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Home My WebLink About2020-01-07 Consultant Review-Analytical Report 2.. VVYYLYI V.VVVF..s..V Y- . YR.. k� htV H ANfiLY7 1CAL ANALYTICAL REPORT Lab Number: L2009081 Client: Axiom Partners, Inc. One Pleasure Island Road, Suite 2C Wakefield, MA 01880 ATTN: Dan Batchelor Phone: (781)213-9198 Project Name: NACC Project Number: 01251.068 Report Date: 03/02/20 The original project report/data package is held by Alpha Analytical,This report/data package is paginated and should be reproduced only in its entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Certifications&Approvals:MA(M-MA086), NH NELAP(2064),CT(PH-0574), IL(200077),ME(MA00086), MD(348),NJ(MA935),NY(11148), NC(25700/666),PA(68-03671), RI(LA000065),TX(T104704476),VT(VT-0935),VA(460195),USDA(Permit#P330-17-00196). Eight Walkup Drive, Westborough, MA 01581-1019 508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com „�45 Page 1 of 17 Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 Alpha Sample Collection Sample ID Client ID Matrix Location Date/Time Receive Date L2009081-01 V1 SOIL N. ANDOVER, MA 02/26/20 07:30 02/26/20 Page 2 of 17 `'` r LFHA V�Ilul u.vtiv�� 1'Y. f� Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the hack of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter (i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds(TICs),if requested,are reported for compounds identified to be present and are not part of the methodlprogram Target Compound List,even if only a subset of the TCL are being reported, If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R" or"RE",respectively. When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific%recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report.In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances,the specific failure is not narrated but noted in the associated QC outlier Summary Report,located directly after the Case Narrative.QC information is also incorporated in the Data Usability Assessment table(Format 11)of our Data Merger too],where it can be reviewed in conjunction with the sample result,associated regulatory criteria and any associated data usability implications. Soillsediments,solids and tissues are reported on a dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. HOLD POLICY-For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples.Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Project Management at 800-624-9220 with any questions. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Tiffani Morrissey Authorized Signature: Title: Technical Director/Representative Date: 03/02/20 'fitI;.a Page 3 of 17 - ---------- METALS Page 4 of 17 Project Name: NACC Lab Number: L2008081 Project Number: 01261.008 Report Date: 03/82/20 SAMPLE RESULTS Lab |D: L2809081-01 Date Collected: 02/28/2007:30 Client |D: V1 Dote Received: 02/26/20 Sample Location: N.ANOOVEF<, K4A Field Prep: Not Specified Sample Depth: TCLP/SpLp Ext. Date: 02/28/28 16:44 Matrix: Soil Dilution Date Doe Pep Analytical Parameter Result Qualifier Units RL MoL Factor pmpomd Analyzed Method Method Analyst TCLP Metals bv EPA 1311 -Mansfield Lab L^ad.TCLP ND mg/| m.aon — 1 03102/2010:340302/2011:40 EPA3U15 1.0010m PS � Page 5of17 � Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 SAMPLE RESULTS Lab |D: L2009081-01 Date Collected: 02/26/2007:30 Client ID: V1 Date Received: 02/26/20 Sample Location: N. ANO0VER^ k4A Field Prep: Not Specified Sample Depft Matrix: Soil Dilution Date nmo Prep Analytical p«mm*mr mowu|t Qualifier Units RL MDL Factor pmnamd Analyzed Method Method Analyst TCLP Metals bv EPA 1311 -Mansfield Lab M*m"ry.TCLp No mg/| 0o010 — 1 03/02/2010:1403m2/2012:48 EpAr47OA 1.7470A OD ALPHA Page Gof17 | Project Name: WACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/82/20 Method Blank Analysis Batch Quality Control Dilution Date Date Analytical Parameter Result Qualifier Units RL K8DL Factor Prepared Analyzed Method Analyst TCLPPWete|nbyEPA1311 -MansfieNLab forsonop|e(u): 01 Batch: VVG1348083-1 � MeroumTCLP Mo mO0 0.0010 — 1 03/02/2010:14 0302C2012:43 1.7470A SD Prep Information Digestion Method: EPA7478A TCLP/SPLP Extraction Date: 02/28/2018:44 Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst � TCLP Metals by EPA 1311 -Mansfield Lab foraannp|o(s): 01 Batch: VVG1346094-1 uaad.TCLp No my0 0.500 — 1 03/02/2010:34 0302/2011:37 1.6010o P3 Prep Information Digestion Method: EPA301G TCLP/GPLP Extraction Date: 02/28/2016:44 LPHA Page 7uf17 � Serial No:03022014:12 Lab Control Sample Analysis Batch Quality Control Project Name: NAGG Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 LCS LCSD %Recovery Parameter %Recovery Qual %Recovery Qual Limits RPD Qual RPD Limits TCLP Metals by EPA 1311 -Mansfield Lab Associated sample(s): 01 Batch:WG1346093-2 Mercury,TCLP 105 80-120 TCLP Metals by EPA 1311 -Mansfield Lab Associated sample(s): 01 Batch:WG1346094-2 Lead,TCLP 91 75-125 - 20 Page 8of17 ALPHA Serial No:03022014:12 Matrix Spike Analysis Batch Quality Control Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 Native MS MS MS MSD MSD Recovery RPD Parameter Sample Added Found %Recovery Qual Found s/Recovery Qual Limits RPD Qual Limits TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 01 QC Batch ID: WG1346093-3 QC Sample: L2009081-01 Client ID: V1 Mercury,TCLP ND 0.025 0.0256 1102 - - 80-120 - 20 TCLP Metals by EPA 1311 - Mansfield Lab Associated sample(s): 01 QC Batch ID: WG1346094-3 QC Sample: L2009081-01 Client ID: V1 Lead,TCLP ND 5.1 4.73 93 - - 75-125 20 Page 9 of 17 P Serial No:03022014:12 Lab Duplicate Analysis Project Name: NACC Batch Quality Control Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 Parameter Native sample Duplicate Sample Units RPD Qual RPD Limits TCLP Metals by EPA 1311 - Mansfield Lab Associated samples): 01 QC Batch ID: WG1346093-4 QC Sample: L2009081-01 Client ID: V1 Mercury,TCLP ND ND mg/I NC 20 TCLP Metals by EPA 1311 - Mansfield Lab Associated samples): 01 QC Batch ID: WG1346094-4 QC Sample: L2009081-01 Client ID: V1 Lead,TCLP ND ND mg/I NC 20 PH Page 10 of 17 „�. A� Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 Sample Receipt and Container Information Were project specific reporting limits specified? YES Cooler Information Cooler Custody Seal A Absent Container Information Initial Final Temp Frozen Container ID Container Type Cooler pH pH deg C Pres Seal Date/Time Analysis(*) L2009081-01A Glass 500mU16oz unpreserved A NA 2.9 Y Absent - 1-2009081-01X Plastic 120ml HNO3 preserved Extracts A NA 2.9 Y Absent HG-C(28),PB-C1(180) L2009081-01X9 Tumble Vessel A NA 2.9 Y Absent - Page 11 of 17 *Values in parentheses indicate holding time in days ......... ........ ...... . ....... . . .... Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 GLOSSARY Acronyms DL Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values,when those target analyte concentrations ate.quantified below the limit ofquantitation(LOQ).The DI,includes any adjLlStDlCrnS from dilutions,concentrations or moisture content,where applicable. (DoD report formats only.) EDL Estimated Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values,when those target analyte concentrations are quantified below the reporting limit(RL).The EDL includes any adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis ofPAHs using Solid-Phase Microextraction(SPME). EMPC Estimated Maximum Possible Concentration:The concentration that results from the signal present it the retention time of an analyte when the ions meet all of the identification criteria except the ion abundance ratio criteria,An EMPC is a worst-case estimate of the concentration, EPA Environmental Protection Agency. 11CS Laboratory Control Simple:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. LCSD Laboratory Controi Sample Duplicate:Refer to LCS. Laboratory Fortified Blank:A sample matrix,,fice from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. LOD Limit of Detection:This value represents the level to which a target analyte can reliably be detected for I specific analyte in a specific matrix by a specific method. The LOD includes any adjustments from dilutions,concentrations or moisture content, where applicable.(DoD report formats only.) LOQ Litilit of Quantitation:The value at which in instrument can accurately measure all analyte at a specific concentration.The LOQ includes any adjustments from dilutions,concentrations or moisture content,where applicable.(DoD report formats Only') Limit of Quantitation:The value at which all instrument can accurately measure all analyte at a specific concentration.The LOQ includes any adjustments from dilutions,concentrations or moisture content,where applicable.(DoD report formats only.) MDL Method Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values,when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any adjustments from dilutions,concentrations or moisture content,where applicable. MS Matrix Spike Sample:A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which all independent estimate of target analyte concentration is available.For Method 332.0,the spike rccovcry is calculated using the native concentration,including estimated values. MSD Matrix Spike Sample Duplicate:Refer to MS. NA Not Applicable. NC Not Calculated: 'Term is utilized when one or more ofthe results utilized in the calculation are non,detect at the parameter's reporting unit. NDPA/DPA N-N itrosodi phenyl am i ne/Dipl tertylarn i tie. NI Not Ignitable. Nil Non-Plastic:Temi is utilized for the analysis of Atterberg Limits in soil. RL Reporting Limit: The value at which an instrument can accurately measure,in analyte at a specific concentration.The RL includes any adjustments from dilutions,concentrations or moisture content,where applicable. RPD Relative Percent Difference: The results from rnatrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing(tie absolute difference between the values;although the RPD value will be provided in the report. SRM Standard Reference Material:A reference sample of known or certified value that is oftlic same or similar matrix as the associated field samples. STLP Scilli-dynamicTank Leaching Procedure per EPA Method 1315. TEF Toxic Equivalency Factors:'file values assigned to each dioxin and filran to evaluate their toxicity relative to 2,3,7,8-TCDD. TEQ Toxic Equivalent:The measure of a sample's toxicity derived by multiplying each dioxin and furan by its corresponding TEF and then summing the resulting values. Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound list(TCL)for the method arid/or program.All TICs are qualitatively identified and reported as estimated concentrations. Footnotes Report Format: Data Usability Report .............................................. Page 12 of 17 Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 1 The reference for this analyte should be considered modified since this analyte is absent from the target analytc list oftlic original method, Terms Analytical Method:Both the document from which the method originates and the analytical reference method.(Example:EPA 82(0B is shown as 1,826013.)The codes for the reference method documents are provided in the References section of the Addendum. Difference:With respect to Total Oxidizable Precursor(TOP)Assay analysis,the difference is defined as the Post-'Treatment value minus the Pre-Treatment value, Final PH:As it pertains to Sample Receipt&Container Information section of the report,Final PH reflects pH of container determined after adjustment at the laboratory,if applicable.If no adjustment required,value reflects Initial PH. Frozen Date/Time:With respect to Volatile Organics in soil,Frozen Date/Titrie reflects the date/time at which associated Reagent Water- preserved vials were initially frozen.Note:If frozen datcAinic is beyond 48 hours from sample collection,value will be reflected in'hold'. Initial lift:As it pertains to Sample Receipt&Container Information section of the report,Initial pit reflects pH of container determined upon receipt,if applicable. PAII Total:With respect to Alkylated PAH analyses,the TAEs,Total'result is defined as the summation of results for all or a subset of the following compounds:Naphthalene,CI-C4 Naphthalenes,2-Methy1naplithalene,I-Methy1naphtlialene,Biphenyl,Acenaplithyleric, Acenaphthene,FlUorene,C I-C3 Fluorenes,Phenanthrene,Cl-C4 Plteji,,tiitlireiie.q/Aiitlii-aceiies,Anthracene,Fluoranthene,Pyrelle,CI-C4 Fluorantlienes/Pyrenes,Benz(a)anthracene,Chryseric,C I-C4 Chrysenes,Benzo(b)fluoranthene,Benzoo)+(k)fluoranthene,Benzo(c)pyrellc, Benzo(a)pyrene,Perylene,Inderio(1,2,3-cd)pyrene,Dibenz(ali)+(ac)anthracene,Benzo(g,h,i)perylene.If a'Total'restilt is requested,the results of its individual components will also be reported, PFAS Total:With respect to PFAS analyses,the'PFAS,Total(5)'result is defined as the summation of results for:PFIlpA,PFI IxS,PFOA, PFNA and PFOS.If a'Total'result is requested,the results of its individual components will also be reported. 'file target compound Chlordane(CAS No.57-74-9)is reported for GC ECD analyses.Per EPA,this compound"refer-,to a mixture of chlordane isomers,other chlorinated hydrocarbons and numerous other components."(Reference:USEPA Toxicological Review of Chlordane,In Support of Summary Information on the integrated Risk Information System(IRIS),December 1997.) Total:With respect to Organic analyses,a'Total'result is defined as the summation of results for individual isomers or Aroclors,Ifa'Total' result is requested,the results of its individual components will also be reported.This is applicable to'Totat'results for methods 8260,8081 and 8082. Data Qualifiers A -Spectra identified as"A Idol Condensates"are byproducts of the extraction/concentration procedures when acetone is introduced in the process. B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that have detectable concentrations of the analyte at less than tell times(lox)the concentration found in the blank.For MCP-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than tell times(lox) the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(lox)the concentration found in the blank AND the analyte was detected above one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ- Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above tile reporting limit.For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanonc). C Co-elution:The target analyte co-elutes with a known lab standard(i.e.surrogate,internal standards,etc.)for co-extracted analyses. 1) Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations of the analyte. E Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. G The concentration may be biased high due to matrix interferences(Le,co-elution)with non-target compound(s),The result should Ere considered estimated, 11 -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of'sample collection. -'file lower value for the two columns has been reported due to obvious interference. Estimated value.This represents all estimated concentration for Tentatively Identified Compounds(TICS). M Reporting Limit(RL)exceeds the MCI'CAM Reporting Limit for this analyte. ND Not detected at the reporting limit(RI,)for the sample. NJ Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICS),where the identification is based on a mass spectral library search. P -The RPD between the results for the two columns exceeds the method-specified criteria. Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate R_PD when the sample concentrations are less Report Format: Data Usability Report ......... ............. Page 13 of 17 Project Name: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 Data Qualifiers than Sx the RL.(Metals only.) R -Analytical results are from sample re-analysis. RE, -Analytical results are from sample re-extraction. Is -Analytical results are from modified screening analysis. Report Format: Oata Usability Report LPHA Page 14 of 17 Protect flame: NACC Lab Number: L2009081 Project Number: 01251.068 Report Date: 03/02/20 REFERENCES 1 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods, EPA SW-846. Third Edition. Updates I - IV, 2007. LIMITATION OF LIABILITIES Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. A: t; Page 15 of 17 Alpha Analytical, Inc. ID No.:17873 Facility: Company-wide Revision 16 Department: Quality Assurance Published Date: 211 712020 1 0:46:05 AM Title: Certificate/Approval Program Summary Page 1 of 1 Certification Information The following analytes are not included in our Primary NELAP Scope of Accreditation: Westborough Facility EPA 6241624.1:mip-xylene,o-xylene EPA 826OC: NPW; 1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene;SCM;lodornethane(methyl iodide), 1,2,4,5-Tetramethylbenzene;4- Ethyltoluene, EPA 8270D: NPW:Dimethylnaphthalone,1,4-Diphenylhydrazine;SCM:Dimethylnaphtha lone,l,4-Diphenylhydrazine. SM4500:NPW: Amenable Cyanide;SCM:Total Phosphorus,TKN,NO2,NO3. Mansfield Facility SM 254OD: TSS EPA 8082A:NPW: PCB: 1,5,31,87,101, 110, 141,151,153, 180, 183,187. EPA TO-15:Halolhane,2,4,4-Trimethyl-2-pentene,2,4,4-Trimethyl-11-pentene,Thiophene,2-Methylth lop hone, 3-Methylthiophone,2-Ethylthiopheno, 1,2,3-Trimethylbenzone,Indan,Indene, 1,2,4,5-Tetramethylbenzene,Benzothlophene, 1-Mothylnaphthalene. EPA TO-12 Non-methane organics EPA 3C Fixed gases Biological Tissue Matrix: EPA 30508 The following analytes are included in our Massachusetts DEP Scope of Accreditation Westborough Facility: Drinking Water EPA 300,0:Chloride,Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE, EPA 180.1,SM2130B,SM4500C1-D,SM2320B,SM2540C,SM4500H-B,SM450ONO2-B EPA 332:Perchlorate; EPA 524.2: THMs and VOCs;EPA 504.1:EDB,DBCP. Microbiology:SM9215B;SM9223-P1A,SM9223B-Colilert-QT,SM9222D. Non-Potable Water SM4500H,B,EPA 120.1,SM2510B,SM2540C,SM2320B,SM4500CL-E,SM4500E-BC,SM4500NH3-BH: Ammonia-N and Kjeldahl-N, EPA 350.1: Ammonia-N, LACHAT 10-107.06-1-B:Ammonia-N,EPA 351.1,SM4500NO3-F,EPA 353.2:Nitrate-N,SM4500P-E,SM4500P-B,E,SM4500SO4-E, SM5220D,EPA 410.4,SM5210B,SM5310C,SM4500CL-D, EPA 1664,EPA 420.1,SM4500-CN-CE,SM254011),EPA 300:Chloride,Sulfate,Nitrate. EPA 624.1:Volatile Halocarbons&Aromatics, EPA 608.3:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT, Endosulfan I,Endosulfan it, Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs EPA 625.1:SVOC(AcidlBase/Neutral Extractabfes),EPA 60014-81-045: PCB-Oil. Microbiology;SM9223B-Colilert-QT; Enterolert-QT,SM9221E, EPA 1600,EPA 1603. Mansfield Facility: Drinking Water EPA 200,7:Al,Ba,Cd,Cr,Cu, Fe,Mn, Nf,Na,Ag,Ca,Zn.EPA 200.8:Al,Sb,As,Ba,Be,Cd,Cr,Cu, Pb,Mn,Ni,Se,Ag,TL,Zn. EPA 245.1 Hg. EPA 522. Non-Potable Water EPA 200.7:Al,Sb,As,Be,Cd,Ca,Cr, Co,Cu,Fe,Pb,Mg,Mn,Me,Ni,K,Se,Ag, Na,Sr,TL,Ti,V,Zn. EPA 200.8:Al,Sb,As,Be,Cd,Cr,Cu,Fe,Pb,Mn,Ni,K,Se,Ag,Na,TL,Zn. EPA 245.1 Hg. SM2340B For a complete listing of analytes and methods, please contact your Alpha Project Manager. Document Type: Form Pre-Qualtrax Document ID: 08-113 Page 16 of 17 V Vt1µ V.YV VLLv �T. 1L F CUSTODY ALP, 14A CHAIN r=aoe�c� � Date Re:.d in La- ✓ �'� � HA Jo '', it +✓ T�-- MA?_�: c3: L'a.�,�.=.55 t°r `.sue.'.-9�..-:...C� Proiect Name: �`� � � � � VAoEx In.S,�atm me sa as ler'l I'If@ Po o- ��? •�� } / I � C4 � P 0, t, t } Z3 Yes tics SSA MCP i salyticat Menlho s 0Yes o C7 qCP.�t}'ti~�tvte'�to-�s dent .�.xiom Pari,.m.Inc, — 0 YFs;&No Matrix Spike RequLred on ihis SDG? fRecru',ed for MCP inorgarri ) Addrosn- Plemre'I land Road,2C' ,Pr ct%!3n3aer 3 Yo5))Ito �,Y?Standards'Info ReiZu re-d for Metals EPA'wivi Targets) Wake geld, 019 r Mare_ aF ct3-9 9 � a, Yes t o +�PC}ES€ GF ALPHAQu e 0 Wier S�,ale Fed Program Crt ria F�.x: ?9t-?.3-S9v2 Email' f3`' tioC 3€lQri'L'r 1.G�^t . s e n a f i d {a{# P Pb T- v DStzndarr9 e*1r L ,L C ! Additional Project Information; Date Duo: _ �� ; r � `� F � �� 't � « L? S AMPLE iNrl ration JU, r Fie-vi t:tL GY3 �5 }�# j 1 #:4Sr#['! .'�, __ otd j ' g —0 Lzb,40 do t C) c - CD Pred`vi ra'Irr 5/ Z)Lzb to do fit..3'"[ sJ 0I -_- ' OIr.^fi.Ilot� Jr+`4rn e ' .{i f •i. i at r t s - r,. lam;use Only) Same;e tG ;Saa r ( Date 79 c'�trix I t.mlliaJl t` �J«:.rF3CJ'c: triSC;itS i 0!9081- -77s ! a ! ' ' 3 z i 1 1 i I 1F i Container T i €� � a-None }Pr= ! Z n *. r o-sue - € r7 'O9«s £'-hR R -. - c C—L* r- r-.OH By: t:a7erTm Rid BT- t F?3rr O. r r ttawtS« I � AN p I:.,- are -Et to not Azcnrtm Ac;C ""'�_".`__``�—.-=-=,-r-°a -1 i.�'- � _" '`.a... _-,,._ t! C _ 0a's.[imp %aCd Cand6ons, -ZZA AC,-«ate — ' See raverse side_ C}==G;hrr Page 17 of 17