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Home My WebLink AboutAir Quality Test v2 prt2 Logged on User:scthieken Page 57 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: 1022-157.R313.M26A Injection Volume: 25.00 Injection Type: Unknown Dilution Factor: 5.0 Instrument Method: AS22 ASAP Operator: scthieken /2L.Date/Time: 29-Oct-2022 / 04:29 Run Time: 14.50 30.0 17 Raphael1239#57 1022-157.R313.M26A ECD_1 PS 25.0 20.0 15.0 c 0 a m 10.0 0 00 5.0 0 U min -1.0 2.00 3.00 4.00 5.00 6.60 7.60 8.00 Time [min] Analyst Comment: No. Time Peak Name Area Height Conc Manually Assigned? Manipulated? min pS*min PS pg/mL 1 4A8 Chloride 0.012 0.036 0.11636 FALSE FALSE gFa Chromeleon(c)Dionex 1996-2009 �13AS-021420-RT-1303 Appendix C- Page 280 of 1178 9 Anions/Inter i Version 7.2.8.10783 Logged on User:scthieken Page 58 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: 1022-157.R313.M26A Injection Volume: 25.00 Injection Type: Unknown Dilution Factor: 5.0 Instrument Method: AS22 ASAP Operator: scthieken Date/Time: 29-Oct-2022 / 04:45 Run Time: 14.50 30.0 Raphael1239#58 1022-157.R313.M26A ECD_1 PS 25.0 20.0 15.0 c 0 Q 10.0 r` v 5.0 0 U min 2.00 3.60 4.00 5.00 6.60 7.60 8.00 Time [min] Analyst Comment: No. Time Peak Name Area Height Conc Manually Assigned? Manipulated? min pS*min PS pg/mL 1 4.48 Chloride 0.011 0.035 0.10871 FALSE FALSE NE13AS-021420-RT-1303 Appendix C-Page 281 of 1178 Chromeleon(c)Dionex 1996-2009 9 Anions/Integra[ORVersion 7.2.8.10783 Logged on User:scthieken Page 59 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: 1022-157.R314.M26A Injection Volume: 25.00 Injection Type: Unknown Dilution Factor: 5.0 Instrument Method: AS22 ASAP Operator: scthieken Date/Time: 29-Oct-2022 / 05:02 Run Time: 14.50 30.0 Raphae11239#59 1022-157.R314.M26A ECD_1 PS 25.0 20.0 uoi 15.0 c 0 0_ 0 a� 10.0 M LO rJ' rl' 5.0 0 U min 2.60 3.00 4.60 5.00 6.60 7.60 8.00 Time [min] Analyst Comment: No. Time Peak Name Area Height Conc Manually Assigned? Manipulated? min pS*min NS pg/mL 1 4.45 Chloride 0.010 0.031 0.10093 FALSE FALSE NgRl3AS-021420-RT-1303 Appendix C-Page 282 of 1178 Chromeleon(c)Dionex 1996-2009 9 Anions/Integrati�li Version 7.2.8.10783 Logged on User:scthieken Page 60 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: 1022-157.R314.M26A Injection Volume: 25.00 Injection Type: Unknown Dilution Factor: 5.0 Instrument Method: AS22 ASAP Operator: scthieken In". Date/Time: 29-Oct-2022 / 05:18 Run Time: 14.50 30.0 Raphael1239#60 1022-157.R314.M26A ECD_1 PS 25.0 20.0 05 15.0 c 0 a m 10.0 LO tM d' d' 5.0 0 U `1' min 2.60 3.60 4.60 5.60 6.60 7.60 8.60 Time [min] Analyst Comment: E2 No. Time Peak Name Area Height Conc Manually Assigned? Manipulated? min pS*min PS pg/mL 4.45 Chloride 0.009 0.032 0.09400 FALSE FALSE g MgR13AS-021420-RT-1303 Appendix C- Page 283 of 1178 Chromeleon(c)Dionex 1996-2009 9 Anions/Inter i Version 7.2.8.10783 Logged on User:scthieken Page 67 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: HPLCStds1433#SS Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method: AS22 ASAP Operator: scthieken I21.Date/Time: 29-Oct-2022 107:10 Run Time: 14.50 30.0 tol Raphael1239#67 [manually integrated] ECD_1 PS 25.0 20.0 uoi 15.0 C o o '. 0- a 10.0 a) .L 0 U 5.0 rr i min -1.0 2.00 3.00 4.00 5.60 6.00 7.00 8.60 Time [min] Analyst Comment: II SJT 10/31/2022 No. Time Peak Name Area Height Conc Manually Assigned? Manipulated? min pS*min PS pg/mL 1 4.44 Chloride 1.080 4.223 7.20478 FALSE TRUE NFn13AS-021420-RT-1303 Appendix C- Page 284 of 1178 Chromeleon(c)Dionex 1996-2009 9 Anions/Integr3tiaff Version 7.2.8.10783 Logged on User:scthieken Page 68 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: HPLCStds1433#SS Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method: AS22 ASAP Operator: scthieken In".Date/Time: 29-Oct-2022 / 07:27 Run Time: 14.50 30.0 Raphael1239#68 [manually integrated] ECD— 1 PS 25.0 20.0 ch 15.0 c Q Cl) 10.0 a> 0 U 5.0 min 2.00 3.00 4.00 5.00 6.00 7.00 8.00 Time [min] Analyst Comment: II SJT 10/31/2022 No. Time Peak Name Area Height Conic Manually Assigned? Manipulated? min pS*min PS pg/mL 1 4.44 Chloride 1.086 4.247 7.24552 FALSE TRUE g M,�R13AS-021420-RT-1303 Appendix C-Page 285 of 1178 Chromeleon(c)Dionex 1996-2009 9 Anions/Inter i Version 7.2.8.10783 Logged on User:scthieken Page 69 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: HPLCStds1433#RB Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method. AS22 ASAP Operator: scthieken In:Date/Time: 29-Oct-2022 / 07:43 Run Time: 14.50 30.0 no Raphael1239#69 HPLCStds1433#RB ECD_1 PS 25.0 20.0 v0i 15.0 c 0 n a� 10.0 ti w v 5.0 0 U min 2.60 3.00 4.60 5.00 6.60 7.00 8.00 Time [min] Analyst Comment: No. Time Peak Name Area Height Conc Manually Assigned? Manipulated? min NS*min PS pg/mL 1 4.50 Chloride 0.006 0.020 0.07686 FALSE FALSE g MRl3AS-021420-RT-1303 Appendix C-Page 286 of 1178 Chromeleon(c)Dionex 1996-2009 9 Anions/Inter I Version 7.2.8.10783 Logged on User:scthieken Page 70 of 107 Instrument:Raphael 10/31/2022 7:56 AM Sequence:Raphael1239 Peak Analysis Report Sample Name: HPLCStds1433#RB Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method: AS22 ASAP Operator: scthieken Date/Time: 29-Oct-2022 / 07:59 Run Time: 14.50 30.0 t; Raphael1239#70 HPLCStds1433#RB ECD_1 PS 25.0 20.0 ai 15.0 c 0 ,z a) 10.0 rn 5.0 0 U I `T I I 1 1 min -1.0 2.00 3.00 4.00 5.00 6.60 7.60 8.00 Time [min] Analyst Comment: No. Time Peak Name Area Height Conc Manually Assigned? Manipulated? min pS*min PS pg/mL 1 4.49 Chloride 0.006 0.020 0.07802 FALSE FALSE M,dRl3AS-021420-RT-1303 Appendix C- Page 287 of 1178 Chromeleon(c)Dionex 1996-2009 9 Anions/Integr I Version 7.2.8.10783 NE01 3AS-021420-RT-1 303 Appendix C-Page 288 of 1178 Logged on User:scthieken Page 4 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#1 Injection Volume: 26.00 Injection Type: Calibration Standard Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken Ini,Date/Time: 27-Oct-2022 11133 Run Time: 9.00 7.00 Mikey384#4 HPLCSTDs1419#1 ECD—1 6.00 5.00 U 4.00 0 U) 0 0 Q au) 3.00 m 2.00 N v m c 0 1.00 E E Q -0.10 2.00 3.60 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/ml- Assigned? Ammonia 2 4.267 Ammonia 0.060 0.265 0.19009 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-OiN�ffiatiAn021420-RT-1303 Appendix C- Page 289 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 5 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: - HPLCSTDs1419#1 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date/Time: 27-Oct-2022 / 11:44 Run Time: 9.00 7.00 Mikey384#5 HPLCSTDs1419#1 ECD_1 6.00 5.00 U 4.00 0 0 0_ 3.00 r u7 2.00 c� c 0 1.00 E E Q CIO -0.10 jr- 2.00 3.00 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.257 Ammonia 0.058 0.263 0.18459 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-027,t te,Ac g,021420-RT-1303 Appendix C-Page 290 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 6 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#2 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor. 1.0 Instrument Method. Mikey Cations 9min Operator scthieken Ini.Date/Time: 27-Oct-2022 / 1155 Run Time: 9.00 7.00 Mikey384#6 HPLCSTDs1419#2 ECD—1 6.00 5.00 U 4.00 a> c C o_ 3.00 LO r` N 2.00 a3 -E O E 1.00 E Q i ➢_� -0.10 �r 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/ml- Assigned? Ammonia 2 4.257 Ammonia 0.110 0.488 0.37941 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-Oj7l fttign Version 7.2.8.10783 021420-RT-1303 Appendix C-Page 291 of 1178 Logged on User:scthieken Page 7 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: ` HPLCSTDs1419#2 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken Ini.Date l Time:= 27-Oct-2022 / 12:05 Run Time: 9.00 7.00 Mikey384#7 HPLCSTDs1419#2 ECD 1 6.00 5.00 U 4.00 an 0 c 0 Q 3.00 0 CD N 2.00 rh (6 C O E 1.00 E Q -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.260 Ammonia 0.109 0.486 0.37620 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-0�1/,ltti(fi%!9n021420-RT-1303 Appendix C-Page 292 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 8 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#3 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor: 1.0 Instrument Method. Mikey Cations 9min Operator. scthieken In'.Date/Time: 27-00-2022 / 12:16 Run Time: 9.00'I 7.00 Mikey384#8 HPLCSTDs1419#3 ECD_1 6.00 5.00 = 4.00 a) in c 0 a aw 3.00 0 a� r N N 2.00 C O E E Q 1.00 c� -0.10 2.00 3.00 4.00 5.60 6.00 7.60 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually----[Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.270 Ammonia 0.207 0.876 0.76275 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-02NMatiQn021420-RT-1303 Appendix C-Page 293 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 9 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#3 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator, scthieken In'.Date/Time: 27-Oct-2022 / 12:27 Run Time: 9.00 7.00 Mikey384#9 HPLCSTDs1419#3 ECD 1 6.00 5.00 4.00 c 0 Q. 0 3.00 N rl' t6 2.00 GO E E Q 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/ml- Assigned? Ammonia 2 4.263 Ammonia 0.207 0.879 0.76486 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-O Nllnie 9-'021420-RT-1303 Appendix C-Page 294 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 10 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#4 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date/Time: 27-Oct-2022 / 1237 Run Time: 9.00 7.00 Mikey384#10 HPLCSTDs1419#4 ECD_1 6.00 5.00 s 4.00 a> c CD 0 °O 0- N 3.00 0' cc -E 0 E 2.00 E Q 1.00 i -0.10. I - I Jv_ 2.0o 3.00 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pglmL Assigned? Ammonia 2 4.280 Ammonia 0.357 1.430 1.41560 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTW NM7,92-021420-RT-1303 Appendix C-Page 295 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 11 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#4 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator ' scthieken In".Date/Time: 27-Oct-2022 ' 112:48 Run Time: 9.00 7.00 Mikey384#11 HPLCSTDs1419#4 ECD 1 6.00 5.00 s 4.00 a> c Cl) Q N m 3.00 E 0 E 2.00 E Q M 1.00 -0.10 2.60 3.00 4.60 5.60 6.60 7.60 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.273 Ammonia 0.357 1.435 1.41612 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N�Mati�n021420-RT-1303 Appendix C-Page 296 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 12 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#5s Injection:Volume: 25.00 Injection Type: Calibration Standard Dilution Factor. 1.0 Instrument Method. Mikey Cations 9min Operator scthieken In".Date/Time: 27-Oct-2022 / 1259 Run Time: 9.00 7.00 Mikey384#12 HPLCSTDs1419#5 ECD_1 6.00 5.00 0 ao N Nr U 4.00 m 'c a) o E o E a� 3.00 Q CIO 2.00 1.00 -0.10 2.00 3.60 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.280 Ammonia 0.719 2.670 3.28033 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-Oa4(1te19atign021420-RT-1303 Appendix C- Page 297 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 13 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#5 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In".Date/Time: 27-Oct-2022 / 13:09 Run Time: 9.00 7.00 Mikey384#13 HPLCSTDs1419#5 ECD_1 6.00 5.00 M N d' Q 4.00 m E a) o E o E 3.00 2.00 1.00 -0.10 2.00 3.00 4.60 5.00 6.60 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS Ng/mL Assigned? Ammonia 2 4.283 Ammonia 0.719 2.671 3.28397 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N9atiQn021420-RT-1303 Appendix C-Page 298 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 14 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#6t Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date/Time: ---Oct-2022 1 13 20 Run Time: 9.00 7.00 Mikey384#14 HPLCSTDs1419#6 ECD_1 r` 6.00 N m 0 5.00 E E Q s 4.00 a� c 0 ro 3.00 of 2.00 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time min Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.277 Ammonia 1.230 4.301 6.61881 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-O l�n(e'Ig 092021420-RT-1303 Appendix C-Page 299 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 15 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#6 Injection Volume: 25.00 Injection Type: : Calibration Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken ln'.Date/Time: 27-Oct-2022' 113:31 Run Time: 9.00 Mikey384#15 HPLCSTDs1419#6 ECD_1 7.00 0 rn 6.00 ry m c 0 5.00 E E Q s 4.00 0 0 0 u) 3.00 2.00 1.00 -0.10 2.00 3.60 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.290 Ammonia 1.233 4.278 6.63608 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-09N(Ui(e' 9-'021420-RT-1303 Appendix C-Page 300 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 16 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#7r Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor 1.0 Instrument Method. Mikey Cations 9min Operator." scthieken In:Date/Time: 27-Oct-2022 / 1341 Run Time: 9.00' 7.00 Mikey384#16 HPLCSTDs1419#7 ECD_1 0 00 N V I 6.00 E E Q 5.00 N y 4.00 a) U) c 0 ID 3.00 w 2.00 1.00 -0.10 2.00 3.60 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.280 Ammonia 1.852 6.137 11.78079 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CT1-02N/1fffi%!9'-021420-RT-1303 Appendix C-Page 301 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 17 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#7 Injection Volume: 25.00 Injection Type: Calibration Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min ` Operator. ' scthieken In'.Date/Time: 27-Oct-2022 / 13:52` Run Time: 9.00 7.00 Mikey384#17 HPLCSTDs1419#7 ECD— 1 r` 00 N V I 6.00 E E 5.00 N s 4.00 c C aau) 3.00 ry 2.00 1.00 -0.10 2.00 3.60 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.287 Ammonia 1.855 6.125 11.80881 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-94/ft 92021420-RT-1303 Appendix C- Page 302 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 18 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#RB Injection Volume. 25.00 Injection Type: Check Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9m1n Operator. scthieken In.Date/Time: 27-Oct-2022 / 14 03 Run Time: 9.00 7.00 Mikey384#18 HPLCSTDs1419#RB ECD_1 6.00 5.00 z 4.00 C Cn c 0 In 3.00 2.00 N r1' cu 1.00 0 E E Q i -0.10-1 T 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.247 Ammonia 0.002 1 0.008 n.a. FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-OJN/ eatiQn Version 7.2.8.10783 021420-RT-1303 Appendix C- Page 303 of 1178 Logged on User:scthieken Page 19 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#RB Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method., Mikey Cations 9min Operator scthieken Mi.Date/Time: 27-Oct-2022 / 14:13 Run Time: 9.00 7.00 Mikey384#19 HPLCSTDs1419#RB ECD_1 6.00 5.00 U 4.00 a) c 0 0- 3.00 ry 2.00 N [t N G 1.00 E E Q i . -0.10 2.00 3.60 4.00 5.00 6.60 7.60 Time [min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.253 Ammonia 0.002 0.008 n.a. FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-O7N/IrMM'021420-RT-1303 Appendix C-Page 304 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 20 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#SS Injection Volume 25.00 Injection Type: Check Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken Date/Time: 27-Oct-2022 / 1424 Run Time: 9.00 7.00 no Mikey384#20 HPLCSTDs1419#SS ECD_1 6.00 5.00 s 4.00 y N C O O. 3.00 Coof E E Q 2.00 1.00 i -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.277 Ammonia 0.446 1 1.748 1.83639 FALSE FALSE Chromeleon(c)Dionex 1996-2009 Version 7.2.8.10783 CTM-O�NLlnieatiAn021420-RT-1303 Appendix C- Page 305 of 1178 Logged on User:scthieken Page 21 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#SS Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator scthieken Id.Date/Time: 27-Oct-2022 1 14:35 Run Time: 9.00 7.00 Mikey384#21 HPLCSTDs1419#SS ECD_1 6.00 5.00 U 4.00 M N W U) N O m 3.00 o' E E a 2.00 Co 1.00 i i -0.10 2.60 3.60 4.00 5.60 6.60 7.60 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/ml- Assigned? Ammonia 2 4.283 Ammonia 0.446 1.746 1.83698 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-024M92021420-RT-1303 Appendix C-Page 306 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 1nvu Instrument:Mikey 10/28/2022 7:34Am Senueomzm/keyuv* K0|key Calibration Table No. Iniection Name In"ect Time Pos. Level Ref.Amount Calibration Point Status DiI.Factor Volume Ammonia Ammonia Detection Parameters Ret. Time Param. Name Param.Value Inj.Type Channel Always Baseline Noise Auto Range Off Any All Channels Always Baseline Noise Start Time 0.231 [min] Any All Channels Always Baseline Noise End Time 1.277[min] Any All Channels Always Cobra Smoothing Width Auto Any All Channels Always Consider Void Peak Off Any All Channels 0.000 Tailing Sensitivity Factor 0.100 Any All Channels 0.000 Rider Detection Off Any All Channels 0.000 Minimum Area Auto Any All Channels 0.000 Inhibit Integration On Any All Channels 2.900 Inhibit Integration Off Any All Channels ohromownn 1996-2009 cTm-027 ration Details vorsic 8.10783 Ni \S-021420-RT-1303 AppendixC- ,307of1178 Logged( w:scthieken le 2 of 2 Instrume. .,key 10/28/2 7:34 AM Sequence:Mikey384 Mikey Calibration Batch Report Sequence: Mikey384 Injection Volume: 25.00 Instrument Method. Mikey Cations 9min Operator.- ' scthieken Inj.Date/Time: 27-Oct-2022 / 13:41 Run Time: 9 Calibration Summary Peak Name Eval.Type Cal.Type Points Offset Slope Curve Coeff.Det. (CO) C9 C2 % Ammonia Area Quad WithOffset 1/A 14.000 -0.022 3.472 1.565 99.998 AVERAGE: -0.0224 3.4719 1.5655 1 99.9980 Injection Name Ret.Time Area Height Amount 14.0 Ammonia External ECD_1 min pS*min PS pg/mL pg/ml- ECD 1 ECD ,1 ECD 1 ECD;1 Ammonia Ammonia Ammonia Ammonia 12.0 HPLCSTDs1419#1 4.267 0.0596 0.265 0.190 HPLCSTDs1419#1 4.257 0.0581 0.263 0.185 10.0 HPLCSTDsl419#2 4.257 0.1103 0.488 0.379 HPLCSTDs1419#2 4.260 0.1094 0.486 0.376 8.0 HPLCSTDs1419#3 4.270 0.2069 0.876 0.763 HPLCSTDs1419#3 4.263 0.2074 0.879 0.765 6.0 HPLCSTDs1419#4 4.280 0.3568 1.430 1.416 HPLCSTDs1419#4 4.273 0.3569 1.435 1.416 HPLCSTDs1419#5 4.280 0.7185 2.670 3.280 4.0 HPLCSTDs1419#5 4.283 0.7191 2.671 3.284 HPLCSTDs1419#6 4.277 1.2303 4.301 6.619 2.0 HPLCSTDs1419#6 4.290 1.2327 4.278 6.636 pS*min HPLCSTDs1419#7 4.280 1.8524 6.137 11.781 0.0 HPLCSTDs1419#7 1 4.287 1 1.8554 1 6.125 1 11.809 1 0.00 1.00 2.00 NF 1 �, g21420-RT-1303 Appendix C- Page 308 of 1178 Chromeleon(c)Dionex 1996-2009 CTM t)L7�a i r ti n Version 7.2.8.10783 Logged on User:scthieken Page 18 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419'#RB Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In Date/Time: 27-Oct-2022 1 1403 Run Time: 9.00' 7.00 Mikey384#18 HPLCSTDs1419#RB ECD_1 6.00 5.00 C 4.00 a> E C a iv 3.00 2.00 v N [Y (6 E 1.00 E E Q -0.10 2.00 3.60 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS"min pS pg/mL Assigned? Ammonia 2 4.247 Ammonia 0.002 0.008 n.a. FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-N/lVM92021420-RT-1303 Appendix C- Page 309 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 19 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#RB Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator.- scthieken In'.Date/Time: 27-Oct-2022 / 14:13 Run Time: 9.00 7.00 nk Mikey384#19 HPLCSTDs1419#RB ECD_1 6.00 5.00 4.00 a) 0 0 3.00 2.00 LO N (0 C 1.00 0 E E Q -0.10 2.00 3.60 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.253 Ammonia 0.002 0.008 n.a. FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-OWN/ e' 9-2021420-RT-1303 Appendix C- Page 310 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 20 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#SS Injection Volume 25.00 Injection Type: Check Standard Dilution Factor. 1.0 Instrument Method. Mikey Cations 9min Operator. scthieken In'.Date/Time: 27-Oct-2022 / 1424 Run Time: 9.00 7.00 Mikey384#20 HPLCSTDsl419#SS ECD_1 6.00 5.00 C 4.00 r` a r N N G O Q 3.00 0 E E Q 2.00 00 1.00 -0.10 2.60 3.00 4.00 5.00 6.00 7,00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.277 Ammonia 0.446 1.748 1.83639 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 Version 7.2.8.10783 CTM-02N/ eatiQn021420-RT-1303 Appendix C- Page 311 of 1178 Logged on User:scthieken Page 21 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSMs1419#SS Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. ' scthieken Id.Date/Time: 27-Oct-2022 114:35 Run Time: 9.00 7.00 07 Mikey384#21 HPLCSTDs1419#SS ECD_1 6.00 5.00 s 4.00 M N 00 E N O 3.00 0 E E Q 2.00 M 1.00 i -0.10 2.00 3.00 4.60 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min ps*min PS pg/mL Assigned? Ammonia 2 4.283 Ammonia 0.446 1.746 1.83698 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-O�N/1ntelg� 92021420-RT-1303 Appendix C- Page 312 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 22 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.1R111.CTM-027 Injection Volume: 25.00 Injection Type: Unknown! Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator scthieken In'.Date/Time. 27-Oct-2022 / 14:45 Run Time: 9.00 7.00 Mikey384#22 [manually integrated] 1022-157.R111.CTM-027 ECD_1 6.00 5.00 LO N (a �. 4.00 E m E � Q c 0 W 3.00 0_ 2.00 1.00 -0.10 2.00 3.00 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: II SJT 10/28/2022 Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.250 Ammonia 0.887 3.023 4.28692 FALSE TRUE Chromeleon(c)Dionex 1996-2009 CTM-94f e,� g'-021420-RT-1303 Appendix C-Page 313 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 23 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R111.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator scthieken In'.Date/Time: 27-Oct-2022 / 14:56 Run Time: 9.00 7.00 71 Mikey384#23[manually integrated] 1022-157.R111.CTM-027 ECD_1 6.00 5.00 LO N G Z 4.00 N E fq Q G O N a) 3.00 o' 2.00 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: II SJT 10/28/2022 Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min ps*min PS pg/mL Assigned? Ammonia 2 4.253 Ammonia 0.887 3.025 4.29002 FALSE I TRUE Chromeleon(c)Dionex 1996-2009 CTM-OJ l/,trMatiRn021420-RT-1303 Appendix C-Page 314 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 24 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157R111-MSCTM-027 ;Injection Volume:- 25.00 Injection Type. Unknown Dilution Factor. 1.0 Instrument Method. Mikey Cations 9min Operator. scthieken In:Date/Time: 27-Oct-2022 / 15:07 Run Time: 9.00' 7.00 Mikey384#24[manually integrated] ECD_1 co LO N 6.00 M C O E E Q 5.00 : 4.00 u> Cn c 0 3.00 2.00 1.00 i -0.10 2.00 3.00 4.60 5.60 6.00 7.00 Time[min] Analyst Comment: II SJT 10/28/2022 Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min Ns*min Ns Ng/mL Assigned? Ammonia 2 4.253 Ammonia 1.502 4.824 8.72668 FALSE I TRUE Chromeleon(c)Dionex 1996-2009 CTM-02N��e'Ig�ati9n021420-RTA 303 Appendix C-Page 315 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 25 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R111-MS.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method." Mikey Cations 9min Operator scthieken Ini.Date/Time: 27-Oct-2022 / 15:17 Run Time: 9.00 7.00 Mikey384#25[manually integrated] ECD_1 Cl) LO N V 6.0D T C O E E Q 5.00 a 4.00 oD c O 3.00 o' 2.00 1.00 i -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: II SJT 10/28/2022 Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS"min PS pg/mL Assigned? Ammonia 2 4.253 Ammonia 1.503 4.833 8.73485 FALSE I TRUE Chromeleon(c)Dionex 1996-2009 CTM-N� e'I %ign021420-RT-1303 Appendix C- Page 316 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 26 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R111-MSD.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken In Date/Time: 27-Oct-2022 / 15:28 Run Time: 9.00 7.00 Mikey384#26[manually integrated] ECD_1 CO N 6.00 W .0 O E }_ Q 5.00 U 4.00 ro c O m 3.00 2.00 1.00 i -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: II SJT 10/28/2022 Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pgImL Assigned? Ammonia 2 4.253 Ammonia 1.516 4.852 8.84258 FALSE TRUE Chromeleon(c)Dionex 1996-2009 Version 7.2.8.10783 CTM-02Nl�tr�eati�n021420-RT-1303 Appendix C-Page 317 of 1178 Logged on User:scthieken Page 27 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R111-MSD.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken In'.Date/Time: 27-Oct-2022 1 15:39 Run Time: 9.00 7.00 71 Mikey384#27[manually integrated] ECD_1 Cl) u7 N V' 6.00 f9 C O E E Q 5.00 U 4.00 aD c 0 3.00 o' 2.00 1.00 i -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: II SJT 10/28/2022 Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.253 Ammonia 1.515 4.858 8.82659 FALSE TRUE Chromeleon(c)Dionex 1996-2009 CTM-02N/1r�te'Iq atiAn021420-RT-1303 Appendix C-Page 318 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 28 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R112.CTM-027 Injection iVolume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator scthieken In;Date/Time: 27-Oct-2022 / 1549 Run Time: 9.00 7.00 Mikey384#28 1022-157.R112.CTM-027 ECD_1 6.00 5.00 Q 4.00 (n c C o_ (u) 3.00 ao 2.00 v c� c 0 1.00 E E Q R� -0.10 r—..._.. .__.... 2.00 3.60 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.187 Ammonia 0.050 0.182 0.15401 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N/1nieV92-021420-RT-1303 Appendix C-Page 319 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 29 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R1I2.CTM-027 Injection Volume: 25.00 r Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken Id.Date/Time:` 27-Oct-2022 / 16:00 Run Time: 9.00 7.00 71 Mikey384#29 1022-157.R112.CTM-027 ECD_1 6.00 5.00 u) 4.00 a> c 0 0_ W 3.00 ry r` r` 2.00 v m 'c 0 1.00 E Q R� -0.10 J. 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min ps*min PS pg/mL Assigned? Ammonia 2 4.177 Ammonia 0.050 0.182 0.15368 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-1:�llntelcatiRn021420-RT-1303 Appendix C- Page 320 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 30 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157R113.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator scthieken In:Date/Time: 27-Oct-2022 / 1611 Run Time: 9.00 7.00 Mikey384#30 1022-157.R113.CTM-027 ECD_1 6.00 5.00 4.00 a> Cn c C Q 3.00 M 2.00 m 1.00 E E Q -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min uS*min PS pg/mL Assigned? Ammonia 2 4.153 Ammonia 0.017 0.056 0.03590 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-94MVI-021420-RT-1303 Appendix C-Page 321 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 31 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R713.CTM-027 Injection Volume: 25.00 Injection Type., Unknown Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date/Time:` 27-Oct-2022 / 16:21' Run Time: 9.00 7.00 11 Mikey384#31 1022-157.R113.CTM-027 ECD_1 6.00 5.00 Q 4.00 m W c 0 0. 3.00 of 0 2.00 v m 1.00 E E Q -0.10 r` 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min ps*min PS pg/mL Assigned? Ammonia 2 4.150 Ammonia 0.017 0.056 0.03647 FALSE FALSE Chromeleon(c)Dionex 1996-2009 1TM-O2NLIrtte' X9'-021420-RT-1303 Appendix C- Page 322 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 32 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R114.CTM-027 Injection Volume: 25.00 Injection Type: Unknown' Dilution Factor: 1.0 Instrument Method. Mikey Cations 9min Operator. scthieken In:Date/Time: 27-Oct-2022 / 16:32 Run Time: 9.00 7.00 Mikey384#32 1022-157.R114.CTM-027 ECD_1 6.00 5.00 s 4.00 0 Cn c 0 0- 3.00 a= 2.00 m N V 'Co 1.00 0 E E i Q i 21 ��- -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.263 Ammonia 0.004 0.016 n.a. FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N/LW92021420-RT-1303 Appendix C-Page 323 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 33 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R114.CTM-027 injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator scthieken In".Date/Time: 27-Oct-2022 / 16:43 Run Time: ' 9.00 7.00 Mikey384#33 1022-157.R114.CTM-027 ECD_1 6.00 5.00 U 4.00 0 U) c 0 Q a i 3.00 tr 2.00 N CO C 1.00 E E i^ Q -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.257 Ammonia 0.004 0.017 n.a. FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-O:TV7/1EVW92-021420-RT-1303 Appendix C-Page 324 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 34 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157!R211.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator scthieken In.Date/Time: 27-Oct-2022 / 16 53 Run Time: 9.00 7.00 Mikey384#34 1022-157.R211.CTM-027 ECD—1 6.00 5.00 0 N = 4.00 c 0 W E c E 0 Q 0 aa) 3.00 tY 2.00 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.260 Ammonia 0.805 2.769 3.78956 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-94 Vh%!9-'021420-RT-1303 Appendix C- Page 325 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 35 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R211.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor, 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date -Time:' 27-Oct--022 1 17:04 Run Time: 9.00 7.00 71 Mikey384#35 1022-157.R211.CTM-027 ECD_1 6.00 5.00 M LO N ,d. U) 4.00 0 m E C E 0. Q aa) 3.00 ry 2.00 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS Ng/mL Assigned? Ammonia 2 4.253 Ammonia 0.806 2.771 3.79555 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-N/1ENW-021420-RT-1303 Appendix C-Page 326 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 36 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157R212.CTM-027 Injection Volume:` 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method. Mikey Cations 9min Operator scthieken In'.Date/Time: 27-Oct-2022 / 17:15 Run Time: 9.00 7.00 17 Mikey384#36 1022-157.R212.CTM-027 ECD_1 6.00 5.00 y 4.00 aU CD c 0 0- W 3.00 0 2.00 v m 0 1.00 E E Q -0.10 -r 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.190 Ammonia 0.043 1 0.156 0.13039 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-OWN/EtrM092021420-RT-1303 Appendix C-Page 327 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 37 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R212.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken Ini.Date/Time: 27-Oct-2022 / 17:25 Run Time: 9.00 7.00 Mikey384#37 1022-157.R212.CTM-027 ECD_1 6.00 5.00 4.00 m c 0 Q ID 3.00 o' Cl) 2.00 00 C O 1.00 E E Q -0.10 2.00 3.00 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.183 Ammonia 0.043 0.157 0.13024 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-0IN/MW-021420-RT-1303 Appendix C-Page 328 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 38 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157R213.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date/Time: 27-Oct-2022 / 17:36 Run Time: 9.00 7 00 Mikey384#38 1022-157.R213.CTM-027 ECD_1 6.00 5.00 y 4.00 a> w c 0 a a0i 3.00 ry 2.00 _r- v 1.00 0 E Q -0.10 2.00 3.00 4.60 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min NS Ng/ml- Assigned? Ammonia 2 4.157 Ammonia 0.008 0.026 0.00503 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-OiV7/ eatiQn021420-RT-1303 Appendix C-Page 329 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 39 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022457.11213.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken In'.Date/Time: 27-Oct-2022 / 17:47 Run Time: 9.00 7.00 17 Mikey384#39 1022-157.R213.CTM-027 ECD_1 6.00 5.00 4.00 a) w c 0 a aui 3.00 2.00 Cl) v .Co c 1.00 0 E E Q -0.10 2.00 3.00 4.60 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.153 Ammonia 0.008 0.026 0.00510 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-027.LInieACgtiAn021420-RT-1303 Appendix C- Page 330 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 40 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157R214.CTM-027 Injection Volume: 2500 Injection Type: Unknown Dilution Factor., 1.0 Instrument Method: Mikey Cations 9min Operator., scthieken ln'.Date/Time: 27-Oct-2022 / 17:57 Run Time: 9.00 7.00 Mikey384#40 1022-157.R214.CTM-027 ECD—1 6.00 5.00 C 4.00 a> U) c C Q a(i 3.00 2.00 N V (0 .0 1.00 O E E a -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min ps*min Ns pg/mL Assigned? Ammonia 2 4.267 Ammonia 0.004 0.017 n.a. FALSE FALSE Chromeleon(c)Dionex 1996-2009 ITM-07r71/tEtMV9-2021420-RT-1303 Appendix C-Page 331 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 41 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R214.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken Id.Date/lime: 27-Oct-2022 / 18:08 Run rime: 9.00 7.00 Mikey384#41 1022-157.R214.CTM-027 ECD_1 6.00 5.00 s 4.00 ah a c 0 Q 3.00 2.00 c(o N V (6 C 1.00 E E Q C I i -0.10 2.60 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min ps*min PS pg/mL Assigned? Ammonia 2 4.267 Ammonia 0.004 0.017 n.a. FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-OaNLlM92 0 21 42 0-RT-1303 Appendix C-Page 332 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 42 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#4 Injection'Volume 2500 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator.• scthieken In.Date/Time: 27-Oct-2022 / 18 19 Run Time: 9.00 7.00 `4 Mikey384#42 HPLCSTDs1419#4 ECD_1 6.00 5.00 U 4.00 a> m r` c Cp O N Q U) 3.00 .c O E 2.00 E 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time(min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/mL Assigned? Ammonia 2 4.287 Ammonia 0.355 1.427 1.40856 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N�ue1g9tign Version 7.2.8.10783 021420-RT-1303 Appendix C-Page 333 of 1178 Logged on User:scthieken Page 43 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name; HPLCSTDs1419#4 Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken Id.Date/Time: 27-Oct-2022 / 18:29 Run Time: 9.00 7.00 Mikey384#43 HPLCSTDs1419#4 ECD_1 6.00 5.00 U 4.00 c rn 0 N u 3.00 `n o m .E 0 E 2.00 E Q 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS Ng/ml- Assigned? Ammonia 2 4.293 Ammonia 0.355 1.423 1.40888 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02NMV-'021420-RT-1303 Appendix C-Page 334 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 44 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157R311.CTM-027 ;Injection Volume: 25.00 Injection Type: Unknown Dilution Factor.' 1.0 Instrument Method. Mikey Cations 9min Operator, scthieken In.Date/Time: 27-Oct-2022 / 18:40 Run Time: 9.00 7.00 Mikey384#44 1022-157.R311.CTM-027 ECD_1 6.00 5.00 M 4.00 N a> `r c m o CL 3.00 E E Q 2.00 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min ps*min PS pg/mL Assigned? Ammonia 2 4.253 Ammonia 0.599 2.126 2.61901 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-Oj4LIntelgatign021420-RT-1303 Appendix C-Page 335 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 45 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: ! 1022-157.R31I.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor. 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken Ini.Date/Time: 27-Oct-2022 1 18:51'+ Run Time: 9.00 7.00 17 Mikey384#45 1022-157.R311.CTM-027 ECD_1 6.00 5.00 cl) CQ 4.00 C\! c O G tY 3.00 E Q 00 2.00 1.00 -0.10 2.00 3.00 4.00 5.00 6.00 7.60 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pglmL Assigned? Ammonia 2 4.253 Ammonia 0.600 2.128 2.62206 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-ORnie'Iq 92-021420-RT-1303 Appendix C- Page 336 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 46 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157R312.CTM-027 Injection Volume: 'r 25.00 Injection Type. Unknown Dilution Factor. 1.0 Instrument Method. Mikey Cations 9min Operator: scthieken In'.Date/Time: 27-Oct-2022 / 19:01 Run Time: 9.00 7.00 Mikey384#46 1022-157.R312.CTM-027 ECD_1 6.00 5.00 z 4.00 0 w c 0 0- aui 3.00 ne r` 2.00 v co 'c 1.00 0 E E Q -0.10 2.00 3.60 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.197 Ammonia 0.030 1 0.113 0.08249 FALSE FALSE Chromeleon(c)Dionex 1996-2009 Version 7.2.8.10783 CTM-O�NLlntegLatiAn021420-RT-1303 Appendix C-Page 337 of 1178 Logged on User:scthieken Page 47 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R312.CTM-027 Injection Volume: 25.00 Injection Type: Unknown Dilution✓=actor. 1.0 Instrument Method: Mikey Cations 9min Operator, scthieken In'.Date/Time: 27-Oct-2022 / 19:12< Run Time: 9.00 7.00 17 Mikey384#47 1022-157.R312.CTM-027 ECD_1 6.00 5.00 z 4.00 0 c 0 a cn 3.00 0 2.00 v m 1.00 E E E Q -0.10 2.00 3.60 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min uS*min PS pg/mL Assigned? Ammonia 2 4.190 Ammonia 0.030 0.113 0.08204 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-OJN�ffiatign021420-RT-1303 Appendix C- Page 338 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 48 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R313.CTM-027 Injection Volume: ' 25.00 Injection Type: Unknown Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date/Time: 27-Oct-2022 / 1923 Run Time: 9.00 7.00 Mikey384#48 1022-157.R313.CTM-027 ECD—1 6.00 5.00 y 4.00 Cn C c 0 n W 3.00 ry 2.00 _0 v m c 1.00 E E Q -0.10 _._..... ®_.. 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min NS Ng/mL Assigned? Ammonia 2 4.170 Ammonia 0.009 0.030 0.00768 FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-N/�e'Ig�ati9n021420-RT-1303 Appendix C-Page 339 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 49 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 11022-157.11313.CTM-027 Injection Volume. 25.00 Injection Type: Unknown Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken Ini,Date/Time: 27-Oct-2022 1 19:33 i Run Time: 9.00 7.00- 1? Mikey384#49 1022-157.R313.CTM-027 ECD-1 6.00- 5.00- Q) 4.00- a) (n CL 3.00- 2.00- .ca C 1.00- 0 E E -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min PS*Min PS tig/mL Assigned? I I Ammonia 2 4.177 Ammonia 0.009 0.030 0.00737 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTMIRVW92021420-RT-1 303 Appendix C-Page 340 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 50 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R314.CTM=027 Injection Volume: 25.00 Injection Type: Unknown Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken In".Date/Time: 27-Oct-2022 / 1944 Run Time: 9.00 7.00 Mikey384#50 1022-157.R314.CTM-027 ECD_1 6.00 5.00 z 4.00 a> c 0 0- 3.00 2.00 Qoo N (6 1.00 0 E E Q -0.10 �- 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height I Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.267 Ammonia 0.003 0.011 n.a. FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-OsN�&CVgn021420-RT-1303 Appendix C-Page 341 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 51 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: 1022-157.R314.CTM-027 Injection Volume: 25.00 Injection Type: ' Unknown Dilution Factor 1.0 Instrument Method: Mikey Cations 9min Operator scthieken ln'.Date/Time:I 27-Oct-2022 / 19:55 Run Time: 9.00 7.00 Mikey384#51 1022-157.R314.CTM-027 ECD_1 6.00 5.00 s 4.00 c C +s In 3.00 2.00 coo N V N 1.00. 0 E Q -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS ug/mL Assigned? Ammonia 2 4.260 Ammonia 0.003 0.011 n.a. FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N�M 92021420-RT-1303 Appendix C-Page 342 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 52 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#RB Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor. 1.0 < Instrument Method: Mikey Cations 9min Operator: scthieken In.Date/Time: 27-Oct-2022 / 20:05 Run Time: 9.00 7.00 Mikey384#52 HPLCSTDs1419#RB ECD_1 6.00 5.00 U 4.00 C (n G O Q ai 3.00 2.00 Ln N `7 m 1.00 0 E E Q C�J I ' -0.10 —� 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS Ng/mL Assigned? Ammonia 2 4.253 Ammonia 0.002 1 0.008 n.a. FALSE FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N�ffiatiQn Version 7.2.8.10783 021420-RT-1303 Appendix C- Page 343 of 1178 Logged on User:scthieken Page 53 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#RB r Injection Volume: 25.00 injection Type: Check Standard Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator. scthieken In'.Date/Time: 27-Oct-2022 1 20:16 Run Time: ' 9.00 7.00 no Mikey384#53 HPLCSTDs1419#RB ECD_1 6.00 5.00 C/) 4.00 c 0 Q 3.00 ry 2.00 u-) N Co C 1.00 0 E Q -0.10 2.00 3.00 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min PS*min PS pg/mL Assigned? Ammonia 2 4.257 Ammonia 0.002 0.008 n.a. FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-02N/ltiteAlW-021420-RT-1303 Appendix C- Page 344 of 1178 version 7.2.8.10783 Logged on User:scthieken Page 54 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#SS Injection;Volume: 25.00 Injection Type: Check Standard Dilution Factor: 1.0 Instrument Method: Mikey Cations 9min Operator: scthieken in'.Date/Time: 27-Oct-2022 / 2027 Run Time: 9.00 7.00 Mikey384#54 HPLCSTDs1419#SS ECD_1 6.00 5.00 U 4.00 0 rn N C O O- 3.00 M of o E E Q 2.00 1.00 -0.10 2.00 3.60 4.00 5.00 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min pS*min PS pg/mL Assigned? Ammonia 2 4.290 Ammonia 0.444 1.742 1.82900 J FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-0 N�MV92021420-RT-1303 Appendix C-Page 345 of 1178 Version 7.2.8.10783 Logged on User:scthieken Page 55 of 56 Instrument:Mikey 10/28/2022 7:35 AM Sequence:Mikey384 Peak Analysis Report Sample Name: HPLCSTDs1419#SS Injection Volume: 25.00 Injection Type: Check Standard Dilution Factor. 1.0 Instrument Method. Mikey Cations 9min Operator scthieken In'.Date/Time: 27-Oct-2022 / 20:37 Run Time: 9.00 7.00 Mikey384#55 HPLCSTDs1419#SS ECD_1 6.00 5.00 = 4.00 0 m °') C N O m 3.00 C 0_ E E Q 2.00 CIO 1.00 -0.10 2.00 3.60 4.00 5.60 6.00 7.00 Time[min] Analyst Comment: Peak Name No. Time Peak Name Area Height Amount Manually Manipulated? min NS*min PS pg/ml- Assigned? Ammonia 2 4.290 Ammonia 0.445 1.744 1.83034 FALSE I FALSE Chromeleon(c)Dionex 1996-2009 CTM-024M 92021420-RT-1303 Appendix C-Page 346 of 1178 Version 7.2.8.10783 `h * s Is The Last Page Of • R--i\j L i NE013AS-021420-RT-1303 Appendix C- Page 347 of 1178 Montrose Air Quality Services, LLC — Newburyport 2 New Pasture Road Unit #5 Newburyport, MA 01950 Wheelabrator North Andover Client Project # J- 2120 Analytical Report ( 1122-053) EPA Method 202 Condensable Particulate Matter Phone: (919) 850 -4392 / Fax: (919) 850 -9012 / www.enthalpy.com -� 800-1 Capitola Drive Durham, NC 27713-4385 I certify that to the best of my knowledge all analytical data presented in this report: • Have been checked for completeness • Are accurate, error-free, and legible • Have been conducted in accordance with approved protocol, and that all deviations and analytical problems are summarized in the appropriate narrative(s) This analytical report was prepared in Portable Document Format (.PDF) and contains 14 pages. QA Review Pei Furrried by--Jerlttirur Buwkei Report Issued: 11/23/2022 x EA# 1122-053 Page 2 of 14 NE01 3AS-021420-RT-1 303 Appendix C-Page 349 of 1178 NE01 3AS-021420-RT-1 303 Appendix C-Page 350 of 1178 Enthalpy Analytical Company: Montrose Air Quality Services, LLC - Newburyport Job No.: 1122-053 EPA Method 202 Analysis Client No.: PROJ-021420 Site: Wheelabrator North Andover Summary Report Net Organic Catch (mg) 0.70 0.35 0.23 0.18 Corrected Inorganic(mg) 19.07 14.29 11.89 3.46 CPM (mg) 19.8 14.6 12.1 3.6 TB Corrected CPM (mg) 17.8 12.6 10.1 1122-053 EPA Method 202 NE01 3AS-021420-RT-1 303 Appendix C-Page 351 of 1178 r NE013AS-021420-RT-1303 Appendix C- Page 352 of 1178 Enthalpy Analytical Company:Montrose Air Quality Services,LLC-Newburyport Job No.:1122-053 EPA Method 202 Analysis Client No.:PROJ-021420 Site:Wheelabrator North Andover Results R1 R2 R3 FTRB Organic Beaker Number 38102 38103 38104 38105 Initial Solvent Volume(ml-) 65 114 74 40 Org.Final Weight 1 (g) 2.507054 11/19/22 09:03 2.495766 11/19/22 09:05 2.494123 11/19/22 09:05 2.506206 11/19/22 09:06 Ong.Final Weight 2(g) 2.506928 11/21/22 09:55 2.495592 11/21/22 09:55 2.493924 11/21/22 09:56 2.505993 11/21/22 09:56 Tare(g) 2.506225 11/11/22 16:35 2.495238 11/11/22 16:36 2.493691 11/11/22 16:36 2.505812 11/11/22 16:37 Organic Catch(mg) 0.70 0.35 0.23 0.18 Inorganic Beaker Number 38097 38098 38099 38100 Weight 1(g) 2.519637 11/19/22 09:01 2.512858 11/19/22 09:02 2.515265 11/19/22 09:02 2.514864 11/19/22 09:02 Weight 2(g) 2.519492 11/21/22 09:49 2.512371 11/21/22 09:51 2.515029 11/21/22 09:51 2.515255 11/21/22 09:54 Tare(g) 2.500421 11/9/22 19:32 2.498077 1119/22 19:33 2.503136 11/9/22 19:33 2.511790 11/11/22 16:33 Initial Water Vol.(mL) 631 618 550 252 Water Added by Lab(ml-) 75 75 75 75 Resuspend Vol.(ml-) 100 100 100 100 Net Inorganic Catch(mg) 19.07 14.29 11.89 3.46 Titrant Normality 0.10 0.10 0.10 0.10 Titrant Vol.(mL) 0.08 0.10 0.11 0.03 Titrant Blank Vol.(mL) 0.08 0.08 0.08 0.08 Corrected Inorganic(mg) 19.07 14.29 11.89 3.46 Condensable Particulate(mg) 19.77 14.65 12.13 3.65 TB Corrected CPM(mg) 17.77 12.65 10.13 1122-053 EPA Method 202 NE01 3AS-021420-RT-1 303 Appendix C-Page 353 of 1178 Enthalpy Analytical Company:Montrose Air Quality Services,LLC-Newburyport Job No.: 1122-053 EPA Method 202 Analysis Client No.:PROJ-021420 Site:Wheelabrator North Andover Reagent In House Hexane Acetone Water Beaker 38107 38106 38101 Weight 1 (g) 2.503883 11/19/22 09:07 2.494530 11/19/22 09:06 2.494152 11/19/22 09:03 Weight 2(g) 2.503890 11/21/22 09:57 2.494527 11/21/22 09:57 2.494055 11/21/22 09:54 Tare(g) 2.503832 11/11/22 16:39 2.494478 11/11/22 16:38 2.493959 11/11/22 16:34 Residue(g) 0.00006 0.00005 0.00010 Vol.(mL) 225 200 250 Max. Residue(g) 0.00015 0.00016 0.00025 1122-053 EPA Method 202 NE013AS-021420-RT-1303 Appendix C-Page 354 of 1178 NE01 3AS-021420-RT-1 303 Appendix C- Page 355 of 1178 Enthalpy Analytical Narrative Summary Company MAQS—Newburyport Client# PROD-021420 Analyst CCB Job# 1122-053 Parameters EPA Method 202 #Sam les 3 Runs +Proof Blank Custody Alyssa Miller received the samples on 11/7/22 at 16.1 °C after being relinquished by Montrose Air Quality Services, LLC — Newburyport. The samples were recieved in good condition. Prior to, during, and after analysis, the samples were kept under lock with access only to authorized personnel by Enthalpy Analytical, LLC. Analysis The samples were analyzed for Condensable Particulate Matter using the analytical procedures in EPA Method 202, Determination of Condensable Particulate Emissions from Stationary Sources (40 CFR Part 51, Appendix M). All samples were weighed on Balance 8 (Sartorius Model ME 5-F, Serial # 23104965), certified by Mettler Toledo through July 31, 2023. QC Notes The method specifies that blank corrections are accomplished by subtracting the particulate mass determined for the `Field Train Recovery Blank' or 2 mg (whichever is less) from the sample weight.. Laboratory reagent blanks were dried down with these samples. Results are reported, but none are used to blank correct the associated sample results. A proof blank was also received, analyzed, and reported; but not used to blank correct the sample results. Reporting Notes Gravimetric analyses are considered to be accurate to ±0.5 mg. Therefore, negative catch weights between 0 and —0.5 mg are set to zero and no investigation is undertaken. Negative catch weights less than -0.5 mg are investigated. There were no fractions with negative catch weights for this set of Method 202 samples. These analyses met the requirements of the TNI Standard. Any deviations from the requirements of the reference method or TNI Standard have been stated above. The results presented in this report are representative of the samples as provided to the laboratory. sh N 001 i4A RT=1303 Appendix C- Page 356 of 1178 eneral ReportingNotes The following are general reporting notes that are applicable to all Enthalpy Analytical, LLC data reports, unless specifically noted otherwise. • Any analysis which refers to the method as "Type" represents a planned deviation from the reference method. For instance a Hydrogen Sulfide assay from a Tedlar bag would be labeled as "EPA Method 16-Type" because Tedlar bags are not mentioned as one of the collection options in EPA Method 16. • The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory cannot determine the presence of the analyte of interest reliably. • The acronym LOQ represents the Limit of Quantification. Below this value the laboratory cannot quantitate the analyte of interest within the criteria of the method. • The acronym ND following a value indicates a non-detect or analytical result below the MDL. • The letter J in the Qualifier or Flag column in the results indicates that the value is between the MDL and the LOQ. The laboratory can positively identify the analyte of interest as present, but the value should be considered an estimate. • The letter E in the Qualifier or Flag column indicates an analytical result exceeding 100% of the highest calibration point. The associated value should be considered as an estimate. • Sample results are presented `as measured' for single injection methodologies, or an average value if multiple injections are made. If all injections are below the MDL, the sample is considered non-detect and the ND value is presented. If one, but not all, are below the MDL, the MDL value is used for any injections that are below the MDL. For example, if the MDL is 0.500 and LOQ is 1.00, and the instrument measures 0.355, 0.620, and 0.442 - the result reported is the average of 0.500, 0.620, and 0.500 - - - i.e. 0.540 with a J flag. • When a spike recovery (Bag Spike, Collocated Spike Train, or liquid matrix spike) is being calculated, the native (unspiked) sample result is used in the calculations, as long as the value is above the MDL. If a sample is ND, then 0 is used as the native amount (not the MDL value). • The acronym DF represents Dilution Factor. This number represents dilution of the sample during the preparation and/or analysis process. The analytical result taken from a laboratory instrument is multiplied by the DF to determine the final undiluted sample results. • The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual sample is spiked with a known amount of analyte so that a percent recovery value can be determined. The MS analysis indicates what effect the sample matrix may have on the target analyte, i.e. whether or not anything in the sample matrix interferes with the analysis of the analyte(s). A NE01 3AS-021420-RT-1 303 Appendix C-Page 357 of 1178 General e o i es (continued) • The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the same manner as a MS, the use of duplicate matrix spikes allows further confirmation of laboratory quality by showing the consistency of results gained by performing the same steps multiple times. • The addition of LD to the Sample ID represents a Laboratory Duplicate. The analyst prepares an additional aliquot of sample for testing and the results of the duplicate analysis are compared to the initial result. The result should have a difference value of within 10% of the initial result(if the results of the original analysis are greater than the LOQ). • The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an additional aliquot at a different dilution factor (usually double the initial factor). This analysis helps confirm that no additional compound is present and coeluting or sharing absorbance with the analyte of interest, as they would have a different response/absorbance than the analyte of interest. • The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the client sample matrix, prepared and analyzed by the laboratory using the same reagents, spiking standards and procedures used for the client samples. The LCS is used to assess the control of the laboratory's analytical system. Whenever spikes are prepared for our client projects, two spikes are retained as LCSs. The LCSs are labeled with the associated project number and kept in-house at the appropriate temperature conditions. When the project samples are received for analysis, the LCSs are analyzed to confirm that the analyte could be recovered from the media, separate from the samples which were used on the project and which may have been affected by source matrix, sample collection, and/or sample transport. • Significant Figures: Where the reported value is much greater than unity (1.00) in the units expressed, the number is rounded to a whole number of units, rather than to 3 significant figures. For example, a value of 10,456.45 ug catch is rounded to 10,456 ug. There are five significant digits displayed, but no confidence should be placed on more than two significant digits. In the case of small numbers, generally 3 significant figures are presented, but still only 2 should be used with confidence. Many neat materials are only certified to 3 digits, and as the mathematically correct final result is always I digit less than all its pre-cursors - 2 significant figures are what are most defensible. • Manual Integration: The data systems used for processing will flag manually integrated peaks with an "M". There are several reasons a peak may be manually integrated. These reasons will be identified by the following two letter designations on sample chromatograms, if provided in the report. The peak was not integrated by the software "NI", the peak was integrated incorrectly by the software "II" or the wrong peak was integrated by the software "WP" These codes will accompany the analyst's manual integration stamp placed next to the compound name on the chromatogram. r NE013AS-021420-RT-1303 Appendix C-Page 358 of 1178 C NE01 3AS-021420-RT-1 303 Appendix C-Page 359 of 1178 Chain Custody Form - Source Page_1_of_1_ ANALYSIS REQUESTED 0 Company Name: Montrose Air Quality Services Q a CLIENT Project Manager: Michael Bruni INFORMATION e-mail: mbruniQlmontrose-env.com Address: 2 New Pasture Road SECTION Newburyport,MA 01950 W - c Phone: (978)499-9300 Fax: (976)499-9303 N > Cell: 339-206-2376 a 'D Sampled by: Michael Bruni m a 2 z Initial Impinger Collection Charge Le Use Ott Field Sample ID #Bottles Collection Date Time volumes(mLr Fraction U1-FF Out-MSl202-R1-A 1 10/27/2022 X Imp Contents&DIH2O Rinse u1-FF Out-M51202-R1-8 1 10/27/2022 X Acetone/Hexane Rinse U1-FF Out-M51202-R1-C 1 10/27/2022 X CPM Filter U1-FF Out-M51202-R2-A 1 10/27/2022 X Imp Contents&DIH2O Rinse U 1-FF Out-M5/202-R2-B 1 10/27/2022 X Acetone/Hexane Rinse U1-FF Out-M5n02-R2-C 1 10/27/2022 X CPM Filter 12-FF Out-M5/202-R3-A 1 10/27/2022 X Imp Contents&DIH2O Rinse U1-FF Out-M5/202-R3-8 1 10/27/2022 X Acetone/Hexane Rinse U1-FF Out-M5/202-R3-C 1 10/27/2022 X CPM Filter U1-FF Out-M5/202-FTR8-A 1 10/28/2022 X Imp Contents&DIH2O Rinse U1-FF Out-M5f202-FTRB-B 1 10/28/2022 X Acetone/Hexane Rinse U1-FF Out-M5/202-FTRB-C 1 10/28/2022 X CPM Filter TAT Requirement PROJECT INFORMATION REPORTING REQUIREMENTS PROJECT SPECIFIC COMMENTS STD 10 Business day 121 Project#: PROJ-021420 Summary Report only ❑ Method 202 Analysis (Wheelabrator N.Andover) Rush 5 Business day ❑ Name:Wheelabrator North Andover Summary Report & ❑ Method 5 analysis not required Rush 2 Business day ❑ PO#: Full Data Package j�'t—C ) Rush 1 Business day ❑ EDD I] Other(specify): 'Initial Impinger charge volumes are required before the following analysis ~" can be started:Method 26,CTM-027&Method 8 Relinquished By Date/Time i E i "" Q Received b �" t tale" ,' 1 4-4,4 Method 23/T09A Relinquished By DatelTime 1, 'L Z. Received by NATO TEF ❑ TEF x DL ❑ TEF x 0 DL ❑ Relinquished B �' '" - Dateffime i [IZ 'I .G Received by 1,WHO TEF ❑ TEF x 0.5 DL ❑ Q13AS-021420-RT-1303 Apperkix --P_4 36 f` 8 11. 1 Of s Is The Last Page s Report. NE013AS-021420-RT-1303 Appendix C-Page 361 of 1178 Wheelabrator Environmental Systems, Inc.—Wheelabrator N.Andover, Inc. Compliance Test Program on Unit Nos. 1 &2 Test Dates: October 18-19,2022&October 25-28, 2022 Particulate, iv1 J N"1 R S �1 it cZIIA I_I I'1' i i;la VlCt.i NE01 3AS-021420-RT-1 303 Appendix C-Page 362 of 1178 Montrose Air Quality Services, LLC 2 New Pasture Road, Unit 5 Newburyport, MA 01950 Project ID: J-0120 helabrator North Andover Particulate Matter, Cadmium, Lead Mercury EPA Methods 5 & 29 Analyses Analytical Report 3961 Element One, Inc. . 6319-D Carolina Beach Rd., Wilmington, NC 28412 910-793-0128 FAX: 910-792-6853 el la -e1la .com NE01 3AS-021420-RT-1 303 Appendix C-Page 363 of 1178 MMM� The following data for Analytical Report 39621 has been reviewed for completeness, accuracy, adherence to method protocol, and compliance with quality assurance guidelines. Review by: Daphne Woodman, B.S. Chemist November 21, 2022 Report Reviewed and Finalized by: Ken Smith, Laboratory Director November 21, 2022 MMMMMMMMM"I ellementOne Certification: NJ NELAP NCO09 39621 MAQS M5-29 Report Packet NE013AS-021420-RT-1303 ApperOix�-:PgSqj464of1178 0" UMMARY OF RESULTS elementOne Certification: NJ NELAP NC009 39621 MACS M5-29 Report Packet NE013AS-021420-RT-1303 Append ig)qgEPg of 1178 Summary of Analysis Unit 1 - Summary of Method 29 Mercury Analysis H202 Empty Average Total Front Half /HNO3 Impinger KMn04 HCI Run Number Catch, pg P9 P9 P9 P9 P9 ----------------- --- --------------- ------------- ------------ ------------ ----------- -------- U1-SDA In-M29-R1 #1 15.6 0.140 13.8 0.304 0.649 0.676 #2 0.142 13.8 0.306 0.656 0.682 U1-SDA In-M29-R2 #1 27.5 0.249 26.5 < 0.2 < 0.5 0.629 #2 0.250 26.7 < 02 < 0.5 0.624 W-SDA In-M29-R2 Dup #1 29.1 0.246 28.1 < 0.2 < 0.5 0.643 #2 0.243 28.4 < 0.2 < 0.5 0.653 U1-SDA In-M29-R3 #1 19.4 0.168 18.4 0.215 < 0.5 0.561 #2 0.170 18.5 0.218 < 0.5 0.562 Ul-SDA In-M29-R4 #1 30.7 0.333 28.8 0.656 < 0.5 0.973 #2 0.327 28.6 0.662 < 0.5 0.964 U1-FF Out-M5/29-R1 #1 1.31 < 0.1 1.30 < 0.2 < 0.5 < 0.4 #2 < 0.1 1.31 < 0.2 < 0.5 < 0.4 U1-FF Out-M5/29-R2 #1 1.39 < 0.1 1.38 < 0.2 < 0.5 < 0.4 #2 < 0.1 1.39 < 0.2 < 0.5 < 0.4 W-FF Out-M5/29-R2 Dup #1 1.38 < 0.1 1.39 < 0.2 < 0.5 < 0.4 #2 < 0.1 1.37 < 0.2 < 0.5 < 0.4 U1-FF Out-M5/29-R3 #1 1.45 < 0.1 1.45 < 0.2 < 0.5 < 0.4 #2 < 0.1 1.46 < 0.2 < 0.5 < 0.4 W-FF Out-M5/29-R4 #1 1.42 < 0.1 1.42 < 0.2 < 0.5 < 0.4 #2 < 0.1 1.41 < 0.2 < 0.5 < 0.4 elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396AOpWdaSM8-V9' Wpctt Mket Page 4 of 66 Summary of Analysis Unit 1 - Summary of Method 5 Particulate Analysis U1-FF Out- U1-FF Out- U1-FF Out- M5/29-R2 M5/29-R3 M5/29-R4 e39621-6 e39621-7 e39621-8 Fraction Catch, mg Catch, mg Catch, mg ---------------- --------------- --------------- --------------- Filter < 0.1 < 0.1 < 0.1 Rinse 5.2 4.0 1.7 Total PM 5.2 4.0 1.7 Unit 1 - Summary of Method 29 Metals Analysis U1-FF Out- U1-FF Out- U1-FF Out- U1-FF Out- M5/29-R1 M5/29-R2 M5/29-R2 M5/29-R3 e39621-5 e39621-6 e39621-6 dup e39621-7 Element Total fag Total pg Total pg Total pg ----------------- --------------- --------------- --------------- --------------- Cadmium 1.25 1.18 1.15 1.40 Lead 13.6 11.3 11.4 12.9 elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 39680 Sidi ket Page 5 of 66 Summary of Analysis Unit 2 - Summary of Method 29 Mercury Analysis H202 Empty Average Total Front Half /HNO3 Impinger KMn04 HCI Run Number Catch, lag P9 P9 P9 P9 P9 ----------------- --- --------------- ------------- ------------ ------------ ----------- -------- L12-SDA In-M29-R1 #1 42.6 0.648 31.0 3.29 2.22 5.25 #2 0.654 31.3 3.33 2.23 5.28 U2-SDA In-M29-R2 #1 63.1 0.172 59.7 0.434 0.610 2.29 #2 0.172 59.5 0.440 0.586 2.29 L12-SDA In-M29-R2 Dup #1 62.9 0.169 58.7 0.401 0.629 2.31 #2 0.172 60.1 0.412 0.615 2.29 U2-SDA In-M29-R3 #1 48.1 0.397 45.6 0.785 < 0.5 1.31 #2 0.397 45.6 0.782 < 0.5 1.32 U2-SDA In-M29-R4 #1 22.7 0.181 20.1 0.319 < 0.5 2.12 #2 0.178 20.0 0.312 < 0.5 2.13 U2-FF Out-M5/29-R1 #1 6.39 0.116 5.83 < 0.2 < 0.5 0.481 #2 0.117 5.75 < 0.2 < 0.5 0.485 L12-FF Out-M5/29-R2 #1 3.58 < 0.1 3.56 < 0.2 < 0.5 < 0.4 #2 < 0.1 3.60 < 0.2 < 0.5 < 0.4 U2-FF Out-M5/29-R2 Dup #1 3.57 < 0.1 3.56 < 0.2 < 0.5 < 0.4 #2 < 0.1 3.59 < 0.2 < 0.5 < 0.4 U2-FF Out-M5/29-R3 #1 1.80 < 0.1 1.79 < 0.2 < 0.5 < 0.4 #2 < 0.1 1.80 < 0.2 < 0.5 < 0.4 U2-FF Out-M5/29-R4 #1 1.59 < 0.1 1.59 < 0.2 < 0.5 < 0.4 #2 < 0.1 1.59 < 0.2 < 0.5 < 0.4 Field Blank #1 < 0.5 < 0.1 < 0.3 < 0.2 < 0.5 < 0.4 #2 < 0.1 < 0.3 < 0.2 < 0.5 < 0.4 Reagent Blank #1 < 0.5 < 0.1 < 0.2 < 0.2 < 0.5 < 0.4 #2 < 0.1 < 0.2 < 0.2 < 0.5 < 0.4 elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 396AOpWQF-WII9--i%O SFRpal Vaket Page 6 of 66 Summary of Analysis Unit 2 - Summary of Method 5 Particulate Analysis U2-FF Out- U2-FF Out- U2-FF Out- M5/29-R1 M5/29-R2 M5/29-R3 e39621-13 e39621-14 e39621-15 Fraction Catch, mg Catch, mg Catch, mg ---------------- --------------- --------------- --------------- Filter < 0.1 < 0.1 < 0.1 Rinse 3.3 1.3 2.3 Total PM 3.3 1.3 2.3 Unit 2 - Summary of Method 29 Metals Analysis U2-FF Out- U2-FF Out- U2-FF Out- U2-FF Out- M5/29-R1 M5/29-R2 M5/29-R2 M5/29-R3 e39621-13 e39621-14 e39621-14 dup e39621-15 Element Total lag Total lag Total lag Total pg ----------------- --------------- --------------- --------------- --------------- Cadmium 0.791 1.54 1.67 0.959 Lead 10.2 12.6 12.5 15.4 Blanks - Summary of Method 5 Particulate Analysis Reagent Blank e39621-18 Fraction Catch, mg ---------------- --------------- Filter ---- Rinse 0.1 Total PM 0.1 Blanks - Summary of Method 29 Metals Analysis Field Blank Reagent Blank e39621-17 e39621-18 Element Total lag Total pg ----------------- --------------- --------------- Cadmium < 0.2 < 0.2 Lead 0.319 0.517 elementOne Certification: NJ NELAR NCOO9 NE01 3AS-021420-RT-1 303 396AO 1*:SM8 ket Page 7 of 66 NARRATIVEANALYTICAL elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 396AOpMAUlCM8a&RWI Mket Cage 8 of 66 Element One Analytical Narrative Client: Montrose Air Quality Services, LLC Element One#: 39621 Gent ID: PROJ-021420 Wheelabrator, North Analyst: PDR, DAZ, RMH Andover Method: Methods 5 & 29 Dates Received: 11/07/22 Analytes: PM, Cd, Pb, Hg Dates Analyzed: 11/11-17/22 Summary of Analysis The Method 5 particulate samples were analyzed in accordance with EPA Method 5 guidelines. Particulate samples were weighed to a constant weight of ±0.5 mg and reported to the nearest 0.1 mg. The Method 29 samples were digested, prepared, and analyzed according to Method 29 protocol. Samples were analyzed for mercury on a PerkinElmer FIMS-100 CVAA mercury analyzer. The samples were analyzed for cadmium and lead on PerkinElmer Nexlon 350X and Nexlon 1000 ICP-MS instruments. Detection Limits The FIMS-100 CVAA instrument reporting limit for mercury was 0.004 tag per aliquot analyzed. The ICP-MS instrument reporting limit was 1.0 pg/L for cadmium and lead. Analysis QA/QC Duplicate analyses relative percent difference (RPD), spike sample recovery, and second source calibration verification data are summarized in the Quality Control Section. All QA/QC data was within the criteria of the method. Additional Comments The reported results have not been corrected for any blank values or spike recovery values. The Method 5 blank correction factor has not been implemented. The reported results relate only to the items tested or calibrated. The ICP analysis of the blank samples revealed detectable traces of lead. ellement0ne Certification: NJ NEI_AP NC009 NE013AS-021420-RT-1303 396A0 I0 8 ket Page 9 of 66 QUALITY CONTROL SUMMARY elementOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396A0 MI9 tl Mket Page 10 Of 66 Summary of Quality Control Data Mercury Duplicate Injection RPD (Method 29 QC limits:< 10%for RPD) Run Number Front Half H2O2/HNO3 Empty Imp KMnO4 HCl ------------------------- ------------- ------------- ------------- ------------- ------------- U1-SDA In-R1 1.4% 0.3% 0.4% 1.0% 0.8% U1-SDA In-R2 0.5% 0.5% NA NA 0.8% U1-SDA In-R2 Dup 1.1% 1.0% NA NA 1.5% U1-SDA In-R3 1.0% 0.2% 1.4% NA 0.3% U1-SDA In-R4 1.8% 0.7% 0.9% NA 0.9% U1-FF Out-R1 NA 0.8% NA NA NA U1-FF Out-R2 NA 1.0% NA NA NA U1-FF Out-R2 Dup NA 1.3% NA NA NA U 1-FF Out-R3 NA 0.9% NA NA NA U1-FF Out-R4 NA 1.0% NA NA NA U2-SDA In-R1 1.0% 1.0% 1.4% 0.3% 0.5% U2-SDA In-R2 0.4% 0.4% 1.4% 4.0% 0.0% U2-SDA In-R2 Dup 1.4% 2.4% 2.7% 2.2% 0.9% U2-SDA In-R3 0.1% 0.0% 0.4% NA 0.7% U2-SDA In-R4 1.6% 0.4% 2.5% NA 0.5% U2-FF Out-R1 0.8% 1.4% NA NA 0.8% U2-FF Out-R2 NA 1.3% NA NA NA U2-FF Out-R2 Dup NA 0.8% NA NA NA U2-FF Out-R3 NA 0.3% NA NA NA U2-FF Out-R4 NA 0.2% NA NA NA Field Blank NA NA NA NA NA Reagent Blank NA NA NA NA NA ellementOne Certification: NJ NELAP NG009 NE013AS-021420-RT-1303 396AOpWW&;M8QO ORWI Wkket Page 11 of 66 Summary of Quality Control Data Mercury Duplicate Analysis RPD (Method 29 QC limits:<20%for RPD) Run Number Front Half H2O2/HNO3 Empty Imp KMnO4 HCI ------------------------- ------------- ------------- ------------- ------------- ------------- U1-SDA In-R2 Dup 2.2% 5.8% NA NA 3.4% U1-FF Out-R2 Dup NA 0.2% NA NA NA U2-SDA In-R2 Dup 1.0% 0.4% 7.1% 3.8% 0.8% U2-FF Out-R2 Dup NA 0.2% NA NA NA Mercury Spike Recoveries (Method 29 QC limits:75-125%for Spike Recoveries) Run Number Front Half H2O2/HNO3 Empty Imp KMn04 HCI ----------------- ----- ------------- ------------ ------------ ----------- -------- U1-SDA In-R3 #1 96% 93% 97% 95% 94% #2 97% 93% 97% 95% 92% U1-FF Out-R3 #1 95% 96% 94% 97% 96% #2 95% 95% 95% 98% 96% U2-SDA In-R3 #1 97% 92% 94% 97% 94% #2 98% 91% 95% 97% 94% U2-FF Out-R3 #1 93% 92% 89% 89% 100% #2 94% 92% 89% 89% 101% elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396Ap ket Page 12 of 66 Summary of Quality Control Data Metals Duplicate Analysis RPD (Method 29 QC limits:<20%for RPD) U 1-FF Out- U2-FF Out- M5/29-R2 M5/29-R2 Element RPD RPD ------------------ ----------------- ----------------- Cadmium 2.8% 7.9% Lead 1.1% 0.7% Metals Analysis Spike Recoveries (Method 29 QC limits:75-125%for Spike Recoveries) U1-FF Out- U2-FF Out- M5/29-R3 M5/29-R3 Element Recovery Recovery ------------------ ----------------- ----------------- Cadmium 79% 86% Lead 123% 107% Second Source Calibration Check Recoveries (Method 29 QC limits:±10%for Second Source Continuing Check Standard*) Element 1 ppb 50 ppb 100 ppb` 125 ppb ----------------- ----------------- ----------------- ----------------- ----------------- Cadmium 104% 100% 99% 101% Lead 95% 92% 97% 102% elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396AO 6 Q PMket Page 13 of 66 z""AMPLE CUSTODY elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 39 ket Page 14 of 66 Chain of Custody Form - Source r r ANALYSIS REQUESTED CAmpany Nemec Montrose Air Quniitjr Soneicas CLIENT Prnjccl Muster', Adadhael 0.xuni INFORMATION a-may: m eun%Pmonfraae-ertv.aam � Address 2 New Pasture Read = SECTidN rdtsbutyport!AA D1450 - rc Pitons' a '1978)499-93D0 Fax (t? 499:Mq,3 Ce€': 339-2011 2"78 semptd by: michaei Nrunr: fie Gallr.tan InRit ttnpingar m Chet9so E CD CU OD Lahrarata USC attl Ftesd Sample aU R®o81es Cailseilan Ogle Tole rrorumra wu-I` Fractmq t.-FF Cm-Msr Ri-A_ 1 t0127=22 =_ X Filter Z ur r Uui Ms2s Ri.e t =712022 X FFanl'12 Arelane Rinse � O In F Inl MWO-R1-C % 1120IN HNO3Aintiv < � u+F Dull-M5 .Rt-E 1 Tk'2y12422 % 1-3 Imp comenvs&Ririe LU u-Fr Gut-Mh l-R1-F 1 i 1017717C22 % 4 ImpCanlaMs&Rinse CCV ui-FF Cw.4524-RI-F i IDri712022 % 5-6 Imp Convents&Rinse L v. ut Fr:tut-M:as R.,.,c 1 l 1912712022 x - €IN HCL Rinse W f Cut-M5� art:-A 1 4. 1aWf2022. % -.. _ .... Finer O_. .,W.�,,._.. -- - ._ L-=FCut M51i-M-3 1 19.27r2022 X _Fror1112 Acelore Rinse Q Ut-rF Oul-M`,'te tit-C 1 10/2712022 X - Frunt 1.9 Oe IN HNO3 Rinse urFFam Ms2s-n2-n 1 IGQ712022 X 1-3 U'-F1 Om M,129 R2 a �v. i I nQW2022 p X -.. 4 tar Camart,s&Rinse (D CO a u f Cur_Ms;�.rrY-r i 10t27f2022 % 5-5 Imp Contents&Rinse M U1 FF tan uSzs-R2-D 1 10 27t2tl22 x 8N HCL Rinse TAT Rogtriramem! PROJECT INFORMATION REPORTING REQUIREMENTS PROJECTSPSCIRC COMMENTS Or STD`D Business day P1 Projem is PRCJ W,1420 'Summary Repotl Only 1-1 Melhod 29 Analyius Cd,Ph and HD lWhoetsbroalor N.Andeverl M Rush 5©Dslnesa day ❑ Name:WheelabratOr Ninth Andover Summary Rapon& ❑ O M Rush 2 BrAinass day ❑ PO Y: _ Full Cats Paok:rde HO onry on non q,M5 Analysis an Frst 3 Out of nine � Rush 1 Business day (.1 - EflD 10 � ',-- v- Oleme ar; g •IDilial imidnQtsrrhatpe W6umea Ott required trefaee the folkratiit8 analy5:s � f car be started:MaDtod 28.CTIe1,027 A.Method 8 Relln4uietted Ay - `` Osten'wne t s e l E (] .Y.'S-# Racarvad p ' "'"'Y- lik—MuUmd 231709A N Rcllrslaisttad by - - '" '�`�Oa1ts+Tima 1 t Redelaea by NATO TEF ❑ TEF x OL U T_EF x 0 DL ❑ d' Relinnuildied BY a" - > s fla d'ilme t j I �)"` (-2 c,4, Received hY qi WHo TEr ( TEE x 0 5 flL❑ ` N Jv _ " ql A t ti Pa' t r'�<M�Pn"JY f "7-.t<`S 1`�, i ' I§ - �f t'.s,.,l t.�^t�I x.� \``-t" t"'!A t-.-_ t.'7 Cfk 3 Cl) O LLI Z Chain of Custody Form - Source .� ._Pace_2�..ar_2_ ANALYSIS REQUESTED Cderueny Name: Moubles.Air Quality Sarvlces CLIENT Fro)W Marager Michael Brunt INFORMATION a-Tell: mbrunilIbmane^naa rmu cpm u5 I Address: 2 New Pasturo Rnad SECTION Irtewhnrypor„AEA 0 SI60 8 Phore- {9711)499,93W Faz _=,•. i(78149g-9'r..C3 �v Cell 539-206�23711 .. Sametag by AFtchael Brunt ColIeL1{Gnrms®IFr _- C:) tXt � U Cru•sa - tRhaP9tp use ah Field 5@ rele iiJ Y solues Ccileceor Oale 'Time wwasIffax __. FrW'ipn N 4t FF Ov!-Y529 R3 A 1 t012772022 X m '_ FRer 4+FF C�-N1aM R3 a 1 ' 10112712022 X Front 1+'2 Acetone Rinse ® O z.0 -.�ur=F❑a _cnttr R3 C 1 1012772 -022 k � X `*mn1`2 0.1N HNO3 Rinse c d6S3 P Ou+FF a na:s-s R3 a t 70f2772(122 g X M -31rr4 comeals b Rinnu ur FF 0,P "Us R3-e 1 77Y27fm022 � R X N y 4 ImpContents b pins. � Me U'FF CW 5%IM-R➢r F 1 : 10270,0J2 - X 5.6 Imo Contents b Rinse urc%ar-a+uap-�3 a 1 IN2772022 X 9NIICLRime 4-FF C.r-SteQ+ Re-A 1 la" 2022 X _ Titer utrFF ON 5Wry-R4.8 1 IR121112021 X Front 112 Amkone RI Iua urFFov.-vxuu-n4-1: 1 1WIII2022 X F^udt'112 C.1N HNO3Rmm C ui FF a�-try n i 10J1g72022 X 1-3 Imp wnlpnL5 B,Rinse .`'�' CL ur-FrCl..,io-Re-.€ 1 iLV21U2U22 X aim.Ef ..mtprAx_14,Rinse•._ CL .rrruw-s+ea -ne-r 1 1U2812022 x 5= ltn C ntah Rinse 1191-w1070-Ire-e 1 107230022 7C 8N14CLRiau Cl) 3 TAT Requirement PROJECT INFORMATION REPORTING REQUIREMENTS PROJECT SPECIFIC COMMENTS �.1c far ?gtr Sjia �a�a /Irxr;:•.1k1 Cl) STO 10 Business dray :1 r rCIect m FROJ-021420 Summary Raped arty ❑ Method 29 Analysis CA Pb,and Hp(VOcalahroalor N.Anmaer) M Rush S eLs{nass day J Name:wheelaMilor North Andove• Summary Report b ❑ Rush 2 8"Iram day *_1 PC# FLLA^DaE,i Package Hg only on rand M5 Amlysis an first 3 out of 4 runs (- Rush 1 Ri airom day :1 EGO M fr'al6 r Q' r. Odher s w a• 'Inigai Impinge-,charge Volumes memipilrod Were tare failatising ansys-S p' 1.J' ,lJ�� caR be started:Metnua 26,MlD27 d Whad 8 N Reil uiandd 9 R:rczr Y Cae7Time i r i t7�L cJ :s'�1 ivpn d � �- ad 231 T09A RaiitxLuisl4ed 8 `- - �(,�,Date7Tima t. rr d?,4*i Heonisan , °' m' NATO TEF fFF z RI "[Eh x 0 CL Rriiruished Ry ti" -rc tkatetYlme , ! 1''1 i c> tte�ioe!n WHC tE.F 17 'EF x 7 5 rl r � ON! � �' . r--7 zz— Ce) O LLI Z Chain of Custody Form - Source Page_1 of_2_ ANALYSIS REQUESTED Company Narre, Montrose Air OMIlly Services CLIENT Project Manapen._ Mictisol Brum INFORMATION e,mou: mbnMiMmonlrose-eirv.cam AddresE 2 New Pasture Read SECTION I,MA 0195D Phone: (97111 499-93D0 Fair, (9711)499.RX3 r&l 339-206-2376 rare pod by Michav Brunt _ W Maitl0-) Collection chargt CD 00 CU I, Fractan L) Laborah"use callyl Meld Sample,ID Buttes CoVactlar.Done Tme vot—tr,1LI, W-�eDnl h-WS R1 A x riller z -,f L2.F,O'd-s'km-n I-" 1 I011W2022 0 0 x Frail 112 Auclonc,Rinse 0- LIZ-I'l'Oul SV29,fa l,C 1 1 UZZI— — FrOMEV20-IN i4kCgRnsv C < (D WIFF 00hWH-H,-U 1 lamae2022 x 1� 0 , *0 UJ 0) VVIW2022 x 4 I C.rd.ris&Fin C z C� mp x 4) Lo 643 Imp Contents A Rnm Z U7-FF CM-'lAPA-RI- 1 IOMW2022 x BN HCf-Rinse E j� (12.FFOW 5IW29 R2 x Filer C) (3 W-FF 0,11-51V29-H2-U 1.. 101111,072 x Flong W Acetone Rnse < U2FFOA rIW21)-Wmll 1 1 Del W2022 2 x Front 1�2 01 N HNO3 Rime LF— CL U�41 0A-&TA20-R2-0 1 lRfl&2022 x 4.-3 Imp contents&Mnse CL Q) N< 1.12-FF 0,A-EV29-f42-U 1 1 Del&12022 x 4]me Ceednits&Reiss UoFFDA-YV29 R2 F t 10L11W2022 x Imp Content,&Rinse co ,m,FF R2-G I I CV1 W2r,2.2 x #A ff- L�Rnse TAT Rsqvl;e7man, —PROJECT INFORMATION REPORTING REQUIREMENTS PROJECT SPECIFIC COMMENTS t,4kfjAC& '~A 9,( 1wi C ,, I"DPH�� STD 10 Busifteas day ED Project*:PRO.1-021420 S"n'rmafe Repvl only 0 Wolhod 29 Analysis Cd,Pb,and HA(Wincolabroater N Anvever) ce) Rush 5 Business day Ll Name:VJhmlmbf;ibw Nndh Andover Summary Repmll A n ED Rush 2 Business day E Pn* Ful Data PacaMs jig nolyxz;�;Analysis on first 3 out of 4 runs ce) Rush 1 H usniess clay 1: EDO pi J_ 1_� qLtrAs I Initial Impingot 0,arge volumes are reQumd before the fcllawu,,g analysis wad 8 C5 C"i TEF a D 01. 9 it U) 0 LU z Chain of Custody Form -Source page---Z—of—2— ANALYSIS REQUESTED C-ampany Name: "hinders Air Quality Services CLIENT Ploiad Marager: Lificheal Saini INFOROAAT" e-mw: c0im Address: 2 No,Pw Road -0 sfic'noN Phone: (978)499 9300 Fax- gyyt 4994303 Call. 339-206-2370 Samp4rd ivy* Michael Brim ----------- Callectan CD 00 Laborarto uses nwd sam pie it, #flohisis ji C.Imcljuh Gate Time w-,--(-Lr x Filter 4) a- 0 0 U24FC—W-119 R3 a I tVIR12022 x Font�)2 Acalane Riftise CL C < L32.FF GO-FJWS-R-'-C x Fimi-I 10 0 IN HNGJ 41M9I 0 t,2-rr 0.- wa-.4.)-u I Z 11 W 2 02 2 1-3 Imp contents&Rinse C z w m.wu-fl -Wev. q3-E IWIWC22 A ImpContents&Ruse 1�4 x 8 trip Contoris&Rmse to W FF 0. 1%121 R3-F 0-F�M..-i-Wd-143-C4 I 1w,glZC22 x BN HCL Rinse U�PF 01,-MVS-R- A I IV-912022 x Filter C3 Lu-FF Cv Wn RA-9 1 x Front 117 AcHone Rnw < L2-FF OW.&Wd.R4-C, 1 S IW,9121(122 x Errant tr, 2,N F-IW3 Rinse (D 4,74,Ow-fi,"-44-D I IGII912022 x 1-3 Irris corlems&Rnse �E UZ FF CZ IM%- RA-E 1_ x 4 mpConIvr1s&Riri;s;r C.ft < u.1-rF C�-&1.1.0-R.-r 1 iQl912G22 x a Rinse —A- vj-` out-W29-Rd-G I WIW2022 x SN SCl Rinse ia.,I9(2G2Z x —FAa-r l(V19M322 x Acelon. TAT Requirement PROJECT INFORMATION REPORTING REQUIREMENTS �PROJECT SPECIFIC COMMENTS C:) PqeAllan*)�ftvk V( f)rt,t-t--,,A tyul, Cl) STD IOBusmatisday :1 Fircrect S:PRDJ-021420 M Summary Report only 7: Method 79 Analysis Cd,Pid and Hg IA'Aaelabrualur N.fividow Rush 5 Sus,neas day J Sarre-Wheglablaor North Ahdovar Summary Report A -- Rush 2 BuWreas day :1 PO* Full Bids,pwkagr Hp on run4.M5 Arwlys&on first 3 net of 4 hire Rush 1 flusmmm day -J Z 4�nf.L Initial mp�lqiu rhatitil volumes are reoilren be"the followiniforralyivs C14 ran be aearled Method 28,CT1.1-027&Method 6 Relinquilthpa By DadtafT!me I ?-I R..Id I *thod 231 TOBA CV Relinquisfird By Z��—j uawfi'irna� r / Z++-� Ra NATc Tcr :1 TFF x rL 0 TEF 9 0 DL I _3RMLwid by 0 -r aalerrime I nnalvad ov.)- TEF x 0 5 UL 17-1 Cl) -/7 < /!-(N, cnl Oki— C�, 1) P,7!1117�,,TL11 co 0 LI-1 z Chain of Custody Form - Source ANALY845 REQUESTED CLIENT Projecl Manager. Micitans Rnini INFORMATION o'l-lail: can 2 New PaMur.Rand SECTION09950 Phone: (97a)499>9300 -ax (976:499-93113 0 Call 339-200-2376 Sampled by, 10,chawl Bruni t In"121"N r CD action 00 CD naarps Laborsdo use only riew -a Ra j.s C.11.ctmn DaIr. 7Cal1.0 Fraction UI-SM—W2S RI A 1 1012712B72 x Fillar Z Ul-sf3A el.V2�-A Ft 1 I0a2712022 0 X P ron!V2 0.1 N I IN03 Rime UIWAIr M29 Rt,C 1 x _im ;s.Ft C < a) "'qg a I;nla DID) x 4 IMP CORIeftL Rilso 0 Ll SDA b'W429 R I-E x Imp Conterits&Rinse C Z C'j V'-8VA h-was 141-F I 111127M22 x ON HM RU,m 4) - UI-SDA" WIG R2,A co x Flo, .0 1 1D(27,12D22 x Front 1 t2 0.1 N HNO3 Rrzut Nti < U1 SDA M-16425,R2.C 1 1a'2712022 x 1 L7— (1) ul-SDO 421 42 3 1 11127122 x E au U-3aA W,:.M2fi-W-F 1 1 W27f2D22 F12 F x ON HCL Rinse CIO TAT RequIrentont PROJECT IKFGRMA'nDN WING RIEDIAREWNTS PROJECT 6PE6'[PIC COMMENTS STD 10 Ehismoss day = Project N:PROJ 021420 Sumrrary Reparl any 0 Mathad TO Analysts Hg Only(WIjechibn3alor N Andover) 't Rush 5 Business day L] Natm Whpulabrallor Norlh Andove, Summary Repart & 1:i0 Rush 2 Buniress day Z! FuA Data Package Cl) Rush 1 15tialr ess day EDD ped Dlher(sfO Inihal Imping.1 ctmlue walurnes are ratrulrel�WoTa the fallowig analysis can he sindow Welhod 26,CTM-027 A MoOod 0 0 Relinquished By O"W-rfiq A I ReLeNed bv Method 231 TOSA cli Relnulsh 0 Byt&l., Oatemme k I AA-- Reoelved bv NATO TIFF 1-3 I'EF XOL D TFFxODL Rofirgul so By A� r 0 228ived by e— Wf�O TEF El 7EFX0,5M- D C"! 0 TZ), 2, 1 O LLI z Chain of Custody Form - Source `2)01 U Pape of 2 ANALYSIS REQUESTED C=ipany Nwns._ Mantrosp Air Quall ServIces WENT Projecl Manager WOaal Brun! INFORMATION a mar. alWyna man tuatanv om Address: 2 New Palum,Rand SECTION Nawtuyw MAO'"a pt-alu,: (978)499 9300 FIX--E-89 Al-lg--9203 m Cell: 319-2c6_2372— Sampled by: Kchael Brunt 00 rWar.-Inn C",s. CD r,- Laboratory use ordl, Field!Sampa 10 9 PwIllm; Callettan Dale Tine Walufflas(mLr Fraction .,-SVA',n-U79-RJ-A I0r27)2022 x Filer z V-Z 0 0 0 x cnml I&U.1 N HNO3 Rinse c- _L12712022_ c < 18)127)�6" x -3 10127,12022 X 4 Imp UDTleMs 6 Rinse Uj 0) (9) Z CN ul,SCA,�-W,-�13-G I IN2,71P,02? x Rinse I Ln 1 1(1127=22 x EN I,ICL Rinse F41er U1.50'4 I-M21 R4 3 1 1W&2022 X t.. 7fa,11 1,12 0 IN HNO3 Insr 2 CY ja < U20-114-G' 1 1V2W20ZZ 'w. -3 Imp atmtents&rinse "I,A rA x Cq -1 50A W29 R4 0 CL plants&R11se W-SOA 1n-MZV,94 E 1 102111022 x 5-a Imp Sxibnls&Rinse < 7 x N HCL Rose &129 FS A 1_ 10/11101322 x F"Irr la a-Ftl-le I lUflD2022 x Fron[VZOAN I-INOBRime 10110l2022 x 1-3 Imp q wilents&f0se _ —Pin Fa 1 1 100 a,2022 x 4 Imp Cuntaa.&Rn.. 10111421372 x Imp Conlents&iinse U29 FB F 1410 1WO22 x CIN H(3-Rmss TAT Requireavent 'PROJECT INFORMATION REPORTING REQUIREMENTS PROJECT SPECIRC COMMENTS 0 CY) STD 10 BLsinLsa day Ld Pmjacg AI._PRK)4 Gr2142¢ Summary Reporl only 0 Method 29 Analysis kj Oily IWt—lahmainr N Andover) Rush 6 Rusrmw;day rE Name:Meejaenatar North Amdover Summary Rep.rf& D Per r 1). 4tsh 2 3usiness day 0 ro x Full Dal"packaga C:) qual,I Sualn.....y 171 OtItar(!pacify," Inthal mporgar cnarge valurnes are reqjlred halare the fulkming annly0q can be slarlad 'VeUad 28,CIM-027&Molhod 8 ReSngwechmi Ualal f,me 11 h Received by' ✓ 0 13Y ®thud 211 TOSA -WO—Inaysh6d By —DaleTime, I, Ri NArC iEl, E:: TEF x IX i I TrF x 0 C0 0 LU z Chain of Custody Form - Source Page of,. 2 ANALYSIS REQUESTED Company Name: Montrose AM Quality Services CLIENT prp,iw.i t4anagor, Wictmiel Brent INFORMATION e-mail: mbrui5Qnr'.1"V.-rn.wM Acidness: 2 New Pasture Road SECTION 10%buryporl,MA 01950 f Phone: (va)499-9300 c2x. 197E,499 930 Call- 3392062370 Sampled by: Xchaal HFUN cotediot 00 CD Laboralia use only Field Sam ple ID o Battles Collecton Date Time Wum I.Lr I'IE Fraction I 110WOU — ' 0 0- x Fiftnt z tf UZ BOA In M29-RI 9 1 I13"IWW x i Front'120AN HNO3Rin&e cL 0 0 CL 0'scl'In•Ma,RI•C 1 I0F10022 x Rn" C < .-=,A.n .-R I . 1 -1-11 0 _J X 4[Trip Corwhirls&Rinse yj 0-) UZEDAIn M29 III E 1 T-1w1w,122 x iiT,,pGontimts&Rinse C 1p-SFA 1urinon x SNM Rn.r. o W-Salk In-WO-R2-A 1 11)(W202a X Film 0 =7 112.15MA In-1,124-RP-I, 1 1Ot115.r1022 x Front l.r20A CN HNO3RinHu <-0 10(1ft(2022 x �E a) t.,ts Rinse 2� 1 1 Oft W2022 x 4 In,P Car1pnis; Firma �E CL (D < U2.15DA In-PA29.RW-E 7 t0r1&r202p x Imp Contents&Rinse 0 C.0 U51)1k.r Suss-We--142-U 1 1 Oft OLQ D22 x SN HGL Rnso C) V� CY) TAT Requirement PROJECT INFORMATION IMPORTING REQUIREMENTS PROJECT SPECIFIC COMMENTS STD 11DWisir-assday 21 PrDAl*:PROJ-021420 Summary Flop FA MeMod 29Aralyszs Pig Only(ViAmclaftraninr N Andover) (71) Rush 5 Business any 1`1 Narne!Wanclabriator Natf,.Andavor Summary Report& 0 0 Rush2 ausinmis any 0 1-0 Full Data Package Rush I Business day 11 FDD ❑91 Other(.pMifyj_ FL — Initial Inip,-Scir&iargo volumes are required betom the follWAing lnalrli�n Received 04,fftlk othad 23 0 TODA cli Re�hquish d By I can be staved Method 25,CTNI-027&Mclhod 0 6 .3e�er91AShDd BY Received by NATO TEF 0 TEF F_�� Uawer� x 01. TIFF x 0 DL ❑ 4 1 ---- WHO 0 5 OL Reinqu.'s ad 13Y Dalemme Recolvedby TEF I I TIFF x -4 1 z? GE) a Cl) 0 Uj z Chain of Custody Form - Source '9o� Pap 2 of-2— ANALYSIS REQUERTEO compar)(Name: Mankmas Air QwI1 Sarvicas CLIENT Ptojacl Manager Michael gruM INFORMATION a-Mau: mbrL)niQMg'w1@- 0 ,AMddr*ss', 2 New Pasture Read ' SECTION N.wbyp.,I,VA 01960 Plone: 1978)498-930C F �904=3� cell, 339,200-237n swnwod by MlcOael Brunt CD 00 Co I- --±ed Sam,pie IV, ffi L, Collection Cale Tme Vb—I.L11 CL U2.SD0.u-AA20-R3 = IVISOW22 _x Fiber w, 00 UZ.SDA, ?J29 H3 9 1 tVIS02022 x C r,.,,l 112 DA N HNO3:Zmo. IJOONA..-w"-41-G 1 a iCJ1912"2 k 1-3-p cant nts&Rinse 0 U2 SDAm-M29.R3-n 'd-jrrz x 4InoContonus LzLJ M C C�4 02 SUA U29 R1 E &Mrse to � Lo U2:1VA 8N HGL Rinse x"_ E U2 SVA WS 84 A U) tl"(A un-I"-Ij A Frarl IQ DIN HNC3 R1,1re CY 112-&tWM20-R4-r. x 1 3 1,rp conlar"Is&Rmse C (D W SDALMZg-HA 0 x 4 Imp Contents&Rinse a 'E U2-qnA Wit-n4-r I VW-91=2 x 5-6 mpqct!l�nMs&_Klmse U21113A4l•M29 q4 F x aN HCL Rirsv 7- [ . I I01191=2 M20-11-1,4 1 ins 1 0 1 3 HN0 OP 912a2z x I —— M29 INUM ZFQc 1 i(IPWO27 x 011110 I 101+912022 x 116 101 H202 Mn-S1_k4%XMN(W 9%H2"4 I _110,"SQ022 x 4%K&INCA i'u%142,%04__, mall wank-2Nt+cl I 10?1 SM022 BN HCL co 0 TATRuaquIrenImt PROJECT INFORMATION REPORTING REQUIREMENTS PROJECT SPECIFIC COMMENTS CV) ST01011cwnessday LK Project N:PRGJ-C121420 Summary Report only _—, MeVrad 29 Analysis 11 Nly lWheefabmslor N,Amov.,j F Rush 5 Misiness day :1 Npmn:WtIvolabrolm North Andover�AnNdi�virSummary r-aparl & L I /Ni 1,x", Ru"2 Rus*ms day L] PO IV: Full Min Package Ruah I Business day EDD Ixi Q.5 C1J Other(spedy): InItal Impfirger chmp volum"are requirod before Ihs tollotwing a Biwa 1� can,,,&Iarlcni.MOW 26,C7M-027&Method B C14 RefirgUlgh d By DoWTime I IReceivedMalhod Z31 TOVA dddC? RaIIfnu1_%h"d F-11 Q-T a 11 4nrwIv-4jd NAro I EF 17J TFF x TX luil;xa L I 1 (1) Cl) -j' lq�v,I C:) w z 'Am NALYTICAL DATA elementOne Certification: NJ NELAP NC009 39621 MAQ 5-29 Report Packet NE01 3AS-021420-RT-1 303 Append tj3G§of 1178 Analytical Calculations Metals- Element Results (pg) =ICP Results (lag/L)*Dilution*Final Volume (L) Where- ICP Results= Raw sample concentration (ppb)--ICP-Data Sheet Dilution= Diluted Volume--ICP-MS Run Sheet Aliquot Final Volume=FH=Final Volume (FV)--sample Submission BH=Received Volume (BV)*Final Volume (FV)--Sample Submission Aliquot (Used) Combined Results=FH+BH Mercury- Mercury Results (pg) =CVAA Results (ua) *Final Volume (ml) Aliquot (ml) Where- CVAA Results= Raw sample reading (pg)--Hg-Data Sheet Aliquot= Sample Aliquot (Alq.)--Hg-Data Sheet Final Volume=Final Volume (FV)*--Sample Submission * With the exception of the BH fraction where- =Received Volume (BV)--Sample Submission elementOne Certification: NJ NELAP NCO09 NE01 3AS-021420-RT-1 303 396Ap M6 ket Page 24 of 66 Analytical Calculations Spike Recovery- Spike (%) _ (Spiked Result (Iaq/L) — Sample Result (lap/L)) X100 Spike Amount (lag/L) Where- Spike Result = Raw sample concentration (ppb)--ICP-Data Sheet Sample Result = Raw sample concentration (ppb)--ICP-Data Sheet Spike Amount--ICP-MS Spike Table Duplicate Analysis RPD- RPD (%) = (Duplicate Result (ua/L) - Sample Result (ug/L)) X100 Average (lag/L) Where- Sample Result and Duplicate Results=Raw sample concentration (ppb)--ICP-Data Sheet Average= (Duplicate + Sample Results) 2 elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396AO 8 l V&ket Page 25 of 66 elementOne AIR TESTING SAMPLE SUBMISSION FORM Lab ID 39621 FH I BH Combined Analysis Due Date 11.15.22 QA/QC/Report Due Date 11-1T22 Cllent Mantrose Alrou'al! SMica,LLC bate Rec 11.07.22 Project No PROJ-021420 LTJ_"Rae 1223 _j r4:-S i a JOSO HCl Lot--41--Q- Rat.Method: Volume MarWY no Loss YINO Acetone Lot: b-Z(j 5 2915 S2M pie Idendfic flon 1 1.11-SDA in-M29-R1 U2-SDA In-M20-RI 17--Feld Blear* 2 1,111,S[)Aln-M29-R2 10 U2-S[)A In-M29-R2 18 Reagent Blank page-2-,- Duoicate --U2-SDA In-M29- 3 LII-SDA In-M29-R3 11 U2-SDAIn-M29-R3 Lli-SDA In-M29-R3 S Eke U2-SDA In-M29-R3 Spike W-SDA In-M29-R4 12 1 U2-SDA In-M29-R4 5 111-17FOut-M2915-RI V(56t-4Z9—/5-R1 6 "UI-FF 6ut-M2916-R2 14 1 U2-FF Out-v;2915-142 U1-FF Out-M2-9i5-RZ_Pu 21tcate U2-FF Ou M2915-R2 Duplicate I U1-FF Out WW6-R3 LI1-FF Out-MW5-R3 Spike U2-FFout--W915-L3_Spjke,_ 8 -J1-FF Out-W?915-R4 16 U2-PF Out-WI2915-144 I Samples 1-17 Analyses Requested Samples 5-7, 13-15, 17 CdPb ------------------------- as - 9- 5 j,4,& er (Samples - -- - - 3! Runs J Fil(Ace(FH) HNO-.(FH) 5%HNOVIO%;F'1a (OH) H140,,fA) KWO,(13) HCI(C) F B -7��,20 �N pH 2.0 (D N pH<2.0?7iN H<2 0 0 N pH<2 0 N Lab 16- ------6;e-d--T—Fv rn I By mi Fv ml 8V rnj Fv MI BW Mt Fv nil too, (�05 ago 3W- 500 Ito 46C> -LA qo 23 go pia -4 3.S 6 2,10 ILIGL 4 1 ta, 405 5 -rqO -Y5 SCE14.6 4C)o I a4o I ID 'D TS l PCs I -4-ib 'S'%S ao 410 aap a -4-160 147-1- gap 10,0 N--1 1164 Ito -j— 141 I i;L 12, v -+4 110 I I 113 167 So I I--;� 1 4157 1 30 1 1 IC � to 1 0 -74741,--6GL-- 16X21 3-39-24 7 1 Ito mll- 17 i 0(,, &0 103 v 41T �b SS Page I of 2 FH Outlet Prep By/Date oA2 at-,&�ff FH Inlet Prep Byff)ate_t�itto- 11/612022 9 AM BH Metat5 Prep SylDat62!M,�og, SH Hg Prep By/Date W- 1 tmv-ga SS t rPJBH Prep BVIDate wa JkL,6-,A'X A Prep By/Date DAS S-jo-a,7 Labeled Bylbate M5 Prep BY/Date, �b�z I B Prep Byloate D il,W- m5compt-tedBy/ba[eZ ��fq�zt Prep 8y1Date_TD %'•�?- U Verification BY7Y-!--W3-- elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396A0pM)Q,1rM8etW 3%W1 Vfflcket Page 26 of 66 elernerittOne AIR TESTING SAMPLE SUBMISSION FORM Lab ID 38981 FH I BH Combined Analysis Due Date 08.01.22 1 QA/QC/Report Due Date 08,0322 Montrose Air Quality Servk—a,LLC I Date RqS _07.22,22 Project No PROJ-014749 1 Fnrri _HWs Lot. apqf>1166 HF Lot, Si 1c;5o HCl Lot: Ref.Method: Volume Marked YD—J-VL-lurne Loss Y I Wn _3 Sam 719 Identification 1-16-Rea ent-blank i-_mP[--is, Hg Analyses Requested LSarryfes 18 Cd,Pb samples 18 PM M-29 Reagent Blank Lab 10 Fraction BV,ml FV,ml comments 6_7_�FH _-T-Acetone Blank —t'a--? _t o G-8A 1 FH I 0,1N HNO3 300 (C)o UnKei C-BA 1 A 0IN HNOi C-8B B '.9 l3H 6%HN02110%H202 a0o So aoonj loom, C14j"oNed t5om7 i C-10 8 14%KMn0.j11G1YdH2SO4 4 bL4 33 imfn 1 4!jot I r-.,%I. 6N HCl DI H2O 11400 Lab Communications � 96porn l +i(ojt-uaa-R) Sil _iaa --------------------------- --------------- SS Page 2 of 2 FH outlet Prep 3y0ate-pC42jt,�i FH Inlet Prep SylDate I 118P2022 9 AM 131-1 Metal.,Prep 3y1Dat02E1_tijhgg6H Hg Prep By/Datq.>�I,' 3s;by FHIBH Prep B iD te P it a A Prep By/Date Labeled ByOate W- 10. ZZ M5 Prep Bptt)a V§W_ i( .t-t B Prep By/Date T.PFL 0,10-'a ID Verification By I Da M5 completed BYq)at6_;pC, It 0Q&Prep By0ate_aftl �1-?-Z jt_ \Q bAOQ�_ elementOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396A0pWQF.M8.-QA SHWI V&,ket Page 27 of 66 elementOne Method 5 Particulate Lab#39621 Client MAOS Page 1 of I Balance checks Date: 11.14.22 2()-2,0000 AO-inf*COM.0tr9LeA Dam 2g 1.24E-06 miltma Datw Fitters A a S Is �rnplo Filter dire 0 D filti--,1,16 22 Btr.- ID N 0 nn In '1w Caftb Dow*Ow Time plus W.eet Tvne Fpt.w.vlt, T'r- - p --- Gi 39627-6 a3-109-13 6 0.3103 930 fl.3269 115 0.3069 39621-7 e3,109-14 7 (1.3120 930 5.3104 1615 03105 39621-9 e3.1Oq05 8 0.3117 93D 0.3099 1615 0.3097 39621.13 'e3-101-24i 13 0.3522 930 0.3523 1615 0,3522 39621-14 e3-109-191 14 0.3148 93D 0.3091 1615 0,3090 39621.15 e3-1 GS-20 15 03140 930 0.3060 1615 t 0,3062 �1 Blank Acetone Rinses c D D D Sampim Sample V.(. 11'4, 15>,- V 14 2 G�� ffil %q In H, PrA 1�L" cleealpilan &S-p" and Lcadiw Tear esev Time rwe ,,aH�u W44 ht 9 39621-6 86 UO 10.0621 930 10,0673 1615 10-0673 39621-7 1 -90 729 1 1. 9 6 930 011997_ 1615 10-8%6 1 39621-8 T 00 785 T;.4438 930 10.4456 1615 T0A456 39621.13 62 960 9-$141 930 9.8174 1616 9.8177 3-46ZI-14 95 748 11,0667 930 11.06JIG 1615 11 Ken 39621-15 70 854 10.1543 930 10,1566 1616 10.1566 77-A:'---- alk-18 102 555 9.82114 930 9.8286 1015 9.8286 C1 AcOrne Blank , 100 9B0 9.8401 1 93D 9,8401 1615 a 9j8401 Total Catches Sempba Fill*, Filter mw n,tgx Rftet Ac�lv-* Bag Hna[Bag A,,u to# ID Tar.,g Catch,g catch, Ace I Catch,rng Mg Bag I D Tara,a catch, T 3e621-6 e3-109-13 0,3103_ 0.3069 <01 6a0 111.0621 10.0673 52 5,2 39621.7 e3-109-14 13.3130 03104 0.1 729 10.895C 10.89% 40 4,0 39621-8 e-5-109-15 0.3117 0,3037 OA 7a3 10.44341 104456 1.7 11 39621.13 r-3-101-24 0,3527 0.34,522 960 [ 519141 5,8174 33 13 30021-14 d3-109-19 4.3148 0.3D90 <0,1 74B 11.0667 11.0680 1.3 1.3 30621-15 e,3-'09-20 0.314fl 0. 0 DA 854 1-10.1542 10 11,66 23 2.3 15&5 [ 9,$284 9,8285 OA 0.1 E1 Blank W l 9.8401 1 9,8401 CA '01 Demerit Cim.,f-c, r-mail 1 098,21 MAOS ldalhuj I-aA-161- elementOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396AOpM*U,1rM8a&09WI PMket Page 28 of 66 Lab 1D#e 3(i(A 1 olentOne Method 29 Hat Plate Worksheet ' Ghent fn�G?S Gate Digested: sl rCr 7Z Initials. � P 'Jorkshaet Prepared by. Sample Lab ID #of filters d gassed Spike Vol Prep Volume Comments Added I (mill i LRB NA t o o -L_RB Spike NA -sa _E1 , e� 1 i i I I Using appropriate 25ppm standard mix A,B,C,Ill E,H&1100ppm standard mix F spike solutions at the I 0 1 mL per 100mL for M29 samples_ i Spike standard us : A latm #02142 - B]at#021421-B C lot#021421-C D lot#021421-D P sat#021421-F E lot#021421-E of#021421_H Notes: I Nitric Acid Lot## 1�4 t11 " mLs Used: I Hydrofluoric Acid Lot## 51's 5C> mts Used: EI€MQnt One,Inc.F240 R1 Hot Pluto Shoot IA29 elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 396AO l OWIll l Page 29 of 66 eiernentOne Method 29 CEM gars W Microwave o sheet Lab i6#e 3 &QI Client: mpQS. Date Digested: tt,i45 ,a`a1 Initials: DP _ Workstteet Prepared by: DA2 Auto #of filters Spike Prep Volume Sample Sample Lab ID Val. Comments Loc. digested Added (mL) 1_ LRB - -- NA l b C> LRB Spike _ NA i �t r I Using appropriate 2,5ppm standard mix A,8,C,D,E,H 100ppm standard mix F spike solutions at the_j Spike standard us A 7#�021421-Ar 10t3mL tsr iu123 sareroptas.p" B lot#021421-B C lot#021�t2'I_ _ratD lot##021421-D E lot#t 021421-F H lot#021421-H Mates: i i i 1 y r Nitric Acid Lot# 2ti�i t`�, mLs Used. � HyrdrofIuoric Acld Lot# I ty mLs Usf:d; a Element One,Ins.P214 P2 Micrvwave Sheet tu429 elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 396AOpWdWr,MB l VWet Page 30 of 6 Sample/Batch Report Lip Uw Name;R2D2 Computer Name:PESERVICE-PC S&nivle File:C:1U,sem%PublicDocwnent5UPerkinElmer Synq aWdCPMMSsmpleNs4.saTn Report DateMme:Wednesday,November 16,2022 15;5G:54 AIS Lan. Batch 10 Sample ID Dcsnripfian Sample Type InItCluant Prep-W. Aliquot Vol- DiluteloVd. 7 QC Std 2 Sample 101 LRB Sample 102 a LRD SPK Spike-I of 2 11)3 3960&4 Sample 104 3-0508-5 Sample 106 d 39608-5 Duplicate of 5 IM 39608,6 Sample 107 s 3960" Sp*a-I of 7 108 39608.7 Sample 109 396115-11 Sample I ILI 39695-12 Sample Ill d 396DS-12 Duplicate of 11 112 39608-13 Sample 113 9 30608-13 Spike-1 d 13 114 3M8-14 Sample 115 39m8-15 Sample 116 LRB Sample 117 a LRB SPK Spike-I of 17 118 39621.5 Sample 119 39621-6 swripie 120 d 39e21 6 Duplicate of20 121 39621.7 Sample 1Z2 s 39621-7 Spike-1 Of 22 123 39621-13 Sample 124 39821-14 Sample 125 d 39821-14 OuprcaLa,Of 25 126 39621-15 Sample 127 a 39621-15 Spike-1 of 27 128 39021-17 Sample 30521-18 129 Sample 1 GG Std 1 SaMp4o 4 QC Slid 4 sw%ga Page I elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 396AOpM)tUSM8--O ORWI Mket Page 31 of 66 Dataset Report User Name:R2D2 Computer Name: PESERVICE-PC Dataset File Petit:C:\Users\Public\Documents\PerkinElmer Syngistix\lCPMS\DataSeAI 1 1622-3M Report DatefTime:Wednesday,November 16,2022 16:50:13 The Dataset Time Sample ID Batch ID Read Type rlelirlipuar" lnlq,.Quant Prep-VaMquot Vol- Diluted Vat. I&M 16 Wad 16-Hov-22 Blank 131ank 15;07:08Wod I64dov-22 Standard 1 Standard#1 15:09-03 Wad I&Naw-22 Standard 2 Standard#2 15:10:57 Wad 16-Now-22 Standard 3 Standard#3 16712-51 Wed 1"olh.22 Standard 4 St.9 rd ard#4 15:14:45 Wed 1 e-Nev-72 Standard 5 Standard#5 15 10;39 Wed 1 ff-Nov-22 QC sw I OC Sta#1 15113:34'.Yed 1044ov-22 CC Sid 2 CC SW 1#2 15:2D:27'hea 16-Nav-22 CC Sid 3 QC Ste#3 15:292P Wed 16-Nov-22 CC Sid 4 QC SM#A 15�24:16 wed 16-Nov-22 CC Sid 5 QC Sid#5 1$-412 Vied 16-Nov.22 OC SW 6 or,Std t$ 15:26:06 Wed 16�Rov.22 CC Sid 7 QC Sid#7 15:32A5 Wed 1"ov=22 OC Std 2 Sample 15:34:40 Vied I"ov-22 LRB SaMP&O 15:W:34'Wod 16-Nw-22 LRB SPK a Spike-1 of 15 15,28:28 Wad I&Mov-22 396OB-4 Sample 15:42:26 Wed 18-Nvd,-22 396Q8-5 Sampb %5:44:20'tN--,d I&Nov-22 39608.5 d rhipliralp of 1 R l5,4G-,14 Wed 16-N av-22 3G,6M-S Sample 15:48:09 Woo 16-Nov-22 30608-6 a S PI-Ma-1 of 20 15,50-03 Wed 1644ov-22 39608,7 sample 15-51:57 Wod 16-Nov-22 $9608-11 Sample 15 53:51%led 16-liw-22 3060a-12 Sample 15,55:45 Wad I S-Ncev-22 99$118-12 d [54ftata of 24 10'.04:29 Wed 16-Nov22 CC Std 1 Sampie 16-05231AIed 16-Nov-22 CC Std 4 Sample 'IfIrOBIGINed 15-14ov22 U6&!i-13 Samp4o 161012 Wed 16-1 39608-13 a Spike-I of 28 15 12:06 Wed 15-Nol,,22 39608-14 samplu 18.14:00 Wed 16-Nov-22 319605,15 Sample 16:15�54'Wed t&Nov-22 LRB Sample 16:1748 Wed I"ov-22 LRB SPK 8 Spike-1 of 32 16:19-,42A4d 1"orv-22 39B21-15 Semple 16:2t-36'Wed IC-Nov-22 a 21-6 Sample 16:23--30 Wod 16-Nov-22 39M-A, d Duplicate of 39 16:2524 Wed 46-Nov-22 30621-7 Sample 1627:1 B Wed 10-Nav-22 39621-7 5 Spy-1 of 37 162913 Wed 16-Iov-22 CC Sid I CC Sid#1 16:31:08 Wed I&A—Im 22 QC Sid 4 CC SW#4 16-31-03 Wad I S-Ww-2,7 30621-13 Sample 16-34157'Afed lr-Nov-22 39621-14 Sample 16-36:5t Wed 16-Nov-22 U621-14 d DupW41e of 42 16--:30.,45 Wed I G-Um-22 313621-15 Samplu 10 40;19'Alea I G-KPY-22 30621-15 5 Spike-I of 44 1fl-42:33 Wed 16-Nvu-22 39621-17 Sample IGA4:27 Wad 16d4ov-22 39621-18 Sample 16--46,22 Wed 18,N5V,22 CC Sid 1 QC Std 1#1 16-48:17 lNed 16-Non,22 CC Std 4 OC SO 94 Page I elementiOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1 303 396AO I Mket Page 32 of 66 Method 6020&200.8 Metals Summary Report Sample ID.Standard 5 Sample Date/Time:Wednesday,November 16,2022 1514.45 Sample Dasedpuon., Number of Replicates:3 Swab IC: Dataset Fl1w C.lUsersiPubitcADocumetftlParldnElmorSyngtst]xUCPMStDalaSetII1622-3aMtandard 6.072 Sample Prep Volume(ML): Intel Sample quantity(Mg), Alquot Volume(mL)., Diluted To Volume(mL)! Autosampler Position: Calibrabon \nalyte Curve Type Slope Correlation Coefficiant Intercept j Linear Thru Zero ic Linear Thru Zero kh Linear Thru Zero "d Linear Thru Ze0.005 10,999990 0.00 'd Linear Thru Ze0.012 O.999990 0.00 10 Linear Thru Zero z1b Linear Thru Ze0.041 0.998936 0.00 (r Linear Thru Zero elementOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396AOPWbW!5;MI9--Q!O BWIXWI Vikket Page 33 of 66 elementOne ICP-MS RUN SHEET 11/16/2022 AJS Loc. Dilution Sample Ili Client Type !Nei9ht(9) Prep Vol(ml) 7 00 Sid 2 Sample 101 LRd Sam le 100x2 m 102 s j LRS SPK Spike-1 012 10Ox2 103 ; 39608-4 Sample s f. 10flx2 104 39608-5 Sample 10Ox2 Sta� d 39606-5 _ - Dupkcate of 5 106396a8-6 1i00ple x2 - -- _ ,07 s 3960M Spike-1 of 7 1OOx2 1Oa - 59008 7 Sarc e 1OOx2 - - 109 396' 11 Sarrap3a_ Q - iOO -- 110 � 3E160&-12 Ill d 1 39608-12 Dtipf"te of 11 { 100x2 112 39606-13 Sample 1 OOk2 113 s 39608-13 i Spike-1 of 13 ': 1 OC1x2 114 39608-14 _ i Sample IOO)Q 115 39608-15 i Sample 1OOx2 116 LRB Sampfe -1 10W 117 s LR®SPK Spike-1 of 17 _j-_-__I_ 10OaC2 118 -- 39621 5 Sam le IOO)Q 119 1 39F,216 Sample 10Ox2 - - i 120 d 3962116 j Duplicate of 20 100x2 121 19621-7 Sample 100x2 122 s 39621-T aSpike_1 of 22 j 1OOx2 _ �� 123 3962.1-13 I Sample 10Ox2 124 � 3962i-14 i Sample - 1OOst2 126 d _ 39621-14 Duplicate of 2� 1 OOx2 m 126 39621-15 Sample - 100x2 127 s 39621-15 1 Spike-1 of 27 j 1 OOx2 128 39621-17 ( 1 Sample 10Ox2 123 39621-18 — Sample 14Ox2 S lkes are oat at 0.02,nL of 26ppm spiking solution lot 021422-A In a final volume of 1OmL Submitted for QC by: Mme: QC Review By: DateMff . D aw 11116122 16:52 NNU Re-Test Required: No: Y,es: Comments: Resubmitted for QC Qaterrimo: QC Review: By: DatelTime: by: T:Worms4glank Formsl;r208 R2 ICP-MS Run Sheet.xls elementOne Certification: NJ NELAR NCO09 NE013AS-021420-RT-1303 396AOPMAUSMB l Mket Page 34 of 66 i wd 0:,G ZZOV91 rt!PV;P pam p vm uswnat�etc�'yi w;,9r °}�+ � •5 �t'q 4t(y��'��c .q,�ytwut a?io-.R�' }��' ',fy, `"''Y� ��,��,; COD CL cau - 3 t N 1 apt C ` a i- ....___. ., .... �. �...._... ._.. c _ (... ,,d." Ya.rI. _.mit 1 Jf C—s-y`g f-m "It {-x' t'Z*ARNa f'rr�d 'S ]D:�(I vfl :9 apFl.FILE F4$Fl S :'NFL Fqb b&142i 4+8}R RRft$� ''+MF;�� f,.��IX¢,�5 Z$�LK 6@F"x 2RaF1415 lit4!a'MyT'-: M � urtad��-+cw+n uev. e •5 �'�P+-0W'�. Ci i -t west OR,*, B ro ss d _ e' N •kLt "` M 1 ak+M'4N4,+W+ll Y*fWd uM1NS�J ANy1, f'"L$+ Fu•a'leageL F+ M+4hia �Hy+s f-.-0 Avil �(.Y....:'.�;`.;'�dszs� x 7rr''u 3+h-3k`'r-7 a _?ti._.. r...... .''�'��. „.:: rS�f K S *� 7` x r 1 _r. l'S. "�-',""e, .m.ar.;b`.a-� ..<E.r^*NLepW R 14 r N O ( Q M O W Z Sample/Batch Report User Name:bubu Cornputst Name:EI-901214 Sample File:C:tUsers',PublWtOocLimetitsTerkinElmei SynglsdxqOMMampl0a3.s&M Report DatadTlma:Thursday,Novembw 17,2022 11:E&W AtS Lac. Bath ID Sample 10 Descriptaq Sample Type Init.Quant, Prop Vol- Mquct Vul. Diluted Va. SuEdis Ratio 7 OC l3ld 2 Sample 201 396E)8-7 Swnp* 202 X6 396,3&13 S&MPW 203 x6s 39606-13 5,-;Ae-I at 3 204 396OB-14 Sample 205 396118-14 FH Sample 206 3r.608-14 BH unjg Sample 207 x5 3013-01-15 Sample 208 x5s 39621-15 SpIke-1 of u 2C9 3MI-17 Samwe 210 39621-11 FH se-"fjp'A 211 39621-17 SH Lmdig Sample 212 39521-18 SErpla 213 39521-18 FH Sample 214 39621 08s Sample 215 321 C9 Sample elementiOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396AOpMAUSM8-Vb' R%Wl PMket Page 36 of 66 Dataset Report User Name.bobo, Computer Name;El-BOBO Dataset He Path-C-\Urers),PubiiaiDocumentskPark!nElmer SyngistIxVCPMSXDataSeM 11 722-3b% Report DateMme:Thursday,November 17,2022 11,55:26 The Dataset TIrne Samplo 11) baun I D Read Typa Descution InK.Quant Prop.Vol-fukqwt Vol. 011uWJ Vol -11:11-66 Thu 1?-Nov-ZZ El4ank Blank 11-1116 Thu IMav-22 Standard I Standard#1 11 A CZ6 Thu 17-t+N.22 Standard 2 Standard 42 11:15,05 Thu I-e-Nov-2-2 Standard 3 standard-93 11:1725 Thu 17-Nov-22 Standard 4 Standard#4 11:18:45'rhu 17-Nov-22 Standard 5 Standard#5 120:06 Thu 47-Nov-22 QC Sid I Qc Siff#1 112125 Thu 17-Nov-22 QG Std 2 Qc Sid 92 11:22:46 Thu,]Mm,22 QC Stcl 3 UO Sw 93 11:24M Thu 17-Nov-22 QC SW 4 Oc stil,-. 11:26-26 Thu 174,lnu,22 cc Std 5 OC Std#5 1 1_26A 8 Thu 17-Hov.22 QG Std 6 Qc sw#0 I t28,,D9 Thu 17-KOV-22 QC Std 2 Sample 11M3 36 Thu 17-Nov-22 393C18-7 sampte 11'.31:56 Thu 17-Nov-22 36,508-13 X5 Sample 11:33-16 Thu 17-Nov-22 39609-13 x5s sp€ke-1 0115 11:34;36 Thu 17-Nov-22 39608-14 Sample 1 1:a5:66 Thu 17-Nov-22 396OB-14 FH Sample 11:37:16 TtIU 17-NM 22 3,34,08-14 BH undig Sample 11:38.,36 Thu 17-Mov-22 M621-16 X5 Sample 11.39:57 Thu 17-Nov-22 39621-15 x55 Spike-1 Lf 20 11,41:17 Mu 17,Nov-22 39621-17 SamWe. 11,42:37 Thu 17,Nuw-22 39521-17 FH SaTnr�a 11 43M Thu 17-Nov-22 QC Std I Qc Std#1 11:45:19 Thu 1744n-27 QC Std 4 QG IM#4 IIA45:41 Thu 17-N,,�-22 39521-17 DH undig Sample 11A,4:01 Thu 17-Nov-22 39621-1a sample 11:49:21 nu 17-Nc,%-22 3M21-18 FH Sample 11:60:42 Thu I 7-NDv-22 39621 c8a Sample t 1:62--02 Thu 17-NwoL-22 39621 G9 sample 11:53:23 Tau 17-Nov-2.2 Qc Std I QG SW#1 11:54--43 Thu 17-Nov-22 QC Std 4 OC Std#4 Page I elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 39680pMAWICMB W- I Mket Page 37 of 66 Method 6020&200.8 Metals Summary Report Sample ID,Blank SamptoDatan'Imo:Thursday,Novembarl?,2022 1111:66 Sample Description: Number of Replicates;3 Batch ID: DatasatFile,-C:%UsarstPublieMocuments%PwidnF-Iivier SyngistixklCPMSVDataS*tAlII722-3btBlank.001 Sample FImp Volume(mL): Initial Sample Qua"(mg): Aliquot Volume(mL): Diluted To Volume(ml.): Autosampler Position: 1 Calibration Analyte Curve Type Slope Correlation Coefficient Intercept Li(7) Linear Thru Zero Pb Linear Thru Ze0.020 0-998462 0.00 Kr Linear Thru Zero ilio(ISI) Linear Thru Zero Sc(IS1) Linear Thru Zero :Zh Linear Thru Zero J Linear Thru Zero elementOne Certification: NJ NELAP NCO09 NE01 3AS-021420-RT-1 303 396AOpWQSM8aQO WQW1 FMket Page 33 of 66 elementOne ICp-MS RUN SHEET 1111712022 AIS Lac, Dilution Sample ID Client Ype Weight(g) prep Vol,(mg 7 QCStd 2 Sample 201 396G8-7 SImpl 3.nav2 202 X5 3960843 Sam le 100x2 Z63 x5 39FDA-19 ....... -plke 1 of 3. .. 100x2 204 39608-14 5vm le —6ox2. 20S 39608 14 FH Sample 160 206.. 39608-14 611 und;g _.. _ Sample __ 310 0' x6 39621-15 SaT tple IM.2y 208 x5s 39621-15 Spike-1 of 8 10OM2 209 39621-11 Saroole 100x2 210 3gt;21-1?FF# S�ma$le 100 211 39,521.17 6H undill Sample 310 212 39621-18 Salt le_.. .,__ 100xz 2x3 J961-181 it Sample � 100 214 39621 CSa Sam fe 300 215 39521 C9 Sample 300 Spikes are post at 0.02mi.of 26ppm spWng soluteons tot 021422-ABCU&F In a final volume of 19ml- Subm tted for QC by: l ®atalTime: 10C Review ay: I AetetTime: 0BW W1712211:63. Re-Test Required: - No: �s:. Cotmt�owts: Re>submFttedfor t3C by: ...--0 Revtow L OY: l?ake +me: elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 39680 _FMB U Mket Page 39 of 66 Method QC Spike Tables Analyte Mass ST1 Conc ST1 Det Lt ST2 Conc ST2 Det Lt ST3 Conc ST 3 Det Lt Li(7) T016 Pb 207,977 50.000 1.000 25.000 tOOO 100.000 1.000 Kr 82,914 Rh 102,905 Li 6-015 elementOne Certification.- NJ NELAP NCO09 NE01 3AS-021420-RT-1 303 396AOpM*UX;M8-,&WQWI Vt%ket Page 40 of 66 Quantitative Analysis -Summary Report Sample ID:Blank Sample Dstw7kne-,Thursday,November 17,2022 11:1 1:56 Report[DatefTlme:Thvrsduy,Novembv 17,2022 111t 6!22 Solutlen Type.1318nk SarripPa Type:Ssrnpbs Aotosemplar Position:I Sample Description: Batch 10- Sample FjlF,C.-tU-%eTs%PubiIJ6DocwmemsT-erkinElme-r Syrg!sWJCPMZampleta3,sam Matrxl File:ClIUsorsTublEe4DmimentstP"inElmer Dalaset File: 11722-3bWank.001 Initial Sample Quantity(rng): Sample Prep Volume(mL): P.Oqw,'A Volume(ml-): DIlutod to Volute (mL) Torch Z Poslition(mm):G-DG Results(Mean Data) is Ana" Mass lnbenslty RSD Cone. RD RSD UnN, Wank Intens. Mode "L(IS I) U(7) 7 1 D0277.3 OA PP171 Standard Ho(IS1) Pb 2a8 623-7 29.4 ppb Sf—,ndard Kr 83 65.0 4.1 upb Standard HO(ISI) 165 996114.2 1.2 pp b pb standard SO(ISI) A6 a86986,4 016 ppb Standard Rh 103 764461,0 0.4 ppb Standard U 6 1926714-4 0.4 Oph Stw-,dard samplo IM Blank Report DaateMme;Thursday,November 17,2022 11:66:22 Page I elementOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396AOpMAQ-ICM8--IO4RW, I Mket Page 41 of 66 Sample/Batch Report War Name:baba yt Computer Name:EI-15080 Sample Pale:CiSUseislPub46Docurznts'.PGridrEtEnaf Syagi&txvCPMSI5aMlcs5.sam Report Dockrtlma:Thufway,November 17,2022 14:31:20 AIS Luc- Batch ID Sample 113 De%cr<p"n Sample Type ti-ift.Quam Prep.Vat. AfiquotVd. DftWVO. Saids Rativ 7 OC Std 2 sampfe 2 OC Me 2 Sample 101 LRB Sample 102 s LRB SPIT Spke I Ot3 103 �ne2gl s3rT4A 104 391325-2 S&TI& 1051 d 39625-2 DUP41cata 016 105 39626--3 Sample 107 a 39525-3 Spike-I of 8 ice 39625-4 Sample log 3962" Samplo 110 39625-4 Fit Sample ill 39625 c8a Sample 112 39625 C9 Sample 113 x2 LRB Sample 114 x2s LRB SPK Spike-2 of 15 115 X5 396251 samp4s 116 x5s .39825-3 Spike-1 of 17 117 X5 396254 Sample 118 )(5 LRB Sample 119 x5s LRB SPK Spike-1 of 2C 125 4 U,621-13 sample 126 x5 M21-14 Sample 127 x6d 39621-14 Duplicate of 23 Page I elementiOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396AO ket Page 42 of 66 I"---)�V , - Dataset Report 6 �7-7- User Name:Bobo Computer Name:El-BOBO Dataset File Path:C:lUsers\PublickDocumentsPerkinEimer SynqistIxVCPMS\DataSet\I 11 722-6b\ Report DateMme:Thursday, November 17,2022 14:30:11 The Dataset Tkne Sample ID Batch 10 Read Type Description Ht.Quant Prep-Vol.Aliquot VoL Muted Vol. 12;40$9 Thu 1 I-Nov-22 Wank Blank 12;42:56 Thu 17-Nw-22 Stondara 1 Standard 91 12.45:T8 Thu 17-Nav4� Slandand 2 Standard 92 12:47:38 Thu 17,Nov-22 SMndaTd 3 Standard 93 12A9;57 Thu Standard 4 Standard#4 12:52:TO Thu 17.Ww-22 Standard 5 Standard#5 12:54'."- Thu 17,Nbv-22 QC Std I QC,91d#1 12,56M Thu 17-Nov-22 QC Std 2 QC StA#2 12:5018 Thu 17-Nov-22 QC Std 3 GC SW#3 13:01:36 Thu 17-Nvv-22 QC Std 4 Or,Sw#4 13;03:56 Thu 17-Nov-22 QC Std 5 GC Sw#5 13:0617 Thu 17-Nov-22 QC Std a GC Std go IVAW Thu'M-Nov-22 QC Iw 7 QC SM Arl 13:10:57Thu J744oy-22 QC Sid 2 Sample 13:17:577hu 17-Nov-22 LRB Sampde 13:20:16 Thu 17-14ov-22 LRB SPK S Spike-1 of 15 t3:22:313,Thu 17-Nov-22 �625-1 SaMp-* 13:24:66 Tbu 17-Nov-22 319625-2 Sample '3:27:16Thu 1744o,-22 39625-22 d Dupl[c�ate of TO 1329:35 Thu 17-Nov22 319625-3 sampse 13:31:56 Thu 11 7-M-22 39625-3 Spike-I of 20 13;34:14-q'hu 17-Nov-22 29625-4 sample 13:36.,34 Thu 17-Nov,22 QC Std I Qc Std#1 13:38-54 Thu 1 T-Nov-22 QC Std 4 QC Std#4 1341716 Thu 17-Nov,-22 .39625-4 Sample 13,43-34 Thu 17-Nov-22 39626-4 FVI SaftV6 1'3-4&5:3 Thu 17-N*v-22 39525 C89 santme 13-4&13 Thu 17-Nov-2.2 39t325 CID Sample 13-50-,33 TIld 17=Nov 22 QC Std 1 QC Sid#1 13:52.'52'rhu 17-Nov-22 QC Std 4 QC Std#4 14-01-12 Thu 17-Nov-22 LRB x2 Sample 14,03,-$2 Thu 17-Nuv-22 LRB SPK x2a Spike-2 of 31 14,05,!51 Thu 17-Nov-72 39625-3 X5 Sample 14MIO Thu 17-"-22 35525-3 X58 Sake-I of 33 14:10,L30 Thu 17-Nqv22 3W2" X5 Sample 141318 Thu 17-N9v22 LRB X-q Sample, 141 5:35 Thu 17-Now22 LRBSPK X51S Spike-i of3s 14;17:57 Thu 17-N-22 39D21-11 X5 sample 14:20:17 Thu I r-N-w-22 36621-14 Xb Sample 14:22,-36 Thu 17-Nov-22 39621,14 x5d Dupficale Of 39 14:24:56 Thu 17-Nov22 QC StdI QC Sw#-1 14,27,16 Thu 17-Nov-22 QC Std 4 GG SId#4 Page I elementOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396A0PM;kW9,M8--V#Wpotl FMket Page 43 of 66 Method 6020&200.8 Metals Summary Report Sample ID:Blank Sample DatelTime.rhursday,November IT,2072112;40:39 Sample Description: Number of Replicates,a Bath to,, Datawt File.-CWsgrslPublFciDocumentskPorkinElmor SynillsNACRASIDMOSWI I 1722-5bStank,001 Sample Prep Volume(mL), Initial Sample Quantity(mq)� Aliquot Volume(ML), Diluted To Volume(mL): Autosampler Position: I Calibration Analyte Gurve Type Slope Correlation Coefficient Intercept Ll(7) Linear Thru Zero V Linear Thru Ze0.042 0.9,99942 0,00 V-1 Linear Thru ZeD.021 0.999936 0,00 Cr Linear Thru Ze0.0117 0.909958 0.00 Mn Linear Thru ZeO.01 3 0,999959 0.00 Co Linear Th ru ZeD.008 0.999968 UO Ni Linear Th ru ZeD.007 0.999937 0,00 Cu Linear Thru ZeD-01 1 0.9D9962 0.00 Cu(66) Linear Thru ZeD 007 0.999934 0.00 As Linear Tli ru ZeO.005 0.999976 0,00 Cd Linear Thru Ze0,005 0,999972 0,00 Cd(1114) Linear Thru Ze0,01 2 0.999948 0.00 Sb Linear Thru Ze0.009 0.999923 0.00 In Linear Thru ZeO.O 12 0.999910 0,00 Pb Linear Thru Ze0.021 0.999928 0-00 Kr Linear Thru Zero Rh OSI) Linear Thru Zero He(181) Linear Thru Zero Sc(IS1) Linear Thru Zero U Linear Thru Zero elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396AOPW4*,crM8Q'0 Qqxttl R%ket Page 44 of 66 elennentOne ICP-MS RIJN SHEET 11/17/2022 AJS Lor— [dilution Sample ID Cllent Type Weight Prep Vol(ml) 7 QC Std 7 5ample 101 LRO Sample 1O0X2 102 5 RRSSI4Y. spike-aof3 AM 103 39625-1 Sample 1O0x2 104 39i 25-2 Sam a 100x2 105 d 35625-2 Dttpkate of G 10Ox2 1015 35625-3 Sam a loOx2 107 s i9Ci2S-3 Splke-2 of S g 30tix2 1D8 39WS 4 Samp&ri tnnxa 149 396a5.4 Sample t 10Ox2 330 39625-4 FH 111 3 ......9525 CSa Sample 105 11:2 "525 09 Sample .__. 105 113....... x2 LRB Sample 100x2 lid . � LRB SPK S 'ke-2af15 100x1 115 x5 39625-3 5alnple 10ox2 116 x55 39G2.5-3 Spike 1 of 17 - 100x2 117 x5 39625-^4 Sample 3OOx2 11S x5 LRB Sam le lOf;x2 319 x5s LRB SPK Spike-1 of 20 fOO�G' 125 x5 3'9621-13 _ :anr p le .. low, 126 x5 3�,521-14 _ Sample kO0x2 127 x5d 396Z1-14 17•uplEcate of 23. ,_ LL 1111 11 2 . . 3pMoa are poet at O.02mL of 26ppm spbkfng so9uttom lot 021422-A&13 in a find volume of 1DmL 30mttted Tot 9C fry: BatajTkne: qQG ROVIO ti BY: DatEYTbme: RMH 11117,12214:33 J Re-TestRaqulmd: o: -._. . ..Yes: �Cwnmsnts. Resubmitted for QC by: l7atetl'lanne: QG RsvNw; �Y T2amedTime; elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396AO S 6 tl Mket Page 45 of 66 Method QC Spike Tables Analyte Mass ST1 Cone ST1 Det Lt. ST2 Conc ST2 Dat Lt ST3 Cone ST 3 Det Lt U(7) 7.016 v 50,944 50,000 1,000 25.000 1.000 100.000 1.000 V-1 50,944 Cr 51.941 50.000 1.000 25.000 1.000 100.000 1.000 Mn 54.938 50.000 1.000 25,000 1.000 100,000 1,000 Co 58,933 50.0,00 1.000 25.000 1,000 100-000 1.000 Ni 59.933 %GOO 1.000 25,000 1,000 100.000 1,000 Cu 62,930 50.000 1.000 25.000 1.000 100.000 1.000 Cu(65)64.928 %000 1.000 25.000 1,000 100,000 1.000 As 74.922 50.000 1,000 25,000 1,000 100.000 1,000 Cd 110.904 50.000 1,000 25.000 1.000 100,000 1-000 Cd(11113.904 60.000 1.000 25,000 1.000 100.000 1.000 Sb 122.904 50.000 1.000 25.000 1,000 100,000 1.000 71 204.975 50.000 1.000 25.000 1,000 100,000 1.000 Pb 207,977 60.000 1,000 25,000 1.000 100.000 1.000 Kr 82.914 U, &015 elementOne Certification: NJ ELAP NC009 NE01 3AS-021420-RT-1 303 396AOPMA*_ICM8-,O QW1 V&,ket Page 46 of 66 Quantitative Analysis-Summary Report Sample ID.Blank Sample Dateffirne:Thutaday,Novpmt>--17,202212,40!39 Report DatelTime:Tnursday,Noyambof 17,2022 14;31;39 Solludon Type:BlerVK Sample Type:Sample Auto,sampli-r PoBltory I Sample Description: Batch M, Samr1a,Fif,,4, SyngintiACPMSL1ampwa5aarn Motrod File,C,kUaorsIPubllokDicumoritsPOTWElmor SyTq3W0C1PMSWathod`ka5,mth Data5at File:C:qJsarsAPubrpMD=umntslPerkinE[mr SyngisL[k,,ICPMSOalaSeL1111722-,lb�Blank.00'I Initial Sample Quanft(mg): Sample Prep Volume(mI ArquatValume(MW: Diluted to Volume(mL)� Torch Z position(nw);0,00 Results(Mean Data) is Analyte Mass, Intensity RSD Cana- SO RSD Units Blank Intons- Mode SO(ISI) U 17) 7 97833A 1.3 Ppb Standard Rh(I Si) V 51 626002 0.6 ppb Standard Rh(IS1) V-1 51 45000-5 2.2 inpitt Standard Rh(l 3 1) Cr 52 104M2 1,8 ppb Standard Rh(181) Mn 55 45TO 3.8 ppb Standard Rh(ISI) Co 59 62.0 2a9 ppb Standard Rh(181) Ni 60 6143 592 ppb Standard Rh(ISI) Cu 63 427-7 61 ppb Standa4d Rh(IS 1) Cu(66) as 3217 30,4 ppb Standard Rh(4S1) As 75 -7U7-2 22,9 ppb Standard Rh(ISI) Cd 111 26.9 46.6 ppb Standard Rh(161) Cal(114) 114 745 80.1 ppb Standard 110(ISI) Bb 123 17(13 1241 ppb Standard ,10(1S1) T1 265 357.T (5.3 ppb Standard Ho(161) Pb 2D8 304,0 22,4 ppb Standard Kr 63 62-3 11,4 P0 Standard Rh(ISI) 103 718484.1 1.5 ppb Standard Ho(ISI) IE15 9CA15913 2,2 ppt> Standard Se(161) 45 849556,7 0,9 ppb Standard a 19134.79.6 0.5 ppb Stdodard Sample JD-.Blank Report DaII,Thiursday,Novembar 17,2M 14:31:39 Page 1 elementOne Certification: NJ NELAP NCO09 NE01 3AS-021420-RT-1 303 39680 1 V&ket Page 47 of 66 "6 fio P,81 6lp, �2 QO 00 Q 0 0 Q C-4 -48 P, — P, �2 Q 0 0 Z,0 0 IZ,0 0 0 us us us us us us us ul us us us us us us us u Cl tl it l : u; io�u;ti�us us it 4r us us IN I's,M "A' I'A' "i Is us I us Is T—. 7. 7. LU � Ica C Z foo ul 0 0 .3 r c sr v,"i t"'.-I'm'�'3 w "o m t'� fsi.,I"i III 'm t.- '4 m, 8 P.8"1 cj�"j 8 8 q 8 F!"R.8 8�-'.P,P, P.P.q"ll a 8 Fl,81 8 8 PI ell a 8 8 a C'. R 8 8 8 P.8 P. 14 L Cu 4 pi P,-P, a 4 a 8 — —— — — —— — ——— — — — —— —— — ua co U 10 in "A "A im,1.3 tm -.4'm"'4 m mi if",u1i,.I"A im "g t W 0 us us 0 rq rl so IC!in n I >> 'T' >c it t3 d A T ZK"8 pi(�i��l N' A'1-)'41 "n A" Z9 z ce) 0 .I'D t ut n.- . v v I F3 Mi ON c c Fj s 41 �Li F 77 a 45 tyou a 0 17, Cb ILI w , . P IN Uj m m (L a 0 U z U U 1A 0 Li I. < CO O LLI z z m U) 6 v u p-,�o 1j,131-X� III Ul U,0 4 49 1p to i L-A u CA) M u. IS UA c <z 7,-n>,,4, 7 rn rn ey ry rB CD !'61 A In — — — — — — — — — — — — — — — — — — — — — — — — — — — —— C) CD cl 6668688 888 86888 A- 88 F; A F; 6 F; A F; A F;A F; F-;gi F;c1 F-;F;F-; u u in i-; PI A P, PI A A A P, pl p p p p PI P. P,p P, P, p m P, a P,P, P,I P,P,P,m P, In P, P,P,m PI �g f-A A GO (D Z 9 C— C.0 Z tY 0 r- -_- --6- 6- -- C, S, SSE -6 -6 3 0-* c 3 s 3 0- 3 0 0 col 0') ce D -0 m > z 0 C-) 0 CD i5 0 . . . . . . . . . . . :I 77 (0 CL rrr 9c A 'A A -4 A A A In -n' .n',,,nUI n," n,n In .,j, Jr n In n In In n.n I. I. I. In I In In In In In I 40, CD I. 6n 0 `on A In 0 0 .. 1. knton I. Inon_" In I. k"k"o In Z, Zi I 'j, 1011 0-1 c"ll Ili:1., 101, Nj �,I I'll, 0- C-1. 'j, lu,, I., U-1 oll ll�I a,, -0 IJA 1119 MERCURY BATCH DIGESTION-RUN WORKSHEET Date Prepared/Digested: ri G 11, Prep By: SIF File#: Block#1 Temperature: Start Time: Machine ID: 7,rn,, z Block#2 Temperature: Ste;)Time: t, Batch Analyst: Block#3 Temperature: Typed By: erified BX: J,,2 0.4ugW N Curve&QC's working std Bid„ ml FV, ml Standard Lot Numbers Lab BLK Standard#1 for working std) "31 batch) 0 40 40 Lot L bi.� 2 0.004'u", 0.01 ml 40 40 Wo kIng Standard 3 0.04 ug 0,10ml 40 40 Lot 4., by:ter; � 4 0.08 Ug 0.20mi 40 40 Standard#2(QC#2): 5 0.16 uq 0,40ml 40 40 Lot#: .ttn5 OL,,-4, 6 0 20u2_ 0.50ml 40 40 Standard#3(QC#3):,,�P,-;- 1 .Lot#: 7 iQC_#2=_0,08ug 0.2ml#2 std 40 40 1 #3 std 40 40 lCurve prepared by:,:,,r.; Initial Review B a. Date: ti,u -4.-A Time,-��_ -_ i-4 I Final QC Review R Time:Date. Ij j I Lfl 1,Z Comments:__ Pre;Ali%01 Afiquolor FV,m1,cr-1" AJS LAB# Method tin Jsed,mL Oak Mass for canc. Comments 9 10 L,1 L LT4 12 Z 13 141 15 16 17 18 t NOTES: Lab blanks and spikes must be prepared with each batch digestion "+"Denotes spike for H9, Use rafinraport wuAiny eJ.4uq;rn1 standare a:t1lu rate Lf 0.20m1 per 43rr-I semplL,unless otherAise noted. Digestion chemicals to be added in order at the following rate per 40m1 volumes. H2 SO, @ 2.Oml...... HMO @ I 0ml....... KldnOo e 6.Omi......... Persulfate @ 3.2m1 H2SO4 Lot# d1 1 _HNO.j Lot#_, HCY Lot Porsuffate Lot KWO, Lot# Hydroy Lot#,,_t-, Clear sa y L es,after di2estion with 2.4 m0l of Hydroxylamine solution. Element One, inc F209 R9 page I of elementOne Certification: NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396A0pMAU,1:QMPa&Wtgmtll V&ket Page 50 of 00 elementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIF File* AlIqual at F%'.rnk-w calumass furwnc. Comma Als LAB Method 20 21 22 23 t. 24 25 26 27 28 29 32, - 331 - 351 36i 37 38 39 40 41 42 43 44 45 46 47 o 49 j C 50 ti 53,1 5=4 Element.One,Inc F209 R9 Page 2 of 3 elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396A0pWQF1,M8--0 WtWl Mket Page 61 of 66 elementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIFRIe#: ,jjtayk Wt I-V Prop,Aliquot A-,',iq uot or FV,,,iL or'T AIS LAB# Method for conc. Comments ,mLl Us-od,mL CWC Mass 55 -'k 56 57 58 59 12SI 60 61 62 63 64 65 66 671 M' 691 70 p. 71 72 -r; 73 74 75 76 77 78 79 80 81 82 84� 87 88 89 Flernent One,Inc F209 R9 Page 3 Of elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396A0pMAQSM8 ket Page 52 of 66 MERCURY BATCH DIGESTION-RUN WORKSHEET Date Prepared/Digested: as Prep By: SIF File#: Block*1 Temperature: '-,1'4';' Start Time 4, c L, Machine ID-- Block#2 Temperature: Batch Analyst:Stop Time: (C." Block#3 Temperature: �E 2 Typed By: Verified By: 0.4ug1m] —AIS Curve&QC's working std BV, ml FV, ml Standard Lot Numbers Lab BLK i Standard#1 for workin std) 1 (31 batch) 1 40 40 Lot 9: HP31 2 0.004 ug 0-01ml 40 40 Working Standard 3 0.04 ug i 0.110MI 1 by:-'�---�40 40 4 0.08_yg_ 0.20ml 40 40 Standard#2(QC#2): 5 0-16 ug 0.40ml 40 40 Lot#: I-",`--r4, 1 6 0,20uq 0.50ml 40 40 Standard#3(QC#3): 7 QC 42=0.08uq 0,2ml#2 std 40 40 8 QC#3=0.08ug 0.2mi#3 std 40 40 Curve prepared Initial Review By: Time:7, Final QC Review By� Date '-7,Z_ Time:7 Comments: 'All(M.,r'V Prep AFq-'jot Aliquot or FV m(-or'T AeS LAB# Method I '' Lso:d.,nL Cak;Mass 1 4or conz- Comments 9 7% -4 10 12 13 14 15 17 & 18 L 19 LL NOTES: Lab blanks and s2ike-q must be preeared with each batch digestion Denotes spike for fig, Use nplibration raorkirg 0-4ag�ml skaridaw.a,,the rate of 0.20r,-J par 4Grnl sample,unless crherwise noted. Digestion chemicals to be added in order at the following rate per 40m]volumes. H2SO4 @ 2.0rrii HNC}, @ 1,0jrr.1..... KtOnC), 6 0nil......... Porsuffiote @ 3.2n71 7 2 SO,Lot L HNC)HN 3 Lot# --i c, HC1 Lot#-, u Persulfate Lot# 4" —'7 Ll -. —KMnO, Lot# �'5:Vrj _Hydrox E....... Clear samples after cliQestior with 2A ml of Hydroxylamine solution, Element One,in,;F209 R9 Dage 1 o`4 elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1 303 396A0pWWcC M8 {het Page 53 of 66 efernent0ne MERCURY BATCH DIGESTION -RUN WORKSHEET SIF File#: �V Aliquotor -V V.'� gj �IreD Aliquct r AiS LAB Method ML UsEd,mL Calc Mass �"conc. Comments 20 21 22 231 24G, 25 26 4- 27 28 29 �H r> 30 31 32 -113 Na 33�! 35 36 37 38 ;7 1 39 4� ..................... 41 42 C�D 43 44 45 461 481 49 52 + 53, ElernentO-TL 1rcF2D9R!) Page 2 of elementOne Certification: NJ NELAP NCO09 NE01 3AS-021420-RT-1 303 396A0pMAQ,`CM8a&WtWl F?Ibket Page 54 of 66 elementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIF File#: V4 1:9:s'FV Pre;iAliquot Aliquotor FV,rr,,Lor"l' A/S LAB# Method s,Used, Calc%las 'or cone, Comments �65 17 L 56 57 60 61 62V uC 63 64 65 L4 66 67 68 69 70 -y, k 71 73 74 + 76 77, 791 & 83 84 85 -3 86 87 88 Element Ong,Inc F209 R9 Page of elementOne Ceitfication: NJ NELAP NCO09 NE01 3AS-021420-RT-1 303 396A0WW4,1rM6--(0 MWI Faket Page 55 of 66 elementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIFFile#: w!(gw FV Proo Aliquot Aliquot or FV,m AIS LAB# Method lrr1,1 Used,ml Calc Mass foraonc. Cram ients 92 ri 93 94 95,,' V 97 98 99 100 101 102 103 104 105 106 107 108 I 110 112 113 114 115 116 117 118 120 121 122 123 124 Ele,rent One,Inc F209,R9 Page 4 ct'- elementOne Certification: NJ NELAP NC009 N E01 3AS-021420-RT-1 303 396A0pMAQSM8 ket Page 56 of 66 MERCURY BATCH DIGESTION-RUN WORKSHEET Date Prepared0gestod-. prep6y: 2fzz SIF File#: Block#1 Temperature: Start Time: s Machine ID: Block#2 Temperature: q� —4 f Stop Time: Batch Analyst: Block#3 Temperature: 0-7 5 Typed By: rifted BY: 9 art.. 0 4ug/ml AlS Curve&QC's working std BV, mi FV,mi Standard Lot Numbers Lab BLK 7 Standard#1 (for working std) 1 QJ batch) a 40 40 Lot 2 0.004 ug 0.01 mi 40 40 Working Standard 3 0,04 uq 010ml 40 40 Lot#: s Do- 1 bv: 4 0,08 ug 0 20ml .40 40 Standard#2(QC 5 0.40ml -40 40 Lot#:H� 6 0.20uq 0.50ml 40 40 Standard#3(QC#3): Lot#: ewe ci;-i 7 QC#2=0.08ug 0.2ml#2 std 40 40 1 8 QC#3=0.08ug 0.2m]#3 std 1 40 40 lCurve prepared by: D�li Initial Review By:-)Q,= DaW 4 1-IL 3a Time: i ti Final QC Review By: Time '61,:c1i FV Prep Alicuot Aicuotnr FV,ml-or'T AIS LAB# Method Used,mi. C O!c Ma S5 for cone. Comments 1-f)I S V, 12i 13 14 15 --V A7 -,r,raa G 14 18 19 NOTES: Lab blanksands ikes must be erep2red with each batch di2estion 'W'Donates spike for Hq, Use calibration workIng 0 Alupml.5tandard at tttu rate of 0,20ml Der Alliml sample,unless otheNylse noted. Digestion chemicals to be added in order at the following rate per 40ml volumes. H2SO4 @ 2.0mi...... HNO,2 @ KW04 u 6.Oml.......-, Persulfate @ 3.2mt H2SO4 Lot 4- NO Lot 4., -1 xo C Peirsuffate,Lot 4 ---Kh4n0 4 Lot# _Hydrox L ot#.--, Clear samples after d!,uestion with 2.4 mill of FILdroxylamine solution. Element One,Inc F20P R9 Page I of L4 elementOne Certification: NJ NELAP NCO09 NE01 3AS-021420-RT-1 303 396A0PMAQX;M8e(W WtW4 FMket Page 57 of 66 elementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIF File#: VA(gV17V PrcpAl,quot Aliqurtor FV,rrl.orl` A/S LAB# Method (mij Used ml Cale Moss ,foi come. Comments 2 ;> 21 T a2l 23 2 4'1 25 26 27 L_28 29 30 31 ,)c 7) 7 32 :y-F 33 34 35 36 37 38 39 40 411 42 -loC t 431 44 45 46 47 -3L + 48 14 L 49 50 52 531 Elerview Ore Inc F209 RO Page 2 of Ll elementOne Certification: NJ ELAP NCO09 NE01 3AS-021420-RT-1303 396A0pMAQ,15',ill®e&QW1 Mket Page 58 of 66 elernentOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIF File#: .A - Wt{gp`FI Prep Aliquot A4igc,ot or FV,mL car"t" A1S LAB P, Method (MIA tise�ti,ML OB17 Mass forconc. Comments 65 ,w C1 ° ` 56 Ili G 57 N 5$ t I ; 60 62 63 �� 64 I 65 - - ' 66 i 67 68 n, 69C. I 70 `G 71 ;AC,6 E 72 73 >: -6ti - 7, �4 f.74 1-r 74 -" LEA 76 i 77` 79 80 I 81 83 86 -t 87 Element One,➢nc F209 R9 Page 3 ox y elementOne Certification; NJ NELAP NC009 NE013AS-021420-RT-1303 39680pMAQXMB I Mket Page 59 of 66 elementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIF File#: 1ti t 'A+t(g1.FV Prep At gjot Alluot or FV,rrL or'T A,'S LAB# Method (mU Use4,mL Calc Mass for conc. Comments 90 i ro i 92 `5 1 93 94! f 95' e t 9s - 99 100 }_ 101 y 102 Ll 104 - 06 1071 1082 1 h 109` 110 i f11 112 113 114 115 116 117 118 119' 120 121 122 I 123 F . 124 &ement Ono,Inc F209 RJ Page 4 ofu elementOne Certification: NJ NELAP NC009 NE013AS-021420-RT-1303 39680 S',MEla&QW1 Mket Page 60 of 66 MERCURY BATCH DIGESTION-RUN WORKSHEET Date Prepared/Digested: 4 0 Prop By: -)ti-t SIF File#: Block#1 Temperature: Start Time: s Machine ID: Block#2 Temperature: C�l S Stop Time: pus, Batch Analyst: Block#3 Temperature: Typed By: Verified By� 0.4ug/ml AIS Curve&OC's working std BV,ml FV, ml Standard Lot Numbers Lab BLK Standard#1 (for workin std) 0 40 40 Lot #: 2 0,004 ug 0.01ml 4 40 40 Working Standard 3 �1 0.04 uq 010ml 1 40 40 Lot 4 0,08 Ug 0-20ml 40 40 Standard#2(QC#2): 5 0,16 Ug 0.40ml 40 40 Lot#:-mi 4 '-i 6 0L,20u�L_ 0.50ml 40 40 Standard#3(0 #3):-,Pi Lot#: H'�t: C'-4 '1 7 QC#2=0108ug 0.2ml#2 std 40 40 , 8 QC t*=O.08u2- 0.2m1#3 std 40 40 [Curve prepared by: Initial Roview By.,�V" 1 Date: Time:1 Final QC Review By: Date: Time: 0 Comments:- V Prep Aliql-T', Aliquoto! AIS LAB# Meth Used.MIL talc Mass rof conc. Comments -T!( 7V S 12 3 13 3 H . 14 70 15 16 17 '� 18 c5 3-1 19 NOTES: Lab blanks and spikes must be pre2aced with each batcr�Jjestion Denotes spike for Hg, Usena ibraLion vjorbjnq 0.4ugiml slardard at Vic rato of 5.211,ml pF,-r40mj sample,Wessalhe"ise noted, Digestion chemicals to be added in order at the followir;g rate per 40ml volumes. H2SO4 @ 2.0ml...... HNO, @ KPXr-,() 4 @ 6.OmL......_ Persulfate @ 3.2rn1 H2SO4 Lot# HNO_ L:,'* HCILot#: Persulfatc Lot# t:;N`7, Lot# i Hydrox LoW ".15-05; E7 Clear samples after diQestion with 2.4,mi of Hyd.roxZlamine solution. Element One,Inc F209 R9 Page oll y elementOne Certification: NJ NELAP NCO09 NE013AS-021420-RT-1303 396A0pWQSM6--0#%jx*1 R%ket Page 61 of 66 elernentOne MERCURY BATCH DIGESTION-RUN W ORKSHEET SIF File 9: NI i n d F5. P•ep Ah qunl AV urt or FV ut or"1" Ito/S LAB# Method frnU Usec,-nL Calc Va" for cone. Comments 22 23 24 25 26 r 27 28 29 t-3 d Li 30 33 32 33 # y, - 34 35 _ r 36' 38 39 40 7- 4i 42 - -r 43 i 4445 SrIA LL I 46 - r- 47 A� f.� 48 nir I i 49 - _ - 50; F 51 { i 52 53F 54 'v Elemew Ot:e,Irc F209 R9 Page 2 of=t elementOne Certification: NJ NELAE NC000 NE013AS-021420-RT-1303 396A0 ket Page 62 of 66 elementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIFFiiet: �V`(g,i FJ Prep Ali yt ati t1liquorar FV.ml_ar"1" A S LAB# Method m;,} "'Aed ML. Cr:IC MASS f•rr Tana. Comments 56 57 ^ 58 -4tA 59 w i 60 61A 62 r+ 63 � 64 - 65 6& j D 67 I •e 68 i 7E - 71 -11� 72 z 73 74 75 76 (,n 77 78 79 a 80 - a 1 811 82 i 83 Jv L 84C,, 85 4! n 86 _ 87F f 8a -a S-" -, 891 Element One,Inc F209 R9 Pace 3 of L4 elementOne Certification: NJ N LAP NCOO9 N E01 3AS-021420-RT-1 303 396A0 M8 ket Page 63 of 66 clementOne MERCURY BATCH DIGESTION-RUN WORKSHEET SIF File#: 1'v't(gVFV' P'epAl,quot Alquolor KmLor"V A/S LAB# Method (MI-) Used,-)L Cale%las"s, for conc. Comments 90 91 92, 93 941 951 _�'4A 96 97 98 14 99 100 101 102 103, 104 105 1061 107'1 1081 109111 ------------4- 112 113 114 1151 116 117 118- 1 9 120�; 12_1 122 123 124 Element One,tnc 720.0 R9 page 4 a, elementOne Certification.- NJ NELAP NC009 NE01 3AS-021420-RT-1 303 396AOpWWUSIV18 1 V&ket Page 64 of 66 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: Blank Sample Da Wednesday,November 16,2022 15:05:15 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Meat Report Unit Li 6 850250.8 ppb I Sc 45 725248 ppb 1> Rh 103 653740.5 ppb I Cd 111 16.1 ppb 1 Cd 114 31.3 ppb 1> Ho 165 983829.3 ppb I Pb 208 2498.8 ppb Kr 83 81.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 1 Sample Da Wednesday,November 16,2022 15:07:09 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Meat Report Unit Li 6 805105.9 ppb (- Sc 45 689498 ppb 1> Rh 103 630751.8 ppb I Cd 111 3679.4 1.10183 ppb 1 Cd 114 8403 1.10612 ppb 1> Ho 165 952820.3 ppb 1 Pb 208 39194.1 0.93572 ppb Kr 83 62.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 2 Sample Da Wednesday,November 16,2022 15:09:03 Sample Description: Concentration Results Analyte Mass Meas.Inten<.Cone.Meat Report Unit Li 6 829126.4 ppb 1 Sc 45 720947 ppb 1> Rh 103 651556.2 ppb 1 Cd 111 170272.3 49.55741 ppb 1 Cd 114 387739.7 49.60456 ppb 1> Ho 165 982332.3 ppb 1 Pb 208 1809773.3 44.60853 ppb Kr 83 72.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 3 Sample Da'Wednesday,November 16,2022 15:10:57 Sample Description: Concentration Results Analyte Mass Meas.Inten<.Cone.Meat Report Unit Li 6 844817.8 ppb 1 Sc 45 736240.1 ppb 1> Rh 103 647626.7 ppb 1 Cd 111 337546.7 98.84025 ppb 1 Cd 114 771932.3 99.35589 ppb 1> Ho 165 992925.6 ppb 1 Pb 208 3645167.4 88.94012 ppb Kr 83 90.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 4 Sample Da Wednesday,November 16,2022 15:12:51 Sample Description: Concentration Results Analyte Mass Meas.Inten<Cone.Meat Report Unit Li 6 799634.3 ppb 1 Sc 45 696452.8 ppb 1> Rh 103 618868.6 ppb 1 Cd 111 651510.8 199.6348 ppb 1 Cd 114 1493692.9 201.1615 ppb 1> Ho 165 962013.2 ppb 1 Pb 208 7774945.9 195.913 ppb Kr 83 89.3 ppb elementOne ICP-Data 1 of 19 a 39621-Metals 65.1 NE013AS-021420-RT-1303 Appendix C-Page 427 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: Standard 5 Sample Da Wednesday,November 16,2022 15:14:45 Sample Description: Concentration Results Analyte Mass Meas.Inten<_Cone.Mear Report Unit Li 6 807244.5 ppb �- Sc 45 691203.8 ppb 1> Rh 103 618311.9 ppb Cd 111 817783.6 250.8442 ppb �- Cd 114 1850118.1 249.4071 ppb 1> Ho 165 953584 ppb �- Pb 208 10180056 258.7721 ppb Kr 83 116.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 1 Sample Da Wednesday,November 16,2022 15:16:39 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Mear Report Unit Li 6 845738.7 ppb �- Sc 45 709554.9 ppb 1> Rh 103 636680.5 ppb Cd 111 59.5 0.01317 ppb �- Cd 114 151.7 0.01592 ppb (> Ho 165 956673.1 ppb �- Pb 208 6163.5 0.09463 ppb Kr 83 79 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 2 Sample Da Wednesday,November 16,2022 15:18:34 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Mear Report Unit Li 6 858311 ppb �- Sc 45 714859.4 ppb (> Rh 103 645939.3 ppb Cd 111 3542.7 1.03561 ppb �- Cd 114 7978.2 1.02556 ppb 1> Ho 165 967761.8 ppb (- Pb 208 37945.7 0.88919 ppb Kr 83 70.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 3 Sample Da Wednesday,November 16,2022 15:20:27 Sample Description: Concentration Results Analyte Mass Meas.Intens Cone.Mear Report Unit Li 6 833118.4 ppb �- Sc 45 706646.4 ppb 1> Rh 103 635321.6 ppb Cd 111 421218.7 125.7382 ppb (- Cd 114 961298.3 126.1158 ppb 1> Ho 165 962686.9 ppb �- Pb 208 5064530.8 127.4884 ppb Kr 83 81.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 4 Sample Da Wednesday,November 16,2022 15:22:22 Sample Description: Concentration Results Analyte Mass Meas.Intens Cone.Mear Report Unit Li 6 914231.2 ppb (- Sc 45 774839.4 ppb (> Rh 103 669512.8 ppb Cd 111 347637.4 98.46626 ppb �- Cd 114 800905.2 99.69499 ppb 1> Ho 165 1019070.1 ppb (- Pb 208 4065444.1 96.61729 ppb Kr 83 95 ppb elementOne ICP-Data 2 of 19 a 39621-Metals 65.2 NE013AS-021420-RT-1303 Appendix C-Page 428 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 5 Sample Da Wednesday,November 16,2022 15:24:16 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 902644.1 ppb �- Sc 45 756139.6 ppb 1> Rh 103 664096.7 ppb Cd 111 175591.2 50.13838 ppb Cd 114 398747.4 50.03965 ppb 1> Ho 165 1004563.9 ppb �- Pb 208 1907675.1 45.9751 ppb Kr 83 66.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 6 Sample Da Wednesday,November 16,2022 15:26:12 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 790160.5 ppb �- Sc 45 708058.7 ppb 1> Rh 103 601928 ppb Cd 111 78.8 0.01993 ppb �- Cd 114 995.8 0.13381 ppb 1> Ho 165 997013.1 ppb �- Pb 208 6027.8 0.08509 ppb Kr 83 155 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 7 Sample Da Wednesday,November 16,2022 15:28:06 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li 6 1029361.8 ppb �- Sc 45 848718.8 ppb 1> Rh 103 705991.6 ppb Cd 111 355861.7 95.60956 ppb �- Cd 114 796569.9 94.05951 ppb 1> Ho 165 1056966 ppb �- Pb 208 3105.5 0.00962 ppb Kr 83 450.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 2 Sample Da Wednesday,November 16,2022 15:32:45 Sample Description: Concentration Results Analyte Mass Meas.IntenE Conc.Mear Report Unit Li 6 792303.3 ppb �- Sc 45 676415.1 ppb 1> Rh 103 613211 ppb Cd 111 3424.2 1.05452 ppb (- Cd 114 7663.4 1.03734 ppb 1> Ho 165 920007.9 ppb �- Pb 208 38377.2 0.94941 ppb Kr 83 55.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 1 Sample Da Wednesday,November 16,2022 16:04:29 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li 6 892716.3 ppb �- Sc 45 777266.4 ppb 1> Rh 103 663362.4 ppb Cd 111 13 -0.00095 ppb �- Cd 114 33.2 0.00019 ppb 1> Ho 165 1026837.3 ppb �- Pb 208 1629 -0.02312 ppb Kr 83 59 ppb elementOne ICP-Data 3 of 19 a 39621-Metals 65.3 NE013AS-021420-RT-1303 Appendix C-Page 429 of 1178 PerkinElmer Nexion 35OX ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Std 4 Sample Da Wednesday,November 16,2022 16:06:23 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 920474.1 ppb �- Sc 45 799071.8 ppb (> Rh 103 665147.7 ppb Cd 111 348978.3 99.49185 ppb �- Cd 114 781514.5 97.92732 ppb i> Ho 165 1050160.8 ppb (- Pb 208 4316005.2 99.5837 ppb Kr 83 75.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: LRB Sample Da Wednesday,November 16,2022 16:15:54 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 882680 ppb �- Sc 45 685482.8 ppb (> Rh 103 659520 ppb Cd 111 34.5 0.00524 ppb (- Cd 114 21.1 -0.00132 ppb 1> Ho 165 1043457.7 ppb �- Pb 208 5285.7 0.06124 ppb Kr 83 65 ppb Method 6020&200.8 Metals Summary Report Sample ID: LRB SPK Sample Da Wednesday,November 16,2022 16:17:48 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 796992.7 ppb (- Sc 45 642979.7 ppb (> Rh 103 589148 ppb Cd 111 129363.9 41.63639 ppb (- Cd 114 296196.1 41.89536 ppb 1> Ho 165 935268.5 ppb �- Pb 208 1770439.3 45.84072 ppb Kr 83 55.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-5 Sample Da'Wednesday,November 16,2022 16:19:42 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li 6 922524.6 ppb �- Sc 45 801862 ppb 1> Rh 103 640571.5 ppb Cd 111 21134.6 6.25218 ppb i- Cd 114 44850.1 5.83077 ppb 1> Ho 165 1059396.4 ppb �- Pb 208 2965791.4 67,79411 ppb Kr 83 79 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-6 Sample Da Wednesday,November 16,2022 16:21:36 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 961906.3 ppb �- Sc 45 820162.9 ppb 1> Rh 103 667787 ppb Cd 111 20743.6 5.88876 ppb �- Cd 114 43275.3 5.39767 ppb (> Ho 165 1117041.4 ppb �- Pb 208 2608434.3 56.54524 ppb Kr 83 85.7 ppb elementOne ICP-Data 4 of 19 a 39621-Metals 65.4 NE01 3AS-021420-RT-1 303 Appendix C- Page 430 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: 39621-6 Sample Da Wednesday,November 16,2022 16:23:30 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li 6 945165.8 ppb �- Sc 45 802012.7 ppb 1> Rh 103 649659.8 ppb Cd 111 19632.1 5.72755 ppb �- Cd 114 41391.5 5.31317 ppb 1> Ho 165 1081300.3 ppb �- Pb 208 2551814.3 57.14916 ppb Kr 83 88 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-7 Sample Da Wednesday,November 16,2022 16:25:24 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 928556.1 ppb �- Sc 45 748046.6 ppb (> Rh 103 643804.7 ppb Cd 111 23851.4 7.02131 ppb �- Cd 114 50089.9 6.48071 ppb (> Ho 165 1073275 ppb �- Pb 208 2851021.8 64.33824 ppb Kr 83 95 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-7 Sample Da Wednesday,November 16,2022 16:27:18 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 948720 ppb �- Sc 45 792807.6 ppb 1> Rh 103 666989.9 ppb Cd 111 164150.9 46.66901 ppb �- Cd 114 373618.1 46.6876 ppb 1> Ho 165 1115328 ppb �- Pb 208 5790040.5 125.802 ppb Kr 83 76.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 1 Sample Da'Wednesday,November 16,2022 16:29:13 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 869884.3 ppb �- Sc 45 742300.4 ppb 1> Rh 103 625601.3 ppb Cd 111 18.7 0.00099 ppb �- Cd 114 43.7 0.00183 ppb 1> Ho 165 991132.8 ppb �- Pb 208 1378.7 -0.02787 ppb Kr 83 69.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 4 Sample Da Wednesday,November 16,2022 16:31:08 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 843379.8 ppb Sc 45 727889.8 ppb 1> Rh 103 599399.5 ppb Cd 111 312918.3 98.98977 ppb �- Cd 114 716457.9 99.61884 ppb 1> Ho 165 965282.8 ppb �- Pb 208 3670777.4 92A3949 ppb Kr 83 78 ppb elementOne ICP-Data 5 of 19 a 39621-Metals 65.5 NE013AS-021420-RT-1303 Appendix C-Page 431 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: 39621-13 Sample Da Wednesday,November 16,2022 16:33:03 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 915081.8 ppb �- Sc 45 774558.1 ppb 1> Rh 103 656091 ppb Cd 111 13696.8 3.95704 ppb (- Cd 114 27579.5 3.49853 ppb (> Ho 165 1087793.4 ppb �- Pb 208 2016845.5 44.8865 ppb Kr 83 88 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-14 Sample Da Wednesday,November 16,2022 16:34:57 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li 6 872858 ppb (- Sc 45 733740.5 ppb (> Rh 103 625235.2 ppb Cd 111 25481.4 7,72345 ppb �- Cd 114 55615.8 7.40968 ppb 1> Ho 165 1051895.5 ppb �- Pb 208 2395405.5 55.16898 ppb Kr 83 77 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-14 Sample Da Wednesday,November 16,2022 16:36:51 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li 6 848982.8 ppb (- Sc 45 706656.5 ppb (> Rh 103 604341.4 ppb Cd 111 26653 8.35896 ppb �- Cd 114 57764.8 7.96289 ppb I> Ho 165 1019482.5 ppb �- Pb 208 2529881.6 60.10177 ppb Kr 83 89 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-15 Sample Da Wednesday,November 16,2022 16:38:45 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li 6 938624.9 ppb I- Sc 45 796212.3 ppb 1> Rh 103 675666.4 ppb Cd 111 17106 4.79639 ppb �- Cd 114 35156.6 4.33273 ppb (> Ho 165 1138093.2 ppb �- Pb 208 2891726.6 61.53995 ppb Kr 83 73.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-15 Sample Da Wednesday,November 16,2022 16:40:39 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 887294.7 ppb �- Sc 45 741351.3 ppb 1> Rh 103 623037.E ppb Cd 111 156944.8 47.7728 ppb �- Cd 114 352368.4 47.14598 ppb 1> Ho 165 1062692.6 ppb �- Pb 208 5602235.1 127.7503 ppb Kr 83 84 ppb elementOne ICP-Data 6 of 19 a 39621-Metals 65.6 NE01 3AS-021420-RT-1 303 Appendix C-Page 432 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: 39621-17 Sample Da Wednesday,November 16,2022 16:42:33 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 790062.6 ppb (- Sc 45 653223.8 ppb (> Rh 103 590164.8 ppb Cd 111 596.3 0.18693 ppb �- Cd 114 -482.2 -0.07188 ppb 1> Ho 165 981897.8 ppb �- Pb 208 67188 1.59709 ppb Kr 83 110.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-18 Sample Da Wednesday,November 16,2022 16:44:27 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li 6 891038.7 ppb �- Sc 45 751571 ppb (> Rh 103 638692.5 ppb Cd 111 918.7 0.26803 ppb �- Cd 114 -833.7 -0.11264 ppb (> Ho 165 1052312.7 ppb (- Pb 208 114814.1 2.58373 ppb Kr 83 73.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 1 Sample Da'Wednesday,November 16,2022 16:46:22 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li 6 891066.2 ppb �- Sc 45 758062.7 ppb 1> Rh 103 628813.6 ppb Cd 111 13.4 -0.00063 ppb (- Cd 114 19.3 -0.00145 ppb (> Ho 165 1000048.1 ppb (- Pb 208 1012.7 -0.03703 ppb Kr 83 63.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 4 Sample Da Wednesday,November 16,2022 16:48:17 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li 6 895177.4 ppb �- Sc 45 761390.8 ppb (> Rh 103 628018.3 ppb Cd 111 327504.5 98.89626 ppb Cd 114 744837.2 98.84817 ppb (> Ho 165 1002226.5 ppb (- Pb 208 4096007.3 98.99337 ppb Kr 83 71.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: Blank Sample Da Thursday,November 17,2022 11:11:56 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li(7) 7 100277.3 ppb Pb 208 623.7 ppb Kr 83 65 ppb 1> Ho(IS1) 165 996114.2 ppb 1> Sc(IS1) 45 886986.4 ppb Rh 103 764461 ppb Li 6 1926714.4 ppb elementOne ICP-Data 7 of 19 a 39621-Metals 65.7 NE013AS-021420-RT-1303 Appendix C- Page 433 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: Standard 1 Sample Da Thursday,November 17,2022 11:13:16 Sample Description: Concentration Results Analyte Mass Meas.Inten<_Conc.Mear Report Unit Li(7) 7 100989.7 ppb Pb 208 21906.2 1.02979 ppb Kr 83 61.7 ppb 1> Ho(IS1) 165 1011747.8 ppb 1> Sc(IS1) 45 892503 ppb Rh 103 771665.4 ppb Li 6 1936240.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 2 Sample Da Thursday,November 17,2022 11:14:36 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 103317.9 ppb Pb 208 219473.9 10.25174 ppb Kr 83 63 ppb 1> Ho(IS1) 165 1045415.6 ppb 1> Sc(IS1) 45 904804 ppb Rh 103 785706.4 ppb Li 6 2055202.9 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 3 Sample Da'Thursday,November 17,2022 11:16:05 Sample Description: Concentration Results Analyte Mass Meas.IntenE Conc.Mear Report Unit Li(7) 7 99913.4 ppb Pb 208 1088486.3 51.75802 ppb Kr 83 67.3 ppb 1> Ho(IS1) 165 1029500 ppb 1> Sc(IS1) 45 886812.9 ppb Rh 103 767328.2 ppb Li 6 1929980.1 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 4 Sample Da Thursday,November 17,2022 11:17:25 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 104616 ppb Pb 208 1607013.6 73.77078 ppb Kr 83 84.7 ppb 1> Ho(IS1) 165 1066529.1 ppb 1> Sc(IS1) 45 922599.2 ppb Rh 103 788058.2 ppb Li 6 2209173.1 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 5 Sample Da Thursday,November 17,2022 11:18:45 Sample Description: Concentration Results Analyte Mass Meas.IntenE Conc.Mear Report Unit Li(7) 7 104914.4 ppb Pb 208 2299579.8 104.0789 ppb Kr 83 78.7 ppb 1> Ho(IS1) 165 1081810.1 ppb 1> Sc(IS1) 45 935155.6 ppb Rh 103 795271.6 ppb Li 6 2236700.4 ppb elementOne ICP-Data 8 of 19 a 39621-Metals 65.8 NE01 3AS-021420-RT-1 303 Appendix C-Page 434 of 1178 PerkinElmer Nexlon 35OX ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Std 1 Sample Da Thursday,November 17,2022 11:20:05 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li(7) 7 101966.2 ppb Pb 208 511 -0.00644 ppb Kr 83 64.3 ppb 1> Ho(IS1) 165 1034586.9 ppb 1> Sc(IS1) 45 897040.4 ppb Rh 103 778189.9 ppb Li 6 1966938A ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 2 Sample Da Thursday,November 17,2022 11:21:25 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 101121.7 ppb Pb 208 23668.8 1.08443 ppb Kr 83 61.3 ppb 1> Ho(IS1) 165 1039761.5 ppb 1> Sc(IS1) 45 898699.9 ppb Rh 103 776128.9 ppb Li 6 1967494.5 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 3 Sample Da Thursday,November 17,2022 11:22:46 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li(7) 7 96669.4 ppb Pb 208 1600162 79.38768 ppb Kr 83 77 ppb 1> Ho(IS1) 165 986884.2 ppb 1> Sc(IS1) 45 857143.8 ppb Rh 103 730489 ppb Li 6 1860112 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 4 Sample Da Thursday,November 17,2022 11:24:06 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li(7) 7 103339.1 ppb Pb 208 1119726.9 52.03172 ppb Kr 83 69 ppb 1> Ho(IS1) 165 1053378.8 ppb 1> Sc(IS1) 45 908685.5 ppb Rh 103 783687 ppb Li 6 2057739.8 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 5 Sample Da Thursday,November 17,2022 11:25:26 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li(7) 7 101638.5 ppb Pb 208 561645 26.55322 ppb Kr 83 69.3 ppb 1> Ho(IS1) 165 1034793.3 ppb 1> Sc(IS1) 45 894423.5 ppb Rh 103 769133.6 ppb Li 6 1969776.4 ppb elementOne ICP-Data 9 of 19 a 39621-Metals 65.9 NE013AS-021420-RT-1303 Appendix C-Page 435 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Std 6 Sample Da Thursday,November 17,2022 11:26:48 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li(7) 7 105786.4 ppb Pb 208 1691.7 0.04962 ppb Kr 83 75.7 ppb (> Ho(IS1) 165 1032109.1 ppb 1> Se(IS1) 45 956676.2 ppb Rh 103 716542.9 ppb Li 6 2274837.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 2 Sample Da Thursday,November 17,2022 11:28:09 Sample Description: Concentration Results Analyte Mass Meas.Intem Conc.Mear Report Unit Li(7) 7 107530.9 ppb Pb 208 22232.8 1.06692 ppb Kr 83 61 ppb 1> Ho(IS1) 165 992084.5 ppb 1> Sc(IS1) 45 957139.1 ppb Rh 103 783655.8 ppb Li 6 2321987.4 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-15 Sample Da Thursday,November 17,2022 11:38:36 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 105427.4 ppb Pb 208 324974.5 15.38218 ppb Kr 83 63 ppb 1> Ho(IS1) 165 1032645.7 ppb 1> Sc(IS1) 45 866626.7 ppb Rh 103 731130.8 ppb Li 6 1923371.5 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-15 Sample Da'Thursday,November 17,2022 11:39:57 Sample Description: Concentration Results Analyte Mass Meas.Inten<_Conc.Mear Report Unit Li(7) 7 112246.5 ppb Pb 208 1559489 68.84098 ppb Kr 83 69 ppb 1> Ho(IS1) 165 1109134.3 ppb 1> Sc(IS1) 45 925755.6 ppb Rh 103 778701.4 ppb Li 6 2262920.8 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-17 FH Sample Da'Thursday,November 17,2022 11:42:37 Sample Description: Concentration Results Analyte Mass Meas.IntenE Conc.Mear Report Unit Li(7) 7 104636.8 ppb Pb 208 39352.3 1.69797 ppb Kr 83 74.7 ppb 1> Ho(IS1) 165 1115234.9 ppb 1> Sc(IS1) 45 877970.8 ppb Rh 103 772250.7 ppb Li 6 1906573.8 ppb elementOne ICP-Data 10 of 19 a 39621-Metals 65.10 NE01 3AS-021420-RT-1 303 Appendix C-Page 436 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 1 Sample Da Thursday,November 17,2022 11:43:59 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 106930.8 ppb Pb 208 270.7 -0.01866 ppb Kr 83 64.7 ppb i> Ho(IS1) 165 1103861.6 ppb (> Sc(IS1) 45 932369.3 ppb Rh 103 798645.1 ppb Li 6 2302996.5 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 4 Sample Da Thursday,November 17,2022 11:45:19 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 106615.1 ppb Pb 208 1154032.7 51.38504 ppb Kr 83 63 ppb 1> Ho(IS1) 165 1099312.3 ppb 1> Sc(IS1) 45 938461.5 ppb Rh 103 788536.5 ppb Li 6 2306789.4 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-17 BH undig Sample Da Thursday,November 17,2022 11:46:41 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 97861.7 ppb Pb 208 15764.2 0.71368 ppb Kr 83 54.3 ppb 1> Ho(IS1) 165 1037941.4 ppb 1> Sc(IS1) 45 827467.7 ppb Rh 103 734697.2 ppb Li 6 1813844.8 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-18 FH Sample Da Thursday,November 17,2022 11:49:21 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 96440.6 ppb Pb 208 47821.1 2.19176 ppb Kr 83 68 ppb 1> Ho(IS1) 165 1054135.5 ppb 1> Sc(IS1) 45 825940.3 ppb Rh 103 727265.2 ppb Li 6 1802673.8 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621 C8a Sample Da Thursday,November 17,2022 11:50:42 Sample Description: Concentration Results Analyte Mass Meas.Inten<.Conc.Mear Report Unit Li(7) 7 98261.4 ppb Pb 208 15592.8 0.66859 ppb Kr 83 51 ppb i> Ho(IS1) 165 1092296.8 ppb 1> Sc(IS1) 45 865858.1 ppb Rh 103 778456.6 ppb Li 6 1872733.9 ppb elementOne ICP-Data 11 of 19 a 39621-Metals 65.11 NE01 3AS-021420-RT-1 303 Appendix C- Page 437 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: 39621 C9 Sample Da Thursday,November 17,2022 11:52:02 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 86536.9 ppb Pb 208 23660.4 1.1873 ppb Kr 83 58 ppb 1> Ho(IS1) 165 951663.6 ppb 1> Sc(IS1) 45 752904.2 ppb Rh 103 671877.1 ppb Li 6 1646310.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 1 Sample Da Thursday,November 17,2022 11:53:23 Sample Description: Concentration Results Analyte Mass Meas.IntenE Conc.Mear Report Unit Li(7) 7 105421 ppb Pb 208 164.7 -0.02321 ppb Kr 83 53.3 ppb 1> Ho(IS1) 165 1082638 ppb 1> Sc(IS1) 45 921143.5 ppb Rh 103 780410.3 ppb Li 6 2273252.9 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 4 Sample Da Thursday,November 17,2022 11:54:43 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 104495 ppb Pb 208 1119975A 51.00547 ppb Kr 83 72 ppb 1> Ho(IS1) 165 1074896.9 ppb 1> Sc(IS1) 45 911195.4 ppb Rh 103 774041.2 ppb Li 6 2248398.5 ppb Method 6020&200.8 Metals Summary Report Sample ID: Blank Sample Da Thursday,November 17,2022 12:40:39 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 97833.4 ppb V 51 52800.2 ppb V-1 51 45000.5 ppb Cr 52 16479.9 ppb Mn 55 457 ppb Co 59 62 ppb Ni 60 614.3 ppb Cu 63 427.7 ppb Cu(65) 65 321.7 ppb As 75 -707.2 ppb Cd 111 26.9 ppb Cd(114) 114 74.6 ppb Sb 123 176.3 ppb TI 205 357.7 ppb Pb 208 304 ppb Kr 83 62.3 ppb (> Rh(IS1) 103 718484.1 ppb 1> Ho(IS1) 165 998159.3 ppb (> Sc(IS1) 45 849558.7 ppb Li 6 1913479.5 ppb elementOne ICP-Data 12 of 19 a 39621-Metals 65.12 NE013AS-021420-RT-1303 Appendix C- Page 438 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: Standard 1 Sample Da Thursday,November 17,2022 12:42:58 Sample Description: Concentration Results Analyte Mass Meas.Inten<.Cone.Mear Report Unit Li(7) 7 100397.6 ppb V 51 85397.6 0.99678 ppb V-1 51 61765.3 0.99375 ppb Cr 52 28791.8 0.96205 ppb Mn 55 9961 1.00714 ppb Co 59 5603.6 0.9921 ppb Ni 60 5941.4 1.00783 ppb Cu 63 8671.3 0.9696 ppb Cu(65) 65 5478.2 0.96134 ppb As 75 3091.8 1.03344 ppb Cd 111 3770.5 0.9729 ppb Cd(114) 114 8962.1 0.97334 ppb Sb 123 9315.4 0.97735 ppb TI 205 12882.3 1.00656 ppb Pb 208 21811.1 1.00523 ppb Kr 83 65.3 ppb 1> Rh(IS1) 103 739610.1 ppb 1> Ho(IS1) 165 1034529.7 ppb 1> Sc(IS1) 45 875153.1 ppb Li 6 1964531 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 2 Sample Da Thursday,November 17,2022 12:45:18 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Mear Report Unit Li(7) 7 103233.9 ppb V 51 373870.9 9.82428 ppb V-1 51 205332.9 9.75595 ppb Cr 52 142178.4 9.76313 ppb Mn 55 97341.6 9.90428 ppb Co 59 57070 9.8389 ppb Ni 60 53484.9 9.66327 ppb Cu 63 86011.6 9.71243 ppb Cu(65) 65 54521.7 9.75136 ppb As 75 36052.6 9.5964 ppb Cd 111 38330.5 9.59418 ppb Cd(114) 114 90481A 9.5435 ppb Sb 123 94624.5 9.72915 ppb TI 205 126692.5 9.78388 ppb Pb 208 219828.8 9.88234 ppb Kr 83 62.7 ppb 1> Rh(IS1) 103 767465.6 ppb 1> Ho(IS1) 165 1074648.3 ppb 1> Sc(IS1) 45 901938 ppb Li 6 2241947.9 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 3 Sample Da Thursday,November 17,2022 12:47:38 Sample Description: Concentration Results Analyte Mass Meas.IntenE Cone.Mear Report Unit Li(7) 7 98872.8 ppb V 51 1630268.5 51.27295 ppb V-1 51 832688.5 51.30515 ppb Cr 52 636953.7 51.08541 ppb Mn 55 473462.2 50.8368 ppb Co 59 279378.3 50.67263 ppb Ni 60 263130.6 50.46626 ppb Cu 63 425919 50.76595 ppb Cu(65) 65 267724.7 50.58398 ppb As 75 180586.6 49.68185 ppb Cd 111 192197.1 50.59457 ppb Cd(114) 114 457966.5 50.80804 ppb Sb 123 472995.6 50.52729 ppb TI 205 634089.1 50.91567 ppb Pb 208 1092096.3 50.98232 ppb Kr 83 69 ppb 1> Rh(IS1) 103 730196.7 ppb 1> Ho(IS1) 165 1036001.3 ppb 1> Sc(IS1) 45 873612.9 ppb Li 6 1921067.9 ppb elementOne ICP-Data 13 of 19 a 39621-Metals 65.13 NE013AS-021420-RT-1303 Appendix C-Page 439 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: Standard 4 Sample Da Thursday,November 17,2022 12:49:57 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Mear Report Unit Li(7) 7 101446.3 ppb V 51 2574782.9 79.24435 ppb V-1 51 1303185.3 79.19346 ppb Cr 52 1013822.4 79.39042 ppb Mn 55 761676.5 79.13086 ppb Cc 59 451465.1 79.2073 ppb Ni 60 424379.6 78.79167 ppb Cu 63 686508.3 79.17184 ppb Cu(65) 65 430750.4 78.75173 ppb As 75 299155.8 79.48249 ppb Cd 111 311489.3 79.31211 ppb Cd(114) 114 736466 79.02882 ppb Sb 123 770226.7 78.64083 ppb TI 205 1023756.7 78.57386 ppb Pb 208 1765674.6 78.77869 ppb Kr 83 67.3 ppb 1> Rh(IS1) 103 754961.6 ppb 1> Ho(IS1) 165 1084090.8 ppb 1> Sc(IS1) 45 905709.5 ppb Li 6 2137106.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: Standard 5 Sample Da Thursday,November 17,2022 12:52:16 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Mear Report Unit Li(7) 7 104209.9 ppb V 51 3294132.8 99.98565 ppb V-1 51 1663697.4 100.0171 ppb Cr 52 1295681.8 99.96903 ppb Mn 55 983035.8 100.2864 ppb Co 59 582353.7 100.314 ppb Ni 60 552599.5 100.7671 ppb Cu 63 885772.9 100.3086 ppb Cu(65) 65 561083.2 100.7319 ppb As 75 385902.3 100.6131 ppb Cd 111 401176.1 100.2939 ppb Cd(114) 114 953080.1 100.4188 ppb Sb 123 1001652.3 100.851 ppb TI 205 1330540.1 100.7046 ppb Pb 208 2284050.9 100.4976 ppb Kr 83 68.7 ppb (> Rh(IS1) 103 768925.2 ppb 1> Ho(IS1) 165 1099408.9 ppb 1> Sc(IS1) 45 925930.4 ppb Li 6 2246158.2 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 1 Sample Da Thursday,November 17,2022 12:54:36 Sample Description: Concentration Results Analyte Mass Meas.Inten:Cone.Mear Report Unit Li(7) 7 99935.2 ppb V 51 51526.7 -0.06797 ppb V-1 51 42635.6 -0.19963 ppb Cr 52 16333.7 -0.033 ppb Mn 55 636.3 0.01855 ppb Cc 59 234 0.03108 ppb Ni 60 565.7 -0.01117 ppb Cu 63 636.7 0.02418 ppb Cu(65) 65 422.3 0,01813 ppb As 75 -665.1 0.01469 ppb Cd 111 147.6 0.0317 ppb Cd(114) 114 371.8 0.03291 ppb Sb 123 247.2 0.00695 ppb TI 205 614 0.01964 ppb Pb 208 925 0.0286 ppb Kr 83 60.7 ppb 1> Rh(IS1) 103 729568.9 ppb 1> Ho(IS1) 165 1033565.6 ppb 1> Sc(IS1) 45 871507.8 ppb Li 6 1931034.6 ppb elementOne ICP-Data 14 of 19 a 39621-Metals 65.14 NE013AS-021420-RT-1303 Appendix C-Page 440 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 2 Sample Da Thursday,November 17,2022 12:56:56 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 100025.6 ppb V 51 82308.1 0.94013 ppb V-1 51 58426.9 0.83984 ppb Cr 52 28677.9 0.99028 ppb Mn 55 10267.5 1.05722 ppb Co 59 5795 1.04329 ppb Ni 60 6170.5 1.07006 ppb Cu 63 9211.7 1.05087 ppb Cu(65) 65 5673.6 1.01505 ppb As 75 2872.1 0.98666 ppb Cd 111 3971.3 1.04167 ppb Cd(114) 114 9332.4 1,03048 ppb Sb 123 9878.7 1.04206 ppb TI 205 13380.2 1.05107 ppb Pb 208 22775.8 1.05476 ppb Kr 83 60.3 ppb 1> Rh(IS1) 103 727844 ppb 1> Ho(IS1) 165 1030248.5 ppb 1> Sc(IS1) 45 873732.4 ppb Li 6 1962891.6 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 3 Sample Da Thursday,November 17,2022 12:59:16 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 93743.9 ppb V 51 2296207.1 77.71741 ppb V-1 51 1165044.8 77.8423 ppb Cr 52 900909.8 77.58191 ppb Mn 55 679954.5 77.71192 ppb Co 59 399976.1 77.19953 ppb Ni 60 377451.2 77,09598 ppb Cu 63 616981.4 78.28192 ppb Cu(65) 65 384683.9 77.37479 ppb As 75 261710.2 76.50721 ppb Cd 111 275994.1 77.31307 ppb Cd(114) 114 651713.2 76.93931 ppb Sb 123 673783.6 75.31425 ppb TI 205 905665.8 76.09109 ppb Pb 208 1564989.9 76.43391 ppb Kr 83 66.7 ppb 1> Rh(IS1) 103 686228.7 ppb 1> Ho(IS1) 165 990403.2 ppb 1> Sc(IS1) 45 829082.6 ppb Li 6 1820666.4 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 4 Sample Da Thursday,November 17,2022 13:01:36 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li(7) 7 96611.3 ppb V 51 1597559 52.00625 ppb V-1 51 814323 51.94404 ppb Cr 52 632386.7 52.51307 ppb Mn 55 467402 51.92267 ppb Co 59 277742.7 52.11876 ppb Ni 60 254343.9 50.46835 ppb Cu 63 410943 50.67514 ppb Cu(65) 65 260709.2 50.96365 ppb As 75 175608.8 49.98412 ppb Cd 111 187562.7 51.08082 ppb Cd(114) 114 445220.6 51.1019 ppb Sb 123 457799.7 49.76236 ppb TI 205 616841.8 50.39844 ppb Pb 208 1072886.4 50.9655 ppb Kr 83 63 ppb 1> Rh(IS1) 103 705774.9 ppb 1> Ho(IS1) 165 1018131.6 ppb 1> Sc(IS1) 45 847951.9 ppb Li 6 1872232.2 ppb elementOne ICP-Data 15 of 19 a 39621-Metals 65.15 NEW 3AS-021420-RT-1303 Appendix C- Page 441 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Std 5 Sample Da Thursday,November 17,2022 13:03:56 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 100358.3 ppb V 51 836699.4 25.46942 ppb V-1 51 434870.6 25.37408 ppb Cr 52 334226.9 26.15438 ppb Mn 55 239333.5 25.67696 ppb Co 59 145236.3 26.34122 ppb Ni 60 129141.4 24.71098 ppb Cu 63 213019.8 25.3687 ppb Cu(65) 65 134077.6 25.30548 ppb As 75 90833 25.09064 ppb Cd 111 96543.6 25.41375 ppb Cd(114) 114 229528.9 25.46352 ppb i Sb 123 232401.4 24.24666 ppb TI 205 313086.9 24.54819 ppb Pb 208 556322 25.36841 ppb Kr 83 64 ppb 1> Rh(IS1) 103 730098.9 ppb 1> Ho(IS1) 165 1060328.3 ppb 1> Sc(IS1) 45 872500.2 ppb Li 6 1966960 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 6 Sample Da Thursday,November 17,2022 13:06:17 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 108059.1 ppb V 51 157732.3 3.51349 ppb V-1 51 139676.2 6.35342 ppb Cr 52 26200.8 0.83238 ppb Mn 55 8763.7 0.91541 ppb Co 59 3814.2 0.69776 ppb Ni 60 20750.2 3.96841 ppb Cu 63 12498.2 1.47637 ppb Cu(65) 65 4990.7 0.9057 ppb As 75 -186.4 0.14477 ppb Cd 111 291.1 0.07136 ppb Cd(114) 114 1387 0.14931 ppb Sb 123 1842.2 0.17097 ppb TI 205 801.4 0.03247 ppb Pb 208 3794.6 0.15675 ppb Kr 83 65.7 ppb 1> Rh(IS1) 103 712487.7 ppb 1> Ho(IS1) 165 1070386 ppb 1> Sc(IS1) 45 981101.7 ppb Li 6 2354829.5 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 7 Sample Da Thursday,November 17,2022 13:08:37 Sample Description: Concentration Results Analyte Mass Meas.Intem Conc.Mear Report Unit Li(7) 7 141064.9 ppb V 51 9054318.4 293.2191 ppb V-1 51 4783238.6 309.4497 ppb Cr 52 3033589.9 248,8345 ppb Mn 55 1603547.7 172.4905 ppb Co 59 890758.2 161.7794 ppb Ni 60 1223557.7 235.3958 ppb Cu 63 1919711.5 229.249 ppb Cu(65) 65 1222589.8 231.4909 ppb As 75 391091.3 107.5054 ppb Cd 111 365017.6 96.20667 ppb i Cd(114) 114 878980.6 97.63787 ppb Sb 123 303.5 0.0171 ppb TI 205 408.3 0.00726 ppb Pb 208 1046 0.04044 ppb Kr 83 69.7 ppb 1> Rh(IS1) 103 729296.8 ppb 1> Ho(IS1) 165 916241.3 ppb 1> Sc(IS1) 45 1100515.3 ppb Li 6 3115120.4 ppb elementOne ICP-Data 16 of 19 a 39621-Metals 65.16 NE01 3AS-021420-RT-1 303 Appendix C- Page 442 of 1178 PerkinElmer Nexion 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 2 Sample Da Thursday,November 17,2022 13:10:57 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 109404 ppb V 51 149963 2.8733 ppb V-1 51 118986 4.36426 ppb Cr 52 33755.2 1.25363 ppb Mn 55 11036.2 1.07344 ppb Co 59 6094.5 1.03567 ppb Ni 60 7044.3 1.16236 ppb Cu 63 10411.3 1.12451 ppb Cu(65) 65 6529.7 1.10795 ppb As 75 3338.6 1.06334 ppb Cd 111 4279.4 1.05982 ppb Cd(114) 114 10169.2 1.06026 ppb Sb 123 10124.3 1.06594 ppb TI 205 13765.2 1.07978 ppb Pb 208 23179.1 1.07111 ppb Kr 83 64 ppb 1> Rh(IS1) 103 770962.2 ppb 1> Ho(IS1) 165 1032775.2 ppb 1> Sc(IS1) 45 953551.4 ppb Li 6 2415386.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 1 Sample Da Thursday,November 17,2022 13:50:33 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 110272.7 ppb V 51 46722.5 -0.36878 ppb V-1 51 39243.2 -0.66406 ppb Cr 52 16195.8 -0.17134 ppb Mn 55 615 0.00993 ppb Co 59 67.7 -0.00032 ppb Ni 60 604 -0.01487 ppb Cu 63 562.3 0.00891 ppb Cu(65) 65 350 -0.0019 ppb As 75 -844.8 -0.01297 ppb Cd 111 28.5 -0.00041 ppb Cd(114) 114 17.1 -0.00668 ppb Sb 123 85.3 -0.01153 ppb TI 205 262.7 -0.01127 ppb Pb 208 391.3 0.00133 ppb Kr 83 64.3 ppb 1> Rh(IS1) 103 806215.5 ppb 1> Ho(IS1) 165 1177984 ppb 1> Sc(IS1) 45 960722.6 ppb Li 6 2386645.7 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Std 4 Sample Da Thursday,November 17,2022 13:52:52 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li(7) 7 107566.8 ppb V 51 1751363.6 50.91112 ppb V-1 51 892549.1 50.81478 ppb Cr 52 692583.3 51.36242 ppb Mn 55 520575.6 51.67778 ppb Co 59 307345.7 51.53883 ppb Ni 60 284256.4 50.40334 ppb Cu 63 462215.2 50.93521 ppb Cu(65) 65 291602.4 50.93978 ppb As 75 192364.7 48.92914 ppb Cd 111 207043.2 50.38815 ppb Cd(114) 114 490135.1 50.2713 ppb Sb 123 509577.3 48.73718 ppb TI 205 686245.4 49.33688 ppb Pb 208 1195417.3 49.9662 ppb Kr 83 61 ppb 1> Rh(IS1) 103 789803.9 ppb 1> Ho(IS1) 165 1157123.5 ppb 1> Sc(IS1) 45 942205.9 ppb Li 6 2323770 ppb elementOne ICP-Data 17 of 19 a 39621-Metals 65.17 NE01 3AS-021420-RT-1 303 Appendix C- Page 443 of 1178 PerkinElmer Nexlon 35OX ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: 39621-13 Sample Da Thursday,November 17,2022 14:17:57 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li(7) 7 119150 ppb V 51 ppb V-1 51 ppb Cr 52 ppb Mn 55 ppb Co 59 ppb Ni 60 ppb Cu 63 ppb Cu(65) 65 ppb As 75 ppb Cd 111 3938.7 0.9237 ppb Cd(114) 114 8686.8 0.85704 ppb Sb 123 ppb TI 205 ppb Pb 208 253111.6 10.15782 ppb Kr 83 64.3 ppb 1> Rh(IS1) 103 813566.9 ppb 1> Ho(IS1) 165 1203787.8 ppb 1> Sc(IS1) 45 979138.8 ppb Li 6 2415129.1 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-14 Sample Da Thursday,November 17,2022 14:20:17 Sample Description: Concentration Results Analyte Mass Meas.Intens Conc.Mear Report Unit Li(7) 7 121874.6 ppb V 51 ppb V-1 51 ppb Cr 52 ppb Mn 55 ppb Cc 59 ppb Ni 60 ppb Cu 63 ppb Cu(65) 65 ppb As 75 ppb Cd 111 7666.1 1.8249 ppb Cd(114) 114 17435.5 1.74815 ppb Sb 123 ppb TI 205 ppb Pb 208 311426.8 12.56682 ppb Kr 83 59 ppb 1> Rh(IS1) 103 804430.8 ppb 1> Ho(IS1) 165 1197513.2 ppb 1> Sc(IS1) 45 966907.2 ppb Li 6 2376137.3 ppb Method 6020&200.8 Metals Summary Report Sample ID: 39621-14 Sample Da Thursday,November 17,2022 14:22:36 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 122509.1 ppb V 51 ppb V-1 51 ppb Cr 52 ppb Mn 55 ppb Co 59 ppb Ni 60 ppb Cu 63 ppb Cu(65) 65 ppb As 75 ppb Cd 111 7646.3 1.80123 ppb Cd(114) 114 17608.3 1.74679 ppb Sb 123 ppb TI 205 ppb Pb 208 309489.5 12.48148 ppb Kr 83 67 ppb 1> Rh(IS1) 103 812837.7 ppb 1> Ho(IS1) 165 1198123.6 ppb 1> Sc(IS1) 45 976544.3 ppb Li 6 2408409.1 ppb elementOne ICP-Data 18 of 19 a 39621-Metals 65.18 NE01 3AS-021420-RT-1 303 Appendix C- Page 444 of 1178 PerkinElmer Nexlon 350X ICP-MS Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 1 Sample Da Thursday,November 17,2022 14:24:56 Sample Description: Concentration Results Analyte Mass Meas.Inten:Conc.Mear Report Unit Li(7) 7 108540.6 ppb V 51 57532.6 -0.05193 ppb V-1 51 49720 -0.04815 ppb Cr 52 15711.5 -0.2084 ppb Mn 55 623.3 0.01069 ppb Co 59 76.7 0.00116 ppb Ni 60 562.3 -0.0222 ppb Cu 63 586.7 0.01148 ppb Cu(65) 65 390.7 0,00504 ppb As 75 -584.4 0.05216 ppb Cd 111 32.2 0,00046 ppb Cd(114) 114 84.2 0.00005 ppb Sb 123 150.9 -0.00516 ppb TI 205 382.7 -0.00239 ppb Pb 208 571 0,00909 ppb Kr 83 56.3 ppb 1> Rh(IS1) 103 806866 ppb 1> Ho(IS1) 165 1160692 ppb 1> Sc(IS1) 45 956133.7 ppb Li 6 2375651.1 ppb Method 6020&200.8 Metals Summary Report Sample ID: QC Sid 4 Sample Da Thursday,November 17,2022 14:27:16 Sample Description: Concentration Results Analyte Mass Meas.Intena Conc.Mear Report Unit Li(7) 7 106533.1 ppb V 51 1724797.8 50.33619 ppb V-1 51 879304.5 50.24552 ppb Cr 52 681113.3 50.71065 ppb Mn 55 505049.3 50.35027 ppb Co 59 299777.2 50.48543 ppb Ni 60 280620.1 49.97373 ppb Cu 63 454068.1 50.25045 ppb Cu(65) 65 285238 50.03891 ppb As 75 193454.2 49.41735 ppb Cd 111 206662.3 50.51181 ppb Cd(114) 114 487710.3 50.23869 ppb Sb 123 513251.5 49.5447 ppb TI 205 683190.4 49.56743 ppb Pb 208 1181091.6 49.81987 ppb Kr 83 67.7 ppb 1> Rh(IS1) 103 786429.4 ppb 1> Ho(IS1) 165 1146553.3 ppb 1> Sc(IS1) 45 948160.4 ppb Li 6 2310112.9 ppb elementOne ICP-Data 19 of 19 a 39621-Metals 65.19 NE01 3AS-021420-RT-1 303 Appendix C- Page 445 of 1178 PerkinElmer FIMS-100 CVAA Mercury Analyzer Sample ID Date Time Mean Sig Mean Rd Mean_Rt Units Alq. Vol. Sig 1 Reading-1 Result-1 Sig 2 Reading-2 Result-2 Cor.Coeff. Calib Blank 11/11/2022 9:23:54 AM 0.00032426 pg 0.00031961 0.00032891 STD1=.004ug 11/11/2022 9:25:36 AM 0.00100547 pg 0.00098771 0.00102322 =.04ug 11/11/2022 9:27:18 AM 0.01218044 N9 0.0121222 0.01223869 =.08ug 11/11/2022 9:29:12 AM 0.02556379 pg 0.02552974 0.02559784 S 104=.16ug 11/11/2022 9:31:07 AM 0.05120624 pg 0.05094347 0.05146902 STD5=.2ug 11/11/2022 9:33:00 AM 0.06199315 pg 0.06172073 0.06226557 Reagent Blank 11/11/2022 9:34:52 AM -6.03E-05 -0.0001918 -0.0001918 pg -8.00E-05 -0.0002545 -0.0002545 -4.06E-05 -0.0001292 -0.0001292 0.004ug=DL 11/11/2022 9:36:34 AM 0.00103403 0.00329041 0.00329041 pg 0.00103766 0.00330196 0.00330196 0.0010304 0.00327885 0.00327885 0.999624097 0.080ug=QC STD 3 11/11/2022 9:40:09 AM 0.02703914 0.08604166 0.08604166 pg 0.02707488 0.08615541 0.08615541 0.02700339 0.0859279 0.0859279 0.999624097 0.080ug=QC STD 2 11/11/2022 9:42:02 AM 0.02463967 0.07840627 0.07840627 pg 0.02462163 0.07834887 0.07834887 0.02465771 0.07846368 0.07846368 0.999624097 Reagent Blank 11/11/2022 9:43:55 AM -6.42E-05 -0.0002043 -0.0002043 pg -7.39E-05 -0.0002351 -0.0002351 -5.45E-05 -0.0001734 -0.0001734 0.999624097 39621-FH LRB 11/11/2022 10:10:08 AM -0.0001451 -0.0002699 -0.0067465 pg 4 100 -0.000166 -0.0003364 -0.0084104 -0.0001242 -0.0002033 -0.0050825 0.999624097 39621-FH LRB SPK 11/11/2022 10:11:50 AM 0.02297437 0.07329894 4.5B11836 pg 1.6 100 0.02291727 0.07311725 4.56982788 0.02303147 0.07348063 4.59253932 0.999624097 39621-lFH 11/11/2022 10:13:44 AM 0.00171786 0.00565828 0.14145697 pg 4 100 0.00170573 0.00561968 0.14049203 0.00172999 0.00569688 0.1424219 0.999624097 39621-2FH 11/11/2022 10:15:28 AM 0.00307888 0.00998919 0.24972963 pg 4 100 0.00307151 0.00996576 0.24914389 0.00308624 0.01001262 0.25031538 0.999624097 39621-2FH DUP 11/11/2022 10:17:12AM 0.00301043 0.00977139 0.24428466 pg 4 100 0.00302761 0.00982604 0.24565095 0.00299326 0.00971673 0.24291837 0,999624097 39621-3FH 11/11/2022 10:18:57 AM 0.00206053 0.00674869 0.16871718 pg 4 100 0.00204985 0.00671471 0.16786765 0.00207121 0.00678267 0.16956671 0.999624097 39621-3FH SPK 11/11/2022 10:20:40AM 0.02634924 0.08403816 2.10095411 pg 4 100 0.02621525 0.08361179 2.09029467 0,02648323 0.08446454 2.11161355 0.999624097 39621-4FH 11/11/2022 10:22:33 AM 0.00408643 0.01319535 0.32988368 pg 4 100 0,00412296 0.01331158 0.33278958 0.00404991 0.01307911 0.32697778 0.999624097 39621-9FH 11/11/2022 10:24:16AM 0.00812487 0.02604611 0.65115271 pg 4 100 0.00808525 0.02592006 0.64800138 0.00816448 0.02617216 0.65430403 0.999624097 0.004ug=DL 11/11/2022 10:25:58 AM 0.00101804 0.00323952 0.00323952 pg 0.00102345 0.00325673 0.00325673 0.00101263 0.00322231 0.00322231 0,999624097 0.080ug=QC STD 2 11/11/2022 10:27:40 AM 0.02471699 0.07865232 0.07865232 pg 0.02474814 0.07875144 0.07875144 0.02468584 0.0785532 0.0785532 0.999624097 Reagent Blank 11/11/2022 10:29:32 AM -5.97E-05 -0.0001899 -0.0001899 pg -5.13E-05 -0.0001632 -0.0001632 -6.81E-05 -0.0002166 -0.0002166 0.999624097 39621-10FH 11/11/2022 10:31:14AM 0.00210285 0.00688336 0.17208394 pg 4 100 0.00209879 0.00687044 0.17176101 0.00210691 0.00689628 0.17240688 0.999624097 39621-10FHDUP 11/11/2022 10:32:55AM 0.00208197 0.006B1692 0.17042288 pg 4 100 0.00206656 0.00676786 0.16919662 0.00209739 0.00686597 0.17164914 0.999624097 39621-11FH 11/11/2022 10:34:38 AM 0.00492762 0.01587211 0.39680272 pg 4 100 0.00492916 0.01587699 0.39692481 0.00492609 0.01586723 0.39668063 0.999624097 39621-11FH SPK 11/11/2022 10:36:20 AM 0.02933037 0.09352447 2.33811179 pg 4 100 0.02920381 0.09312173 2.32804333 0.02945693 0.09392721 2.34818025 0.999624097 39621-12FH 11/11/2022 10:38:14 AM 0.0021915 0.00716545 0.17913617 pg 4 100 0.00220942 0.00722248 0.18056194 0.00217358 0.00710842 0.17771041 0.999624097 39621-1A 11/11/2022 10:39:58 AM 0.00185743 0.00610241 0.30512043 pg 4 200 0.00185326 0.00608912 0.30445597 0.00186161 0.0061157 0.3057849 0.999624097 39621-2A 11/11/2022 10:41:42 AM 0.00108247 0.00363638 0.18181882 pg 4 200 0.00107309 0.00360653 0.18032652 0.00109185 0.00366622 0.18331113 0.999624097 39621-2A DUP 11/11/2022 10:43:26 AM 0.00117113 0.00391852 0.19592598 pg 4 200 0.00116875 0.00391095 0.19554756 0.00117351 0.00392609 0.19630441 0.999624097 39621-3A 11/11/2022 10:45:10AM 0.00130321 0.00433879 0.21693973 pg 4 200 0.00129388 0.00430913 0.2154563 0.00131253 0.00436846 0.21842316 0.999624097 39621-3A SPK 11/11/2022 10:46:54 AM 0.025606 0.0816731 4.0836551 pg 4 200 0.02559967 0.08165294 4.08264717 0.02561234 0,08169326 4.08466304 0.999624097 0.004ug=DL 11/11/2022 10:48:47 AM 0.00108002 0.00343676 0.00343676 pg 0.00107514 0.00342123 0.00342123 0.00108491 0.0034523 0.0034523 0.999624097 0.080ug=QC STD 2 11/11/2022 10:50:28 AM 0.02481668 0.07896955 0.07896955 pg 0,02461832 0.07833834 0.07833834 0.02501504 0.07960076 0.07960076 0.999624097 Reagent Blank 11/11/2022 10:52:20 AM -8.54E-05 -0.0002717 -0.0002717 pg -8.26E-05 -0.0002628 -0.0002628 -8.82E-05 -0.0002806 -0.0002806 0.999624097 39621-4A 11/11/2022 10:54:02AM 0.0040813 0.01317902 0.65895094 pg 4 200 0.00406315 0.01312124 0.65606211 0.00409946 0.0132368 0.66183977 0.999624097 39621-5A 11/11/2022 10:55:45 AM -2.24E-05 0.00012056 0.00602788 pg 4 200 -2.74E-05 0.0001048 0.00523998 -1.74E-05 0.00013632 0.00681579 0.999624097 39621-6A 11/11/2022 10:57:28 AM 1.68E-05 0.00024515 0.01225773 pg 4 200 1.78E-06 0.00019751 0.0098753 3.17E-05 0.0002928 0.01464017 0.999624097 6A DUP 11/11/2022 10:59:11 AM -0.0001257 -0.0002083 -0.0104128 pg 4 200 -0.0001178 -0.000183 -0.0091494 -0.0001337 -0.0002335 -0.0116762 0.999624097 7A 11/11/2022 11:00:54 AM -8.09E-05 -6.56E-05 -0.0032818 pg 4 200 -7.43E-05 -4.47E-05 -0.0022358 -8.75E-05 -8.66E-05 -0.0043278 0.999624097 39bt1-7A SPK 11/11/2022 11:02:36 AM 0.02378681 0.07588421 3,79421073 pg 4 200 0.02363505 0.0754013 3.77006484 0.02393857 0.07636713 3.81835661 0.999624097 39621-8A 11/11/2022 11:04:30 AM 6.26E-05 0.00039103 0.01955128 pg 4 200 4.72E-05 0.00034189 0.01709464 7.80E-05 0.00044016 0.02200793 0.999624097 39621-9A 11/11/2022 11:06:14 AM 0.02074233 0.06619632 3.30981606 pg 4 200 0.02060139 0.06574785 3.28739261 0.02088326 0.06664479 3.33223951 0.999624097 39621-10A 11/11/2022 11:08:07 AM 0.00268436 0.0087338 0.43668982 pg 4 200 0.0026649 0,00867185 0.4335926 0.00270383 0.00879574 0.43978704 0.999624097 39621-10A DUP 11/11/2022 11:09:51 AM 0.00249549 0.00813279 0.4066394 pg 4 200 0.0024612 0.00802367 0.40118346 0.00252978 0.00824191 0.41209535 0.999624097 0.004ug=DL 11/11/2022 11:11:35 AM 0.00101267 0.00322243 0.00322243 pg 0.00101142 0.00321845 0.00321845 0.00101392 0.00322641 0.00322641 0.999624097 0.080ug=QC STD 2 11/11/2022 11:13:17 AM 0.02480879 0.07894443 0.07894443 pg 0.02475383 0.07876954 0.07876954 0.02486375 0,07911932 0.07911932 0.999624097 Reagent Blank 11/11/2022 11:15:09 AM -6.25E-05 -0.000199 -0.000199 pg -5.36E-05 -0.0001706 -0.0001706 -7.15E-05 -0.0002275 -0.0002275 0.999624097 39621-11A 11/11/2022 11:16:52 AM 0.00486352 0.01566814 0.78340683 pg 4 200 0.00487261 0.01569706 0.78485305 0.00485443 0.01563921 0.78196062 0.999624097 39621-11A SPK 11/11/2022 11:18:35 AM 0.02869771 0.09151127 4.57556355 pg 4 200 0.02861973 0.09126312 4.56315597 0.02877569 0.09175942 4.58797112 0.999624097 39621-12A 11/11/2022 11:20:29 AM 0.00192282 0,00631049 0.31552445 pg 4 200 0.00194718 0.00638798 0.31939915 0.00189847 0.006233 0.31164976 0.999624097 39621-13A 11/11/2022 11:22:13 AM -9.49E-05 -0.00011 -0,0055019 pg 4 200 -0.0001088 -0.0001543 -0.0077148 -8.10E-05 -6.58E-05 -0.003289 0.999624097 39621-14A 11/11/2022 11:23:56AM -8.67E-05 -8.41E-05 -0.0042037 pg 4 200 -9.23E-05 -0.000102 -0.0050997 -8.11E-05 -6.62E-05 -0.0033077 0.999624097 39621-14A DUP 11/11/2022 11:25:40 AM -5.99E-05 1.35E-06 6.76E-05 pg 4 200 -4.37E-05 5.29E-05 0.00264442 -7.61E-05 -5.02E-05 -0.0025092 0.999624097 39621-15A 11/11/2022 11:27:23 AM -4.90E-05 3.60E-05 0,00180042 pg 4 200 -5.05E-05 3.12E-05 0.00156139 -4.75E-05 4.08E-05 0.00203944 0.999624097 39621-15A SPK 11/11/2022 11:29:06 AM 0.02226946 0.07105583 3.55279133 pg 4 200 0.02220821 0.07086095 3.5430473 0.0223307 0.07125071 3.56253535 0.999624097 39621-16A 11/11/2022 11:30:59 AM 9.47E-05 0.00049325 0.02466263 pg 4 200 0.00010966 0.00054079 0.02703957 7.98E-05 0.00044571 0.02228569 0.999624097 39621-17A 11/11/2022 11:32:43 AM -8.45E-06 0.00016494 0.00824721 pg 4 200 -3.43E-05 8.27E-05 0.00413485 1.74E-05 0.00024719 0.01235956 0.999624097 0.004ug=DL 11/11/2022 11:34:26 AM 0.00112214 0.00357078 0.00357078 pg 0.00111871 0.00355986 0.00355986 0.00112557 0.0035817 0.0035817 0.999624097 0.080ug=QC STD 2 11/11/2022 11:36:07 AM 0.02487596 0.07915818 0.07915818 p9 0.02474435 0.0787394 0.0787394 0.02500757 0.07957697 0.07957697 0.999624097 Reagent Blank 11/11/2022 11:38:00 AM -2.16E-05 -6.86E-05 -6.86E-05 pg -4.83E-05 -0.0001537 -0.0001537 5.15E-06 1.64E-05 1.64E-05 0.999624097 39621-18A 11/11/2022 11:39:43AM -1.97E-05 0,00012917 0.00645865 pg 4 200 1.62E-05 0,00024351 0.01217556 -5.56E-05 1.48E-05 0.00074173 0.999624097 39621-1B 11/11/2022 11:41:27 AM 0.00158002 0.00521964 0.65245492 pg 4 500 0.00157204 0.00519424 0.64928056 0.001588 0.00524503 0.65562929 0.999624097 39621-2B 11/11/2022 11:43:11 AM 0.00066314 0.00230203 0.28775379 pg 4 500 0.0006664 0.0023124 0.2890503 0.00065988 0.00229166 0.28645727 0.999624097 39621-2B DUP 11/11/2022 11:44:55 AM 0.0011631 0.00389296 0.48662049 pg 4 500 0.00114032 0.00382048 0.47756048 0.00118588 0.00396544 0.49568049 0.999624097 39621-3B 11/11/2022 11:46:39 AM 0.00074761 0.00257084 0.32135443 pg 4 500 0.00075915 0.00260754 0.32594295 0.00073608 0.00253413 0.31676591 0.999624097 39621-3B SPK 11/11/2022 11:48:23 AM 0.02381254 0.07596609 9.49576096 pg 4 500 0.02388188 0.07618675 9.52334412 0.02374319 0.07574542 9.46817781 0.999624097 39621-4B 11/11/2022 11:50:16 AM 0.00110669 0.00371346 0.46418265 pg 4 500 0.00108848 0.00365552 0.45693977 0.0011249 0.0037714 0.47142553 0.999624097 39621-5B 11/11/2022 11:52:00AM 4.69E-05 0.00034097 0.04262182 pg 4 500 5.26E-05 0.00035932 0.04491503 4.11E-05 0.00032263 0.04032861 0.999624097 39621-6B 11/11/2022 11:53:43 AM 0,00015301 0.00067873 0.08484134 pg 4 500 0.00014828 0.00066368 0.08295982 0.00015774 0.00069378 0.08672286 0.999624097 39621-6BDUP 11/11/2022 11:55:26AM 2.61E-05 0.00027503 0.03437853 pg 4 500 5.01E-05 0.00035118 0.04389771 2.21E-06 0.00019887 0.02485935 0.999624097 0.004ug=DL 11/11/2022 11:57:09 AM 0.00108251 0.00344467 0.00344467 pg 0.00106782 0.00339793 0.00339793 0.0010972 0.00349141 0.00349141 0.999624097 0.080ug=QC STD 2 11/11/2022 11:58:51 AM 0.02521556 0.08023883 0.08023883 pg 0.02522045 0.08025439 0.08025439 0.02521067 0.08022326 0.08022326 0.999624097 Reagent Blank 11/11/2022 12:00:44 PM -7.76E-05 -0.0002469 -0.0002469 pg -8.69E-05 -0.0002764 -0.0002764 -6.83E-05 -0.0002174 -0.0002174 0.999624097 39F91-7B 11/11/2022 12:02:27 PM 0.00026349 0.0010303 0.12878794 pg 4 500 0.0002529 0.00099661 0.12457617 0.00027408 0.001064 0.13299971 0.999624097 7B SPK 11/11/2022 12:04:10 PM 0.02451623 0.07820532 9.77566529 pg 4 500 0.02441478 0.0778825 9.73531214 0.02461768 0.07852815 9.81601845 0.999624097 8B 11/11/2022 12:06:05 PM -2.47E-05 0.0001133 0.01416242 pg 4 500 -2.52E-05 0.00011158 0.01394771 -2.41E-05 0.00011502 0.01437714 0.999624097 39bZ1-96 11/11/2022 12:07:49 PM 0.00552597 0.01777612 2.22201457 pg 4 500 0.00551759 0.01774944 2.21867941 0.00553435 0.0178028 2.22534974 0,999624097 39621-11B 11/11/2022 12:13:01 PM 0.00081123 0.00277326 0.34665735 pg 4 500 0.00080492 0.00275319 0.34414921 0.00081753 0.00279332 0,34916548 0.999624097 39621-11B SPK 11/11/2022 12:14:45 PM 0.02425049 0.0773597 9.66996296 pg 4 500 0.02420469 0.07721395 9.65174387 0.02429629 0.07750546 9.68818206 0.999624097 39621-12B 11/11/2022 12:16:39 PM 0.00079082 0.00270833 0.33854084 pg 4 500 0.00076442 0.00262432 0.32804031 0.00081722 0.00279233 0.34904137 0.999624097 elementOne NE01 3AS-021420-RT-1 303 Appendix C- Page 446 of 1178 Hg-Data 1 of 3 e 396 -Hg 66.1 PerkinElmer FIMS-100 CVAA Mercury Analyzer Sample-ID Date Time Mean-Sig Mean_Rd Mean_Rt Units Alq. Vol. Sig 1 Reading-1 Result-1 Sig 2 Reading-2 Result-2 Cor.Coeff. 39621-13B 11/11/2022 12:18:23 PM 7.00E-05 0.00041464 0.0518294 pg 4 500 7.45E-05 0.000429 0.05362494 6.55E-05 0.00040027 0.05003386 0.999624097 0.004ug=DL 11/11/2022 12:20:06 PM 0.00104245 0.00331719 0.00331719 pg 0.00103278 0.00328643 0.00328643 0.00105212 0.00334796 0.00334796 0.99962an97 0.080ug=QC STD 2 11/11/2022 12:21:48 PM 0.02508123 0.07981139 0.07981139 pg 0.02510645 0.07989164 0.07989164 0.02505601 0.07973113 0.07973113 0.999' Reagent Blank 11/11/2022 12:23:40 PM -5.73E-05 -0.0001823 -0.0001823 pg -9.54E-05 -0.0003035 -0.0003035 -1.92E-05 -6.11E-05 -6.11E-05 0.999� 39621-14B 11/11/2022 12:25:23 PM -3.76E-06 0.00017989 0.02248597 pg 4 500 -3.19E-06 0.00018168 0.02270962 -4.32E-06 0.0001781 0.02226232 0.999624097 39621-14B DUP 11/11/2022 12:27:07 PM -6.18E-05 -4.70E-06 -0.0005872 pg 4 500 -5.73E-05 9.35E-06 0.00116924 -6.62E-05 -1.87E-05 -0.0023436 0.999624097 39621-15B 11/11/2022 12:28:51 PM -0.0002038 -0.0004568 -0.0571017 pg 4 500 -0.0001814 -0.0003853 -0.0481645 -0.0002263 -0.0005283 -0.066039 0.999624097 39621-15B SPK 11/11/2022 12:30:34 PM 0.02225189 0.07099992 8.87498989 pg 4 500 0.02226063 0.07102774 8.87846758 0.02224314 0.0709721 8.87151221 0.999624097 39621-16B 11/11/2022 12:32:28 PM -0.0001778 -0.0003741 -0.0467597 pg 4 500 -0.0001652 -0.0003339 -0.0417371 -0.0001905 -0.0004143 -0.0517824 0.999624097 39621-17B 11/11/2022 12:34:13 PM -0.0001889 -0.0004093 -0.0511593 pg 4 500 -0.0001811 -0.0003845 -0.048062 -0.0001967 -0.0004341 -0.0542566 0.999624097 39621-18B 11/11/2022 12:35:57 PM -6.28E-06 0.00017187 0.0214832 pg 4 500 -8.27E-06 0.00016552 0.02068962 -4.28E-06 0.00017821 0.02227678 0.999624097 0.004ug=DL 11/11/2022 12:37:40 PM 0.00111697 0.00355432 0.00355432 pg 0.00110217 0.00350722 0.00350722 0.00113177 0.00360143 0.00360143 0.999624097 0.080ug=QC STD 3 11/11/2022 12:39:23 PM 0.02736516 0.0870791 0.0870791 pg 0.02739754 0.08718215 0.08718215 0.02733278 0.08697606 0.08697606 0.999624097 Reagent Blank 11/11/2022 12:41:16 PM -9.89E-05 -0.0003147 -0.0003147 pg -8.40E-05 -0.0002672 -0.0002672 -0.0001138 -0.0003622 -0.0003622 0.999624097 Calib Blank 11/14/2022 11:50:39 AM -6.56E-05 pg -8.82E-05 -4.30E-05 STD1=.004ug 11/14/2022 11:52:20 AM 0.00177481 p9 0.00173058 0,00181905 STD2=.04ug 11/14/2022 11:54:02 AM 0.01386328 pg 0.01390734 0.01381923 STD3=.08ug 11/14/2022 11:55:56 AM 0.02666238 p9 0.02685235 0.0264724 STD4=.16ug 11/14/2022 11:57:51 AM 0.05195763 pg 0.05203074 0.05188453 STD5=.2ug 11/14/2022 11:59:44 AM 0.06344305 pg 0.06393887 0.06294724 Reagent Blank 11/14/2022 12:01:36 PM 3.47E-05 0.00010765 0.00010765 pg 3.82E-05 0.00011848 0,00011848 3.12E-05 9.68E-05 9.68E-05 0.004ug=DL 11/14/2022 12:06:43 PM 0.00136912 0.0042516 0.0042516 pg 0.0013723 0.00426149 0.00426149 0.00136594 0.00424171 0.00424171 0.999436733 0.080ug=QC STD 3 11/14/2022 12:12:11 PM 0.02615178 0.08121051 0.08121051 pg 0.02599394 0.08072037 0.08072037 0.02630961 0.08170064 0.08170064 0.999436733 0.080ug=QC STD 2 11/14/2022 12:14:05 PM 0.02688185 0.08347765 0.08347765 pg 0.02676445 0.08311307 0.08311307 0.02699926 0.08384224 0.08384224 0.999436733 Reagent Blank 11/14/2022 12:15:57 PM 6.94E-05 0.00021542 0.00021542 pg 6.60E-05 0.00020495 0.00020495 7.27E-05 0.0002259 0.0002259 0.999436733 0.004ug=DL 11/14/2022 1:20:45 PM 0.001478 0.00458971 0.00458971 pg 0.00147709 0.0045869 0.0045869 0.0014789 0.00459251 0.00459251 0.999436733 0.080ug=QC STD 2 11/14/2022 1:22:27 PM 0.02691548 0.08358209 0.08358209 pg 0.02696084 0.08372293 0.08372293 0.02687013 0.08344124 0.08344124 0.999436733 Reagent Blank 11/14/2022 1:24:20 PM 8.76E-05 0.00027192 0.00027192 pg 9.25E-05 0.00028735 0.00028735 8.26E-05 0.00025648 0.00025648 0.999436733 39621-1C 11/14/2022 1:31:21 PM 0.00222114 0.00678979 0.67897886 pg 4 400 0.00221261 0.0067633 0.6763296 0.00222968 0.00681628 0.68162812 0.999436733 39621-2C 11/14/2022 1:33:04 PM 0.00205193 0.00626433 0.62643289 pg 4 400 0.00205995 0.00628921 0.62892123 0.00204392 0.00623945 0.62394455 0.999436733 39621-2C DUP 11/14/2022 1:34:47 PM 0.00212182 0.00648135 0.64813469 pg 4 400 0.00210664 0.00643423 0.64342254 0.00213699 0.00652847 0.65284685 0.999436733 39621-3C 11/14/2022 1:36:30 PM 0.00184339 0.00561673 0.56167342 pg 4 400 0.00184086 0.00560887 0.56088658 0.00184593 0.0056246 0.56246026 0.999436733 39621-3C SPK 11/14/2022 1:38:13 PM 0.02583629 0.08012316 8.01231568 pg 4 400 0.02600382 0,08064338 8.06433844 0.02566876 0.07960293 7.96029292 0.999436733 39621-4C 11/14/2022 1:40:07 PM 0.00315264 0.00968241 0.96824149 pg 4 400 0.00316739 0.00972821 0.97282062 0.0031379 0.00963662 0.96366236 0.999436733 39621-5C 11/14/2022 1:41:50 PM 0.00094801 0.00283627 0.28362668 pg 4 400 0.00096131 0.00287757 0.287757 0.00093471 0.00279496 0.27949635 0.999436733 0.004ug=DL 11/14/2022 1:43:34 PM 0.00151454 0.00470317 0.00470317 pg 0.00150071 0.00466025 0.00466025 0.00152836 0.00474609 0.00474609 0.999436733 0.080ug=QC STD 2 11/14/2022 1:45:16 PM 0.02688785 0.08349628 0.08349628 pg 0.0268785 0.08346724 0.08346724 0.0268972 0.08352532 0.08352532 0.999436733 Reagent Blank 11/14/2022 1:47:09 PM 7.89E-05 0.00024515 0.00024515 pg 8.91E-05 0.00027681 0.00027681 6.88E-05 0.0002135 0.0002135 0.999436733 39621-6C 11/14/2022 1:48:52 PM 0.00070486 0.00208118 0.20811765 pg 4 400 0.00073602 0.00217795 0.21779544 0.00067369 0.0019844 0.19843986 0.99943F733 39621-6C DUP 11/14/2022 1:50:36 PM 0.0007072 0.00208844 0.20884419 pg 4 400 0.00068705 0.00202589 0.20258908 0.00072734 0.00215099 0.2150993 0.999, 39621-7C 11/14/2022 1:52:19 PM 0.00075062 0.00222328 0.22232777 pg 4 400 0.00071316 0.00210698 0.21069776 0.00078807 0.00233958 0.23395778 0.999• 39621-7C SPK 11/14/2022 1:54:03 PM 0.0248118 0.07694176 7.69417624 pg 4 400 0.02485564 0.07707788 7.70778807 0.02476797 0.07680564 7.68056441 0.999436733 39621-8C 11/14/2022 1:55:57 PM 0.00041342 0.00117615 0.11761533 pg 4 400 0.00041265 0.00117377 0.11737742 0.00041418 0.00117853 0.11785324 0.999436733 39621-9C 11114/2022 1:57:40 PM 0.01699723 0.05267476 5.26747612 pg 4 400 0.01695065 0.05253011 5.25301079 0.01704381 0.05281941 5.28194145 0.999436733 39621-10C 11/14/2022 1:59:34 PM 0.00739798 0.02286569 2.28656864 pg 4 400 0.00739721 0.02286331 2.28633131 0.00739874 0.02286806 2.28680597 0.999436733 39621-10C DUP 11/14/2022 2:01:18 PM 0.00745543 0.02304408 2.30440828 pg 4 400 0.0074876 0.02314401 2.31440059 0.00742325 0.02294416 2.29441597 0.999436733 39621-11C 11/14/2022 2:03:00 PM 0.00426703 0.01314298 1.31429771 pg 4 400 0.00425247 0.01309776 1.30977618 0.00428159 0.01318819 1.31881923 0.999436733 39621-11C SPK 11/14/2022 2:04:43 PM 0.02847336 0.08831219 8.831219 pg 4 400 0.02838628 0,08804177 8.8041768 0.02856044 0.08858261 8.85826119 0.999436733 0.004ug=DL 11/14/2022 2:06:37 PM 0.00148964 0.00462587 0.00462587 pg 0.00149825 0.00465261 0.00465261 0.00148103 0.00459913 0.00459913 0.999436733 0.080ug=QC STD 2 11/14/2022 2:08:19 PM 0.02722064 0.0845297 0.0845297 pg 0.02708744 0.08411607 0.08411607 0.02735384 0.08494333 0.08494333 0.999436733 Reagent Blank 11/14/2022 2:10:11 PM 9.48E-05 0.0002945 0.0002945 pg 8.22E-05 0.00025532 0.00025532 0.00010746 0.00033369 0.00033369 0.999436733 39621-12C 11/14/2022 2:11:54 PM 0.00687733 0.0212489 2.12489011 pg 4 400 0.0068608 0.02119756 2.1197565 0.00689387 0.02130024 2.13002371 0.999436733 39621-13C 11/14/2022 2:13:38 PM 0.00158882 0.00482621 0.48262123 pg 4 400 0.00158224 0.00480578 0.48057763 0.00159541 0.00484665 0.48466483 0.999436733 39621-14C 11/14/2022 2:15:23 PM 0.00121983 0.00368035 0.36803532 pg 4 400 0.00123627 0.0037314 0.3731399 0.00120339 0.00362931 0.36293074 0.999436733 39621-14C DUP 11/14/2022 2:17:06 PM 0.00122914 0.00370926 0.37092636 pg 4 400 0.00120666 0.00363947 0.36394686 0.00125162 0.00377906 0.37790586 0.999436733 39621-15C 11/14/2022 2:18:50 PM 0.00056374 0.00164296 0.16429611 pg 4 400 0.00054598 0.00158782 0.15878217 0.0005815 0.0016981 0.16981006 0.999436733 39621-15C SPK 11/14/2022 2:20:34 PM 0.02599346 0.08061123 8.061123 pg 4 400 0.0258973 0.08031261 8.03126078 0.02608962 0.08090985 8.09098522 0.999436733 Reagent Blank 11/14/2022 2:39:15 PM 0.00011034 0.00034263 0.00034263 pg 0.00012195 0.00037869 0.00037869 9.87E-05 0.00030657 0.00030657 0.004ug=DL 11/14/2022 2:40:57 PM 0.00116363 0.00361348 0.00361348 pg 0.00118482 0.00367928 0.00367928 0.00114244 0.00354768 0.00354768 0.999436733 0.080ug=QC STD 3 11/14/2022 2:42:39 PM 0.02722603 0.08454645 0.08454645 pg 0.02710453 0.08416913 0.08416913 0.02734754 0.08492378 0.08492378 0.999436733 Reagent Blank 11/14/2022 2:46:41 PM 0.00011597 0.00036012 0.00036012 pg 0.00014112 0.00043824 0.00043824 9.08E-05 0.00028199 0.00028199 Calib Blank 11/14/2022 3:14:36 PM 8.68E-05 pg 9.66E-05 7.71E-05 STD1=.004ug 11/14/2022 3:16:18 PM 0.00176663 pg 0.00174754 0.00178573 STD2=.04ug 11/14/2022 3:18:00 PM 0.01387883 pg 0.01389485 0.0138628 STD3=.08ug 11/14/2022 3:19:57 PM 0.02701502 pg 0,0269735 0.02705653 STD4=.16ug 11/14/2022 3:21:52 PM 0.05157411 pg 0.05132217 0.05182605 STD5=.2ug 11/14/2022 3:23:45 PM 0.0638641 pg 0.06388985 0.06383835 Reagent Blank 11/14/2022 3:25:42 PM 6.69E-06 2.07E-05 2.07E-05 pg 1.74E-05 5.39E-05 5.39E-05 -4.01E-06 -1.24E-05 -1.24E-05 0.004ug=DL 11/14/2022 3:33:14 PM 0.00128081 0.00396875 0.00396875 pg 0.001276 0.00395384 0.00395384 0.00128562 0.00398365 0.00398365 0.999449698 0.080ug=QC STD 3 11/14/2022 3:34:56 PM 0.02601861 0.08062202 0.08062202 pg 0.02604666 0.08070894 0.08070894 0.02599056 0.0805351 0.0805351 0.999449698 0.080ug=QC STD 2 11/14/2022 3:36:49 PM 0.02610721 0.08089656 0.08089656 pg 0.02622888 0.08127356 0.08127356 0.02598554 0.08051957 0.08051957 0.999449698 Reagent Blank 11/14/2022 3:38:41 PM -1.60E-06 -4.95E-06 -4.95E-06 pg 1.15E-05 3.58E-05 3.58E-05 -1.47E-05 -4.57E-05 -4.57E-05 0.999449698 39621-16C 11/14/2022 3:50:58 PM 0.00047765 0.00152836 0.15283626 pg 4 400 0.0004848 0.00155052 0.15505185 0.0004705 0.00150621 0.15062066 0.999449698 39621-17C 11/14/2022 3:52:42 PM 0.00068835 0.00218125 0.21812488 pg 4 400 0.00069525 0.00220262 0.22026235 0.00068145 0.00215987 0.21598741 0.999449698 39621-18C 11/14/2022 3:54:25 PM 0.00037298 0.00120405 0.12040464 pg 4 400 0.00037341 0.00120538 0.12053758 0.00037255 0.00120272 0.1202717 0,999449698 0.004ug=DL 11/14/2022 3:57:51 PM 0.00130962 0.00405803 0.00405803 pg 0.0013228 0.00409887 0.00409887 0.00129644 0.00401719 0.00401719 0.999449F9B 0.080ug=QC STD 2 11/14/2022 3:59:33 PM 0.02635126 0.08165279 0.08165279 pg 0.02627274 0.08140949 0.08140949 0.02642978 0.0818961 0.0818961 0.999 Reagent Blank 11/14/2022 4:01:25 PM -7.05E-05 -0.0002184 -0.0002184 pg -8.53E-05 -0,0002644 -0.0002644 -5.57E-05 -0.0001725 -0.0001725 0.999. Calib Blank 11/16/2022 9:03:43 AM 0.00032411 pg 0.00057925 6.90E-05 STD1=.004ug 11/16/2022 9:05:25 AM 0.00074714 pg 0.00072749 0.00076679 STD2=.04ug 11/16/2022 9:07:08 AM 0.00972882 pg 0.00966984 0.0097878 STD3=.08ug 11/16/2022 9:09:02 AM 0.01959107 pg 0.01963906 0.01954307 elementOne NE01 3AS-021420-RT-1 303 Appendix C- Page 447 of 1178 Hg-Data 2 of 3 e 396 1-Hg 66.2 PerkinElmer FIMS-100 CVAA Mercury Analyzer Sample-ID Date Time Mean-Sig Mean Rd Mean_Rt Units Alq. Vol. Sig 1 Reading-1 Result-1 Sig 2 Reading-2 Result-2 Cor.Coeff. STD4=.16ug 11/16/2022 9:10:57 AM 0.03912142 pg 0.03908423 0.03915861 STD5=.2ug 11/16/2022 9:12:51 AM 0,04938044 pg 0.04946204 0.04929884 R Blank 11/16/2022 9:14:43 AM -0.0001146 -0.0004664 -0.0004664 pg -0.0001314 -0.0005348 -0.000534E -9.78E-05 -0.0003981 -0.0003981 C =DL 11/16/2022 9:18:07 AM 0.00099626 0.00405295 0.00405295 pg 0.00101143 0.00411465 0.00411465 0.00098109 0.00399125 0.00399125 0,999949615 O.u.._4=QC STD 3 11/16/2022 9:21:42 AM 0.01786806 0.07269032 0.07269032 pg 0.01781818 0.0724874 0.0724874 0.01791794 0.07289324 0.07289324 0.999949615 0.080ug=QC STD 2 11/16/2022 9:23:35 AM 0.01980068 0.08055254 0.08055254 pg 0.01990817 0.08098981 0.08098981 0.01969319 0.08011526 0.08011526 0.999949615 Reagent Blank 11/16/2022 9:25:28 AM -6.66E-05 -0.0002711 -0.0002711 pg -4.57E-05 -0.0001857 -0.0001857 -6.76E-05 -0.0003564 -0.0003564 0.999949615 39621-10B 11/16/2022 9:41:17 AM 0.00106222 0.00478769 0.59846088 pg 4 500 0.00108574 0.00488338 0.61042238 0.00103869 0.004692 0.58649938 0.999949615 39621-10B DUP 11/16/2022 9:42:59 AM 0.00110783 0.00497326 0.62165762 pg 4 500 0.00112146 0.0050287 0.62858795 0.0010942 0.00491782 0.61472729 0.999949615 0.004ug=DL 11/16/2022 9:44:40 AM 0.00105098 0.00427558 0.00427558 pg 0.00106454 0.00433072 0.00433072 0.00103743 0.00422043 0.00422043 0.999949615 0.080ug=QC STD 2 11/16/2022 9:46:23 AM 0.01969023 0.08010323 0.08010323 pg 0.01970377 0.0801583 0.0801583 0.0196767 0,08004815 0.08004815 0.999949615 Reagent Blank 11/16/2022 9:48:15 AM -9.10E-06 -3.70E-05 -3.70E-05 pg 2.55E-05 0.00010391 0.00010391 -4.38E-05 -0.000178 -0.000178 0.999949615 Calib Blank 11/17/2022 10:33:41 AM 0.00018618 pg 0.00014091 0.00023146 STD1=.004ug 11/17/2022 10:35:22 AM 0.0012611 pg 0.00124308 0.00127911 STD2=.04ug 11/17/2022 10:37:05 AM 0.01239471 p9 0.01241315 0.01237627 STD3=.08ug 11/17/2022 10:38:59 AM 0.02387541 pg 0.02391262 0.0238382 STD4=.16ug 11/17/2022 10:40:54 AM 0.04744251 pg 0.04707182 0.0478132 STD5=.2ug 11/17/2022 10:42:48 AM 0.05915774 pg 0.05891422 0.05940126 Reagent Blank 11/17/2022 10:44:39 AM -5.43E-05 -0.0001832 -0.0001832 pg -8.35E-05 -0.0002815 -0.0002815 -2.52E-05 -8.49E-05 -8.49E-05 0.004ug=DL 11/17/2022 10:46:21 AM 0.00121858 0.00410854 0.00410854 pg 0.00120674 0.00406862 0.00406862 0.00123043 0.00414847 0.00414847 0.999928759 0.080ug=QC STD 3 11/17/2022 10:48:03 AM 0.02408047 0.08118897 0.08118897 pg 0.02405116 0,08109014 0.08109014 0.02410979 0.08128781 0.08128781 0.999928759 0.080ug=QC STD 2 11/17/2022 10:49:56 AM 0.02407622 0.08117463 0.08117463 pg 0.02414552 0.08140829 0.08140829 0.02400691 0.08094097 0.08094097 0.999928759 Reagent Blank 11/17/2022 10:51:48 AM -7.75E-05 -0.0002613 -0.0002613 pg -4.59E-05 -0.0001548 -0.0001548 -0.0001091 -0.0003677 -0.0003677 0.999928759 39621-1BH 11/17/2022 10:57:09 AM 0.01345961 0.04556317 13.7828602 pg 2 605 0.01344131 0.04550145 13.7641881 0.01347792 0.0456249 13.8015322 0.999928759 39621-2BH 11/17/2022 10:59:04 AM 0.02582486 0.08725346 26.6123054 pg 2 610 0.02576011 0.08703513 26.5457157 0.02588962 0.08747179 26.6788951 0.999928759 39621-2BH DUP 11/17/2022 11:00:59 AM 0.02737367 0.09247536 28.204985 pg 2 610 0.0272309 0.09199403 28.0581776 0.02751643 0.0929567 28.3517925 0.999928759 39621-3BH 11/17/2022 11:02:53 AM 0.01758207 0.05946233 18.4333221 pg 2 620 0.01756397 0.05940131 18.4144065 0.01760017 0.05952335 18.4522377 0.999928759 39621-3BH SPK 11/17/2022 11:04:46 AM 0.03956311 0.13357292 41.4076042 pg 2 620 0.03958002 0.13362991 41.4252734 0.03954621 0.13351592 41.389935 0.999928759 39621-4BH 11/17/2022 11:06:38 AM 0.0281189 0.09498796 28.7338593 pg 2 605 0.02821078 0.09529774 28.8275671 0.02802702 0.09467819 28.6401514 0.999928759 39621-5BH 11/17/2022 11:08:31 AM 0.00191073 0.0066253 1.30849748 pg 4 790 0.00190325 0.00660011 1.30352255 0.0019182 0.00665049 1.3134724 0.999928759 39621-6BH 11/17/2022 11:10:13 AM 0.00208037 0.00719727 1.38547496 pg 4 770 0.00206957 0.00716084 1.3784626 0.00209117 0.0072337 1.39248732 0.999928759 0.004ug=DL 11/17/2022 11:11:55 AM 0.00125399 0.00422792 0.00422792 pg 0.00127834 0.00431 0.00431 0.00122965 0.00414584 0.00414584 0.999928759 0.080ug=QC STD 2 11/17/2022 11:13:38 AM 0.02396455 0.08079814 0,08079814 pg 0.02390388 0.08059357 0.08059357 0,02402523 0.08100271 0.08100271 0.999928759 Reagent Blank 11/17/2022 11:15:30 AM -0.0001639 -0.0005526 -0.0005526 pg -0.0001715 -0.0005781 -0.0005781 -0.0001563 -0.000527 -0.000527 0.999928759 39621-6BH DUP 11/17/2022 11:17:12 AM 0.00207549 0.00718081 1.38230519 pg 4 770 0.00208887 0.00722594 1.39099306 0.0020621 0.00713567 1.37361733 0.999928759 39621-7BH 11/17/2022 11:18:55 AM 0.00218695 0.00755661 1.45464764 pg 4 770 0.00217648 0.00752132 1.44785479 0.00219742 0.0075919 1.46144049 0.999928759 39621-7BH SPK 11/17/2022 11:20:37 AM 0.02491853 0.08419769 16.2080559 pg 4 770 0.02500008 0.08447265 16.2609854 0.02483698 0.08392273 16.1551263 0.999928759 39621-8BH 11/17/2022 11:22:31 AM 0.00210069 0.00726577 1.416B2539 pg 4 780 0.00211122 0.0073013 1.42375366 0.00209015 0.00723024 1.40989711 0.999928759 39621-9BH 11/17/2022 11:24:15 AM 0.02953168 0.09975125 31.172265 pg 2 625 0.02938357 0.09925189 31.0162143 0.02967979 0.10025061 31.3283156 0.999928759 7r 'OBH 11/17/2022 11:26:10AM 0.05437272 0.18350453 59.6389725 pg 2 650 0.05447109 0.18383619 59.7467602 0.05427435 0.18317288 59.5311849 0.999928759 JBH DUP 11/17/2022 11:28:05 AM 0.05414404 0.18273351 59.3883918 pg 2 650 0.05348761 0.18052031 58.6691 0.05480047 0.18494672 60.1076837 0.999928759 35,-.-11BH 11/17/2022 11:29:59AM 0.04223512 0.14258176 45.6261645 pg 2 640 0.042226 0.14255104 45.6163333 0.04224423 0.14261249 45.6359958 0.999928759 39621-11BH SPK 11/17/2022 11:31:51 AM 0.0639577 0.21582094 69.0626992 pg 2 640 0.06412983 0.21640131 69.2484186 0.06378556 0.21524056 68.8769798 0.999928759 39621-12BH 11/17/2022 11:33:44 AM 0.02012294 0.06802903 20.0685642 pg 2 590 0.0201639 0,06816715 20.1093106 0.02008197 0.06789091 20.0278178 0.999928759 0.004ug=DL 11/17/2022 11:35:37 AM 0.00119025 0.004013 0.004013 pg 0.00120687 0.00406904 0.00406904 0.00117363 0.00395697 0.00395697 0.999928759 0.080ug=QC STD 2 11/17/2022 11:37:18 AM 0.02378285 0.08018551 0.08018551 pg 0.02359952 0.07956742 0.07956742 0.02396617 0.0808036 0.0808036 0.999928759 Reagent Blank 11/17/2022 11:39:10 AM -0.0001595 -0.0005378 -0.0005378 pg -0.0001478 -0.0004983 -0.0004983 -0.0001712 -0.0005772 -0.0005772 0.999928759 39621-13BH 11/17/2022 11:40:52 AM 0.00911086 0.03090106 5.79394962 pg 4 750 0.00917423 0.0311147 5.83400629 0.0090475 0.03068743 5.75389296 0.999928759 39621-146H 11/17/2022 11:42:44 AM 0.00525533 0.01790187 3.58037425 pg 4 800 0.00522064 0.01778491 3.55698117 0.00529002 0.01801884 3.60376733 0.999928759 39621-14BH DUP 11/17/2022 11:44:26 AM 0.00524339 0.01786162 3.57232347 pg 4 800 0.00522131 0.01778717 3.55743465 0.00526547 0.01793606 3.58721229 0.999928759 39621-15BH 11/17/2022 11:46:09 AM 0.00286676 0.00984865 1.79737919 pg 4 730 0.00286175 0.00983175 1,79429354 0.00287178 0.00986556 1.80046483 0.999928759 39621-15BH SPK 11/17/2022 11:47:52 AM 0.02461106 0.08316105 15.1768915 pg 4 730 0.02461189 0.08316386 15.1774042 0.02461023 0.08315824 15.1763788 0.999928759 39621-16BH 11/17/2022 11:49:46 AM 0.00264186 0.00909036 1.59081293 pg 4 700 0.00264457 0.00909952 1.59241559 0.00263914 0.0090812 1.58921027 0.999928759 39621-17BH 11/17/2022 11:51:30 AM 0.0004078 0.00155808 0.12075143 pg 4 310 0.00040739 0.00155671 0.12064472 0.00040821 0.00155946 0.12085814 0.999928759 39621-18BH 11/17/2022 11:53:14 AM 0.00037319 0,00144138 0.07206904 pg 4 200 0.00038009 0.00146467 0.07323365 0.00036628 0.00141809 0.07090442 0.999928759 39621-FH LRB 11/17/2022 11:54:58 AM 0.00025175 0.00103197 0.02579925 pg 4 100 0.000234 0.00097212 0.02430303 0.00026951 0.00109182 0.02729546 0.999928759 39621-FH LRB SPK 11/17/2022 11:56:41 AM 0.02114995 0.07149168 4.46822995 pg 1.6 100 0.02098493 0.07093531 4.43345668 0.02131497 0.07204805 4.50300322 0.999928759 0.004ug=DL 11/17/2022 11:58:34 AM 0.00119859 0.00404114 0.00404114 pg 0.00119798 0.00403907 0.00403907 0.0011992 0.0040432 0.0040432 0.999928759 0.080ug=QC STD 2 11/17/2022 12:00:16 PM 0.01205494 0.04064405 0.04064405 pg 0.02409017 0.08122165 0.08122165 1.97E-05 6.65E-05 6.65E-05 0.999928759 0.080ug=QC STD 2 11/17/2022 12:02:08 PM 0.0241734 0.08150229 0.08150229 pg 0.02412646 0.08134401 0.08134401 0.02422034 0.08166056 0.08166056 0.999928759 Reagent Blank 11/17/2022 12:04:01 PM -0.0001271 -0.0004285 -0.0004285 pg -0.0001212 -0.0004087 -0.0004087 -0.000133 -0.0004483 -0.0004483 0.999928759 39621-5FH 11/17/2022 12:05:43 PM 0.00062322 0.00228438 0.05710955 pg 4 100 0.0006224 0.00228164 0.0570409 0.00062403 0.00228713 0.05717819 0.999928759 39621-6FH 11/17/2022 12:07:26 PM 0.00057377 0.00211768 0.05294204 pg 4 100 0.00058017 0.00213923 0.05348079 0,00056738 0.00209613 0.0524033 0.999928759 39621-6FH DUP 11/17/2022 12:09:09 PM 0,00045783 0.00172678 0.04316956 pg 4 100 0.00044849 0.00169528 0.04238207 0.00046718 0.00175828 0.04395705 0.999928759 39621-7FH 11/17/2022 12:10:52 PM 0.00041553 0.00158415 0.03960376 pg 4 100 0.00040935 0.00156333 0.03908323 0.00042171 0.00160497 0.04012429 0.999928759 39621-7FH SPK 11/17/2022 12:12:35 PM 0.02256166 0.07625137 1.90628416 pg 4 100 0.02254303 0.07618854 1.90471341 0.0225803 0.0763142 1.90785491 0.999928759 39621-8FH 11/17/2022 12:14:28 PM 0.00080781 0.00290675 0,0726687 pg 4 100 0.0007718 0.00278535 0.06963383 0.00084382 0.00302814 0.07570357 0.999928759 39621-13FH 11/17/2022 12:16:10 PM 0.00132771 0.00465964 0.116491 pg 4 100 0.00132194 0.00464019 0.1160047 0.00133348 0.00467909 0.1169773 0.999928759 39621-14FH 11/17/2022 12:17:54 PM 0.00046763 0.0017598 0.043995 pg 4 100 0.00047707 0.00179163 0.04479064 0.00045819 0.00172797 0.04319936 0.999928759 39621-14FH DUP 11/17/2022 12:19:37 PM 0.00056869 0.00210053 0.05251326 pg 4 100 0.00058162 0.00214412 0.0536031 0.00055576 0.00205694 0.05142341 0.999928759 39621-15FH 11/17/2022 12:21:21 PM 0.00048332 0.00181271 0.04531775 pg 4 100 0.00049997 0.00186884 0.04672088 0.00046667 0.00175658 0.04391461 0.999928759 0.004ug=DL 11/17/2022 12:23:05 PM 0.00121297 0.00408962 0.00408962 pg 0.00121781 0.00410592 0.00410592 0.00120814 0.00407332 0.00407332 0.999928759 0.080ug=QC STD 2 11/17/2022 12:24:46 PM 0.02386677 0.08046846 0.08046846 pg 0.02393803 0.0807087 0.0807087 0.02379552 0.08022823 0.08022823 0.999928759 Reagent Blank 11/17/2022 12:26:39 PM -0.0001414 -0.0004768 -0.0004768 pg -0.0001193 -0.0004022 -0.0004022 -0.0001636 -0.0005514 -0.0005514 0.999928759 39621-15FH SPK 11/17/2022 12:28:22 PM 0.02209223 0.07466863 1.86671587 pg 4 100 0.02196077 0.07422542 1.85563543 0.02222369 0.07511185 1.87779631 0.999928759 39621-16FH 11/17/2022 12:30:17 PM 0.00043679 0.00165583 0.04139577 pg 4 100 0,00043928 0.00166423 0.04160587 0.0004343 0.00164743 0.04118567 0.999928759 3' '7FH 11/17/2022 12:32:00 PM 0.00027784 0.00111992 0.02799809 pg 4 100 0.00027394 0.00110676 0.02766908 0.00028175 0.00113308 0.0283271 0.999928759 3FH 11/17/2022 12:33:44 PM 9.56E-05 0.00050563 0.01264087 pg 4 100 9.24E-05 0.0004947 0.01236747 9.89E-05 0.00051657 0.01291426 0.999928759 0.L- g=DL 11/17/2022 12:47:38 PM 0.00112633 0.0037975 0.0037975 pg 0.00112855 0.003805 0.003805 0.00112411 0.00379 0.00379 0,999928759 0.080ug=QC STD 2 11/17/2022 12:49:19 PM 0.02318223 0.07816048 0.07816048 pg 0.02319036 0,07818788 0.07818788 0.0231741 0.07813308 0,07813308 0.999928759 Reagent Blank 11/17/2022 12:51:11 PM -0.0001412 -0.0004761 -0.0004761 pg -0.0001191 -0.0004015 -0.0004015 -0.0001634 -0.0005508 -0.0005508 0.999928759 elementOne NE01 3AS-021420-RT-1 303 Appendix C-Page 448 of 1178 Hg-Data 3 of 3 e 396 -Hg 66.3 Wheelabrator Environmental Systems, Inc.—Wheelabrator N.Andover, Inc. Compliance Test Program on Unit Nos. 1 &2 Test Dates:October 18-19,2022&October 25-28,2022 MUNTAOSE NE013AS-021420-RT-1303 Appendix C-Page 449 of 1178 --SGS[, SG$ PROJECT INFORMATION SUMMARY(When applicable,see QC Annotations for delalls) Client Project PROJ-021420 FINAL LAB REPORT p SGS Project# B7268 ak m Analytical Protocols) M23 PROJ-021420 ... No.Samples Submitted 7 Additional DC Sampie(s) 0 No.Laboratory Method Blanks 1 67268 No.Ol I Batch CS3 1 . 1 22-Nov-2022 Data Rece iv.d 03-11 -22,04-Nov-22,07-Nov-22 Condition Received Good Temperature upon Reoeipt(<C) 1.8(Traps&Fillers),22.1(Solvents) Extraction within Holding Time Ves +`SESj1�e-n:rV V3y t p'-v'I Ldh Analysis within Holding Time Ves SGS NORTH AME ICA Montrose Air Quality Services Mike Brunt 2 New Pasture Rd Newburyport,MA 01950 Phone:(978)499-9300 Email:mbmni@montrose-env.com This report Is approved by Tamara ti.domper tamam.budumpta&gs.wm Senior Project Manager �s rve>a a�.m�m�mmoal b��nm�nae asev«var$d<<i nnv��m'n-as wm�ev�e�ms ono m+mws.Ani.Aumem rsarewn t<meumimum o� sus am,...m,mm<ew �x m<moe<n�<mam�.s� a n. a m,<.,�<m.mao,<�mimm�.m mm�mnmm aroma.w,�,m„aM9�„emnaa�.. P11-1m1o,,.mat<1-111..«mm—," ��m<e.miu am�mwmd.mrvwnd nam rim>,rem�,mm«<,wmmwm«�mP�ear _pmYs amnas�n<memom��mc�ma�a.ieimie aansmmummc.0 my*a<cmnv<m'sw=r�ai�rTMm ma�mnpm wax�amsnp� ww�®ni,m�,mam�eoamme. me carymy vpmYo�ti mmveromnmuM�mmeaimez u��am amarceipm n�em�n mumnanmanm aaomemdme mium pp mm<tmie W uum ey me Gnp airy 1s uNrvnul<nm aama<m m ay c<pmttalM�o me luu ea me�oihs la w�� NE013A5-6r14Y0-Rim9908 °"c�P.)4&W91kC 'A�@M9dvY41YWB'^a'°'"'c as^ eosl'era soo w NE013AS021420-RT-1303 Appendix C-Page 451 of 1178 OC ANNOTATIONS: APPENDIX A:GENERAL DATA QUALIFIERS i DATA ATTRIBUTES 1.Please see Appendices attached for data qualiferiatlribule and lab identifier deacfiptions which may be contained in the B The annyte was found in the method blank,at a concentration that was at least 10%of the concentration in the project. ample. M23W-R1,M23-U1-R2:the rcooled detection limit(DL)of 2,3,7,8-TCDD is above SOP criteria,however, ,,is Method C Two or more con lute.In EDDs,C tlenoles the lowest IUPAC can ener in a welution d criteria. geners coe g group an additional co-elulers for the group are shown with the number of the lowest IUPAC co-eluter. The reported pe t rewvery of labeled extraction standard ES 12.3.4,6.7.8-HpCDF is above criteria.causing labeled standard E The reported—contrarian exceeds the calibration range(upper point of the oallbralion curve)and is an estimated SS 1.2 3AS,B,9-HpCDF lobe below criteria. value. EMPC Represehis an Estimated Maximum Possible Concentration,EMPC,arise incases where the sighaVnoise it,is not sUfcient for peak idenlifirdin-(the determined ion-abundance ratio is outside the allowed theoretical range), where there is a c,,I,ti,g interference. Hlh If the standard recovery is below the method or SOP specified value'H'is assigned.if the obtained value is less than half the specified value'h'is assigned. J Indicates that an analyt,has a concentration below the repoding limit(lowest point of the calibration curve)and is an estimated value. ND Indicates a non-defect, NR or R Indicates a value that is not reportable. PR Due to interference,the associated congener is poorly resolved DI Indicates the presence of a quantitative interference. at Denotes'Siogle Ion Mode-and is utilized for PCBs where the secondary ion trace has a significantly elevated r.m.level due to background PFK.Responses for such peaks are calculated using an EMPC approach based solely on the primary ion areas)and may be considered estimates. u The an,lyt,was not detected.The estimated detection limit(EOL)may be reported for this anatyle. v The labeled standard recovery was found to be outside of the method conlml limits. NE013AS021420-RT-1303 Appendix C-Page 452 of 1178 NE013AS-021420-RT-1303 Appendix C-Page 453 of 1178 g µy -? l-' T` APPENDIX B:DRBC/TMDL SPECIFIC DATA QUALIFIERS/DATA ATTRIBUTES SGS CERTIFICATIONS J The reported result is an estimate.The value is less than the minimum calibatien level but greater than the Alaska DEC LAP 17-012 estimated detection limit(EDL). Alaska DEC LCP NC00919 U The a,style w not detected in the sample at the estimated detection limit(EDL). Arkansas 20-05" E The reported concentration is an estimate.The value exceeds the upper calibration range(upper point ofthe Califonia(FLAP) FLAP Cart 02914 calibration curve). CILIA 3[)1013708 D Dilution Data.Result was obtained from the analysis of a dilution. Connecticut PH-0258 B Analyte found in the sample and associated method blank. USDA Soil Permit P330-20-00103 C Co-eluting congener American Association for Laboratory Accreditation(A2LA) 2726Dl(ISO 17025:2017,2W9 TNI,DoD FLAP QSM 5.3) Cxx Co-elutes with the indicated congener,data is reported under the lowest IUPAC cengener.'Xx denotes the Florida DOH E87634 IUPAC number with the lowest numericel designated congener. Louisiana DEQ 4115 NR Ana1Ne is not reportable because of problems in sample preparation or analysis. Louisiana DOH LA031 V Labeled standard recovery is not within method control limits. Maine 2020079 X Results from re-injection/repeat/secondcolumn analysis. Massachusetts M-NC919 Michigan 9950 EMPC Estimated ion-abundance n,concentration.Indicates that apeak is identified but did not meet the method specified ion-abundance ratio. Minnesota(Primary NELAP For Method 23) 037-999459 Montana 0106 New Hampshire(Secondary NELAP) 2083 New Jersey NCl W APPENDIX C:LAB IDENTIFIERS New York 11685 AR Indicates use of the archived portion of the sample extract. North Carolina DEQ 481 CU Indicates a sample that required additional clean-up prior to MS injectimuprocessing. North Dakota R-197 D Indicates a dilution of the sample extract.The number that follows the"D"indicates the dilution factor. Ohio 87785 DE Indicates a dilution pertormed with the addition of ES(extraction standard)solution. Oregon NC200002 Pennsylvania 68-03675 DUP Designation for a duplicate sample. South Carolina 99029002 MS Designation for a matrix spike. Texas T104704260 MSD Designation for Is matrix spike duplicate. US Coast Guard 1671VI59.317/SGS RJ Indicates a reinjection of the sample extract. Vermont VT-87634 S Indicates a sample split.The number that follows the"S"indicates the split factor. U ginia 460214 Washington C913 Rev.12-0c1-2021 NE013AS-021420-RT-1303 Appendix C-Page 454 of 1178 NE013A8021420-RT-1303 Appendix C-Page 455 of 1178 Pa sd6 B7268 - TEQ B7268 - TEQ Project to:PROJ-021420 Project ID:PROJ-021420 Sample Summary Method 23 Sample Summary Method 23 Part 1 ._vim _ Part 1 '� j AnxlNe -met M2]-U1R1 M23L1-R2 M23U1-R] M23U2-FB M21V2A1 M23L2A3 MAU2-R3 Amrt. Ol2�diae� -1411 M2341fA2 M U1- V2 2 2 2 (to5l 11a2) (864) (749) (882) (842) 38.9 (7.89J (105] (112J (8641 (7.41) (6.32) (e42) 399 46.6 p7.21 l2I.31 (eI37 13661 147 [t5o7 (3.26) 46.3 IJ].2 12].61 (673) (36.6] 119n 11 =211 1831) 332 1741) 30 969 (9331 too Q.41) 00 t54 t5I 1111) 171 292 211 (a 1) 112 (863) 292 29] (86) 312 360 (9) (1t6J 103 (B 70) 106 (1261 (9) [1151 (8>s) 106 112fi1 sxpc00 (836) 30W 2540 23>0 (7.62) 2510 o-xpco0 (833) 200 f1.62) 0 (17.6) 5150 3960 3920 30 3370 3360 3440 0 (176) 11. 39e0 3920 3e 3670 33W 3440 (366) (313f 125 1369) [1397 (3.66) 13531 32.5 29.4 (3.69) (13.91 17.5 43.9 12961 419 R.77) 28S 126.91 524 (2967 419 (2»I I2B.9) (3.62) 140 113 115 (35) 746 (3.62) 1. 113 115 (3.5) 74.6 102 134 (4.t47 98.2 192.21 (J.3) 75 76.9 f04 (4 t41 13221 (3.6) 75 76.9 1. 113 982 (3.71) 1' 114 (3344) 112 1a7a7 331 114 In,2. (3.44) 112 (s 37) 243 214 (5.07) 252 211 160 163>) 335 259 (5.97) 252 215 (6.69) (26) (17.1) (17.1) (5.131 11611 11z9) It69) 16691 (2s) 117ei) 11731 151e) ItB 1) 1129) laa9) (296) 392 112 116 (2441 111 111 322 (2 se) (244) 312 111 31 sxpc0r (1) 173 1. 143 (561) (1201 1is 141 rxpc0v (a) (Soil 11201 11m 185 332 143 329 263 329 13.5 404 349 332 14.6 329 no 329 a41 0 11f0 .1 1. in 0.0]8 160 12 21 i8alxom;taxcw8xvel 0 BTa 703 no Alan 70a 1010 1210 reolxo�x;exec�e7nscl 0 268 2t1 20t O.WB 180 258 36e *e01xo-ovt;vnacwl 11 102 10.1 684 "1 11111 0.16 1bi 241 264 1e01xo-01rz;Belvo-8xecl 11.2 BM - )42 10.1 708 1010 t220 re01x0.Ovx;weo-8xecl B.Be 282 217 20B 6.76 136 Zet ]6B -1 -111-111 942 601 141 20.1 713 1- 110 maT6o1xo-OL ee"'.-1 ne 2W T3J 211 1 11.6 1 101 280 1 3. �i 344KA402142PRT-1303 AOGenenc 9 se o11171 ;�A114WA5021420RT1 AP rc,c Page 411.111Is B7268 - TEO B7268 -Totals Project ID:PROJ-021420 Project to:PROJ-021420 Summary Sample S Sample Summary Method 23 p ry � Part 1 Method 23 Part 2 3 U a- Mmxatl Blank FnalNa MellloN Blank -Al M Ut-AT M2-Ar M234 B -02-m M23L2- M21V2-R3 Anaty4 0>2W tb B 1 P129-U1-R2 M21U1-R3 M23U2�ia M21U2Ai M2]L2A2 M29ULR] e)288_1BH]a (7 B9) (10.5) (102) IB 64) (741) (8.62) (0.42) o, .l, (3].21 127.el (613) 138.61 47 ryI, low 96J 919 1010 6040 55]0 (9.33) 8).9 945 832 (7.41) 80 154 159 1. 2550 1e30 1990 t 6730 (B.B31 3J4 29922 29] (86) 260 312 3680 5Bi0 5ti0 411 0 4460 5360 4600 (9) It161 1 103 (6.]8) 1. 11261 5940 5160 4J50 38 3820 4290 sxpc00 (0.30) 3000 2640 2370 (J.621 2511 211 2320 0 0 15D -1 1120 JO 1311 -1 o (176) 5150 3980 392. 3B 38J0 "w 3440 0 1520 1300 1310 0 731 2000 (3661 (3'31 325 294 (369) (139i 3J.5 439 P..cor 0 141 11 1000 0 11 1244 t530 1296) 33J l2.]]) 202 12891 524 wcoP: 20J1 t690 1510 00 1530 (3621 40 115 (36) 746 102 134 xpcoP. 2 11 89 iJ48 0�1 14.t9) 113 (0221 p ]5 J69 349 332 329 2. t.x'�.�To-xrcoi 9B2 104 oco �.x.1.c.tswcxP (3 i11 129 114 102 (3.441 10] 91.4 t12 (63i) 335 248 254 15 m) 252 215 2wMnixo-a;emPo-ol 0 Z1100 :Y11W 31800 98 20400 20100 M691 (25) (tJ.1) (1>.8) 15187 (t6.1) (129) (16.91 PCN PtPeaP[1 0 ZlMW 231W 22]W ::98 21200 3000D 338D0 12967 392 31 311 121 322�axPco� 3t2 2Bt .�J.eenPcoP (ej i>3 154 143 (561) (120f 119 tot 130 1 2)WO 19600 22100 1. 21300 30000 ]]a00 OcoF 18.5 404 349 332 14 ol 3. S63 329 T4m]]fNst MO:dPcm) 0 40400. W00 010D 00'. bWD )9DD ®1D iPA1xOm.mPcw1 bt t86 tbt 0.01t4 1. ffi 232 nsino9$aPmO 0m 1- .0 in WOD 7u* -0 1x.Rlxmm:meo-aeP[I 0 340 20D .:100 O.Df id t� 300 :d22 nslNDn;dPaNl 100 1040D:. 0840 E 8/60 186 0DB0 ]3]0 aa9D aMm i201xo-0u2,N11Pow1 11.9 290 t12 16) 10 1de 20T 5U Tv MMN;BePMI 0 10 0N0 0210 'a',. 010D I'm M wNamm TPalxPOvt.parc�Pcl 11.3. 263 200 tW t0 106 911 :429 afla N.Gbs;sepal MA lDroD:. 0000 tY280 it. Btp I- 0210 TaY31neMM:�Pc.1 180 1Dm0 Bai9 -.eb10 =186 BSOD - "/4)0 ;02R0 ue+Pc1 22T 2B0 216 180 ID 180 916 d21 17 Ill 11 �� pinsozuz4RT.13m roP=Penc.w9a 4. 117B }y4wz14zo Rr.1]B] 4o 1,.c.P. 451.1117e 87268 - Others B7268 - Us Project to:PROJ-021420 Project to:PROJ-021420 Sample Summary Sample Summary PartsjD�j G Method 23 Part 3 1`s :_. Method 23 Rx)xx MMnp�D).xx U1 u- 0>28B 1NeID RII]-131A1 M21Ui-AZ MZ1 -R3 M23432F0 M23412A1 -2- M4 Analy4e 0)2880tN18� 1 U1-AZ M23V1-R] M23L2F0 M2N12 -A3 M2}U2-R] Po 109 >.91 e.e2 8.42 9.08 er PcnaP.lxmm,NUPcwI 326 102 9.16 U2 6i3 133 J.04 t2.1 )41 0.2 0 1060 96J 919 4840 5530 68 3 12.4 e.6 Ill 6.)4 B6 2500o 11. 6>30 121 ].91 11.7 8.71 it] 1 0 5410 4680 49)0 4890 w. sxpc00 8.38 103 >.62 95 e.71 9.2J vpcoo 0 2940 2520 2- 0 26t0 21. 2360 0 1>6 162 20.8 20.3 19.8 19] 135 17.4 3.66 4.64 0 8 8 4.B3 39233 1520 1260 1280 )31 11. 296 7. 2.)J 6.0] ].16 ].1] 2 1t0 929 864 6J2 1350 362 104 .e3 .2 ].50 14. B33 e50 BBt 04.14 11.2 38 11.3 8.49 8136 p P 0 554 46J 469 0 3P J4B 42B 3Ji 13.] 10t 9.93 344 >95 9>9 13 6.3] 205 14) 50J12 o 114 137 ..-W-lxo-o.UP-M 25 17 41 1].e 5.le 16.1 1. 16.9 iiep i1W 1010 tOBO 50>0 55J0 a rvpcoP 2896 38.09 J1 313 21 231 301 2500 2090 2000 0 1900 6040 6280 %xpc0r 609 56t 9.81 5.32 B.t] 5470 4680 4020 5230 5800 165 152 14.8 V1 18.2 nP<oo 0 2940 2520 2380 0 2610 2t50 2360 789 10.5 10.2 864 741 8.82 842Go 8.26 6.J3 161 8.33 t'0.1 1510 0 low 1J00 2210 902 11�J J.3] 1122 6.24 11 9.04 0 14� t210 t130 .3 50 80 Ix coo 103 006 09 11i0 1030 1913 1100 a B.3B i62 9.5 B.J1 9.2J xacOP 0 t564 46J 469 0 - 3. 42B 41 5.41 3% 464 392 4.. 3.36 9.2 77J 6R J.69 7 12.6 12.6 4.. 116 9]8 125 4.17 474 4. 351 536 5.33 11-�8 RT 3w Mpe�xu c.weo gcooi ll]a u6o)3um14zoxr l]m pp ec woe 4etulne 1)J��As021424 -1 gyp£ ' n P c k = c k cy wo 0 r¢� .0. �z m LL aLU A m '\�VAAAAAAADA)AAAAAAVAAAAAAAC °' m ', i//i// a o .16 Id a a ', �VAAVAA\\�AVAAAAAVAAAVAVVA\AA.`4� . � "- n � � w� -�VAVAVAVAAVAAAAAAVAVAAAAAVAAAVA�A\�AA�AAAVAVAA�AAVAVA�AA ae, � �� nA A A AAAVAAAAAAAVVAAAAAAAAVAAAAVAAAAAv °� . �VAA�AAAAVAAAAAAAVAAAAAAAAAA\�`�r.,� _ �\�AAVAAAAAAAAAAAAAAAAAAAAAA� °� �I 4 � a, �vvvwvvvv��wvvwv�wwv�. �� jvvVvvovvovovvv�v�p �� CY C W ai F7� $ ' H� g g 00 �vwvvv�wAVvwvvvvvvvvvv�\� k o h m v�\\v v»wvovvvwvvyv�w�� a� I IL 17 Id V $ ��v��vv�vvvvvvvv��vvvvvvvvvv� ° �vvvvvvvvvv�wvvvvvvvvvvvvvvvvv i°�� ae i Mean Recoveries of Extraction Standards(N=8) ', Mean Recoveries of Sampling Standards(N=8) Project ID:PROJ-021420 sm.p�.. Project ID:PROJ-021420 B7268 B7268 1ze � 3 C goo 3e ; x am o t y 0 NEOtusn21410-RT-t303 Melhotl SpecKwlion LlmFs:Te162iIN4'4�S:�fS4%�.Hd81a-Oc1e ES:2S130%(F=fall) NE0I-21120RT1303 Me1M1od SpedfvaflfPV.�IpPo✓.'1 IM4f .(F=fail) — ® - - Yap _ _ — _ __ ,_ w - - _. _ d _ __ in fn la _____ ___ NE013A5021<20 RT 1303 ppe arcC g 600111]e e]]se 0 cl2e NE013NSaltal0-Ri-t 303 � rcC p 69 o111]e BrzeB Pea<1]Mm _ - - - - - - - - - NE013ASA21426RT-1am Pp-C Pa 470 a111]B e]2se Wane fe of xo NE01-21420.RT-1303 APPa- Paae 471 a111]0 0]2ss Dyer o1m Sample ID: M23-Ul-RI Method 23 Sample ID: M23-U1-R2 Method 23 cnemD p,Pla mb L,borsroP.42 en a arse. rs.N m sa wNa I Lab Proect liD -Al �2022 Name: + Lab Prv)o,ID B]260 Date ftecenetl'. Pry ecl lD: PROJ12.2 WeIOhWolume'. t Lab Sample lD B]260196200E_OO1 Dale Ezlfaded: 2-.2022 Prvlec11O. PROD.0214N.-2 WeiphWvlume: 1 Lab SahNl, BI260_1-1-2_ 0ate Eztrzdetl: 0&Nw-2022 Date Coikcled'. 25Cct-2022 -U.l,M1No 19620 Dale Analyzed: 2ITN4522 Oate Colkded: 25OG 2022 OC 1- Nv: 19628 Date Analyed-. 2 17 11-022 2 me gnat ed: 1I04 ES S IM1. 2 Plulivn: ilme Anal ed: 1]:5126 Alwalyfa Cn E lPgl DL 1pgl WPC Ip91 DudiMlars $bndaM S Becpvedez Duallgers nalyte 11c.Ipgl IP91 IP9) Gu DL EMPC alHiars E9 Recoveries DualHlers C.-ND 105 75.4 ND 468 J - EMPC 37.2 J1.7.1- 17 933 89.3 94.5=MM 90 374 836 2. 94.2 EMPC 116 I9.1 tm B26 acpv 3.- ocoD111 Pcov 2640 acDO 0 5.1w m 005 P 3980 0v 102 EMPC 35.J 66 32.5 738 419 J 9 2 140 6B2 113 752 e)i 988 129 104 119 335 ]] 248.6 240 3. 25 60.1 ND t]t731 0 342 aaxpcPs 173 esaxMof fi].8 nsxpcof 154 ab 78 404 fi38 349 729 Tools 9bntivN 991g9 Recovadez Tablz bntlaN SSASPwrks i.Ofi0 1,180 961 95.9 2,550 2,550 210 ]8.2 6040 ]1.4 5,1]0 5,1]0 ]20 a.lpm0 5940 5,940 52 V Wwp 5,160 5.160 476 V T. 114 03 aJ 1,4500 IT- 1,35I00 I'll xsimf 86.5 2 2 12. 1 pf t". 10 92 962 TvbI PCODIFs 2T,1W TWIPCDDIEz 22.100 TEO: T.TEDsC=O T11 TEDz N 24 256 TEQ ND=O 192 211 TEO:ND=IXl1 247 17 262 1Cy�i TEO_NG=DL2 198 21) wn+nylm.xc xetos.Vsr. TC-0:NC=C1. 254 339 269 TED:Na0. 204 27.1 NE@lsRRP/t1g@8.%tMtl3 sysR�lh9w2k'+P WA2a ttie xewf o=.fe4.2f xe,-mn fe rl onaM1:2*f rvEBMgs�nI3bAFBA563 svSR�lAdyi**P e"8 a1- necofa..0 11.xe.zoafs:41 myn.1 Sample ID: M23-U9-R3 Method 23 Sample ID: M23-U2-FB Method 23 and Data sarrole mta tahonmry min mPlew Labammry cn cn sa m as Name: "+-•....�.,.,.,,_..,�,Manx: Alr Lab Project lID 0J260 Date Recened 03 No+-2022 Name: +•+ ...+-•Maldx. Alt Lab Project lD'. BJ2fie Dale Rereivetl. O1Nw 2022 Prate- P-20220 pM1Waume. i a NI,8I2601I DF 003 Date Evbaded. -2022 Project. PROJ�02142o We18bWolume: I ID B)26B_t962B DF_0040ale Exbaded. 1.2 Dale Colktled 26-0d 2032 QC 1, No. 15626 Dale Anallxed. 26Nov-2022 Date Colkde0: 19-0d2@2 OC Batrl,No: 19628 Dale Analveed: 30.Nw-2022 S IA'. 2 Plwwn: lime Anal ea 16:30W conc 511: 2 Tlme Anal ed: 192493 A�ulyla rc.(p9) a(p91 111W) Qu.IMlers 3h Pecavade nda. E6 s QualMlers nalyfe IP91 -1 1 EMPQ IP91 DQuelHlers Slantla. QualMers Do ND 864 1112 NO J.41 s.4vada EMPC 27.6 J 3 1173 e66 .2 91.3 ND 1.41 91 29i e9.5 ND BG.) 103 62.1 ND 8.10 809 axalpcoP 211. NKm sinpcbD ND 162 vcoD p 3920 coo 1.2 D 3B J So 80.5 NO 369 33 J j 92 ND 2 JJ 115 141 ND 3.5 J62 EMPC B22 1. ND 56.1 i@ 113 ND 3.44 t11 D 50t Np 17 133 NO 5.18 74.0 159 V N 244 13B V J4aNpcw' 143 ]eaxpcpf 768 >ealµcpf ND 5.61 Jao-lpcn 798 332 )) ND 1411 66.5 teals ntla. S6/AS Pacovadas Plats Slantla. 39/A9 PesowrNz 093 919 ND ].41 981 1.690 84 ND 6.13 ND ]9fi 4 4.1. 192 ND Boi Mcpo 41.,)50 4.]50 528 V lymo ND >62 ND o4aeaxpcos SBS V 0] Tll 969 1,310 wo-imf 81.5 ND 369 ND xsimf B6 1 WO "6 1, NO 3.09 ND 1,10 Np ND 1929 929 ND 351 ND Talal Pc00ffz 2t.60o E,000 TobI PCDDIFs 38 ITEF TEQs ITEF IEQz iEQ'.ND=O 1J0 tot TEQ:N0=0 0038 ome tEO:ND=C42 iB4 145 206 wn,rvn tE0:N2dJ2 8]5 6.I2 75 iEQ:ND=DL 1B9 209 211 "" ""P TEQ:NROL 11 174 115 ve,'...w•_ N041srko9nIQA1P6A� �A L49'xe3+P oWF9d 11]e P.vov c,=.ma.n Ne.x4a+4.x m.ha-*P NE6MX80T19MitFA§B3 susp�LgpgyxaP 'H�a»)e n.vmv..lm.zt-Na-ma 1e11 mWu: Sample ID: M23-U2-R1 Method 23 Sample ID: M23-U2-R2 Method 23 cnem wla san,aa mla er�mm cn.nrom tebmatory�mrsl soma.wu <a Name. Al, lab Project tD 0)268 Dale Received. 03=2023 Name. _-- .+Malnx: tab Pfojecl lD'. B7268 Dale RereNed'. 0-2.2 Pto)MI PROD-021420 + Wet19M1Wolume: i Lab SamplelO BJ2681I DF 045 Dale-1b d. 21.1.11 PROD-021420 Wei9M1Wolume: 1 Lae Sample 100)268_19628_OF_OO6 Date Exlradavt: 06Nov1022 Colkdetl. 18 Od3022 QDBaILM1 No. 1962E Dale Analyzed. 22.112022 Dale Colkded: 19-0d-2022 D. Dale Analttod: 261)vl o72 SOId: 2 Dlaron. Time Anal eG: 20.11.16 S IM1: 2 DIulOion�N 20:5>5> Alulyle ..(P9) M(P9) EMPQW ualMlers tla. E6 Recovedes Qu 11- -1a nc.lPel DL IP91 mpcip9) Qu.IMkrs land.. tE3ePecovedas Quallflers o ND 602 81.6 Do NO 8.42 92.1 EMPC 366 J 90.7 147 80 4 81. 2fi0 B].) 312 1Cfi 1114 EMPQ 126 801 ncoD 3,510 cib Kro Big ac0o 2,140 �o-scm 91.3 0 3,3]0 0o 745 u 3,360 op 9d.8 EMPC 139 703 37.5 JOB 2" J 91.7 EMPQ 209 J 56.5 ]46 ]26 102 ]93 87 769 93.5 0) W 252 816 215 B2 ND i6.i 633 ND 129 713 sxvcOf 312 142 V 211 137 V ecpP EMPC 130 eulpcof 60 ealMcpf 1i9 x]ae4pclu JB.9 329 562 263 145 Taalz land.. verles Tdale hntla. SSIAS Racowdes A3055o 90.3 1 010 9I> 141 5- 100 1 060 9,460 )59 BO.J aN 1p.D 5.120 5,120 455 V a.l xamD 4,200 4290 51J V 0 131 leaicos BJ 1430 1.I30 nesir�s B].2 96J JJ4 1180 T"I'll1.330 1,4)0 1,2. 809 an fbsof 74B 1)CB TahI PCAD]Fc 20A00 31,200 TahI PODDJFs 21A. 30,000 ITEF 1EQs ITEF TEQs iEQ:ND=o 59 160 iEQ'.ND=O 242 256 iEQ:NRGtl2 164 15t 185 D velm. E. ND=Dt/2 24J 119 261 -y w TED'.Nlkp. ti0 3p.1 191 'T"n3"#' TEQ:ND=q. 252 23.11 269 IufiSleXa�liPt.ifFA�3 sssA�tklAn�s.Pb1�aW�a 1»e x.vo+uen=a.x�xe.xaa ts4x mww-*f NE61sr5Wt12dB96FAtf@3 uaRgtWCd4T"�P�`RPPa 11]e S=wl u.mm.2l.xo.xa ls.2 m.yn.n Sample ID: M23-U2-R3 Method 23 Sample ID: Method Blank B7268 19628 Method 23 imle Dat Dllent Oat ramie Dah - .r.MMaMx'. Lab Project lD:ta B]368 Dale Receivetl'. -N-2022 .- -.�=�MaMx: qlr lab Pro�ec ID 87268 Dale Remivetl: Na PrpjecllN Mr PRO--2204 WeIgM1Wolume: 1 Lab Sample lD B]263_19626_DF 00]Dale Extadetl'. -2022 Prvecl lD. PROJ 021420 WeiOM1Wplume'. 1 Lab Sample lD MB119626 SD3 Dale E%12deg'. -N-2022 Dale Cdkdetl: 14Oc1-2022 DC1- No: Dale Analyrsetl'. 2 21 44 3222 Dat Colkdetl: n/a BatcM1 No: 20.N I-. 2 O'llulipn: time Anal etl 21:4432 SpN: Oilullpn: ilme Analnea 16:1809 Anatyte n.(P9) eDL(pg) ET1Pv(pg) vuallllers Dab ES Respveaes vuallllers Analyte nc.(pg) DL(pg) EMPC 1pg) vualNkrs tntlaN ES Rrcevetlez vualmers p 33B Ce ND 7.89 05 P. 190 6)9 ND 0.26 657 9 901 ND 360 937 ND 0.1 634 ND rcm 2�320 cpp 9fi.3 ocoD ND 6.36 rcm 642 3.490 Cp 83.7 ND 1].6 Dp ]65 439 73.6 ND 3fi6 60 524 ND 2.1 665 134 73q NO 362 745 104 93.1 4.14111.7 06 ND ND 6.37 615 ND t69 )4B NO 6.69 67.1 V ND 2.96 192 V axpcvF 141 axpcCs 61B vcvr ND 6 ff 6B2 329 69.9 ND 1B5 SB.9 Tatiz tntlam SSIAS Recpverlez TWIz aavN 99IR3 Rrcoverhs 912 966 65]0 105 ND 7,. ND 111 6,730 6,s76 62.5 ND 6.26 ND 77 ND >6.3 as xpcoC 4660 4,660 V IWcpD ND 63B ND desaxvcoF 51 V 04 04 2.W0 2.260 aebrwr 90.2 ND 3.66 ND aeo-rrnF 86.3 1.530 1560 ND 3.26 ND 1.580 ND 4. ND T.-.1 691 ND 4.47 ND TofaI P.D.- 33a. 3],500 -1PCDOIFs ND ND TEQ T 0 ITEF TEvz TEO:ND=O 263 356 tl,.a t,,,,,. TE(1:N20 6 0 TEo:ND:DIl1 364 136 359 wmn m TED:N6IX2 969 969 rk vn mn TE-0:ND=OL 264 2)3 359 TEO'.NaDI 194 19.4 194 NE4lfvlb9f11P4NP999i scs,�,gSpy.�aP `8�a117e Revel.-I..11 xe.xpn ls.11 m.MLarF NBBlfAs19f14�§Pt4MA ses4y„M,,,p,�wpavw�all]a Rroe+oemea.zi.xQ.zos ls.l mmra.7z Sample R-ipt NPtifi-i- Chain of Custody Form•Source vrol=a I.e. «=k1n �vo.a..��.ie..,..i..-.�., ae{n..ns.�/==+nc n Avon PNgLY319 uu v.olKle Aim• erol Pl n+n,.ssl1.: g r=.1..1 ee.: euFxr emepemN wnty S.nlae. g',. e.al..� �.d.�=. Dn.mm.el..ol«: •^^ cwpno.a u.D - aPxanox Pmmalmmo�al�.-e nox I,.- ID .�� n]a1d9a f axsrntis=f= nrasah '� 25-oct-22 Na vl N Ti4e nl T 26Oct-22 Nv B Fa1ax1 T Boer-22 Bl?� IS-OcP22 letiotat"u FB crn T 19(lct,22 Nn _ otq ncnv�,T I� t30c1-22 Na r aRn % Towne Pvue P"ram ✓commenp. 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