ug/Kg 96 70-130 1,2-Dichloropropane 5000 4700 ug/Kg 94 70-130 1,3,54rimethylbenzene 5000 4790 ug/Kg 96 70-13 . 0 TestAmerica Westfield Page 29 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 360-91911/2-A Matrix: Solid Analysis Batch: 91964 Analyte 1,3 -Dichlorobenzene 1,3-Dichloropropane 1,4-6chlorobenzene 1,4 -Dioxane 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-1sopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromoform Bromomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorobromomethane Chlorodibromomethane Chloroethane Chloroform Chloromethane cis -1, 2-D ichloroethene cis- 1,3-Dichloropropene Dibromomethane Dichlorobromometha ne Dich lorod ifl uoro methane Ethyl ether Ethylbenzene Ethylene Dibromide Hexachlorobutadiene Isopropyl ether Isopropylbenzene m -Xylene & p -Xylene Methyl tert-butyl ether Methylene Chloride n-Butylbenzene N-Propylbenzene Naphthalene o -Xylene sec-Butylbenzene Styrene Tert-amyl methyl ether Tert-butyl ethyl ether tert-Butylbenzene Tetrachloroethene Tetrahydrofuran Toluene Spike Added 5000 5000 5000 50000 5000 50000 5000 50000 5000 5000 50000 50000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 10000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 5000 50000 5000 LCS LCS Result Qualifier 4860 4690 4680 48300 4440 31400 4550 31900 4650 4960 43000 20700 4810 4490 4660 5400 5910 4770 4730 4790 4650 5740 4780 4700 4970 4660 4520 4740 4160 5310 4730 4680 5000 4900 4730 9620 4870 5500 4550 4820 4490 4760 4680 4800 4830 4950 4740 4510 46100 4840 Page 30 of 45 TestAmerica Job ID: 360-41013-1 TestAmerica Westfield 6/18/2012 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 91911 %Rec. Unit D %Rec Limits ug/Kg 97 70.130 ug/Kg 94 70-130 ug/Kg 94 70.130 ug/Kg 97 70-1130 ug/Kg 89 70-130 ug/Kg 63 70.130 ug/Kg 91 70.130 ug/Kg 64 70.130 U g/Kg 93 70.130 ug/Kg 99 70.130 ug/Kg 86 70.130 ug/Kg 41 70.130 ug/Kg 96 70-130 ug/Kg 90 70.130 ug/Kg 93 70.130 ug/Kg 108 70.130 ug/Kg 118 70.130 ug/Kg 95 70.130 ug/Kg 95 70.130 ug/Kg 96 70.130 ug/Kg 93 70.130 ug/Kg 115 70.130 ug/Kg 96 70-130 ug/Kg 94 70.130 ug/Kg 99 70.130 ug/Kg 93 70-130 U09 90 70.130 ug/Kg 95 70.130 ug/Kg 83 70.130 ug/Kg 106 70.130 ug/Kg 95 70.130 ug/Kg 94 70.130 ug/Kg 100 70.130 ug/Kg 98 70.130 ug/Kg 95 70.130 ug/Kg 96 70.130 ug/Kg 97 70.130 ug/Kg 110 70.130 U09 91 70.130 ug/Kg 96 70.130 ug/Kg 90 70.130 ugX9 95 70.130 ug/Kg 94 70.130 ug/Kg 96 70.130 ug/Kg 97 70.130 ug/Kg 99 70.130 ug/Kg 95 70.130 ug/Kg 90 70.130 ug/Kg 92 70.130 ug/Kg 97 70.130 TestAmerica Westfield 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) LCS LCS Lab Sample ID: LCS 360-91911/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 91954 98 70-130 Prep Batch: 91911 Spike LCS LCS 101 70-130 %Rec. Analyte Added Result Qualifier Unit D %Rec Limits trans-1,2-Dichloroethene 5000 4840 ug/Kg 97 70.130 trans-1,3-Dichloropropene 5000 4750 ug/Kg 95 70.130 Trichloroethene 5000 4670 ug/Kg 93 70.130 Triic loroAu roe6ane 5000 5030 ug/Kg 101 70-1-30 Vinyl chloride 5000 4450 ug/Kg 89 70-130 LCS LCS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene 98 70-130 Dibromofluoromethane 101 70-130 Toluene -d8 (Surr) 100 70-130 Lab Sample ID: LCSD 360-91911/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 91954 Prep Batch: 91911 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 1,1,1,2 -Tetrachloroethane 5000 4880 ug/Kg 98 70.130 5 20 1,1,1 -Trichloroethane 5000 5210 ug/Kg 104 70.130 7 20 1,1,2,2 -Tetrachloroethane 5000 4670 ug/Kg 93 70-130 0 20 1,1,2 -Trichloroethane 5000 4410 ug/Kg 88 70.130 3 20 1,1-Dichloroethane 5000 5260 ug/Kg 105 70.130 4 20 1,1-Dichloroethene 5000 5040 ug/Kg 101 70-130 7 20 1,1-Dichloropropene 5000 4990 ug/Kg 100 70-130 6 20 1,2,3-Trichlorobenzene 5000 5220 ug/Kg 104 70.130 0 20 1,2,3-Trichloropropane 5000 4490 ug/Kg 90 70.130 3 20 1,2,4-Trichlorobenzene 5000 4710 ug/Kg 94 70.130 0 20 1,2,4-Trimethylbenzene 5000 5250 ug/Kg 105 70.130 11 20 1,2-Dibromo-3-Chloropropane 5000 4680 ug/Kg 94 70.130 0 20 1,2 -Dichlorobenzene 5000 4560 ug/Kg 91 70.130 3 20 1,2-Dichloroethane 5000 4650 ug/Kg 93 70.130 3 20 1,2-Dichloropropane 5000 4810 ug/Kg 96 70.130 2 20 1,3,5-Trimethylbenzene 5000 5220 ug/Kg 104 70-130 9 20 1,3 -Dichlorobenzene 5000 4960 ug/Kg 99 70.130 2 20 1,3-Dichloropropane 5000 4560 ug/Kg 91 70.130 3 20 1,4 -Dichlorobenzene 5000 4830 ug/Kg 97 70.130 3 20 1,4 -Dioxane 50000 49300 ug/Kg 99 70.130 2 20 2,2-Dichloropropane 5000 4820 ug/Kg 96 70.130 8 20 2-Butanone (MEK) 50000 33300 ug/Kg 67 70-130 6 20 2-Chlorotoluene 5000 5010 ug/Kg 100 70.130 10 20 2-Hexanone 50000 33600 * ug/Kg 67 70.130 5 20 4-6hlorotoluene 5000 5100 ug/Kg 102 70.130 9 20 4-Isopropyltoluene 5000 5450 ug/Kg 109 70-130 9 20 4-Methyl-2-pentanone (MIBK) 50000 44700 ug/Kg 89 70-130 4 20 Acetone 50000 22500 ug/Kg 45 70.130 8 20 Benzene 5000 4970 ug/Kg 99 70.130 3 20 Bromobenzene 5000 4740 ug/Kg 95 70-130 5 20 Bromoform 5000 4550 ug/Kg 91 70.130 2 20 Bromomethane 5000 5370 ug/Kg 107 70.130 0 20 Carbon disulfide 5000 6370 ug/Kg 127 70-130 8 20 TestAmerica Westfield Page 31 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 360-91911/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 91954 Prep Batch: 91911 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Carbon tetrachloride 5000 5290 ug/Kg 106 70-130 10 20 Chlorobenzene 5000 4940 ug/Kg 99 70-130 4 20 Chlorobromomethane 5000 4750 ug/Kg 95 70-130 1 20 Chlorodibromomethane 5000 4590 uglKg 92 70-130 1 20 Chloroethane 5000 6250 ug/Kg 125 70-130 9 20 Chloroform 5000 4860 ug/Kg 97 70-130 2 20 Chloromethane 5000 5010 ug/Kg 100 70-130 6 20 cis-1,2-Dichloroethene 5000 5150 ug/Kg 103 70-130 4 20 cis- 1,3-Dichloropropene 5000 4510 ug/Kg 90 70-130 3 20 Dibromomethane 5000 4490 ug/Kg 90 70-130 1 20 Dichlorobromomethane 5000 4670 ug/Kg 93 70-130 2 20 Dichlorodifluoromethane 5000 4430 ug/Kg 89 70-130 6 20 Ethyl ether 5000 5140 ug/Kg 103 70-130 3 20 Ethylbenzene 5000 5120 ug/Kg 102 70-130 8 20 Ethylene Dibromide 5000 4680 ug/Kg 94 70-130 0 20 Hexachlorobutadiene 5000 5580 ug/Kg 112 70-130 11 20 Isopropyl ether 5000 5040 ug/Kg 101 70-130 3 20 Isopropylbenzene 5000 5220 ug/Kg 104 70-130 10 20 m -Xylene & p -Xylene 10000 10500 ug/Kg 105 70-130 9 20 Methyl tert-butyl ether 5000 4960 ug/Kg 99 70-130 2 20 Methylene Chloride 5000 5610 ug/Kg 112 70-130 2 20 n-Butylbenzene 5000 4970 ug/Kg 99 70-130 9 20 N-Propylbenzene 5000 5220 ug/Kg 104 70-130 8 20 Naphthalene 5000 4400 ug/Kg 88 70-130 2 20 o -Xylene 5000 5160 ug/Kg 103 70 - 130 8 20 sec-Butylbenzene 5000 5170 ug/Kg 103 70-130 10 20 Styrene 5000 4850 ug/Kg 97 70-130 1 20 Tert-amyl methyl ether 5000 4990 ug/Kg 100 70-130 3 20 Tert-butyl ethyl ether 5000 5100 ug/Kg 102 70-130 3 20 tert-Butyl benzene 5000 5320 ug/Kg 106 70-130 12 20 Tetrachloroethene 5000 4820 ug/Kg 96 70-130 7 20 Tetrahydrofuran 50000 44700 ug/Kg 89 70- 130 3 20 Toluene 5000 4950 ug/Kg 99 70-130 2 20 trans-1,2-Dichloroethene 5000 5120 ug/Kg 102 70-130 6 20 trans-1,3-Dichloropropene 5000 4670 ug/Kg 93 70-130 2 20 Trichloroethene 5000 4870 ug/Kg 97 70-130 4 20 Trichlorofluoromethane 5000 5300 ug/Kg 106 70-130 5 20 Vinyl chloride 5000 4760 ug/Kg 95 70-130 7 20 LCSD LCSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene 100 70-130 Dibromofluoromethane 98 70-130 Toluene -d8 (Surr) 97 70-130 TestAmerica Westfield Page 32 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8270D - Semivolatile Organic Compounds (GC/MS) Lab Sample ID: MB 360-91885/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 91895 Prep Batch: 91885 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac 1,2,4-Trichlorobenzene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 1,2 -Dichlorobenzene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 1,3 -Dichlorobenzene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 1,4 -Dichlorobenzene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2,2'-oxybis[l-chloropropane] ND 330 50 ug/Kg 06/13/1218:29 06/14/1209:53 1 2,4,5 -Trichlorophenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2,4,6 -Trichlorophenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2,4-Dichlorophenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2,4 -Dimethylphenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2,4-Dinitrophenol ND 330 55 ug/Kg 06/13/12 1829 06/14112 09:53 1 2,4-Dinitrotoluene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2,6-Dinitrotoluene ND. 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2-6hloronaphthalene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2 -Chlorophenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2 -Methylnaphthalene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2-Methylphenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 2-Nitrophenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 3 & 4 Methylphenol ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 3,3'-Dichlorobenzidine ND 670 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 4-Bromophenyl phenyl ether ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 4-Chloroaniline ND 670 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 4-Nitrophenol ND 1700 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Acenaphthene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Acenaphthylene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Acetophenone ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Aniline ND 1700 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Anthracene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Azobenzene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Benzo[a]anthracene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Benzo[a]pyrene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Benzo[b]fluoranthene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Benzo[g,h,i]perylene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Benzo[k]fluoranthene ND 180 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Bis(2-chloroethoxy)methane ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Bis(2-chloroethyl)ether ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Bis(2-ethylhexyl) phthalate ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Butyl benzyl phthalate ND 330 50 ug/Kg 06/13/1218 . :29 06/14/12 09:53 1 Chrysene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Di -n -butyl phthalate 213 J 330 52 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Di-n-octyl phthalate ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Dibenz(a,h)anthracene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Dibenzofuran ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Diethyl phthalate ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Dimethyl phthalate ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Fluoranthene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Fluorene ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Hexachlorobenzene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Hexachlorobutadiene ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 Hexachloroethane ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 TestAmerica Westfield Page 33 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 360-91885/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 91895 Prep Batch: 91885 Analyte Indeno[1,2,3-cd]pyrene Isophorone Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene Surrogate 2, 4, 6-Tribromophen of 2-Fluorophenol Nitrobenzene -d5 Phenol -d5 Terphenyl-d14 2-Fluorobiphenyl Lab Sample ID: LCS 360-91885/2-A Matrix: Solid Analysis Batch: 91895 Analyte 1,2,4-Trichlorobenzene 1,2 -Dichlorobenzene 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene 2, 2'-oxybis[1-chloropropane] 2,4,5 -Trichlorophenol 2,4, 6 -Trichlorophenol 2,4-Dichlorophenol 2,4 -Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2 -Chlorophenol 2 -Methylnaphthalene 2-Methylphenol 2-Nitrophenol 3 & 4 Methylphenol 3, 3'-Dich lorobenzid ine 4-13romophenyl phenyl ether 4-Chloroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Acetophenone Aniline Anthracene MB MB ~ Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 ND 1700 88 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 ND 330 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 ND 170 50 ug/Kg 06/13/12 18:29 06/14/12 09:53 1 MB MB %Recovery Qualifier Limits Prepared Analyzed Dil Fac 63 30-130 06/13/12 18:29 06/14/12 09:53 1 82 30-130 06/13/12 18:29 06/14/12 09:53 1 77 30-130 06/13/12 18:29 06/14/12 09:53 1 82 30-130 06/13/12 18:29 06/14/12 09:53 1 97 30-130 06/13/12 18:29 06/14/12 09:53 1 70 30-130 06/13/12 18:29 06/14/12 09:53 1, Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 91885 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 1330 916 ug/Kg 69 40-140 1330 929 ug/Kg 70 40-140 1330 903 ug/Kg 68 40-140 1330 944 ug/Kg 71 40-140 1330 913 ug/Kg 68 40-140 1330 1240 ug/Kg 93 30-130 1330 1180 ug/Kg 88 30-130 1330 1200 ug/Kg 90 30-130 1330 1240 ug/Kg 93 30-130 1330 991 ug/Kg 74 30-130 1330 1240 ug/Kg 93 40-140 1330 1180 ug/Kg 89 40-140 1330 939 41K9 70 40-140 1330 1100 ug/Kg 82 30-130 1330 1140 ug/Kg 85 40-140 1330 1110 ug/Kg 83 30-130 1330 1120 ug/Kg 84 30-130 1330 1090 ug/Kg 82 30-130 1330 915 ug/Kg 69 40-140 1330 992 ug/Kg 74 40-140 1330 558 J ug/Kg 42 40-140 1330 1160 J ug/Kg 87 30-130 1330 1070 ug/Kg 81 40-140 1330 988 ug/Kg 74 40-140 1330 951 ug/Kg 71 40-140 1330 316 J* ug/Kg 24 40-140 1330 1140 ug/Kg 85 40-140 TestAmerica Westfield Page 34 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCS 360-91885/2-A Client Sample ID: Lab Control Sample Matrix: Solid Analysis Batch: 91895 Prep Type: Total/NA Analysis Batch: 91895 Spike LCSD LCSD Prep Batch: 91885 %Rec. RPD Spike LCS LCS Result Qualifier Unit %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Azobenzene 1330 1270 ug/Kg 96 40-140 Benzo[a]anthracene 1330 1110 ug/Kg 83 40-140 Benzo[a]pyrene 1330 1080 ug/Kg 81 40-140 Benzo[b]fluoranthene 1330 1030 ug/Kg 77 40-140 Benzo[g,h,i]perylene 1330 1150 ug/Kg 86 40-140 Benzo[k]fluoranthene 1330 1290 ug/Kg 97 40-140 Bis(2-chloroethoxy)methane 1330 1100 ug/Kg 83 40-140 Bis(2-chloroethyl)ether 1330 647 ug/Kg 49 40-140 Bis(2-ethylhexyl) phthalate 1330 1230 ug/Kg 93 40-140 Butyl benzyl phthalate 1330 1170 ug/Kg 87 40-140 Chrysene 1330 1150 ug/Kg 86 40-140 Di -n -butyl phthalate 1330 1370 ug/Kg 103 40-140 Di-n-octyl phthalate 1330 1370 ug/Kg 103 40-14 0 Dibenz(a,h)anthracene 1330 1160 ug/Kg 87 40-140 Dibenzofuran 1330 1180 ug/Kg 88 40-140 Diethyl phthalate 1330 1180 ug/Kg 89 40-140 Dimethyl phthalate 1330 1100 ug/Kg 82 40-140 Fluoranthene 1330 1200 ug/Kg 90 40-140 Fluorene 1330 1160 ug/Kg 87 40-140 Hexachlorobenzene 1330 1040 ug/Kg 78 40-140 Hexachlorobutadiene 1330 959 ug/Kg 72 40-140 Hexachloroethane 1330 1010 ug/Kg 75 40-140 Indeno[1,2,3-cd]pyrene 1330 1160 ug/Kg 87 40-140 Isophorone 1330 889 ug/Kg 67 40-140 Naphthalene 1330 968 ug/Kg 73 40 - 140 Nitrobenzene 1330 1090 ug/Kg 82 40-140 Pentachlorophenol 1330 1260 J ug/Kg 95 30-130 Phenanthrene 1330 1130 ug/Kg 85 40-140 Phenol 1330 1160 ug/Kg 87 30-130 Pyrene 1330 1110 ug/Kg 83 40-140 Surrogate 2, 4, 6-Tribromophenol 2-Fluorophenol Nitrobenzene -d5 Phenol -d5 Terphenyt-d14 2-Fluorobiphenyl LCS LCS %Recovery Qualifier 67 72 73 76 91 72 Limits 30-130 30-130 30-130 30-130 30-130 30-130 Lab Sample ID: LCSD 360-91885/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 91895 Prep Batch: 91885 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 1,2,4-Trichlorobenzene 1330 954 ug/Kg 72 40-140 4 30 1,2 -Dichlorobenzene 1330 919 ug/Kg 69 40-140 1 30 1,3 -Dichlorobenzene 1330 876 ug/Kg 66 40-140 3 30 1,4 -Dichlorobenzene 1330 905 ug/Kg 68 40-140 4 30 2,2'-oxybis[l-chloropropane] 1330 894 ug/Kg 67 40-140 2 30 TestAmerica Westfield Page 35 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 360-91885/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 91895 Prep Batch: 91885 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 2,4,5 -Trichlorophenol 1330 1200 ug/Kg 90 30-130 3 30 2,4,6 -Trichlorophenol 1330 1180 ug/Kg 88 30-130 0 30 2,4-Dichlorophenol 1330 1230 ug/Kg 93 30-130 3 30 2,4 -Dimethylphenol 1330 1250 ug/Kg 94 30-130 1 30 2,4-Dinitrophenol 1330 973 ug/Kg 73 30-130 2 30 2,4-Dinitrotoluene 1330 1170 ug/Kg 88 40-140 6 30 2,6-Dinitrotoluene 1330 1100 ug/Kg 83 40-140 7 30 2-Chloronaphthalene 1330 919 ug/Kg 69 40-140 2 30 2 -Chlorophenol 1330 1070 ug/Kg 80 30-130 3 30 2 -Methylnaphthalene 1330 1160 ug/Kg 87 40-140 2 30 2-Methylphenol 1330 1070 ug/Kg 80 30-130 4 30 2-Nitrophenol 1330 1170 ug/Kg 88 30-130 5 30 3 & 4 Methylphenol 1330 1030' ug/Kg 78 30-130 5 30 3,3'-Dichlorobenzidine 1330 905 ug/Kg 68 40.140 1 30 4-Bromophenyl phenyl ether 1330 968 ug/Kg 73 40-140 2 30 4-Chloroaniline 1330 569 J ug/Kg 43 40-140 2 30 4-Nitrophenol 1330 1140 J ug/Kg 86 30.130 2 30 Acenaphthene 1330 1050 ug/Kg 79 40-140 2 30 Acenaphthylene 1330 970 ug/Kg 73 40.140 2 30 Acetophenone 1330 933 ug/Kg 70 40.140 2 30 Aniline 1330 312 J ug/Kg 23 40.140 1 30 Anthracene 1330 1070 ug/Kg 80 40-140 6 30 Azobenzene 1330 1180 ug/Kg 88 40-140 8 30 Benzo[a]anthracene 1330 1100 ug/Kg 83 40-140 0 30 Benzo[a]pyrene 1330 1070 ug/Kg 80 40.140 1 30 Benzo[b]fluoranthene 1330 1040 ug/Kg 78 40.140 1 30 Benzo[g,h,i]perylene 1330 1090 ug/Kg 82 40-140 6 30 Benzo[k]fluoranthene 1330 1190 ug/Kg 89 40-140 9 30 Bis(2-chloroethoxy)methane 1330 1120 ug/Kg 84 40-140 2 30 Bis(2-chloroethyl)ether 1330 633 ug/Kg 47 40.140 2 30 Bis(2-ethylhexyl) phthalate 1330 1250 ug/Kg 93 40- 140 1 30 Butyl benzyl phthalate 1330 1130 ug/Kg 85 40-140 3 30 Chrysene 1330 1120 ug/Kg 84 40-140 2 30 Di -n -butyl phthalate 1330 1350 ug/Kg 101 40-140 2 30 Di-n-octyl phthalate 1330 1290 ug/Kg 97 40 - 140 6 30 Dibenz(a,h)anthracene 1330 1110 ug/Kg 83 40.140 5 30 Dibenzofuran 1330 1130 ug/Kg 85 40-140 5 30 Diethyl phthalate _ 1330 1100 ug/Kg 82 40 - 140 7 30 Dimethyl phthalate 1330 1050 ug/Kg 79 40-140 4 30 Fluoranthene 1330 1200 ug/Kg 90 40-140 0 30 Fluorene 1330 1130 ug/Kg 85 40-140 3 30 Hexachlorobenzene 1330 1010 ug/Kg 76 40-140 3 30 Hexachlorobutadiene 1330 1000 ug/Kg 75 40.140 4 30 Hexachloroethane 1330 976 ug/Kg 73 40-140 3 30 Indeno[1,2,3-cd]pyrene 1330 1120 ug/Kg 84 40.140 3 30 Isophorone 1330 906 ug/Kg 68 40-140 2 30 Naphthalene 1330 1010 ug/Kg 75 40-140 4 30 Nitrobenzene 1330 1130 ug/Kg 84 40.140 4 30 Pentachlorophenol 1330 1230 J ug/Kg 92 30.130 3 30 Phenanthrene 1330 1070 ug/Kg 81 40-140 5 30 TestAmerica Westfield Page 36 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 360-91885/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 91895 Prep Batch: 91885 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Phenol 1330 1110 ug/Kg 83 30-130 4 30 Pyrene 1330 1090 ug/Kg 82 40-140 2 30 LCSD LCSD Surrogate %Recovery Qualifier Limits 2,4, 6-Tribromophenol 64 30-130 2-Fluorophenol 76 30-130 I Nitrobenzene -d5 74 30-130 Phenol -d5 72 30 - 130 Terphenyl-d14 89 30-130 2-Fluorobiphenyl 69 30-130 Method: 8015B - Diesel Range Organics (DRO) (GC) Lab Sample ID: MB 360-91884/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA ; Analysis Batch: 91988 Prep Batch: 91884 MB MB Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Petroleum Hydrocarbons 3.30 3.3 3.3 mg/Kg 06/13/12 18:22 06/16/12 00:53 1 (C9 -C36) Diesel Range Organics IC10-C28] ND 3.3 3.3 mg/Kg 06/13/12 18:22 06/16/12 00:53 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac o-Terphenyl 84 40-140 06/13/12 18:22 06/16/12 00:53 1 Lab Sample ID: LCS 360-91884/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 91988 Prep Batch: 91884 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Petroleum Hydrocarbons 167 119 mg/Kg 71 60-140 (C9 -C36) LCS LCS Surrogate %Recovery Qualifier Limits o-Terphenyl 75 40-140 Lab Sample ID: LCSD 360-91884/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 91988 Prep Batch: 91884 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Petroleum Hydrocarbons 167 121 mg/Kg 73 60-140 2 50 (C9 -C36) LCSD LCSD Surrogate %Recovery Qualifier Limits o-Terphenyl 74 40 -140 TestAmerica Westfield Page 37 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover TestAmerica Job ID: 360-41013-1 Method: 8082 - Polychlorinated Biphenyls (GC/ECD) Lab Sample ID: MB 360-91886/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 91901 Prep Batch: 91886 Analyte PCB -1016 PCB -1221 PCB -1232 PCB -1242 PCB -1248 PCB -1254 PCB -1260 PCB -1262 PCB -1268 Surrogate Tetrachloro-m-xylene Tetrachloro-m-xylene DCB Decachlorobiphenyl DCB Decachlorobiphenyl Lab Sample ID: LCS 360-91886/2-A Matrix: Solid Analysis Batch: 91901 Analyte PCB -1016 PCB -1260 Surrogate Tetrachloro-m-xylene Tetrachloro-m-xylene DCB Decachlorobiphenyl DCB Decachlorobiphenyl MB MB Spike LCS LCS Matrix: Solid Added Result Qualifier Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 100 30 ug/Kg 06/13/1218:43 06/14/1210:42 1 ND 100 58 ug/Kg 06/13/1218:43 06/14/1210:42 1 ND 100 86 ug/Kg 06/13/1218:43 06/14/1210:42 1 ND 100 35 ug/Kg 06/13/1218:43 06/14/1210:42 1 ND 100 95 ug/Kg 06/13/1218:43 06/14/1210:42 1 ND 100 58 ug/Kg 06/13/1218:43 06/14/1210:42 1 ND 100 42 ug/Kg 06/13/1218:43 - 06/14/1210:42 1 ND 100 53 ug/Kg 06/13/1218:43 06/14/1210:42 1 ND 100 48 ug/Kg 06/13/1218:43 06/14/1210:42 1 MB MB %Recovery Qualifier Limits Prepared Analyzed Dil Fac B 96 30-150 06/13/12 18:43 06/14/12 10:42 1 110 30-150 06/13/12 18:43 06/14/1210:42 1 97 30-150 06/13/12 18:43 06/14/12 10:42 1 111 30-150 06/13/12 18:43 06/14/12 10:42 1 Lab Sample ID: LCSD 360-91886/3-A Spike LCS LCS Matrix: Solid Added Result Qualifier Unit 500 522 ug/Kg Analyte 500 534 ug/Kg LCS LCS 500 PCB -1260 %Recovery Qualifier Limits LCSD LCSD 91 30-150 Tetrachloro-m-xylene 88 102 30-150 99 30-150 92 30-150 30-150 DCB Decachlorobiphenyl 106 30-150 Lab Sample ID: LCSD 360-91886/3-A Matrix: Solid Analysis Batch: 91901 Spike Analyte Added PCB -1016 500 PCB -1260 500 LCSD LCSD Surrogate %Recovery Qualifier Limits Tetrachloro-m-xylene 88 30 - 150 Tetrachloro-m-xylene 99 30-150 DCB Decachlorobiphenyl 88 30-150 DCB Decachlorobiphenyl 101 30-150 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 91886 %Rec. D %Rec Limits 104 40-140 107 40-140 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 91886 LCSD LCSD %Rec. RPD Result Qualifier Unit D %Rec Limits RPD Limit 497 ug/Kg 99 40-140 5 30 525 ug/Kg 105 40-140 2 30 TestAmerica Westfield Page 38 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Method: 6010C - Metals (ICP) Spike Added Arsenic Lab Sample ID: MB 360-91916/1-A Barium 503 Matrix: Solid 183 Chromium Analysis Batch: 91991 Silver 77.7 Selenium MB MB Zinc Analyte Result Qualifier 149 Arsenic ND mg/Kg Barium ND 06/15/1212:20 1 Cadmium ND mg/Kg Chromium ND 06/15/1212:20 1 Silver ND mg/Kg Selenium ND 06/15/1212:20 1 Zinc 0.422 J mg/Kg Lead ND 06115/1212:20 1 Lab Sample ID: LCDSRM 360-91916/3-A LCDSRM mg/Kg Matrix: Solid 06/14/1210:47 06/15/1212:20 1 Analysis Batch: 91991 0.24 mg/Kg 06/14/1210:47 Spike Analyte 0.21 Added Arsenic 06/14/1210:47 135 Barium 0.049 503 Cadmium 06/14/1210:47 183 Chromium 261 Silver 77.7 Selenium 160 Zinc 721 Lead 149 Lab Sample ID: LCSSRM 360-91916/2-A Matrix: Solid Analysis Batch: 91991 Analyte Spike Added Arsenic 135 Barium 503 Cadmium 183 Chromium 261 Silver 77.7 Selenium 160 Zinc 721 Lead 149 Client Sample ID: Method Blank TestAmerica Westfield Page 39 of 45 6/18/2012 Prep Type: Total/NA Prep Batch: 91916 RL MDL Unit D Prepared Analyzed Dil Fac 1.0 0.11 mg/Kg 06/14/1210:47 06/15/1212:20 1 0.50 0.12 mg/Kg 06/14/1210:47 06/15/1212:20 1 0.20 0.0066 mg/Kg 06/14/1210:47 06/15/1212:20 1 0.50 0.12 mg/Kg 06/14/1210:47 06115/1212:20 1 0.50 0.026 mg/Kg 06/14/1210:47 06/15/1212:20 1 0.50 0.24 mg/Kg 06/14/1210:47 06/15/1212:20 1 2.5 0.21 mg/Kg 06/14/1210:47 06/15/1212:20 1 0.50 0.049 mg/Kg 06/14/1210:47 06/15/1212:20 1 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 91916 LCDSRM LCDSRM %Rec. RPD Result Qualifier Unit D %Rec Limits RPD Limit 114 mg/Kg 84.2 62.9.117. 9 30 0 419 mg/Kg 83.3 70.6.119. 10 30 1 154 mg/Kg 83.9 66.1 _ 113. 10 30 7 223 mg/Kg 85.5 65.5.119. 12 30 5 67.3 mg/Kg 86.7 62.0.122. 9 30 7 133 mg/Kg 83.0 60.8.120. 9 30 0 611 mg/Kg 84.8 67.7.118_ 8 30 2 123 mg/Kg 82.4 66.8-116. 8 30 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 91916 LCSSRM LCSSRM %Rec. Result Qualifier Unit D %Rec Limits 125 mg/Kg 92.4 62.9.117. 0 461 mg/Kg 91.7 70.6.119. 1 169 mg/Kg 92.3 66.1 _ 113. 7 251 mg/Kg 96.1 65.5--119. 5 73.9 mg/Kg 95.1 62.0-122. 7 145 mg/Kg 90.7 60.8.120. 0 665 mg/Kg 92.2 67.7-116. 2 133 mg/Kg 89.4 66.8-116. 1 TestAmerica Westfield Page 39 of 45 6/18/2012 QC Sample Results Client: Woodard & Curran Inc Project/Site: North Andover Method: 7471A - Mercury (CVAA) Lab Sample ID: MB 360-91844/1-A Matrix: Solid Analysis Batch: 91860 MB MB Analyte Result Qualifier Mercury ND Lab Sample ID: LCDSRM 360-91844/3-A LCDSRM Matrix: Solid Analysis Batch: 91860 Analyte Mercury Lab Sample ID: LCSSRM 360-91844/2-A Matrix: Solid Analysis Batch: 91860 Analyte Mercury TestAmerica Job ID: 360-41013-1 Method: SM 2510B - Conductivity, Specific Conductance Lab Sample ID: MB 360-91819/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Soluble Analysis Batch: 91855 MB MB Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Specific Conductance ND 4.0 4.0 umhos/cm 06/13/12 10:16 1 Lab Sample ID: LCS 360-91819/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Soluble Analysis Batch: 91855 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Specific Conductance 5660 5660 umhos/cm 100 85-115 Page 40 of 45 TestAmerica Westfield 6/18/2012 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 91844 RL MDL Unit D Prepared Analyzed Dil Fac 0.10 0.024 mg/Kg 06/13/12 08:53 06/13/12 11:58 1 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 91844 Spike LCDSRM LCDSRM %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 16.2 15.2 mg/Kg 93.8 43.3.125. 27 30 3 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 91844 Spike LCSSRM LCSSRM %Rec. Added Result Qualifier Unit D %Rec Limits 16.2 11.6 mglKg 71.8 43.3.125. 3 Method: SM 2510B - Conductivity, Specific Conductance Lab Sample ID: MB 360-91819/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Soluble Analysis Batch: 91855 MB MB Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Specific Conductance ND 4.0 4.0 umhos/cm 06/13/12 10:16 1 Lab Sample ID: LCS 360-91819/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Soluble Analysis Batch: 91855 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Specific Conductance 5660 5660 umhos/cm 100 85-115 Page 40 of 45 TestAmerica Westfield 6/18/2012 Lab Chronicle Client: Woodard & Curran Inc TestAmerica Job ID: 360-41013-1 Project/Site: North Andover Client Sample ID: C13-1 Lab Sample .ID: 360-410134 Date Collected: 06/07/1214:30 Matrix: Solid Date Received: 06/08/1218:20 Percent Solids: 74.5 Analyst Lab CMR Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Total/NA Prep 5035 TAL WFD 91800 ' 06/12/1216:11 Total/NA Analysis 8260C 1 91862 06/13/12 04:10 Total/NA Prep 5035 RA 91911 06/14/1215:20 Total/NA Analysis 8260C RA 1 91954 06/15/12 02:39 Total/NA Prep 3546 91885 06/13/1218:29 Total/NA Analysis 8270D 10 91895 06/14/1212:23 Total/NA Prep 3546 91886 06/13/1218:43 Total/NA Analysis 8082 1 91901 06/14/1212:06 Total/NA Prep 3546 91884 06/13/1218:22 Total/NA Analysis 8015B 10 91988 06/16/12 03:32 Total/NA Prep 7471A 91844 06/13/1208:53 Total/NA Analysis 7471A 1 91860 06/13/1212:14 Total/NA Prep 3050B 91916 06/14/1210:47 Total/NA Analysis 6010C 1 91991 06/15/1214:15 Total/NA Analysis Moisture 1 91773 06/11/1214:21 Soluble Leach DI Leach 91819 06/12/12 12:46 Soluble Analysis SM 2510B 1 91855 06/13/12 10:21 Analyst Lab CMR TAL WFD CMR TAL WFD CMR TAL WFD CMR TAL WFD MJM TAL WFD JLG TAL WFD MJM TAL WFD BRB TAL WFD MJM TAL WFD JLG TAL WFD BH TAL WFD TJS TAL WFD BH TAL WFD TJS TAL WFD BH TAL WFD AMS TAL WFD AMS TAL WFD Client Sample ID: C13-2 Lab Sample ID: 360-41013-2 Date Collected: 06/07/1214:30 Matrix: Solid Date Received: 06108/1218:20 Percent Solids: 82.8 Laboratory References: TAL WFD = TestAmerica Westfield, Westfield Executive Park, 53 Southampton Road, Westfield, MA 01085, TEL (413)572-4000 Page 41 of 45 Analyst Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Total/NA Prep 5035 TAL WFD 91800 06/12/1216:11 Total/NA Analysis 8260C 1 91862 06/13/12 04:33 Total/NA Prep 5035 RA 91911 06/14/1215:20 Total/NA Analysis 8260C RA, 1 91954 06/15/12 03:02 Total/NA Prep 3546 91885 06/13/1218:29 Total/NA Analysis 8270D 10 91895 06/14/1212:54 Total/NA Prep 3546 91886 06/13/1218:43 Total/NA Analysis 8082 1 91901 06/14/1212:27 Total/NA Prep 3546 91884 06/13/1218:22 Total/NA Analysis 8015B 20 91988 06/16/12 04:04 Total/NA Prep 7471A 91844 06/13/12 08:53 Total/NA Analysis 7471A 1 91860 06/13/1212:16 Total/NA Prep 30508 91916 06/14/1210:47 Total/NA Analysis 6010C 1 91991 06/15/1214:17 Total/NA Analysis Moisture 1 91773 06/11/1214:21 Soluble Leach DI Leach 91819 06/12/12 12:46 Soluble Analysis SM 2510B 1 91855 06/13/12 10:22 Laboratory References: TAL WFD = TestAmerica Westfield, Westfield Executive Park, 53 Southampton Road, Westfield, MA 01085, TEL (413)572-4000 Page 41 of 45 Analyst Lab CMR TAL WFD CMR TAL WFD CMR TAL WFD CMR TAL WFD MJM TAL WFD JLG TAL WFD MJM TAL WFD BRB TAL WFD MJM TAL WFD JLG TAL WFD BH TAL WFD TJS TAL WFD BH TAL WFD TJS TAL WFD BH TAL WFD AMS TAL WFD AMS TAL WFD TestAmerica Westfield 6/18/2012 f i i Client: Woodard & Curran Inc Project/Site: North Andover Laboratory TestAmerica Westfield TestAmerica Westfield TestAmerica Westfield TestAmerica Westfield TestAmerica Westfield TestAmerica Westfield Certification Summary TestAmerica Job ID: 360-41013-1 Authority Program EPA Region Certification ID Connecticut State Program 1 PH -0494 Maine State Program 1 MA00014 Massachusetts State Program 1 M-MA014 New Hampshire NELAC 1 2539 Rhode Island State Program 1 LA000057 Vermont State Program 1 VT -10843 Accreditation may not be offered or required for all methods and analytes reported in this package . Please contact your project manager for the laboratory's current list of certified methods and analytes. TestAmerica Westfield Page 42 of 45 6/18/2012 State Accreditation Matrix Method Name ._ Description Primary Accreditation New Hampshire (NELAC) Mass 180.1 Turbidity, Nephelometric P P 245.1 Mercury (CVAA) NP/P NP 300 Anions, Ion Chromatography NP/P NP/P 410.4 COD NP NP 524.2 Volatile Org Comp (GC/MS)(list upon request) P P 524.2 Trihalomethane compounds P P 608 Organochlorine Pest(PCBs (list upon request) NP NP 624 Volatile Org Comp (GC/MS)(list upon request) NP NP 625 Semivolatile Org Comp (GC/MS)(list upon request) NP NP 1010 Ignitability, Pensky-Martens Closed -Cup Method SW 1103.1 E.coli ambient/source 3546 Microwave Extraction SW 5035 Closed System Purge and Trap SW 6020 Metals (ICP/MS) (list upon request) NP 10-107-06-2 Nitrogen, Total Kjeldahl NP NP 200.7 Rev 4.4 Metals (ICP)(list upon request) NP/P NP/P 200.8 Rev 5.4 Metals (ICP/MS) (list upon request) NP/P NP/P 3005A Preparation, Total Recoverable or Dissolved Metals NP/P 3010A Preparation, Total Metals NP/P 3020A Preparation, Total Metals NP/P 30508 Preparation, Metals SW 3510C Liquid -Liquid Extraction (Separatory Funnel) NP 50308 Purge and Trap NP 6010C Metals (ICP)(list upon request) NP/SW 7196A Chromium, Hexavalent NP/SW 7470A Mercury (CVAA) NP 7471A Mercury(CVAA) SW 8081 B Organochlorine Pesticides (GC)(list upon request) NP/SW 8082A PCBs by Gas Chromatography(list upon request) NP/SW 8260C Volatile Org Comp. (GC/MS)(list upon request) NP/SW 8270D Semivolatile Comp.(GC/MS)(list upon request) NP/SW 9012A Cyanide, Total and/or Amenable NP/SW 90308 Sulfide, Distillation (Acid Soluble and Insoluble) NP 9045C pH SW CT ETPH Conn - Ext. Total petroleum Hydrocarbons (GC) NP/SW Enlerolert Enterococcus ambient/source L107041C Nitrogen, Nitrate NP L107-06-16 Nitrogen Ammonia NP NP L204001A CN Cyanide, Total P NP/P L210 -001A Phenolics, Total Recoverable NP NP MA-EPH Mass - Extractable Petroleum Hydrocarbons (GC) NP/SW MAVPH Mass -Volatile Petroleum Hydrocarbons (GC) NP/SW SM 2320B Alkalinity NP/P NP/P SM 2340B Total Hardness (as CaCO3) by calculation NP/P NP SM 25108 Conductivity, Specific Conductance NP/P NP/P SM 2540C Solids, Total Dissolved (TDS) NP/P NP/P SM 2540D Solids, Total Suspended (TSS) NP NP SM 3500 CR D Chromium, Hexavalent NP SM 4500 Cl F Chlorine, Residual NP SM 4500 H+ B pH NP/P NP/P SM 4500 NO2 B Nitrogen, Nitrite NP P SM 4500 P E Phosphorus, Orthophosphate NP/P NP SM 4500 P E Phosphorus, Total NP NP SM 4500 S2 D Sulfide, Total NP SM 52108 BOD, 5 -Day NP NP SM 5310B Organic Carbon, Total (TOC) NP/P NP SM 9215E Heterotrophic Plate Count (SimPlate) P SM 9222D Coliforms, Fecal (Membrane Filter) NP SM 9223 Coliforms, Total, and E.Coli (Colitert-P/A) P SM 9223 lColiforms, Total, and E.Coli (Enumeration) P Not all organic compounds are accreditied under YNI For methods with multiple compounds all compounds may not meet TNI criteria, a listing should be obtained from the laboratory The lab carries additional accreditations with several states. This is the laboratories typcial listing but is subject to change based on the laboratories current certification standing. NP=Non Potable P= Potable SW=Solid Waste Page 43 of 45 WI -QA -040r10 last updated 3/21/20/18/2012 Login Sample Receipt Checklist Client: Woodard & Curran Inc Job Number: 360-41013-1 Login Number: 41013 List Number: 1 Creator: Ard, Vanessa L Question List Source: TestAmerica Westfield Answer Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. N/A The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the sample IDs on the containers and True the COC. Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in N/A diameter. Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. 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